T4a (Autosaved) 8 Februari 2018

Menentukan Sifat Fisis
1. Tekanan Uap
Log(P) A+B/T+Clog(T)+DT+ET^2
Komponen A B C D E
Methanol 45.6171 -3.24E+03 -1.40E+01 6.64E-03 -1.05E-13
Air 29.8605 -3.25E+03 -7.30E+00 2.42E-09 1.81E-08
2. Kapasitas panas gas (Cp) J/gmolK

Cp A+BT+CT^2+DT^3+ET^4
Komponen A B C
Metanol 8.0840 1580.4590 239.0950
Oksigen 6.8371 339.2095 268.7000
2. Kapasitas panas liquid(Cl)

Cl A+BT+CT^2+DT^3+ET^4
Komponen A B C
Metanol 13.4310 -5.13E-02 1.31E-04
Air 8.7120 1.25E-03 -1.80E-07
4. Kapasitas Panas Campuran Liquid

deltaH CpdT
Shortcut Menara Distilasi

1. menentukan nilia tekanan
2. menentukan nilau suhu
3. menghitung tekanan uap (Po) dengan persamaan Antoine
4. menghitung fraksi umpan
5. menghitung Ki, dengan persamaan Ki=Pi/Pt
6. menghitung yi, dengan persamaan xi=yi/Ki, sehingga sigmayi =1 yang belum mendekati satu diubah suhunya
dari perhitungan neraca panas didapatkan suhu

T 99.5388208313 372.6888208313 K
P 1.15 874 mmHg
Perhitungan Kondisi Umpan

Komponen Feed(kg/jam) Feed (kgmol/jam) Zf=xi Po Ki
Metanol 2817.71294754 88.0535296107 0.2720781636 2607.7474783 2.9836927669
Air 4240.43425716 235.5796809531 0.7279218364 225.634082257 0.2581625655
Jumlah 7058.1472047 323.6332105638 1
Perhitungan Spesfikasi Hasil
Komponen Distilat Bottom
kg/jam kmol/jam xd kg/jam kmol/jam
Metanol 2760.89068462 86.2778338945 0.9973364408 56.8222629186 1.7756957162
Air 4.147557363 0.2304198535 0.0026635592 4236.28669979 235.3492611
Jumlah 2765.03824199 86.508253748 1 4293.10896271 237.12495682
Menentukan Kondisi Operasi Atas Menara Distilasi dengan sigmax =1 (melihat dew point)
Suhu Distilat 66.604312969 339.754312969 K
Tekanan 1.05 798 mmHg
Komponen Distilat(kg/jam) Distilat (kgmol/jam) xd=yi Po Ki

Metanol 2760.89068462 86.2778338945 0.9973364408 823.772819718 1.0322967666
Air 4.147557363 0.2304198535 0.0026635592 6.31E+01 0.0791166236
Jumlah 2765.03824199 86.508253748
Menentukan Kondisi Operasi bawah menara distilasi sigma y = 1 (melihat bubble point)
Suhu Distilat 145.84093827 418.9909382698 K
Komponen Feed(kg/jam) Feed (kgmol/jam) xb=xi Po Ki

Metanol 56.8222629186 1.7756957162 0.0074884388 9424.39350256 9.9204142132
Air 4236.28669979 235.3492610996 0.9925115612 885.673707067 0.9322881127
Jumlah 237.1249568158 1
Menentukan Komponen Kunci
Feed Menara Top Menara

Tbub feed 372.6888208313
Komponen PO a Komponen
Metanol (LK) 2607.7474783 11.5574183307 Metanol
Air (HK) 225.634082257 1 Air
Komponen alfa avg

Metanol 12.0289725552 3.5917033837
Air 1 1
Penentuan Tray Minimum

Nm
Perhitungan refluks minimum, refluk optimum, dan jumlah plate aktual
Kondisi umpan cair jenuh Teta 3.0062009192
Komponen Alfa xi,Fi alfaxi,Fi alfaxiFi/(alfa-Teta)

Metanol 12.0289725552 0.2720781636 3.2728207628 0.3627289812
Air 1 0.7279218364 0.7279218364 -0.36283596
1 -0.0001069788
Komponen Alfa di xi.d alfaxi.d alfaxi.d

Metanol 12.0289725552 0.9973364408 11.9969326749
Air 1 0.0026635592 0.0026635592
Rm 0.332
Rm/(Rm+1) 0.249
R 0.4984378159
R/(R+1) 0.3326383055
Nm/N
N
Perhitungan Efisiensi Plate
Penentuan feed plate

Viskositas
Komponen
Cp Sigma yCp Metanol
Air
viskositas rata2 suhu distilat
Cp Sigma yCl
diubah suhunya
yi=Kixi BM
0.8117976488 32
0.1879221688 18
1
xb R
0.0074884388 2.8251079338 D
0.9925115612 L
1 V
LO/V1
Suhu Distilat 66.59644438 339.746444381 K

xi=yi/Ki Komponen Distilat(kg/jamDistilat (kgmol/j xd=yi

0.9661334542 Metanol 2760.890685 86.2778338945 0.9973364408
0.0336662393 Air 4.147557363 0.2304198535 0.0026635592
1 Jumlah 2765.038242 86.508253748
yi=Kixi
0.0742884143
0.9253067303
1
Bottom Menara
Tdew feed 339.754312969 Tbub feed
PO a Komponen PO
823.77281972 13.0477859011 Metanol 9424.3935026
63.13506567 1` Air 885.67370707
4.3469724056
xiFi/(alfa-Teta)
alfaxi.d/(alfa-teta)
1.3296283181
0.0026635592
1.3322918773
0.42
10.349934299
Eo 27.5488949913
Na 37.5693264731
log(Nr/Ns) -0.7470027116
Nr/Ns 0.1790594674
Nr+Ns 38
0.179059Ns+Ns 38
NS 32.2290783882
Nr 5.7709216118
Umpan masuk stage 6
log(vis)=A+B/T + CT +DT^2
A B C D vis
-9.0562 1.25E+03 2.24E-02 -2.24E-05 4.53E-01
-10.2158 1.79E+03 1.77E-02 -1.26E-05 4.23E-01
ositas rata2 suhu distilat 0.4378687262 cP

1.5
86.508253748
129.762380622
216.27063437
0.60000000
Po Ki xi=yi/Ki x0 y2
8.24E+02 1.03E+00 9.66E-01 0.997336441 9.79E-01
6.31E+01 7.91E-02 3.37E-02 0.002663559 0.0212721
1 1 1.0000639
0.999957417 0
418.9909382698
a
10.6409317871
1
Isobutilen 39.2295 -2109.4 -12.567 0.0077304 -1.3659E-13
H2O 29.8605 -3152.2 -7.3037 2.4247E-09 0.000001809
Asam Metakrilat 17.5903 -3294 -2.593 6.4226E-12 -1.5429E-06
Metakrolein 1.0846 -1918.4 4.4532 -0.014392 0.000009018
Asam Asetat 28.3756 -2973.4 -7.032 -1.5051E-09 2.1806E-06
Distribusi komposisi (trial)

Komponen Feed Top Bottom
Isobutilen 0.110082975 0.11008298 0
H2O 150.2020227 150.202023 0
Asam Metakrilat 74.09585314 0.74095853 73.3548946
Metakrolein 1.178800669 1.17880067 0
Asam Asetat 2.020094158 1.71708003 0.30301412
TOTAL 227.6068537 153.948945 73.6579087
Check Feed Bubble Point

T 412.082021 K 139.082021 C
P 2.5 atm
Komponen BM Kmol/jam Kg/jam Xi Pi
Isobutilen 56.108 0.11008298 6.17653557 0.000483654 27144.0875
H2O 18.015 150.202023 2705.88944 0.6599187165 2625.3423
Asam Metakrilat 86.06 74.0958531 6376.68912 0.3255431545 358.1713
Metakrolein 70.091 1.17880067 82.6233177 0.0051791088 4730.8358
Asam Asetat 60.052 2.02009416 121.310694 0.0088753661 1386.0266
TOTAL 227.606854 9292.68911 1
Check Top Bubble Point dan Dew Point

Tdew 400.9494573 K 127.949457 C
P 2.4 atm
Komponen BM Kmol/jam Kg/jam Yi Pi
Isobutilen 56.108 0.11008298 6.17653557 0.0007150616 22644.3599156882
H2O 18.015 150.202023 2705.88944 0.9757 1893.6169
Asam Metakrilat 86.06 0.74095853 63.7668912 0.0048 238.2056
Metakrolein 70.091 1.17880067 82.6233177 0.0077 3726.5683
Asam Asetat 60.052 1.71708003 103.11409 0.0112 1012.3486
TOTAL 153.948945 2961.57027 1
Check Bottom Bubble Point dan Dew Point

Tbulb 465.3089243 K 192.308924 C
P 2.6 atm
Komponen BM Kmol/jam Kg/jam Yi Pi
Isobutilen 56.108 0 0 0.0000 58571.4234
H2O 18.015 0 0 0.0000 9848.3891
Asam Metakrilat 86.06 73.3548946 6312.92223 0.9959 1818.1166
Metakrolein 70.091 0 0 0.0000 12517.4624
Asam Asetat 60.052 0.30301412 18.1966042 0.0041 4988.9087
TOTAL 73.6579087 6331.11883 1.0000
Menghitung nilai relative volatility
Komponen alfa feed alfa bottom alfa top alfa avg

