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tiu chun quc gia tcvn -
1 : 2009
Xut bn ln 1
Silicon xm khe cho kt cu xy dng Phng php

th
Phn 1: Xc nh chy
Structural silicone sealants Test methods
Part 1: Determination of flow (rheological) properties
1 Phm vi p dng
Tiu chun ny quy nh phng php xc nh tnh cht lu bin ca silicon xm khe cho
kt cu xy dng loi mt v nhiu thnh phn ng rn ho hc.
Ghi ch: Tt c cc phn trong TCVN -16 : 2009 khng cp n an ton sc kho, trc khi thi
cng phi c k hng dn an ton khi s dng ca nh sn xut.
2 Ti liu vin dn
Cc ti liu vin dn sau l cn thit cho vic p dng tiu chun. i vi cc ti liu vin
dn ghi nm ban hnh th p dng bn c nu. i vi cc ti liu vin dn khng ghi nm
ban hnh th p dng phin bn mi nht, bao gm c cc sa i.
- TCVN ... : 2009 Silicon xm khe cho kt cu xy dng - Yu cu k thut.
3 Thut ng, nh ngha
Tiu chun ny khng nu thut ng v nh ngha, tt c cc thut ng trong cc phn

ca tiu chun TCVN -16 : 2009 c nh ngha iu 3 trong TCVN : 2009.
4 Nguyn tc th
Tnh cht lu bin ca silicon xm khe cho kt cu xy dng c xc nh thng qua s

bin dng di t trng ca khi vt liu xm khe c hnh dng nht nh khi n nh
iu kin th nghim theo phng nm ngang hoc thng ng.
5
tcvn -1 : 2009
5 Ly mu th
Mu th c ly ngu nhin loi mt thnh phn hoc hn hp mu nhiu thnh phn

theo t l qui nh ca nh sn xut t mt l hng vi khi l ng khng t hn 5 % trong
bao gi kn sao cho m bo c tnh i din.
6 Thit b v dng c
- Khun th lm t thp khng g hnh ch U hai u h c phn b mt y ko

di v mt pha thm 51 mm, kch thc nh hnh 1, hai ci.
- T lm lnh iu chnh c nhit (4,4 2) 0C.
- T sy c qut ht, iu chnh c nhit (50 2) 0C.
- Cn, chnh xc 0,1 g.
- Dao ct mu.
19 Kch thc: mm
13
152
51
Hnh 1 Khun th hnh ch U hai u h
- a g.
- Thc o, chnh xc 0,1 mm.
6
- Cc bng nha hoc thu tinh, dung tch 600 ml.
tcvn -1 : 2009
7 Cch tin hnh
7.1 Silicon xm khe cho kt cu xy dng mt thnh phn (loi S)
7.1.1 chy theo phng thng ng
- Ly t nht 100 g mu th cn nguyn trong bao kn n nh ti thiu 16 gi

iu kin chun.
- Lau sch hai khun th hnh 1 bng metyletylketon hoc dung mi tng ng, sau
lm sch bng dung dch ty ra v ra li bng nc ct hoc nc kh ion ri sy kh. Tip
, n nh mt khun trong 2 gi nhit (4,4 2) 0C v khun cn li trong 2 gi
nhit (50 2) 0C.
- Ngay sau khi kt thc thi gian n nh, ln lt ly tng khun th ra v qut lp lt ln
b mt khun (nu cn) theo ch dn ca nh sn xut, mu th vo y khun
trong vng 10 pht. C th dng dao h tr khi mu vo khun v to phng sao
cho mu th ngang bng vi mp trn ca thnh khun v phng hai u khun. t
tng khun mu th vo trong tng t n nh khun th iu kin trc trong 4
gi theo phng thng ng vi phn y ko di nm pha di. Cui giai on ny, ly
tng khun mu th ra khi cc t n nh v o khong cch t mp di cng ca mu
th ti b mt u khun nm trn phn y ko di, ly chnh xc n 1,5 mm.
7.1.2 chy theo phng ngang
- Qu trnh tin hnh tng t nh iu 7.1.1 ca tiu chun ny ch vi s thay i sau:

