How to design glycol dehydrators
..- for 100° F.-plus dew-point depression
UNTIL about 2 years ago,_ glycol 1Y CHARLES R. PERRY
dehydration was never seriusly eoo- ‘Sivalls Tonks, Ine.
Sideted when dew-point depressions in
fexcess of 75* were required except in rate which may be wsed for gs strip-
Stew plat units where vacuum regen- ping of the gyco
seed was us. Howererpyosi " Procatdaign dla tor uthyene
‘hydration unite are now being built glycol dehydration of natural gas for
ty Several. manufacturers for” dew- dewpoint” depressions inthe 60°
point depressions greater than 100° F. 115% F. range have been calculated
Tn ha" erusd gueprocan mea to and conse and ae prsted ee
reconsider the type of dehydration to Although these calculations represent
be used where highslew-point depres: theoretical performances, they. have
Sons are required. somrlated very. well with field text
"A number of developments ave data. They were calculated from pub-
contributed. to. this breakthrough of shed! equilrium and veporspressire
the old 75° F. depression limit for data.
‘lycol dehydration, Most important of
these isthe fact that plycol dehydra- How it works. Fig. 1 shows a typi-
tion equipment is being designed far cal glycoldehyération flowshect, in
rmoze completely and thoroughly than which lean glycol is pumped into the
ever before. Gone ste the days of top of an abvorber column counter:
fule-ofshumb design of glycol dehy- current to the gas stream to be ehy-
‘ration equipment such as “four tray drated, The rich glyeol stream leaves
‘contracts and 98% lyeol instead, the bottom of the absorber, passes
fry plyeol concentrations are’ being through the power side of « glycol
fcturately calculated and Snezeased, powered pump (0 level controller and
Required absorber transfer units are motor valve), and info a flash cham
boing carefully determined. ben, or goe-pycol separator. Here, en-
“Another important contibution to tained and daslved. gar ib removed
highdew-point depressions is the de- from the glycol; (this gas may then
Nelopmment of the’glyeol- powered be used for the stripping of the
pump, which provides a small quan- glycol).
fity of accurately measured gas’ pro- The sich glycol passes through
portioned to the glycol circulation feat exchange, countercurrent 1 ihe
Prevented at gas condoning coateene lean glyco) through a filter, an
vntersty of CLfasoms Norgene "into the stripping stl, Water vapor
ry Gas Out ‘VACUUM PUMP
(On vacuum regeneration units only)
Woter Vapor And Stripping
[ison TES en pagran ner gly GorOor
7] ‘CONDENSER
Nz / sre srk
To Fu Gos On Veco
concentration Unite
en CO
0%
/2\ ‘Shipping
"Ges
Wet Go, oiycor|
WotTes ich TES, ~ FILTER
HEAT EXCHANGER
FLASH CHAMBER
etycot FoweRED Lg TASH CHA
(GLYCOL PUMP Tean TES
GLYCOL DEHYDRATION UNITS are now being designed and built for dow-point
depressions in excess of 100" F. Fig. 1
and stripping gas (f any) are removed
from the top of the stripping. sil
through a parti reflax condenser.
‘Lean glycol leaves the reboiler, passes
through the heat exchanger counter-
current tothe rch glycol, and through
the pump back into the. absorber
Tn a typical dehydration design
oblem, the process engineer will be
fiven the inlet gan condlions (pres
Sure, temperature, and degree of sat-
tration), and the required: dryness of
the outlet_gas. He must then design
the most economical plant which will
provide the desired performance.
‘The first step in 4 design problem
should be to assume @ glycol eircula-
tion rate and estimate the dry glycol
concentration. Next, the absorber cal-
umn should be sized. Once these two
steps have been completed, the re-
mainder of the process design is rou-
tine, such as heat exchange, line siz-
ing filter sizing, and so forth.
Te is extremely important that a
complete material and heat balance
be made around each piece of equip:
ment, Reboiles, sipping columns,
and eat exchangers. are. frequently
Undersized by design engineers using
rule-of-thumb design data. Also, act
Curate material balances are absolutely
essential in the use of the data pre-
seated below.
Regeneration System
Design of the glycol reconcentra
tion sil should be done in'a conven
tional mannec to dtermine the nm
ber of theoredoal trays required to
provi the desire outlet dry pyeol
Eoncentration, However, 2 number of
problems arse in the eesga of the
Feooneentration sl: accurate equll-
Flom data for watersietiylene pico)
Eten at higher temperafres a not
reas avelabes aly the glyel tem:
perature should never exceed 400" F.
{0 prevent excessive decomposition.
Since 100% tithylene glycol has
a vapor pressure of only 65 mi, mit
scary’ at tis temperate, itis neces.
Sry that the reboler operating pres
Sr be reed fo ncrense dy S01
concentration above that show on
Boiling, point curves. This may be
dove by" gas sipping ot vacush co
eneaton
Dry. seo! coneentations may be
sccostly predicted fom vapor pres
Sure carver for units ing. vacaum
Reprinted from THE OIL AND GAS JOURNAL, August 8, 1960.Que TE Conetation—at Allowable Mas Volecty-1B. per hr. 29.
abo +
12000 -
ro.00 i
>
«0 |
fe io, oye
at, F ‘ood wis +
‘About ReboterPrere—MM Hg. tt
CONCENTRATION of ott 2000 : a
‘mated Irom these cores Ag. 2.
regeneration. However, design of a 710 x 0 TAO
Stil sing gas stripping is quite com.
plex when feflux tates‘and theoretical
frays are considered, since the part
pressure of the sipping. gas ‘ares Siven Fae
Throogh the column due to changes in
watervapor concentration, Data pre- _Direstfred reboiers for triethylene
sented below may be used to predict glycol normally are designed with eat
dey=slyeot concentrations when gas fivnes of 8.000 to 10,600 Ditu./ir=
stripping is sed. These values may be sq, Te Steamheated reboilers and the
increased somewhat by increasing re- heat exchangers should be designed in
flux ratios andthe numberof theoreti- accordance ‘wih the Standard of Tu-
cal trays in the tipping section of bular Exchanger Manufacturers ASSO-
the column. distion.
‘Stipping-till column eroseseo-
Sonal args ean be deernined from Vacuum regeneraon. Reconcentra-
flood point corcelations as presented ton of glycol under vacoum hos Deca
in. published Hiterature? from vapor succsssully used in plaats for some
and Tiguid loadings and the type of years. Vatium is usally maintained
packing usod. Most process engineers by’ sicam cjetors or. motor-deiven,
Eesignelyeolsrpping sls to operate vacuum puns, ‘This type of recom
at between 60 and’ 80% ‘of flood centration should be employed Wher
point of the column ver possible where high Concentra.
WT. % TEG In Dry Glycol Outlet
BS 998s
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y