Isobutilen 75.78521206 95.062 32.215 64.760512596
H2O 7.329851313 7.950 5.417 6.9353518618
HK Asam Metakrilat 1 1.000 1.000 1
Metakrolein 13.20830517 15.644 6.885 11.708101446
LK Asam Asetat 3.869731194 4.250 2.744 3.6352216416
Distribusi sesungguhnya
log⁡〖⁡�� /𝑏�=𝐴+𝐶⁡log⁡〖 (𝛼�) 〗⁡〗
𝐶=⁡⁡⁡log⁡〖�� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗〗 /log⁡𝛼��⁡
3165138.1755
𝐴=log⁡〖�ℎ� /𝑏ℎ� 〗
A = -1.99563519
C = 4.904212925
Komponen BM fi, kmol/jam alfa di/bi di, kmol/jam

Isobutilen 56.108 0.11008298 64.7605126 7716423.9589 0.1100829752
H2O 18.015 150.202023 6.93535186 134.63060974 149.0945882003
HK Asam Metakrilat 86.06 74.0958531 1 0.0101010101 0.7409585314
Metakrolein 70.091 1.17880067 11.7081014 1755.6987315 1.178129637
LK Asam Asetat 60.052 2.02009416 3.63522164 5.6666666667 1.7170800341
TOTAL 227.606854 152.840839378
Top section
Tdew 400.9780923 K 127.978092 C
Tbulb 399.4809877 K 126.480988 C
P 2.4 atm
Komponen di Zi Pi dew Pi bulb Ki dew
Isobutilen 0.110082975 0.00072025 22655.1709 22095.035827 12.4205981002
H2O 149.0945882 0.9754892 1895.25904 1810.942622 1.0390674587
Asam Metakrilat 0.740958531 0.00484791 238.463971 225.26708526 0.130736826
Metakrolein 1.178129637 0.00770821 3728.92673 3607.1080237 2.0443677253
Asam Asetat 1.717080034 0.01123443 1013.19177 969.86697811 0.5554779426
TOTAL 152.8408394 1
Bottom section
Tbulb 465.4126217 K 192.412622 C
Tdew 467.7933613 K 194.793361 C
P 2.6 atm
Komponen bi Zi Pi dew Pi bulb Ki dew
Isobutilen 0 0 60520.7799 58651.792796 30.6279250578
H2O 1.107434546 0.014812 10390.7428 9962.3423416 5.2584730913
Asam Metakrilat 73.35489461 0.98112619 1939.30188 1808.7197345 0.9814280791
Metakrolein 0.000671032 8.9751E-06 13027.5051 13130.439856 6.5928669515
Asam Asetat 0.303014124 0.00405283 5256.97549 5055.9637253 2.6604126955
TOTAL 74.76601431 1
Menghitung Reflux Minimum
Persamaan 11.61
Coulson and Richardson, 4th Volume 6
trial nilai teta 1.391387831
komponen alfa xif alfa xi alfa-teta atas/bawah

Isobutilen 64.7605126 0.00048365 0.03132168 63.369124765 0.0004942736
H2O 6.935351862 0.65991872 4.5767685 5.5439640312 0.8255407995
HK Asam Metakrilat 1 0.32554315 0.32554315 -0.391387831 -0.8317661641
Metakrolein 11.70810145 0.00517911 0.06063753 10.316713616 0.0058776015
LK Asam Asetat 3.635221642 0.00887537 0.03226392 2.243833811 0.0001465105
TOTAL 0.0001465105
q= 0.9998534895
Persamaan 11.60
komponen alfa xid alfa xi alfa-teta atas/bawah

Isobutilen 64.7605126 0.00072025 0.04664349 63.369124765 0.0007
H2O 6.935351862 0.9754892 6.76536084 5.5439640312 1.2203
Asam Metakrilat 1 0.00484791 0.00484791 -0.391387831 -0.0124
Metakrolein 11.70810145 0.00770821 0.09024853 10.316713616 0.0087
Asam Asetat 3.635221642 0.01123443 0.04083965 2.243833811 0.0182
TOTAL Rm+1 1.2356
Rm = 0.2356
R= 0.3534
Menghitung Jumlah Tray Minimum
Persamaan 11.58
xd lk 0.0112
xd hk 0.0048
xb lk 0.0041
xb hk 0.9811
alfa lk 3.6352
Nm 4.9042
Nm 5
Menghitung Jumlah Tray Teoritis
Fig 11.11 Coulson and Richardson, 4th Volume 6

Menghitung Efisiensi Plate
Persamaan 11.67
Menghitung viskositas pada Feed alfa LK avg 3.6352216416

T 412.082021 K
miu, Cp x ln(miu) x Eo 52.3741513165

0.0429383286 0.000483654 -0.0015225 N real 26.5185946498
0.1974177499 0.659918716 -1.0706741 N real 27
0.4042546387 0.325543155 -0.2948478
0.1389320669 0.005179109 -0.0102224
0.2974903666 0.008875366 -0.0107603
total -1.388027
miu mix 0.249567211 cp

0.249567211 mNs/m2
Mennetukan Letak Feed Plate
Persamaan 11.62
B= 74.7660 log(Nr/Ns) -0.723893341

D= 152.8408 Nr/Ns 0.4848608477
xf hk = 0.3255 Nr 8.8164779262
xf lk = 0.0089 Nr 9
xb lk = 0.0041
xb hk = 0.9811
Menghitung Diameter dan Tinggi MD
Menghitung Diameter Column Berdasarkan Kecepatan Uap Maksimum

Tray Spacing = 0.4 m (0.15 m - 1 m)
Top Section Bottom Section
L 1039.593019 kg/jam L 10332.282128 kg/jam

D 2941.572808 kg/jam B 6351.1163012 kg/jam
V 3981.165827 kg/jam V 3981.1658269 kg/jam
1.105879396 kg/s 1.1058793964 kg/s
Didekati dengan rho air Didekati dengan rho asam metakrilat
rho Vap 1.299577 kg/m3 rho Vap 5.77531 kg/m3
rho Liq 937.3093 kg/m3 rho Liq 832.3414 kg/m3
Uv 0.902807501 m/s Uv 0.4024455494 m/s
Dc 1.095494887 m Dc 0.7783370928 m
Diameter column diambil nilai yang paling besar agar memnuhi kriteria
Menghitung Tinggi Menara
Space kosong plate paling atas = 1m
Space kosong plate terakhir = 2m
Space total Tray Column = 10.4 m
Tinggi Menara = 13.4 m
H/D = 12.2319147
Summary
Feed 9292.689109 kg/jam
Distilate 2941.572808 kg/jam
Bottom 6351.116301 kg/jam
Reflux min 0.235609335
Tray actual 27
Column Diameter 1.095494887 m
Column Height 13.4 m
log miu = A + B/T + CT + DT^2
Molecular Weight Komponen
Isobutilen 56.108 kg/kmol Isobutilen
H2O 18.015 kg/kmol H2O
Asam Metakrilat 86.06 kg/kmol Asam Metakrilat
Metakrolen 70.091 kg/kmol Metakrolen
ACoH 60.052 kg/kmol Asam Asetat
Ki Ki*Xi
14.286361844 0.00690966 35.7159046112
1.3817591226 0.91184871
0.1885112076 0.06136853
2.4899135575 0.01289553
0.7294877004 0.00647447
0.9994969
Ki Yi/Ki
12.414671006 5.7598E-05
1.0382 0.9398
0.1306 0.0369
2.0431 0.0037
0.5550 0.0201
1.0005479
Ki Ki*Xi
32.1115 0.0000
5.3993 0.0000
0.9968 0.9991
6.8626 0.0000
2.7351 0.0015
1.00061294
di, kg/jam bi, kmol/jam bi, kg/jam

6.1765355723 0 0
2685.9390064 1.10743455 19.9504333502
63.766891216 73.3548946 6312.9222303816 0.994
82.576284387 0.00067103 0.0470332882
103.11409021 0.30301412 18.196604154
2941.5728078 74.7660143 6351.1163011741
Ki bulb Zi/Ki Zi*Ki

12.113506484 5.7988E-05 0.0087247024
0.9928413498 0.93881219 0.9685060144
0.1235016915 0.03708144 0.000598725
1.9775811534 0.00377046 0.0152436154
0.5317253169 0.0202248 0.005973632
0.99994688 0.9990466891
Ki bulb Zi/Ki Zi*Ki

29.682081374 0 0
5.0416712255 0.00281679 0.0746772573
0.9153439952 0.9996924 0.8980679647
6.6449594415 1.3613E-06 5.963911508E-05
2.5586860958 0.00152338 0.0103699259
1.00403393 0.9831747869
(1.2 - 1.5) x Rm
Rm/(Rm+1) 0.19068271
R/(R+1) 0.26112779
dengan pembacaan grafik diperoleh:
Nm/N 0.36
sehingga diperoleh:
N 13.8888889
%
, 4th Volume 6
Untuk diameter column lebih dari 1 m, dipilih tray spacing 0.3 m - 0.6 m (Coulson, section 11.11)
eq. 11.79 Coulson Richardson
Vol. 6

Vol. 6
= A + B/T + CT + DT^2
A B C D
-5.119 341.26 0.019893 -0.000031057
-10.2158 1792.5 0.01773 -0.000012631
-4.2607 846.54 0.007605 -7.7782E-06
-2.0243 411.52 0.00225 -0.000004468
-3.8937 784.82 0.006665 -7.5606E-06
Formula Name CAS Number A B C
CH4O Methyl Alcohol 67-56-1 8.08404 1580.4585 239.096
H2O Water 7732-18-5 8.05573 1723.6425 233.08
C2H4O2 Acetic Acid 64-19-7 7.27594 1327.1634 183.913
Distribusi Komposisi (TRIAL)

Feed (kg/jam) Top Bottom Fraksi mol feed
Acetic Acid 91751.15 11751.15 80000 0.9859841207
Water 1304.2533 1100 204.2533 0.0140158793
TOTAL 93055.4033 93055.4033
Check Feed Buble Point

T 106.29 C
P 1 atm
Nama MW kmol/jam kg/jam Xi Pi
Acetic Acid 60.05 1134.346378 68117.5 0.4220753763 504.3310879491
Water 18.01528 1553.198174 27981.3 0.5779246237 947.943043553
TOTAL 2687.544552 96098.8 1