Sau khi y mu th vo khun, ln lt t tng khun mu th vi mt y theo
phng ngang vo trong tng t n nh khun th iu kin tr c . Cui cng, ly
tng khun mu th ra khi cc t n nh kim tra chy ca cc mu th bng
trc quan. nh gi mu th bin dng hay khng bin dng thng qua vic quan st
chy ca mu th.
7.2 Silicon xm khe cho kt cu xy dng nhiu thnh phn (loi M)
7.2.1 chy theo phng thng ng
- Qu trnh tin hnh tng t nh iu 7.1.1 ca tiu chun ny ch vi s thay i sau:

n nh cc thnh phn ca mu th trng thi ring r trong bao kn iu kin
7
chun ti thiu 16 gi. Sau , cn khi lng cc thnh phn theo t l qui nh ca nh
sn xut vi chnh xc 1 % c c t nht 200 g hn hp mu th. cc thnh
phn mu th vo nhau ri trn u bng tay trong 5 pht thnh mt hn hp ng nht.
Ln lt ly tng khun th ra mu th vo y khun trong vng 10 pht (hoc
di hn nu nh sn xut yu cu). Quy trnh tip theo v cch xc nh chy theo
phng thng ng c thc hin nh iu 7.1.1 ca tiu chun ny.
tcvn -1 : 2009
7.2.2 chy theo phng ngang
Qu trnh tin hnh tng t nh iu 7.1.2 ch vi s thay i nh nu iu 7.2.1.
8 Tnh ton kt qu
- chy ca silicon xm khe cho kt cu xy dng theo phng ngang l vic nh gi

mu th bin dng hay khng bin dng trong khun th.
- chy ca silicon xm khe cho kt cu xy dng theo phng thng ng tnh bng
mm, ly chnh xc n 1,5 mm, l gi tr trung bnh cng chy theo phng thng
ng ca mu th trong hai khun th.
9 Bo co kt qu th nghim
Bo co kt qu th nghim bao gm cc ni dung sau:
1. C quan gi mu.
2. Ngy gi mu v ngy tr kt qu th nghim.
3. Loi mu v yu cu th nghim.
4. Cc kt qu th nghim km theo phng php th.
5. Nhn xt kt qu th nghim.
6. Ngi th nghim, ngi kim tra, th trng n v kim tra.
8
2 : 2009
Xut bn ln 1

th
Phn 2: Xc nh kh nng n chy
Part 2: Determination of extrusion rate
1 Phm vi p dng
Tiu chun ny quy nh phng php xc nh kh nng n chy ca silicon xm khe

cho kt cu xy dng loi mt v nhiu thnh phn ng rn ho hc.
2 Ti liu vin dn
- TCVN ... -1 : 2009 Silicon xm khe cho kt cu xy dng. Phn 1: Xc nh chy.
3 Nguyn tc th
Xc nh thi gian n chy ton b khi lng mu th qui nh ra khi v cha di p lc

c nh l 345 kPa.
9
4 Ly mu
- Theo iu 5 ca TCVN ... -1 : 2009.
5 Thit b v dng c
- Sng xm mch, dung tch 177 ml.
tcvn .. -2 : 2009
- V cha bng nha polyetylen, u pha trc c ng knh trong (13,7 0,05) mm, dung
tch 177 ml.
- Thit b cung cp kh nn c b phn ni trc tip vi sng xm mch to p lc kh

nn 345 kPa (50 psi).
- ng h bm giy, chnh xc n 0,1 giy.
- Cc, dung tch 500 ml.
6 Cch tin hnh
6.1 Kh nng n chy ca silicon xm khe cho kt cu xy dng loi mt thnh

phn
- n nh mu th cn nguyn trong bao kn ti thiu 16 gi iu kin chun.
- Ly t nht 400 g mu c n nh trn np y 177 ml vo v cha. Lp b

phn ni thit b cung cp kh nn vi sng xm mch v t lc nn l 345 kPa. Bt
my nn kh lc nn chuyn chuyn ng ln pittng phun p ht mu th ra khi
v cha vo cc 500 ml v ng thi dng ng h bm giy o thi gian t lc mu th
bt u ra khi v cha n khi ra ht.
6.2 Kh nng n chy ca silicon xm khe cho kt cu xy dng loi nhiu

thnh phn
- n nh cc thnh phn ca mu th trng thi ring r trong bao kn iu kin

chun t nht 16 gi.
10
- Cn khi lng cc thnh phn theo t l qui nh ca nh sn xut vi chnh xc 1
% c c ti thiu 400 g hn hp mu th, sau vo nhau ri trn u bng tay
trong 5 pht thnh mt hn hp ng nht.
- y hn hp mu th trn vo v cha v lp v cha vo sng xm mch sao