Tdew 97 C
P 0.9 atm
Nama MW kmol/jam kg/jam Yi Pi
Acetic Acid 60.05 1.9567027477 117.5 0.0013038735 356.0211855513
Water 18.01528 1498.7277467 27000 0.9986961265 682.082367267
TOTAL 1500.6844494 1

Tdew 120.26 C
P 1.1
Acetic Acid 60.05 1132.3896753 68000 0.9541054357 818.0011578421
Water 18.01528 54.470427326 981.3 0.0458945643 1505.180384072
TOTAL 1186.8601026 1
komponen alfa feed alfa bottom alfa top alfa avg

HK Acetic Acid 1 1 1 1
LK Water 1.8796046213 1.840071215 1.9158476938 1.8785906439
log⁡〖⁡�� /𝑏�=𝐴+𝐶⁡log⁡〖 (𝛼�) 〗⁡〗 A -2.7624710461

C 15.345287008
=⁡⁡⁡log⁡〖�� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗〗 /log⁡𝛼��⁡
Nama MW fi (kg/jam) fi (kmol/jam) alfa di/bi

Acetic Acid 60.05 91751.15 1527.912573 1 0.0017279412
Water 18.01528 1304.2533 72.39705961 1.8785906439 27.514521553
TOTAL 93055.4033 1600.309632 27.5162494942
SAMA
TOP SECTION
Tdew 97.11473809 C P 0.9 atm
Tbulb 97.5550888 C
Komponen di Zi Pi dew Pi bulb
Acetic Acid 2.6355889061 0.036356112 357.60595951 363.7416659166
Water 69.85810557 0.963643888 684.93815251 695.9910114006
TOTAL 72.493694476 1
Bottom Section
Tdew 120.90445532 C P 1.1 atm
Tbulb 120.87670628 C
Komponen bi Zi Pi dew Pi bulb
Acetic Acid 1525.2769839 0.998338181 835.56206243 834.7997580724
Water 2.5389540369 0.001661819 1536.2771574 1534.92740166
TOTAL 1527.815938
Persamaan 11.61
komponen alfa xif alfa*xi alfa-teta

Acetic Acid 1 0.422075376 0.4220753763 -0.2459526417
Water 1.8785906439 0.577924624 1.085683791 0.6326380022
TOTAL
Persamaan 11.60
komponen alfa xid alfa xi alfa-teta
Acetic Acid 1 0.036356112 0.0363561124 -0.2459526417
Water 1.8785906439 0.963643888 1.8102923913 0.6326380022
TOTAL Rm +1
Rm
R
Persamaan 11.58
xd lk 0.9636438876
xd hk 0.0363561124
xb lk 0.0016618193
xb hk 0.9983381807
alfa lk 1.8785906439
Nm 15.345287008
Nm 16

Persamaan 11.67

T 379.29 K
Komponen miu, Cp x ln(miu) x Eo

asam asetat 0.412834 0.4220753763 -0.37341463 Nreal
water 0.261722 0.5779246237 -0.77469242 Nreal
TOTAL -1.14810706
miu mix 0.3172367119 cp
Persamaan 11.62
B= 1527.815938 log(Nr/Ns) -0.900240216

D= 72.493694476 Nr/Ns 0.406472007
xf hk = 0.4220753763 Nr 13.5830533649
xf lk = 0.5779246237 Nr 14
xb lk = 0.0016618193
xb hk = 0.9983381807
Tray Spacing = 0.5 m
L 239200.84358 kg/jam L 335299.6435784

D 93055.4033 kg/jam B 1600.309632463
V 332256.24688 V 333699.3339459
92.293401911 kg/s 92.6942594294
Didekati dengan rho air Didekati dengan rho asam asetat
rho Vap 1.299577 kg/m3 rho Vap 2.1
rho Liq 937.3093 kg/m3 rho Liq 1050
Uv 1.2143888059 m/s Uv 1.0108084326

Dc 8.6290006264 m Dc 7.4565408818
Hasilnya ga logis, masa diameternya 10 meter -_-

Space total Tray Column = 23 m
Tinggi Menara = 26 m
H/D = 3.0130951573
Summary
Feed #REF! kg/jam
Distilate Tmax kg/jam
Bottom 0 kg/jam
Reflux min 72.493694476
Tray actual 0
Column Diamete 0m
Column Height 0m
Molecular Weight
Tmin Tmax Code Name MW Unit
-15.99 199.45 1.2 Methyl Alcohol 32.04 g/mol
0.01 373.98 1.2 Water 18.01528 g/mol
16.66 318.8 1.2 Acetic Acid 60.05 g/mol
0.4210981584
Ki Ki*Xi
0.6635935368 0.2800864917
1.2472934784 0.7208416142
1.0009281059
Ki Yi/Ki
0.5204988093 0.0025050462
0.9971964434 1.0015038994
1.0040089455
Ki Yi/Ki
0.9784702845 0.9750990406
1.8004550049 0.0254905367
1.0005895773
di (kmol/jam) di, kg/jam bi, kmol/j bi, kg/jam
2.6355889061 158.2671138107 1525.277 91592.8828861893
69.8581055703 1258.5133321182 2.538954 45.7399678818
72.4936944764 1416.7804459289 1527.816 91638.6228540711
total massa 93055.4033 total mol 1600.3096324631
Ki dew Ki bulb Zi/Ki Zi*Ki

0.5228157303 0.5317860613 0.069539 0.0193336738
1.001371568 1.0175307184 0.962324 0.9805372572
1.031863 0.9998709311

0.9994761512 0.9985643039 0.998861 0.9969048705
1.8376521022 1.8360375618 0.000904 0.0030511627
0.999766 0.9999560332
atas/bawah
-1.7160839312
1.7161216798
3.7748638E-05
0.9999622514
atas/bawah
-0.1478175317
2.861498021
2.7136804892
1.7136804892
2.5705207338
Rm/(Rm+1) 0.631497
R/(R+1) 0.719929
Nm/N 0.595
sehingga diperoleh:
N 26.89076
on, 4th Volume 6
58.3054931665 %
46.1204508222
47
maan 11.62
on and Richardson, 4th Volume 6
(0.15 m - 1 m) Untuk diameter column lebih dari 1 m, dipilih tray spacing 0.3 m - 0.6 m (Coulson, section 11.11)
Vol. 6

Vol. 6
kg/m3
kg/m3
m/s
m
Name A B C D Tmin Tmax
Methyl Alc -9.0562 1.2542E+03 2.2383E-02 -2.3538E-05 230 513
Acetic Acid -3.8937 7.85E+02 6.67E-03 -7.56E-06 2.90E+02 5.93E+02

Water -10.2158 1.7925E+03 1.7730E-02 -1.26310E-05 273 643
section 11.11)
Coulson Richardson
miu @ 25 Cmiu @ Tmax
0.539 0.047
1.13E+00 5.30E-02
0.911 0.056
H2O Water 7732-18-5 8.05573 1723.6425 233.08
C2H4O2 Acetic Acid 64-19-7 7.27594 1327.1634 183.913
Distribusi Komposisi (TRIAL) bagi 2

Acetic Acid 4587.5575 7.9133556905 4579.644144 0.9859841207
Water 65.212665 62.925666606 2.286998394 0.0140158793
TOTAL 4652.770165 4652.770165

T 116.92827541 C
P 1 atm
Acetic Acid 60.05 76.395628643 4587.5575 0.9547605925 731.8683640199
Water 18.01528 3.6198529804 65.212665 0.0452394075 1352.550781568
TOTAL 80.015481623 4652.770165 1

Tdew 97.97 C
P 0.9 atm
Acetic Acid 60.05 0.1317794453 7.913355691 0.0363561124 369.6012264276
Water 18.01528 3.4929052785 62.92566661 0.9636438876 706.540953812
TOTAL 3.6246847238 1

Tdew 120.90443586 C
P 1.1
Acetic Acid 60.05 76.263849197 4579.644144 0.9983381807 835.5615277388
Water 18.01528 0.1269477018 2.286998394 0.0016618193 1536.276210668
TOTAL 76.390796899 1

LK Water 1.8480793105 1.838615302 1.9116304365 1.861375547
log⁡〖⁡�� /𝑏�=𝐴+𝐶⁡log⁡〖 (𝛼�) 〗⁡〗 A -2.7624710461

C 15.572659284
=⁡⁡⁡log⁡〖�� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗〗 /log⁡𝛼��⁡

Acetic Acid 60.05 4587.5575 76.39562864 1 0.0017279412
Water 18.01528 65.212665 3.61985298 1.861375547 27.514521553
TOTAL 4652.770165 80.01548162 27.5162494942
SAMA
TOP SECTION
Tdew 97.11473809 C P 0.9 atm
Tbulb 97.5550888 C
Acetic Acid 0.1317794453 0.036356112 357.60595951 363.7416659166
Water 3.4929052785 0.963643888 684.93815251 695.9910114006
TOTAL 3.6246847238 1
Bottom Section
Tdew 120.90445532 C P 1.1 atm
Tbulb 120.87670628 C
Acetic Acid 76.263849197 0.998338181 835.56206243 834.7997580724
Water 0.1269477018 0.001661819 1536.2771574 1534.92740166
TOTAL 76.390796899
Persamaan 11.61

Acetic Acid 1 0.954760592 0.9547605925 -0.2459526417
Water 1.861375547 0.045239408 0.0842075269 0.6154229053
TOTAL
Persamaan 11.60
Acetic Acid 1 0.036356112 0.0363561124 -0.2459526417
Water 1.861375547 0.963643888 1.7937031683 0.6154229053
TOTAL Rm +1
Rm
R
Persamaan 11.58
xd lk 0.9636438876
xd hk 0.0363561124
xb lk 0.0016618193
xb hk 0.9983381807
alfa lk 1.861375547
Nm 15.572659284
Nm 16