cho pittng b y li ra pha sau. Ly v cha ra khi sng xm mch dng ng ln
sao cho u hn hp mu th hng ln trn v n nh trong 3 gi iu kin
chun. Lp dng c ni thit b cung cp kh nn vi sng xm mch v t lc nn l
345 kPa. Bt my nn kh lc nn chuyn chuyn ng ln pittng phun p ht mu
th ra khi v sng vo cc 500 ml v ng thi dng ng h bm giy o thi gian t
lc mu th bt u ra khi v cha n khi ra ht.
tcvn -2 : 2009
Ch : Sau khi trn u hn hp cc thnh phn ca silicon xm khe cho kt cu xy dng th thi
gian n nh hn hp ny iu kin chun (hoc iu kin ring khc) c th di hn hoc
ngn hn 3 gi tu theo yu cu ca nh sn xut.
7 Tnh ton kt qu
Kh nng n chy, tnh bng giy, chnh xc n 1 giy, l khong thi gian t lc hn
hp mu th bt u ra khi v cha cho n khi chy ra ht.
Theo iu 9 ca TCVN ... -1 : 2009.
11
12
3 : 2009
Xut bn ln 1

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Phn 3: Xc nh cng Shore A
Part 3: Determination of shore A hardness
1 Phm vi p dng
Tiu chun ny quy nh phng php xc nh cng Shore A ca silicon xm khe cho
kt cu xy dng loi mt v nhiu thnh phn ng rn ho hc.
2 Ti liu vin dn
13
- TCVN 1595-1 : 2007 (ISO 7619-1:2004) Cao su, lu ho hoc nhit do. Xc nh cng
n lm. Phn 1: Phng php s dng thit b o cng ( cng Shore).
3 Nguyn tc th
cng Shore A c o theo TCVN 1595-1 : 2007 trn tm phng to thnh t silicon xm
khe cho kt cu xy dng c n nh iu kin qui nh i vi mi loi.
4 Ly mu
Theo iu 5 ca TCVN ... -1 : 2009.
tcvn -3 : 2009
5 Thit b v dng c
- Dng c o cng Shore A c thang o t 0 n 100.
- Khun hnh ch nht lm bng ng, kch thc (di x rng x cao) = (130 x 40 x 6) mm.
- Hai tm nhm phng c chiu dy t (0,6 1,6) mm, kch thc (di x rng) = (80 x 150)
mm.
- Dao li mng.
- Thc kim loi thng.
- T dng mu, iu chnh c nhit (38 2) 0C v m 95 %.
6 Cch tin hnh
6.1 cng ca silicon xm khe cho kt cu xy dng loi nhiu thnh phn
- Mi mu th cn hai tm nhm phng.

chun t nht 24 gi.
14
% c c ti thiu 250 g hn hp mu th, sau trn u cc thnh phn vo nhau
- t khun ng ln b mt tm nhm phng cn chnh ng tm, sau hn

hp mu th vo y khun ng ri dng thc kim loi to phng b mt ngang bng vi
mp trn ca cnh khun. Dng dao li mng xn dc xung quanh bn trong khun ng v
ngay lp tc nng khun ng ra khi tm mu th. Tip tc tin hnh t ng t to
tm mu th th hai.
- Sau khi to c hai tm mu th th n nh chng thm 14 ngy iu kin chun.
- Sau khi kt thc gian on n nh, s dng thit b o cng loi D (thang A) theo
TCVN 1595-1:2007 xc nh cng iu kin chun ti ba v tr khc nhau, cc
v tr o cch nhau t nht 25 mm v cch mp cnh t nht 13 mm. Nu mt trong s
su gi tr o nhn c sai lch qu 15 % so vi gi tr trung bnh cng ca su ln o
th phi tin hnh to hai tm mu th mi v o li.
tcvn -3 : 2009
6.2 cng ca silicon xm khe cho kt cu xy dng loi mt thnh phn
- Mi mu th cn hai tm nhm phng.
- n nh mu th cn nguyn trong bao kn ti thiu 24 gi iu kin chun.
- t khun ng ln b mt tm nhm phng cn chnh ng tm, sau ly ti

thiu 250 g mu th n nh trn y vo khun ng ri dng th c kim loi to
phng b mt ngang bng vi mp trn ca cnh khun. Dng dao li mng xn dc xung
quanh bn trong khun ng v ngay lp tc nng khun ng ra khi tm mu th.
Tip tc tin hnh tng t to tm mu th th hai.
- Sau khi to c hai tm mu th th n nh chng thm 07 ngy iu kin chun;

tip n nh 07 ngy nhit (38 2) 0C v m 95 %; v cui cng n nh
07 ngy iu kin chun.
Ch : Nh sn xut c th yu cu n nh nhit v m khc so vi qui nh trong tiu

chun ny, tuy nhin thi gian n nh khng c qu 21 ngy v nhit khng qu 50 0C.
- Sau khi kt thc gian on n nh, s dng thit b o cng loi D (thang A) theo
TCVN 1595-1:2007 xc nh cng iu kin chun ti ba v tr khc nhau, cc
15
v tr o cch nhau t nht 25 mm v cch mp cnh t nht 13 mm. Nu mt trong s
su gi tr o nhn c sai lch qu 15 % so vi gi tr trung bnh cng ca su ln o
th phi tin hnh to hai tm mu th mi v o li.
7 Tnh ton kt qu
cng shore A ca mu th, tnh theo n v, chnh xc n 1, l gi tr trung bnh

cng ca su ln o trn hai tm mu th.
Theo iu 9 ca TCVN ... -1 : 2009.
16
4 : 2009
Xut bn ln 1

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Phn 4: Xc nh nh hng ca lo ho nhit n s

tn hao khi lng, to vt nt v phn ho
Part 4: Determination for effect of heat aging on weight loss, cracking, and chalking
1 Phm vi p dng
17
Tiu chun ny quy nh phng php xc nh nh hng ca lo ho nhit n s tn
hao khi lng, to vt nt v phn ho ca silicon xm khe cho kt cu xy dng loi mt
v nhiu thnh phn ng rn ho hc.
2 Ti liu vin dn
3 Nguyn tc th
Xc nh s thay i khi lng v trng thi b mt ca tm mu th c chun b t

mu th sau khi sy nhit (88 5) 0C so vi tm mu th c gi iu kin chun
trong cng thi gian 21 ngy.
4 Ly mu
Theo iu 5 ca TCVN ... -1 : 2009.
5 Thit b v dng c
- T sy, c th iu chnh c nhit (88 5) 0C.
tcvn -4 : 2009
- Khun bng ng hnh ch nht, kch thc trong (130 x 40 x 6,4) mm.
- Ba tm nhm phng, chiu dy t (0,6 1,6) mm; di x rng = (152 x 80) mm.
- Thc thng bng kim loi hoc nha, di khong 152 mm.
- Dao li mng.
- Dao bay bng thp, di khong 152 mm.
6 Cch tin hnh
6.1 i vi silicon xm khe cho kt cu xy dng nhiu thnh phn
18
- Mi mu th cn ba tm nhm phng. nh du v cn ln l t tng tm nhm phng vi
chnh xc n 0,01 g.

chun t nht 24 gi.

% c c ti thiu 400 g hn hp mu th, sau trn u cc thnh phn vo nhau
- t khun ng ln b mt tm nhm phng cn chnh ng tm, sau hn

hp mu th vo y khun ri dng thc kim loi to phng b mt ngang bng vi mp
trn ca cnh khun. Dng dao li mng xn dc xung quanh bn trong khun ng v
ngay lp tc nng khun ra khi tm mu th. Tip tc tin hnh tng t to tm
mu th th hai v th ba.
- Sau khi to c ba tm mu th, cn ln lt tng tm vi chnh xc n 0,01 g. Sau

n nh c ba tm mu th 07 ngy trong iu kin chun.
- Ly hai trong ba tm mu th trn ra khi t n nh iu kin chun cho vo

t sy v sy nhit (88 5) 0C trong 21 ngy, tm mu th cn li vn n nh
tip trong iu kin chun lm i chng.
- Sau khi kt thc thi gian sy, ly hai tm mu th ra lm ngui mt gi iu kin

chun. Tip , cn ln lt c ba tm mu th chnh xc n 0,01 g. Tnh s tn hao
khi lng (M, %) ca tng tm mu th theo cng thc sau:
M = [(m2 m3) /(m2 m1)] x 100
Trong :
tcvn -4 : 2009
m1 khi lng tm nhm, g.
m2 Khi lng tm mu th (khi lng tm nhm + mu th sau khi to mu), g.
m3 khi lng tm mu th sau 21 ngy sy cng bc, g.
Nu sai lch gia hai ln o trn cng mt mu th vt qu 0,51 % th phi tin hnh to
tm mu th mi v o li.
- ng thi, kim tra s to vt nt v phn ho ca hai tm mu th qua sy (mu 1;