Persamaan 11.67

T 389.92827541 K

water 0.236679 0.0452394075 -0.06519234 Nreal
TOTAL -1.01412437
miu mix 0.3627198984 cp
Persamaan 11.62
B= 76.390796899 log(Nr/Ns) -0.5993033115

D= 3.6246847238 Nr/Ns 0.5491941201
xf hk = 0.9547605925 Nr 16.3071426595
xf lk = 0.0452394075 Nr 17
xb lk = 0.0016618193
xb hk = 0.9983381807
L 12330.553519 kg/jam L 16983.3236844

D 4652.770165 kg/jam B 80.0154816232
V 16983.323684 V 16903.30820277
4.7175899123 kg/s 4.6953633897
Uv 0.9028075012 m/s Uv 0.7514606779

Dc 2.2626457524 m Dc 1.9463766536

H/D = 9.2811700538
Summary
Feed #REF! kg/jam
Bottom 0 kg/jam
Reflux min 3.6246847238
Tray actual 0
Column Diamete 0m
Column Height 0m
Molecular Weight
0.01 373.98 1.2 Water 18.01528 g/mol
16.66 318.8 1.2 Acetic Acid 60.05 g/mol
0.4210981584 Diameter 2.2626457524 m

1.9463766536 m
Tinggi 21 m
Ki Ki*Xi
0.9629846895 0.9194198327
1.779672081 0.0805113105
0.9999311432
Ki Yi/Ki
0.5403526702 0.0672821926
1.0329546108 0.9329005142
1.0001827068
Ki Yi/Ki
0.9994755116 0.9988620722
1.8376509697 0.0009043172
0.9997663894
di (kmol/jam) di, kg/jam bi, kmol/j bi, kg/jam
0.1317794453 7.9133556905 76.26385 4579.6441443095
3.4929052785 62.9256666059 0.126948 2.2869983941
3.6246847238 70.8390222964 76.3908 4581.9311427036

0.5228157303 0.5317860613 0.069539 0.0193336738
1.001371568 1.0175307184 0.962324 0.9805372572
1.031863 0.9998709311

0.9994761512 0.9985643039 0.998861 0.9969048705
1.8376521022 1.8360375618 0.000904 0.0030511627
0.999766 0.9999560332
atas/bawah
-3.8818879352
0.1368287176
-3.7450592176
4.7450592176
atas/bawah
-0.1478175317
2.9145862999
2.7667687682
1.7667687682
2.6501531522
Rm/(Rm+1) 0.638568
R/(R+1) 0.726039
Nm/N 0.62
sehingga diperoleh:
N 25.80645
on, 4th Volume 6
56.5443249753 %
45.639330957
46
maan 11.62
Vol. 6

Vol. 6
kg/m3
kg/m3
m/s
m
Methyl Alc -9.0562 1.2542E+03 2.2383E-02 -2.3538E-05 230 513

Water -10.2158 1.7925E+03 1.7730E-02 -1.26310E-05 273 643
Untuk 15 MD diameter 2,6 m H 21 m

section 11.11)
Coulson Richardson
0.539 0.047
1.13E+00 5.30E-02
0.911 0.056
H2O Water 7732-18-5 8.05573 1723.6425 233.08
C2H4O2 Acetic Acid 64-19-7 7.27594 1327.1634 183.913
Distribusi Komposisi (TRIAL)

Acetic Acid 91751.15 158.26711381 91592.88289 0.0017007837 0.9859841207
Water 1304.2533 1258.5133321 45.73996788 0.0135243445 0.0140158793
TOTAL 93055.4033 93055.4033 1

T 116.92827541 C
P 1 atm
Acetic Acid 60.05 1527.9125729 91751.15 0.9547605925 731.8683640199
Water 18.01528 72.397059607 1304.2533 0.0452394075 1352.550781568
TOTAL 1600.3096325 93055.4033 1

Tdew 97.97 C
P 0.9 atm
Acetic Acid 60.05 2.6355889061 158.2671138 0.0363561124 369.6012264276
Water 18.01528 69.85810557 1258.513332 0.9636438876 706.540953812
TOTAL 72.493694476 1

Tdew 120.90443586 C
P 1.1
Acetic Acid 60.05 1525.2769839 91592.88289 0.9983381807 835.5615277388
Water 18.01528 2.5389540369 45.73996788 0.0016618193 1536.276210668
TOTAL 1527.815938 1

LK Water 1.8480793105 1.838615302 1.9116304365 1.861375547
log⁡〖⁡�� /𝑏�=𝐴+𝐶⁡log⁡〖 (𝛼�) 〗⁡〗 A -2.7624710461

C 15.572659284
=⁡⁡⁡log⁡〖�� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗〗 /log⁡𝛼��⁡

Acetic Acid 60.05 91751.15 1527.912573 1 0.0017279412
Water 18.01528 1304.2533 72.39705961 1.861375547 27.514521553
TOTAL 93055.4033 1600.309632 27.5162494942
SAMA
TOP SECTION
Tdew 97.977042093 C P 0.9 atm
Tbulb 97.5550888 C
Acetic Acid 2.6355889061 0.036356112 369.70133826 363.7416659166
Water 69.85810557 0.963643888 706.72115636 695.9910114006
TOTAL 72.493694476 1
Bottom Section
Tdew 120.90445532 C P 1.1 atm
Tbulb 120.87670628 C
Acetic Acid 1525.2769839 0.998338181 835.56206243 834.7997580724
Water 2.5389540369 0.001661819 1536.2771574 1534.92740166
TOTAL 1527.815938
Persamaan 11.61

Acetic Acid 1 0.954760592 0.9547605925 -0.7915625063
Water 1.861375547 0.045239408 0.0842075269 0.0698130407
TOTAL
Persamaan 11.60
Acetic Acid 1 0.036356112 0.0363561124 -0.7915625063
Water 1.861375547 0.963643888 1.7937031683 0.0698130407
TOTAL Rm +1
Rm
R
Persamaan 11.58
xd lk 0.9636438876
xd hk 0.0363561124
xb lk 0.0016618193
xb hk 0.9983381807
alfa lk 1.861375547
Nm 15.572659284
Nm 16

Persamaan 11.67

T 389.92827541 K

water 0.236679 0.0452394075 -0.06519234 Nreal
TOTAL -1.01412437
miu mix 0.3627198984 cp
Persamaan 11.62
B= 1527.815938 log(Nr/Ns) -0.5993033115

D= 72.493694476 Nr/Ns 0.2515919195
xf hk = 0.9547605925 Nr 9.2468064995
xf lk = 0.0452394075 Nr 10
xb lk = 0.0016618193
xb hk = 0.9983381807
L 52379.131147 kg/jam L 145434.534447

D 1416.7804459 kg/jam B 91638.62285407
V 53795.911593 V 53795.91159292
14.943308776 kg/s 14.9433087758
Uv 0.9028075012 m/s Uv 0.7514606779

Dc 4.0269835617 m Dc 3.4722874224

H/D = 5.2148213863
Summary
Feed #REF! kg/jam
Bottom 0 kg/jam
Reflux min 72.493694476
Tray actual 600.75013639
Column Diamete 0m
Column Height 0m
Molecular Weight
0.01 373.98 1.2 Water 18.01528 g/mol
16.66 318.8 1.2 Acetic Acid 60.05 g/mol
0.4210981584 0.984283337
Ki Ki*Xi
0.9629846895 0.9194198327
1.779672081 0.0805113105
0.9999311432
Ki Yi/Ki
0.5403526702 0.0672821926
1.0329546108 0.9329005142
1.0001827068
Ki Yi*Ki
0.9994755116 0.9978145639
1.8376509697 0.0030538439
1.0008684078
di (kmol/jam) di, kg/jam bi, kmol/j bi, kg/jam 0.111709
2.6355889061 158.2671138107 1525.277 91592.8828861893 0.888291
69.8581055703 1258.5133321182 2.538954 45.7399678818
72.4936944764 1416.7804459289 1527.816 91638.6228540711

0.5404990326 0.5317860613 0.067264 0.0193336738
1.0332180649 1.0175307184 0.932663 0.9805372572
0.999927 0.9998709311

0.9994761512 0.9985643039 0.998861 0.9969048705
1.8376521022 1.8360375618 0.000904 0.0030511627
0.999766 0.9999560332
atas/bawah
-1.2061720773
1.206186209
1.41317338E-05
0.9999858683
atas/bawah
-0.0459295534
25.692952926
25.6470233726
24.6470233726
36.9705350589
26.5056911603
600.750136389
15.5726592835
Rm/(Rm+1) 0.961009
R/(R+1) 0.973664
Nm/N 0.7
sehingga diperoleh:
N 22.85714
on, 4th Volume 6
56.5443249753 %
40.4234074191
46
maan 11.62
Vol. 6

Vol. 6
kg/m3
kg/m3
m/s
m
Methyl Alc -9.0562 1.2542E+03 2.2383E-02 -2.3538E-05 230 513

Water -10.2158 1.7925E+03 1.7730E-02 -1.26310E-05 273 643
section 11.11)
Coulson Richardson
0.539 0.047
1.13E+00 5.30E-02
0.911 0.056
REBOILER PADA MD-02 (Kern, hal 465)
Tugas : Memanaskan produk bawah MD-02 sebanyak 91638.62 kg/jam
dengan menggunakan steam sebanyak 7018.22 kg/jam
Alat : Kettel
Fluida Dingin : Hasil Bawah Menara Distilasi