2; 3; 4) v so snh vi mu i chng n nh iu kin chun (mu 0).
19
Hnh 1: mu i chng iu kin chun (mu 0) v
cc mu b nt v phn ho b mt (mu 1; 2; 3; 4)
6.2 i vi silicon xm khe cho kt cu xy dng mt thnh phn
Qu trnh tin hnh tng t nh mc 6.1 ca tiu chun ny ch khc l khng phi trn
mu th.
7 Tnh ton kt qu
- nh hng ca lo ho nhit n s tn hao khi lng ca mu th, tnh theo %, chnh

xc n 0,01 %, l gi tr trung bnh cng s tn hao khi lng ca hai tm mu th sau
khi sy.
- nh hng ca lo ho nhit n s to vt nt v phn ho ca mu th c nh gi

bng cch c hay khng s to vt nt v phn ho trn b mt ca hai tm mu th sau
khi sy so snh vi mu i chng n nh iu kin chun.
Theo iu 9 ca TCVN ... -1 : 2009.
20
5 : 2009
Xut bn ln 1
21
th
Phn 5: Xc nh thi gian khng dnh b mt
Structural Silicone Sealants Test methods
Part 5: Determination of Tack-Free Time
1 Phm vi p dng
Tiu chun ny quy nh phng php xc nh thi gian khng dnh b mt ca silicon
xm khe cho kt cu xy dng loi mt v nhiu thnh phn ng rn ho hc.
2 Ti liu vin dn
3 Nguyn tc th
Thi gian khng dnh b mt ca mu th c xc nh bng cch o khong thi gian

t lc bt u to mu cho n thi im mnh polyetylen khng cn dnh vi b mt
mu th.
4 Ly mu
Theo iu 5 ca TCVN ... -1 : 2009.
tcvn -5 : 2009
22
5 Thit b v dng c
- Qu cn hnh ch nht, kch thc (41 x 19) mm, chiu dy c thit k sao cho qu
cn c khi lng 30 g.
- Su mnh polyetylen trong sut loi t trng thp, kch thc (di x rng x dy) = (127 x
25 x 0,15) mm.
- Su tm phng hnh ch nht bng vt liu c, v d nh thp trng km hay nhm

kch thc (di x rng) = (152 x 76) mm.
- Khun hnh ch nht bng ng, thp hoc vt liu tng ng khc, chiu dy 3,2
mm, kch thc trong (95 x 25,4) mm, kch thc ngoi (120 x 31) mm.
- Thc kim loi thng.
- ng h, c th o c pht v gi.
6 Cch tin hnh
6.1 To tm mu th
- n nh mu th (hoc cc thnh phn ca mu th) cn nguyn trong bao kn ti

thiu 24 gi iu kin chun. i vi mu th mt thnh phn cn khong 250 g trc khi
tin hnh th; i vi mu th nhiu thnh phn cn khong 250 g thnh phn chnh vi
mt lng cht ng rn tng ng theo qui nh ca nh sn xut.
- Lau sch khun v tm phng bng metyletylketon hoc xylen hay dung mi tng -
ng.
- Mi mu th cn t nht hai tm phng, qu trnh to tm mu th nh sau: t khun

ln trn b mt tm phng cn chnh ng tm, sau mu th (hoc hn hp
mu th trn u trong vng 5 pht thnh mt hn hp ng nht) t t vo khun
sao cho trnh to bt kh. Dng thc kim loi to phng b mt ngang bng vi mp trn
ca cnh khun to chiu dy ng u gia cc tm mu th. Tip tc tin hnh t -
ng t to cc tm mu th sau.
6.2 Nu thi gian khng dnh b mt cha bit th s tin hnh th trc vi mt tm mu
th nh sau: dng mnh polyetylen qun xung quanh u ngn tay ri chm nh ln b
23
mt tm mu th, c mt khong thi gian xc nh theo bng 1 th chm ln b mt
tm mu th tng ng cc v tr khc
tcvn -5 : 2009
nhau. Sau khi chm ln b mt tm mu th, ngay lp tc nhc ln v kim tra xem mnh
polyetylen c ko theo mu th ln hay khng. Nu mnh polyetylen khng ko theo mu
th th qu trnh kim tra vi tm mu th trc c hon thnh.
Bng 1 Tm tt khong thi gian th nghim
10 pht tip 160 pht tip