T= 393.9 K 120.8767 C P= 1.0133
249.6 F 14.89
T out Reboiler = 120.90 C 393.90 K

249.6 F
Fluida panas : Steam Saturated
P= 140.000 Psia 9.52 atm (Tabel 7)
T= 353.02 F
H= 868.20 Btu/lb
(1) Duty
Neraca panas di sekitar Reboiler : Rin-Rout =Racc
F*HF + Qr = Qc + D*HD + B*HB
Qr = Qc + D*HD + B*HB - F*HF 4697414.97
Beban Reboiler Qr = 4697414968.572 J/jam 4697414.97 KJ/JAM
= 4473728.5415 Btu/jam 4697414.97 KJ/JAM
T1 T2
tw2 tw1
Hot fluid Cold fluid Difference

K F K F
451.3 353.02 Higher Temp 393.90 249.63 103.39
451.3 353.02 Lower Tem 393.88 249.58 103.44
0 Difference 0.05 0.05
m steam = 5152.88 lb/jam - Laju alir fluida dingin, Wc = 91638.62

2339.41 kg/jam 5152.877840932 202028.34
t 2  t1
LMTD   103.42 F
2.3 log t 2
t1
(2) Trial UD
UD = 200-700 untuk Aqueous Solution-steam (Miu<2 cp)
Diambil UD = 200 (Kern, 1950)
(3) delt = weighted delt = delt LMTD Tc = Ta = 353.02 F

= 103.42 F tc = ta = 249.60 F
(4) Luas transfer panas Qr

A A= 216.2957 ft2 20.0945286
U D  Δt
(5) Jenis HE : Shell & Tube Heat Exchanger hal.230 kern
(6) Trial Lay Out HE
TRIAL AWAL : L, ft = 18 a" = 0.1963
OD, in = 0.75 3/4 in
pass = 1 Triangular pitch
A
Nt 
L    OD
= 61.21 tubes 1206 pada IDs =
Diambil : Shell Tube
ID, in 39 Nt 1206
Pass, n 1 OD, in 0.75
L, ft 18 Pt, in 1
Clearance(C'),in 0.3800 ga usah ah… 1.0000
Baffle Space,in 7.8000 ID,in 0.62
Koreksi UD :
A= 4261.2804 ft2 Check maximum flux : Q/A = 1049.85547
UD = 10.1517 harus mendekati UD trial. (batasan untuk organic`s reboiler
70.000 to 125.000 Btu/jam ft2)
HOT FLUID : TUBE SIDE, steam COLD FLUID : SHELL SIDE, liquid from MD
DIRT FACTOR
(7) Flow area : (7) Asumsikan ho sistem komponen terbanyak air..jd, an
at'= 0.302 in2 [Table 10] ho = 900
tc = 249.60
Nt at'
at 
144  n ho  (TV  ta )
= 2.5293 ft2 tw  ta 
m hio  ho
(8).
G t  = 288.384403
at
= 2037.3146 lb/jam ft2 dtw = 38.81
emang asumsinya udah benar???

Dari Fig 15.11 diperoleh :
D G
(9) Hitung Re  t
ho = >900
 hence use ho trial.
Pd Ta= 353.02 F
miu = 0.0363 lb/ft jam (Fig 15)
D=IDt= 0.62 in [Table 10]
= 0.0517 ft
Re = 2899.8
(10) steam condensing :
hio = 1500 Btu/jam ft2 F
(12) Clean overall coeficient

h io  h o
UC  = 562.5000 Btu/hr ft2 F
h io  h o
h io  h o
UC 
(13) Dirt factor h io  h o
(U C  U D )
Rd 
UC  UD
= 0.0967 > Rd min = 0.003
PRESSURE DROP
(1) Re = 2899.76 diperoleh Reboiler sejajar bottom
f= 0.0003 [Fig 26]
(2) s= 0.3106 hydrostatic head <<<
2
f Gt Ln
 Pt  fluid velocity <<
5, 22  10 10  D  s  
= 0.0000 psi DP <<
(3). 2
 4n  V
 Pr    negligible
 s  2g '
dgn (V^2)/2g' = 2.50E-02 [Fig 27]
Pr  0.3220 psi
(4).P
T  Pt  Pr
= 0.3220 psi < 2 psi
Oke !
SUMMARY :
Lay Out : SHELL TUBE

IDshell, in 39 Nt 1206
IDbundle, in 39 OD, in 0.75
circle supp. plates = 39 Pt, in 1 Triangular
BWG 16
Operation Condition
HOT fluid fluid COLD fluid
1500 houtside 900.0000
UC 562.5000
UD 10.1517
Rd calc. 0.0967
Rd req'd. 0.003
0.3220 Calc dP 0
2 Allow. dP 2
Ada = 1 reboiler
harga pembuatan steam lebih besar dari harga alat ya??
atm
psi
klo 5 reboiler :
dTw= 28.446
P= 70.000 Psia
T= 302.92 F
H= 907.90 Btu/lb
1197.24 tubes 1200
steam total yg dibutuhkan :

R-01 7018.22 kg/jam T= 353.02 F P=
R-02 #REF! kg/jam T= 292.71 F P=
R-03 #REF! kg/jam T= 417.33 F P=
4697414969 J/jam 4473729 Btu/jam

neraca panas reboiler BHB
QC 7059818.634
DHD 410164.9284
BHB 615247.3927
FHF 8085230.955
QR 0.00000000
kg/jam
lb/j
m2
39 in
BWG 16
n 1
Triangular pitch
De, ft 0.0592
Btu/jam ft2 < 125.000 < Heat flux maximum untuk natural circulation (12500)
(batasan untuk organic`s reboiler ??? kern
70.000 to 125.000 Btu/jam ft2)
HELL SIDE, liquid from MD
istem komponen terbanyak air..jd, anggap ho asam asetat! T= 393.8767 K

Komponen A B miu, mNs/m2
F H2O 658.2500 283.1600 0.2221
C6H12O6 0.0000
H2SO4 0.0000
Yeast 0.0000
F C2H5OH 686.6400 300.8800 0.2892
yup!!
k(cµ/k)^1/3 0.37
btu/(ft2.j. oF) De 0.710721868 in
0.059226822 ft
at 0.80 ft2
Gs 251670.3092 lb/ jam. ft2
Re #DIV/0!
jh 100
ho 624.7169529
er sejajar bottom
static head <<<
d velocity <<
140.000 Psia
60.000 Psia
300.000 Psia
xi,f wi/miui
#DIV/0! #DIV/0!
#DIV/0! 0.0000
#DIV/0! 0.0000
#DIV/0! 0.0000
#DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0!
Kondenser
Tugas : Mengembunkan uap hasil atas menara distilasi
Jenis :
Kondisi Operasi :
P= 0.9 atm 684
T masuk = 371.127042 K 97.9770420929
Kec. Distilat = 72.4936945 kgmol/j 20.1371373545
Refluks rasio = 1.5
distilat 1416.78045 kg/jam
Komposisi Umpan Masuk
Komp. di,kmol/j xD BM
Asam Asetat 2.63558891 0.0363561124 60.05
Air 69.8581056 0.9636438876 18.01528
Jumlah 72.4936945 1
kondenser total, suhu keluar kondenser pada T boiling point dimana:
y i  K i  xi  1
Tbp = 371.1270420929 K 98.1270420929 C

T h,in
T c,out
Neraca Panas sekitar kondenser :

Q c  L0  H L  DH D  V  HV
V
Lo D
T referensi = 298 K
komponen D,kmol/jam Lo, kmol/j V, kmol/j D,kg/jam
Asam Asetat 2.6355889061 3.95338336 6.5889722652 158.267113811
Air 69.8581055703 104.787158 174.645263926 1258.51333212
Jumlah 72.4936944764 108.740542 181.234236191 1416.78044593
Perhitungan entalpi
komponen hD, kJ/kmol h0, kJ/kmol H1, kJ/kmol D.hD
Asam Asetat 9801.681344664 9801.68134 31743.3591794 25833.202613
H2O 5501.605328168 5501.60533 45097.5575574 384331.725821
Jumlah 15303.28667283 15303.2867 76840.9167367 410164.928434
Sehingga beban kondenser :

7059818.63 kj/jam 6691387.8791
pendingin yang digunakan adalah air pada suhu 40oC=104oF
hot fluid cold fluid

208.6286757672 F higher temp. 150 F
208.6286757672 F lower temp. 104 F
0F diff. 46 F
40
perhitungan air yang dibutuhkan Cp air =
sehingga :
m air = 145464.954 lb/jam
65982.4702 kg/jam
trial UD
Kern table 8 untuk asam asetat dengan air, UD = 250- 500
diambil UD = 150 Btu/jam.ft2.F
TLMTD 
 Thin  t cout    Thout  tcin 
ln
 Thin  tcout 
 Thout  tcin 
delta LMTD 79.4207484 C 174.957347049
luas transfer panas

Q 26243.6020573
A
U D  TLMTD
A= 254.972159 ft2 23.6876886957
Layout trial awal : 8 ft

2.4384 m OD= 0.75 in
at= 0.2618 ft2/ft

at' 2.0944 ft2
A
Nt 
  L  OD
A
Nt 
  L  OD Nt= 162.402649108 buah
tabel 9 Kern :
diambil Nt 166 buah
SHELL TUBE
ID,in : 17.25 OD, in :
L, ft : 8 Pt, in :
pass : 1 at :
Nt : 166 at':
Horizontal 12 BWG ID,in :
tube pass :
square
koreksi Ud :
wt = 145464.9538935 lb/hr A= 260.62 ft2
Ws = 3123.434171095 lb/hr Ud= 146.749381724 Btu/jam.ft2.F
heat flux = Q/A 25674.8825075
LIHAT KERN 483!!

HOT FLUID : shell side, vapor
Asumsi ho = 300 Btu/hrft2F
tw = 144.11785 F
tf = 176.373263 F
G" = 12.9261833
sf = 0.92875526
μf = 0.34985499 cp
kf = 0.65371473 Btu/hrftF
Fig.12.9 ho = 590 Btu/hrft2F
hio . ho
Uc=
hio  ho
387.685521
Rd= Uc  UD
Rd 
U c .U D
0.00423493 > 0,002 (Table 12, Kern)
PRESSURE DROP
HOT FLUID : shell side, vapor

B: 2.9325 in
C': 0.5625
Pt: 1.3125 in
as = ID x C'B/144Pt
= 0.15055246 ft2
Gs = 20746.4844 lb/hrft2
De = 1.78395172 in
0.06031472 ft
μ (at Tin) = 0.34985499 cp
 Pr  (4n / s) (V 2 / 2g)
0.84664909 lb/fthr
Re = 1477.96589
(N+1) = 12L/B
32.7365729
s= 0.92875526
Fig. 29 f = 0.0027
= 0.00093512 psi
Allowable ∆P 2,0 psi
Havp
Komponen A Tc n
asam aseta 11.575 592.71 -0.65
mmHg Air 52.053 647.13 0.321
C
gmol/s
Cp liq
Komponen A B C
Asam Aseta -18.944 1.10E+00 -2.89E-03
Air 92.053 -0.039953 -0.00021103
BM mean rho
2.1831845508 1050 kg/m3
17.3603144551 1000 kg/m3
19.5434990058 1001.817806 rho campuran
T h,out
T c,in
Lo, kg/j V, kg/j

237.400670716 395.6677845
1887.76999818 3146.28333
2125.17066889 3541.951115 0.6
L0.h0 V1.H1
38749.8039195 209156.1132
576497.588732 7876074.842
615247.392651 8085230.955
Btu/jam
different
58.6286757672 F ta = 127 F
104.628675767 F Tv = 208.62868 F
-46 F
1 Btu/lb.F
T 371.12704
Cp liquid
komponen A B
As asetat -18.944 1.0971
H2O 92.053 -0.039953
Jumlah
F
Viskositas Cairan
log10μ = A+B/T+CT+DT^2
BTU/jamf2
Komponen A B
m2 Asam Asetat -3.8937 7.85E+02
H2O -10.2158 1792.5
BWG 12 Jumlah
Conductivity
C' 0.5625 A B C
B 2.9325 As. Asetat -1.2836 0.5893 592.71
De, in 0.95 Air -0.2758 0.004612 -5.5391E-06
ft 0.079166667
0.75 Densitas Cairan

1.3125
0.1707 0.113145139
0.1963 Densitas A B
0.532 As. Asetat CH3COOH 0.35182 0.26954
2 Air H2O 0.3471 0.274
ρair = 62.5 lb/ft3

ρkondensat = 1001.817806 kg/m3
58.04720396 lb/ft3 Cp mean 77.818874 kJ/kmolK
btu/jam.ft2 μ mean 0.349855 cp
k mean 0.6537147 W/mK
ρ mean 0.4062273 g/cm3
COLD FLUID : tube side, water
Flow area massa 1416.7804 kg/jam
Cp mean 0.9757921 Btu/lbF
0.113145139 ft2 μ mean 0.9385131 lb/hrft
Gt = wt/at k mean 0.6537147 Btu/hrftF
1285649.17 lb/hrft2 ρ mean 58.047204 lb/ft3
v = Gt/3600ρ
5.713996311 ft/s
ta = 127 F
Fig. 25 Kern
hi 1593.875 Btu/hrft2F blumcek
hio 1130.588667 Btu/hrft2F
μair = 1 cp
2.42 lb/fthr
COLD FLUID : tube side, water

Re = 282630.3134
Fig. 26 f = 0.00012
s= 1
fGt2 Ln
Pt 
5.22  101 0 Ds
= 1.371340452
Fig. 27 (v^2/2g) 0.16
 Pr  (4n / s) (V 2 / 2g)
= 1.28
= 2.651340452 psi
Allowable ∆P 10 psi
D Cp xi
2.93E-06 139.521 5.07E+00
5.3469E-07 7.55E+01 7.27E+01
77.8188744124 kJ/kmolK
komposisi xi
PO 0.1674561342 0.0002896678
H2O 569.95943108 0.9859230841
PG 5.5155774616 0.0095409162
DPG 2.4547928915 0.004246332
578.09725757 1
C D Cp xi Cp.xi
-0.0028921 2.9275E-06 133.814391988 0.0363561 0.0387617
-0.00021103 5.3469E-07 75.2115717361 0.9636439 74.152825
Kj/KmolK
C D myu xi myu.xi
6.67E-03 -7.56E-06 0.4500 0.0363561 1.64E-02
0.01773 -0.000012631 2.85E-01 0.9636439 0.3334954
0.3499 CP
k x k.x
0.1449727274 0.0363561124 0.0052706448
0.6729084211 0.9636438876 0.6484440869
0.6537147317
W/mK
n Tc rho x rho.x
0.26843 592.71 0.4012901564 0.0363561 0.0145894
0.28571 647.13 0.4064135655 0.9636439 0.3916379
0.4062273 g/cm3
Hvap 39509.500574 kJ/kmol

μ steam 0.0148 cp
Mr mean 19.05753436 kg/kmol
cp steam 0.458 Btu/lbF

Hvap 943.7278513 Btu/lb
μ steam 0.0358021396 lb/hrft
k steam 0.0137 Btu/hrftF
ρ steam 0.0367151204 lb/ft3
REBOILER (RB-02)
Tugas : Menguapkan sebagian hasil bawah Menara Distilasi (MD-02)

dengan menggunakan pemanas steam jenuh
Alat : Thyrmosyphon Reboiler
Cairan masuk dalam bubble point pada suhu 412 K dan uap keluar dalam dew point pada suhu 424,5 K
Cold fluid Suhu masuk, t1 = 393.88 K 249.58 F

Suhu keluar, t2 = 393.90 K 249.63 F
sampai sini Beban panas, Qb = 1121958.29 kcal/jam 4452267 Btu/jam
Jumlah cairan = 91638.6229 kg/jam 202025.18 lb/jam
Tekanan = 1.0 atm
Steam Suhu masuk, T1 = 477.9722 K 400.95 F

Suhu keluar, T2 = 477.9722 K 400.95 F
hfg = 825.1 Btu/lb
Jumlah steam yang dibutuhkan = 5396.0333077 lb/jam
2447.6407084 kg/jam
Dt hot fluid cold fluid difference

400.95 higher temp. 249.63 151.32 Ta = 400.95
400.95 lower temp. 249.58 151.37 ta = 249.60
0.00 difference 0.05 -0.05
LMTD = 151.3470 oF
Delta t =LMTD = 151.3470 F
UD UD diantara 100-200 Btu/jam.ft^2.F

Diambil UD = 132 Btu/jam.ft^2.F
A = Q/(delta t*UD)
A= 222.8608 ft^2
Dipakai tube :
OD = 0.75 in
BWG = 16
L= 14 ft
at' = 0.1963 ft^2
Nt = A/(L*at')
Nt = 81.0934 buah
Spesifikasi Alat
Tube Shell
Nt = 376 IDs = 23.25

L= 14 ft B= 4.65
OD = 0.75 in n= 1
ID = 0.62 in
BWG = 16
PT = 1 in
n= 2
Koreksi UD :
A= 1033.3232 ft^2
UD = 28.4689 Btu/jam.ft^2.F
Tube side (steam) Shell side (Hasil Bawah MD-02)
at' = 0.1963 ft^2 Asumsi ho = 300
at = (Nt*at')/(144*n) ho  (TV  ta )
tw  ta 
= 0.2563 ft^2 hio  ho
Gt = W/at = 21055.1803 lb/ft^2.jam
IDt = 0.0517 ft tw = 274.82754 F
Sifat-sifat fisis steam = Delta tw = tw-ta = 25.224492 F

Cp = 3.2379 btu/lb/F
Miu = 0.04114 lb/ft/j Dari Fig 15,11, diperoleh ho = > 300
k= 0.02114 btu/ft/j/F Maka dipakai hv = 300
hio untuk steam = 1500 C' = 0.3800 in

Pressure drop
Ret = (De*Gt)/miu = 26442.65879 a  ID S  C'B = 0.2853 ft^2
S
Dari Fig 26 diperoleh : 144  PT
f= 0.00016
W
spesific volume untuk steam = 0.932 GS  = 708122.6623 lb/ft^2.jam
s= 0.0149 aS
2
f Gt L n De = 0.73 in
 Pt  0.0608 ft
5, 22  10 10  D  s  
miu = 0.2133 cp
= 0.0494 psi 0.5163 lb/ft/j
(V^2)/2g' = 0.0013 [Fig 27]
2 Res = 83435.2905
 4n  V
 Pr    = 0.6974
 s  2g ' Dari Fig 29 diperoleh :
f= 0.0023
Delta P total = 0.7468 N+1 = 36.1290
Rho = 55.2843 lb/ft3
s= 0.8845
2
0,5  f  GS  DS  (N  1)
PS 
5,221010  De s
= 14.3707 psi
h io  h o
UC  = 250.0000
h io  h o
(U C  U D ) = 0.0036
Rd 
UC  UD
(U C  U D )
Rd 
UC  UD Oke!!!
SUMMARY :
Lay Out : Tube Shell

Nt 376 ID, in 23.25
OD, in 0.62 Pass, n 1
Pt, in 1 triangular L, ft 14
BWG 16
pass 2
Operation Condition
hot fluid fluid cold fluid