10 pht u, theo, theo,
1 pht th mt ln 2 pht th mt 5 pht th mt

ln ln
Tng thi gian th

10 pht 20 pht 3 gi
nghim
Ch : Thng tin v thi gian khng dnh b mt c th c cung cp bi nh sn xut hoc in

trc tip trn bao b sn phm s gip cho vic kim tra nhanh hn.
6.3 Sau khi tin hnh theo 6.2 s s b xc nh c khong thi gian khng dnh b
mt, lc mi bt u th chnh thc. Tri mnh polyetylen ln mt na b mt mu
th thi gian thch hp v t t t qu cn ln trn mnh polyetylen ri yn trong
30 giy. Ngay sau , nhc qu cn ra khi mnh polyetylen ri dng ngn tay ci cng
ngn tr ko t t mnh polyetylen ln theo gc ko 90 0 so vi b mt ngang tm mu
th vi tc khng i l 25 mm /15 giy (hnh 1).
6.4 Nu mnh polyetylen khng hoc hu nh khng dnh silicon th lp li php th

theo 6.3 trn tm mu cha th.
24
Hnh 1 Cc giai on ca qu trnh kim tra thi gian khng dnh b mt
6.5 Nu mnh polyetylen cng khng dnh silicon th ghi li thi gian th nghim t thi
im mu th trong khun c gt phng cho n khi ko mnh polyetylen ln.
tcvn -5 : 2009
6.6 Khi th theo 6.3 hoc 6.4, nu mnh polyetylen cn dnh silicon th ch thm mt
na khong thi gian qui nh gia hai ln ko tm polyetylen ln thuc khong thi gian
th nghim ri lp li php th t 6.3 trn cc tm mu cha th cho n khi mnh
polyetylen khng dnh silicon khi th theo 6.4.
6.7 Nu thi gian khng dnh b mt gn ng bit trc th chn thi gian th
nghim ph hp vi thi gian khng dnh b mt nh trc, rt ngn i mt khong thi
gian bng khong thi gian qui nh gia hai ln ko tm polyetylen ln thuc khong
thi gian th nghim bt u tin hnh th s b t y. Php th s b v chnh
thc c tin hnh nh m t trn.
6.8 Khi th theo 6.7, nu mnh polyetylen khng dnh silicon th li bt u tin hnh
th s b trn tm mu cha th khong thi gian thch hp ngn hn.
7 Tnh ton kt qu
Thi gian khng dnh b mt ca mu th l khong thi gian c xc nh theo 6.5,

tnh theo pht, chnh xc n 1 pht, 2 pht hoc 5 pht tng ng vi khong thi gian
cho gia hai ln ko tm polyetylen ln.
Theo iu 9 ca TCVN ... -1 : 2009.
25
6 : 2009
Xut bn ln 1

th
Phn 6: Xc nh cng bm dnh
Part 6: Determination of tensile adhesion properties
1 Phm vi p dng
Tiu chun ny quy nh phng php xc nh cng bm dnh ca silicon xm khe

cho kt cu xy dng loi mt v nhiu thnh phn ng rn ho hc.
2 Ti liu vin dn
3 Nguyn tc th
26
Xc nh cng bm dnh ca mu th ko c to thnh bng cch cho mu th vo
khun hnh ch nht kch thc (L x W x H = 50,8 x 9,5 x 12,7) mm c ghp t hai tm
knh ni kch thc (6,3 x 25,4 x 76,2) mm c chn di v hai u bng ming m
polytetrafluoretylen (teflon). Mu c n nh cc iu kin qui nh, sau c
ko vi tc 12,7 mm /pht.
4 Ly mu
Theo iu 5 ca TCVN ... -1 : 2009.
tcvn -6 : 2009
5 Thit b v dng c
- My th c l vn nng, chnh xc ca ti trng l 1 %, c th iu chnh c tc

12,7 mm /pht.
- Cc ph kin g lp th ko bao gm:
+ u gi c nh v u gi di chuyn: dng gi cc m kp.
+ Hai m kp: c thit k sao cho gi cht hai b phn c nh mu ng thi

loi b s lch tm ca ti trng khi chuyn ln mu th ko. Ti trng t ln
mu th ko phi vung gc vi b mt ngang ca mu th ko.
+ Hai b phn c nh mu: c gi bi hai m kp v truyn lc ko n mu

th ko.
- Dao bay bng thp.
- Sng xm mch.
- 50 tm knh ni, trong sut, khng ph, kch thc (di x rng x dy) = (76,2 x 25,4 x
6,3) mm.
- Ming m lm t teflon hoc mt vt liu ph hp khng to bm dnh vi silicon xm

khe.
- a thu tinh.
- Dung dch lm sch tm knh ni (nh isopropanol, dng theo t l vi nc l 50 : 50).
27
- Vt liu lt (nu cn).
- T sy c qut ht, c th iu chnh c nhit (88 5) 0C.
- T lnh, c th iu chnh c nhit (-29 2) 0C.
- Nc kh ion hoc nc ct.
- My th gia tc thi tit.
tcvn -6 : 2009
6 Cch tin hnh
6.1 To mu th ko
- Lau cc tm knh ni bng vi khng x sch, kh, sau lau sch hon ton bng mt
dung dch lm sch. Trc khi bay hi dung dch lm sch, lau kh tm knh ni bng
vi lanh th sch, kh.
- Qut mt lp lt ln b mt tm knh ni (nu cn). Sau ghp hai tm knh ni