1500 houtside 300
UC 250.0000
UD 28.4689
Rd calc. 0.0036
Rd required 0.003
0.7468 Calc dP 14.3707
10 Allow. dP 2
Neraca Panas Reboiler MD-02
cp cairan A B C
C2H4O2 AS.ASETAT -18.944 1.0971 -0.002892
salah harusC3H8O3 GLISEROL 132.145 8.6007 -0.001975
Reboiler MD-02 INPUT

lam dew point pada suhu 424,5 K T MASUK 393.87671
KOMPONEN MR FASE m n=m/mr
Asam Asetat 60.05 91592.9 1525.2773
Air 18.01528 45.74 2.5389558
F
F
Shell
in
D cp gas A B C D
2.928E-06 C2H4O2 AS.ASETAT 34.85 3.76E-02 2.83E-04 -3.08E-07
1.807E-06 C3H8O3 GLISEROL 9.656 4.29E-01 -2.68E-04 3.18E-08
OUTPUT
K T KELUAR 393.90446 K
cp.dT Q m n=m/mr cp.dT Q
143.38763 218705.9 91592.9 1525.2773 77.0246 117483.8195
3323.8443 8439.0938 45.74 2.5389558 139.5792 354.38546
E
9.26E-11
2.77E-11
kebutuhan panas
sek sek reflux sek
ACCUMULATOR (AC-03)
Tugas: Menampung condensat dari CD 1416.7804459289

Alat: Silinder Horizontal
Kondisi Operasi: T: 371.1270420929
P: 0.9
Umpan masuk: 1416.7804 kg/jam

0.8668504931 lb/s
komposisi kg/j MR X
Asam asetat 7.9134 60.05 0.0363561124
AIR 62.9257 18 0.9636438876
JUMLAH 70.8390 22.6974 1
rho (liq)= 1001.817805621 kg/m3

Volume umpan= 0.000392836 m3/s 1.4142096876
Dari Fig 5-4 Evans diperoleh :
Untuk flow rate = 0.0138811316 cuft/s
Maka : L/D ratio = 1
L, shell length = 1 ft
D, drum diameter = 1 ft
Holding times = 5 menit
cara membaca fig 5-4 evans
PERHITUNGAN TEBAL DINDING
Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c
Jari-jari dalam, R
Di = 1 ft
R= 0.5 ft
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar =
Pdes =Pudara*1.1 =
Maximal allowable stress

Material = Stainless steel
S= 18750
Joint Effisiensi, E=
Corrosion All., c =
Maka tebal dinding :

t = 0.1249 in
Dipilih tebal plat standar =
PERHITUNGAN TEBAL HEAD
Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt =
t = 0.1249
Dari Tabel 5-8 B&Y, diambil sf =
OD = ID + 2t = 12.2498040924
a = ID/2 = 6
Dari Tabel 5-7 B&Y
untuk t=0.1875 in, OD=12an in maka diperoleh
AB = a-icr = 5.125
BC = r-icr = 13.125
AC = ((BC^2)-(AB^2))^0.5 =
b = r - AC = 1.9169540264
OA = t + b + sf =
kg/jam
371.13 K 98.13 C
0.90 atm
rhoi moli xi trial awal : 5 menit

1050 0.1318 0.0363263965
1000 3.4959 0.9636736035
3.6276 1
0.0138811316 cuft/s
0.8328678961 cuft/men
1 1.3872367199 cuft 0.1178508 cum

1 ft 1.2090018713 ft 0.3685083 m
1 ft 1.2090018713 ft 0.3685083 m
5 menit
14.5082
2.5082
ft = 12 in
ft = 6 in
1 atm
0.99 atm
-0.147 psig
psig
0.85
0.125 0.3048
3.1735943419
0.1875 in = 3/16 in
1 ft = 12 in
in
0.1875 in
2
12.375 in
in
icr = 0.875
r = 14
in
in
12.0830459736 in
in
4.1045 in 0.3420378355 ft
0.1042531323 m
V 1
CD-01
AC-01
Lo D
P=1 a t m
MD-01
Densitas (g/ml)
Komponen A B n Tc (K)
PO 0.31226 0.27634 0.29353 482.25
AIR 0.3471 0.274 0.28571 647.13
PG 0.31839 0.26106 0.20459 626
DPG 0.33335 0.265 0.2857 654
KOH Storage Tank
Tugas = Menyimpan Isobutilene sebanyak 800 kg/jam selama 30 hari
Alat = Tangki cone head
Jumlah = 1
Kondisi =
Tekanan = 1 atm
Suhu = 303 K 30 C
Kapasitas = 800 kg/jam
Komponen Densitas
KOH 2044 kg/m3
Dimensi Tanki
Komponen Debit (kg/jam) Rho (kg/m3) Fv (m3/jam)

KOH 800 2044 0.391389432
Waktu penyimpanan (t) = 1 hari

= 24 jam
Jumlah Tanki = 1 Buah Massa dala 19200 kg
Volume = Fv x t = 9.39334638 m3 331.7229 ft3
Over design = 20%
Volume sesungguhnya = 11.27201566 m3 Volume bin = volume silinder + volume kerucut
= 71.00167625 bbl
P design = 1.2 atm 17.64 psi Diambil teta = 50
Diambil B = 0,1 D 0.6328182
L/D = 2 ulrich (1984) volume kerucut = 39.493662
D= 1.93 m
Diameter tangki = 6.33 ft 75.93818 in
L= 3.86 m jari jari tan 37.96909 in
= 12.66 ft
Volume silinder 398.0674762 ft3 VOLUME BIN = 437.56114 ft3
12.390352 m3
Pemilihan tinggi course: Tinggi Tangki = H + h' + h 16.804262
Course = 6 8 ft 5.121939
N course = 2.109393895 1.582045421
3 2
L= 18 16 ft
Dimameter & Tinggi Standard:

(Brownel and Young)
Diameter tanki = 10 ft 3.05 m
= 120 in
Panjang tanki = 14 ft 4.27 m
= 168 in
volume 1099.557429 1
Bahan konstruksi: (Tabel 13.1 Brownell Young)
Jenis = Carbon Steel
Tipe = Stainless Steel 316 AISI
Max. Allowable Stress (f) = 12650 psi 860.54422 atm
Corosion allowance (c) = 0.125 (Rule of thumb = 1/8 - 3/16)
Joint Effiency (Ɛ) = 80% (Tabel 13.2 Brownell Young)
Tebal Shell Tanki

Lebar tiap course = 8 ft
N course = 1.75
Tekanan pada masing-masing course:

P design = 1 atm
14.69594878 psi
Tebal shell pada tiap course:
�=(�×𝑟�)/(𝐸×𝑓⁡−0,6×�)+�
standard
t= 0.1802 in 1.75 in
Tebal dan Tinggi Head
Code flanged and dished

OD Keterangan:
ID = diameter dalam head
OD = diameter luar head
icr b
OA t = tebal head
B A
icr = jari-jari dalam sudut dish
sf r = jari-jari dish
r
ID b = tinggi head
t
sf = straight flange
a
C
ID
t
a
C
Tebal Head
�_ℎ𝑒𝑎�=(0.885�×𝑟)/(𝑓×𝜖−0.1�)+�
standard
t head = 0.149398357 in 1.625 in
Tinggi Head
Data: ID = 72.68818021 in 6.0573484 ft
OD = 75.93818021 in 6.3281817 ft
t head = 1.625 in 0.1354167 ft
icr = 5.25 ft Table 5.7 (Brownell and Young)
r= 36 ft Table 5.7 (Brownell and Young)
sf = 2 in 0.1666667 ft Standard straight flange (sf) berkisar 1,5
𝑎=𝐼𝐷/2
a= 3.0287 ft
𝐴�=𝑎−��𝑟 AB = -2.2213 ft
�𝐶=𝑟−��𝑟 BC = 30.7500 ft
𝐴𝐶=√( 〖�𝐶〗 ^2− 〖𝐴�〗 ^2⁡) AC = 30.6697 ft
𝑏=r−AC b= 5.3303 ft
𝑂𝐴=�+𝑏+𝑠𝑓 OA = 5.6324 ft
olume kerucut
ft
ft3
ft
m
am sudut dish
Brownell and Young)
Brownell and Young)
straight flange (sf) berkisar 1,5-2,25 in
Isobutilene Storage Tank
Tugas = Menyimpan triacetin 5257 kg/jam selama 30 hari
Alat = Tangki silinder horisontal dengan torispherical head
Jumlah = 1
Kondisi =
Tekanan = 1 atm
Suhu = 303 K
Kapasitas = 5257 kg/jam
dianggap diacetin dan monoacetin flowratenya kecil sehingga tidak mempengaruhi
Komponen A B n Tc
Gliceril triac 0.34964 0.2463 0.2857 704
Dimensi Tanki
Komponen Debit (kg/jam) Rho (kg/m3) Fv (m3/jam)

Triacetin 5257 1152.837012 4.560054842
Total 5257 4.560054842
Rho campuran = 1152.837012 kg/m3

Waktu penyimpanan (t) = 30 hari
= 720 jam
Jumlah Tanki = 1 Buah
Volume = Fv x t = 3283.239486 m3
Over design = 20%
Volume sesungguhnya = 3939.887383 m3
= 24817.08835 bbl 139135.81
P design = 1.2 atm 17.64 psi
L/D = 0.6 d 18.288 m

D= 20.30 m l 7.3152 m
799.062057 = 66.59 ft 0.4
L= 12.18 m 2.5
= 39.95 ft
479.437234 139135.8099 tinggi caira 40 ft
12.192 m
Pemilihan tinggi course:
Course = 6 8 ft
N course = 6.658850474 4.994137856
7 5
L= 42 40 ft
Dimameter & Tinggi Standard:

(Brownel and Young)
Diameter tanki = 70 ft 21.34 m
= 840 in
Panjang tanki = 40 ft 12.19 m
= 480 in
153938.04 1
Bahan konstruksi: (Tabel 13.1 Brownell Young)
Jenis = Carbon Steel
Tipe = SA 285 Grade C
Max. Allowable Stress (f) = 13750 psi 935.37415 atm
Corosion allowance (c) = 0.125 (Rule of thumb = 1/8 - 3/16)
Joint Effiency (Ɛ) = 80% (Tabel 13.2 Brownell Young)
Tebal Shell Tanki