thnh mt khun c khong trng bn trong l hnh hp ch nht c kch thc (L x W x H
= 50,8 x 9,5 x 12,7) mm c chn di v hai u bng ming m teflon (xem hnh 1).
- Mi mu th cn 25 mu th ko.
- n nh mu th (hoc cc thnh phn ca mu th ring r) cn nguyn trong bao kn

ti thiu 24 gi iu kin chun.
- Ly khong 400 g mu th (hoc mu th c trn u theo t l qui nh ca nh

sn xut vi chnh xc 1 % trong vng 5 pht thnh mt hn hp ng nht) y
vo v cha v lp v cha vo sng xm mch sao cho pittng b y li ra pha sau.
Dng sng xm mch cho mu th vo khun hnh hp ch nht, ngay lp tc dng a
thu tinh ln u mu th in y khun v thm t cc b mt tm knh ni.
Dng dao bay to phng b mt mu th ngang bng vi mp trn ca cnh tm knh ni.
Tip tc tin hnh tng t to cc mu th ko khc. nh du cc mu th ko theo
cc k hiu ring.
28
6.2 n nh mu th ko
n nh tt c cc mu th ko trong 21 ngy iu kin chun. Sau tho cc

ming m hai u ca cc mu th ko ra trc khi tin hnh cc bc tip theo.
6.3 Tin hnh th
- t tc ko o cc mu th ko l 12,7 mm /pht.
- o v ghi li chiu di nh nht thc t (L), chiu cao nh nht thc t (H) ly chnh xc
n 0,8 mm.
- Ghi li ti trng ti a P (N) ng vi gin di vi sai s 1 N.
6.3.1 Tin hnh o nm mu th ko iu kin chun ngay sau 21 ngy dng h

iu kin chun.
tcvn -6 : 2009
Khong trng hnh ch nht,

Kch thc:
mm kch thc (50,8 x 9,5 x 12,7) mm
Ming m
bng teflon
Hai tm knh ni,
kch thc (76,2 x 25,4 x 6,3) mm
(hnh 1
Ming m
a)
bng teflon
Silicon xm khe W
(hnh 1 H
b) Tm knh ni
Hnh dng silicon xm khe

trong khun hnh ch nht,
Hai tm knh ni kch thc (50,8 x 9,5 x 12,7)
L mm
(hnh 1
c)
29
Hnh 1 - Hnh dng v kch thc mu th ko: hai tm knh ni v ming m
teflon lp ghp thnh khun hnh hp ch nht (hnh 1 a); mt ct ngang
mu th ko sau khi ly ming m teflon ra (hnh 1 b); mu th ko sau khi
ly ming m teflon ra (hnh 1 c).
6.3.2 Ngm nm mu th ko khc trong nc kh ion hoc nc ct nhit chun

trong 7 ngy. Ly mu th ko ra khi nc iu kin chun trong 10 pht ri o
ngay.
6.3.3 n nh nm mu th ko khc trong t sy c qut ht nhit (88 5) 0C

trong 1 gi v tin hnh o ngay iu kin n nh.
6.3.4 n nh nm mu th ko khc trong t lnh nhit (-29 2) 0C trong 1 gi v

tin hnh o ngay iu kin n nh.
tcvn -6 : 2009
6.4.5 a nm mu th ko khc vo my th gia tc thi tit v duy tr trong 625 chu k

(5.000 gi). Mt chu k thi tit s c 4 gi chiu tia cc tm 60 0C v tip theo 4 gi nc
ngng 40 0C. m bo l b mt bm dnh nhn trc tip ngun tia UV. Ly mu th ra
khi my th gia tc thi tit, n nh iu kin chun trong 1 gi v tin hnh o
ngay iu kin chun.
7 Tnh ton kt qu
- Cng bm dnh ca mu th (T), tnh theo kPa, chnh xc n 1 kPa, l gi tr trung

bnh cng cng bm dnh ca 5 mu th ko, c tnh theo cng thc sau:
P
T x103
S
Trong :
P Ti trng ko ti a, N;
S = L x H l din tch b mt bm dnh thc gia mu th v b mt hai tm

knh ni, mm2.
30
- Trong 05 gi tr thu c i vi mi iu kin th, nu c gi tr no sai lch so vi gi
tr trung bnh qu 15 % th phi tin hnh to li 05 mu th ko mi v o li.
Theo iu 9 ca TCVN ... -1 : 2009.
31

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tiu chun quc gia tcvn -

Silicon xm khe cho kt cu xy dng Phng php

Structural silicone sealants Test methods

Part 1: Determination of flow (rheological) properties

- TCVN ... : 2009 Silicon xm khe cho kt cu xy dng - Yu cu k thut.

3 Thut ng, nh ngha

Tiu chun ny khng nu thut ng v nh ngha, tt c cc thut ng trong cc phn

Tnh cht lu bin ca silicon xm khe cho kt cu xy dng c xc nh thng qua s

Mu th c ly ngu nhin loi mt thnh phn hoc hn hp mu nhiu thnh phn

- Khun th lm t thp khng g hnh ch U hai u h c phn b mt y ko

- T lm lnh iu chnh c nhit (4,4 2) 0C.

- T sy c qut ht, iu chnh c nhit (50 2) 0C.

- Cn, chnh xc 0,1 g.

Hnh 1 Khun th hnh ch U hai u h

- Thc o, chnh xc 0,1 mm.

7 Cch tin hnh

7.1 Silicon xm khe cho kt cu xy dng mt thnh phn (loi S)

7.1.1 chy theo phng thng ng

- Ly t nht 100 g mu th cn nguyn trong bao kn n nh ti thiu 16 gi

7.1.2 chy theo phng ngang

- Qu trnh tin hnh tng t nh iu 7.1.1 ca tiu chun ny ch vi s thay i sau:

7.2 Silicon xm khe cho kt cu xy dng nhiu thnh phn (loi M)

7.2.1 chy theo phng thng ng

- Qu trnh tin hnh tng t nh iu 7.1.1 ca tiu chun ny ch vi s thay i sau:

7.2.2 chy theo phng ngang

Qu trnh tin hnh tng t nh iu 7.1.2 ch vi s thay i nh nu iu 7.2.1.

- chy ca silicon xm khe cho kt cu xy dng theo phng ngang l vic nh gi

Bo co kt qu th nghim bao gm cc ni dung sau:

2. Ngy gi mu v ngy tr kt qu th nghim.

4. Cc kt qu th nghim km theo phng php th.

6. Ngi th nghim, ngi kim tra, th trng n v kim tra.

Silicon xm khe cho kt cu xy dng Phng php

Phn 2: Xc nh kh nng n chy

Structural silicone sealants Test methods

Part 2: Determination of extrusion rate

Tiu chun ny quy nh phng php xc nh kh nng n chy ca silicon xm khe

- TCVN ... : 2009 Silicon xm khe cho kt cu xy dng - Yu cu k thut.

- TCVN ... -1 : 2009 Silicon xm khe cho kt cu xy dng. Phn 1: Xc nh chy.

Xc nh thi gian n chy ton b khi lng mu th qui nh ra khi v cha di p lc

- Theo iu 5 ca TCVN ... -1 : 2009.

- Sng xm mch, dung tch 177 ml.

- Thit b cung cp kh nn c b phn ni trc tip vi sng xm mch to p lc kh

- ng h bm giy, chnh xc n 0,1 giy.

- Cn, chnh xc 0,1 g.

- Cc, dung tch 500 ml.

6 Cch tin hnh

6.1 Kh nng n chy ca silicon xm khe cho kt cu xy dng loi mt thnh

- n nh mu th cn nguyn trong bao kn ti thiu 16 gi iu kin chun.

- Ly t nht 400 g mu c n nh trn np y 177 ml vo v cha. Lp b

6.2 Kh nng n chy ca silicon xm khe cho kt cu xy dng loi nhiu

- n nh cc thnh phn ca mu th trng thi ring r trong bao kn iu kin

- y hn hp mu th trn vo v cha v lp v cha vo sng xm mch sao

Theo iu 9 ca TCVN ... -1 : 2009.

Silicon xm khe cho kt cu xy dng Phng php

Phn 3: Xc nh cng Shore A

Structural silicone sealants Test methods

Part 3: Determination of shore A hardness

- TCVN ... : 2009 Silicon xm khe cho kt cu xy dng - Yu cu k thut.

- TCVN ... -1 : 2009 Silicon xm khe cho kt cu xy dng. Phn 1: Xc nh chy.

Theo iu 5 ca TCVN ... -1 : 2009.

- Dng c o cng Shore A c thang o t 0 n 100.

- Thc kim loi thng.

- T dng mu, iu chnh c nhit (38 2) 0C v m 95 %.