Lebar tiap course = 8 ft
N course = 5
Tekanan pada masing-masing course:

P design = 1.2 atm
Tebal shell pada tiap course:

�=(�×𝐷)/(2×𝑓×Ɛ)+�
standard
t= 0.2373 in 1.75 in
Tebal dan Tinggi Head
Code flanged and dished

OD Keterangan:
ID = diameter dalam head
OD = diameter luar head
icr b
OA t = tebal head
B A
icr = jari-jari dalam sudut dish
sf r = jari-jari dish
r
ID b = tinggi head
t
sf = straight flange
a
C
ID
t
a
C
Tebal Head 17.635139
�_ℎ𝑒𝑎�=(0.885�×𝑟)/(𝑓×𝜖−0.1�)+� 21.162166
standard
t head = 0.224347928 in 1.625 in
Tinggi Head
Data: ID = 836.75 in 69.729167 ft
OD = 840 in 70 ft
t head = 1.625 in 0.1354167 ft
icr = 5.25 ft Table 5.7 (Brownell and Young)
r= 36 ft Table 5.7 (Brownell and Young)
sf = 2 in 0.1666667 ft Standard straight flange (sf) berkisar 1,5
𝑎=𝐼𝐷/2
a= 34.8646 ft
𝐴�=𝑎−��𝑟 AB = 29.6146 ft
�𝐶=𝑟−��𝑟 BC = 30.7500 ft
𝐴𝐶=√( 〖�𝐶〗 ^2− 〖𝐴�〗 ^2⁡) AC = 8.2788 ft
𝑏=r−AC b= 27.7212 ft
𝑂𝐴=�+𝑏+𝑠𝑓 OA = 28.0233 ft
am sudut dish
Brownell and Young)
Brownell and Young)
straight flange (sf) berkisar 1,5-2,25 in
NAMA DC-02
TUGAS MEMISAHKAN GLISEROL, METHANOL dengan FAME, ASAM FOSFAT
SIFAT FISIS KOMPONEN
LIGHT STREAM
KOMPONEN F massa, kg/jamBM, kg/kmol RHO, kg/m3 MIU, cP
FFA (ASAM LINOLEAT) 1690.4143046 280.4455 890 7.7
TOTAL 1690.4143046
HEAVY STREAM
KOMPONEN F massa, kg/jamBM, kg/kmol RHO, kg/m3 MIU, cP

METHANOL 1062.967947 32.04 792 0.59
GLISEROL 2229.28 92.09 1260 48.062
TOTAL 3292.247947
total semua 4982.6622517
PENENTUAN FASA
TERDISPERSI
QL 67.074633169 ft3/s
QH 109.87810299 ft3/s
RHO LIGHT 55.560742 lb/cuft
RHO HEAVY 69.225991458 lb/cuft
VISKO LIGHT 0.0013716351 lb/ft.s
VISKO HEAVY 0.0016475475 lb/ft.s
Ψ 0.6037770782
SETTLING VELOCITY FASA
TERDISPERSI
g d 2 ( D  C )
Ud (SCHWEITZER, 1979)
18  C
ASUMSI PERHITUNGAN
dd 150 µm 0.000492126 ft
g 9.8 m/s2 32.152232 ft/s2
Ud -0.003588152 ft/s -0.001093669 m/s

0.0010936688
PENENTUAN DIAMETER
SILINDER
DIGUNAKAN SILINDER
HORIZONTAL
ASUMSI
I = 80% D
L/D = 1.5
Uc=Ud
A = IL = 0.8D . 1.5D = 1.2

D^2
(Qc/1.2 Ud)^0.5 = D
D 0.4444816655 m 1.4582732276 ft
L 0.6667224983 m 2.1874098413 ft
2.286 7.5 ft
INTERFACE CAIRAN
I 1.1666185821 FROM BOTTOM TANK

0.2916546455 FROM UPPER TANK
r 0.7291366138 ft
h 0.4374819683 ft
CEK NILAI I 1.1666185821
Ai 0.6379682419 ft2 0.0592691853 m2

Al 0.2373767605 ft2
Ah 0.5972983559 ft2
P 1.3522497905 ft 0.4121657229 m
SECONDARY SETTLING
QD
Uc = 0.0089016742 m/s 0.0292049687 ft/s
AI
1
 18  D u C  2
dc =   3.4399607E-05 ft 0.000010485 m
 g ( 
 D   c ) 
10.484999893 mikrometer
WAKTU TINGGAL
Hd = 10% D (SCHWEITZER, 1979)
Hd 0.0444481666 m
t=
1
2 HD AI 1.5240503497 s 0.0254008392 menit
QD
CEK TURBULANCE LEVEL
LIGHT PHASE
vL 282.56613252 ft/s 86.146004955 m/s

DL 0.5775926029 ft 0.1760907961 m
Re 1753.3599415
HEAVY PHASE
Vh 183.95848892 ft/s 56.070545628 m/s

Dh 0.6790601156 ft 0.2069775166 m
Re 1108.4996343
INTERFACIAL SHEAR
VELOCITY RATIO 0.6510280878
MECHANICAL DESIGN
BAHAN KONSTRUKSI CARBON STEEL

TIPE SA 299
f 18750 psia
C 0.125 in
E 80% (DOUBLE WELDED BUTT JOIN)
P OPERASI 1 atm 14.7 psi

P DESIGN 1.2 atm 17.64 psi
rv 8.7496438102 in
P ri
t shell = +C 0.1352968466 in 0.1875 in
f E  0,6P
OD = ID + 2*t shell 17.87428762 in
AME, ASAM FOSFAT
Xi RHO.Xi LN(MIU).Xi F volume, m3/jam
1 890 2.041220329 1.899341915
890 2.041220329 1.899341915 0.000527595

55.560742 0.001371635 67.07463317
lb/cuft lb/ft.s ft3/jam
7.7
miu 7.7
Xi RHO.Xi LN(MIU).Xi F volume, m3/jam

0.322869955 255.7130045 -0.17035676 1.342131246 0.000372814
0.677130045 853.1838565 2.622180576 1.769269841 0.000491464
1 1108.896861 2.451823816 3.111401088 0.000864278
69.22599146 0.001647548 109.878103
lb/cuft lb/ft.s ft3/jam
11.60950102
0.007801215
dc harus lebih kecil dari dd
SYARAT WAKTU TINGGAL 2-5 MENIT

SYARAT RE<5000
SYARAT RE<5000
SYARAT R<2
(STANDART)
NAMA MX-02
TUGAS MENCAMPUR CRUDE GLYCEROL SEBANYAK 34514.2814 KG/JAM DENGAN ASAM FOSFAT
SIFAT FISIS
KOMPONEN RHO, kg/m3 Massa, kg/jamFraksi RHO.FRAKSI
KOMPONEN RHO, kg/m3 Massa, kg/jamFraksi RHO.FRAKSI
GLYCEROL 1260 2229.28 0.237619494 299.4005625
METHANOL 792 1062.967947 0.11330201 89.73519223
FFA 890 1690.4143046 0.180181669 160.3616857
GARAM ANORGANIK 2560 2399.0596026 0.255716343 654.6338378
ASAM FOSFAT 1880 2000 0.213180483 400.7793088
TOTAL 9381.721854 1 1604.910587
DIMENSI MIXER
1
WAKTU TINGGAL 1 jam ASUMSI SUDAH WELL-MIXED
MASSA TOTAL DALAM
MIXER 9381.721854 kg/jam
RHO CAMPURAN 1604.910587 kg/m3
VOLUME CAIRAN 5.845635221 m3/jam
VOLUME MIXER 5.845635221 m3 36.7696265 barrel
OVER DESIGN 20%
VOLUME MIXER REAL 7.014762266 m3
KARENA VOLUME < 3000

BARREL, MAKA D/H=1
DT=ZL=(4*VL/PHI)^(1/3) 2.075141744 m 81.69849385 in 6.808207821

ZR 2.490170092 m 98.03819262 in 8.169849385
ZL = DT = ID STANDART 84 in 2.1336 m (TABEL 5.7 BROWNELL)
TEBAL DINDING MIXER

BAHAN KONSTRUKSI HIGH ALLOY SA-167-11 (APENDIX E BROWNELL, ITEM 4)
f 18750 psi
c 0.125 (RULE OF THUMB)
E 80% (TABEL 13.2 BROWNELL)
Psistem 1 atm 14.7 psi

Phidro 0.33118702 atm 4.868449199 psi
Pdesign 1.597424424 atm 23.48213904 psi
Wshell=(P*r)/(f*E-0.6*P)
+c 0.190811805 in 0.25 in (STANDART)
TEBAL HEAD TANGKI
OD 84 in (TABEL 5.7 BROWNELL)

icr 0.3125 in (TABEL 5.7 BROWNELL)
r 84 in (TABEL 5.7 BROWNELL)
Whead=(0.885.r.P)/(2.f.E- OA
0.2.P)+c 0.183197851 in 0.25 in (STANDART)
sf
ID Real = OD - 2Whead 83.6336043 in 2.124293549 m
VOLUME MIXER KOREKSI 538575.7624 in3 8.825641019 m3
TINGGI HEAD TANGKI
a 41.81680215 in 0.1875
AB 41.50430215 in
BC 83.6875 in
AC 72.67042424
b 11.32957576 in
sf 2 in (TABEL 5.6 BROWNELL)
OA 13.51277361 in 0.34322445 m
H TOTAL MIXER 111.5509662 in 2.833394542 m

DIMENSI PENGADUK (BROWN PAGE 507)
JENIS IMPELLER TURBINE WITH 6 BLADES
DIAMETER IMPELLER (Di) 27.8778681 in

PANJANG SUDU
PENGADUK (L) 5.57557362 in
LEBAR BLADE (Wi) 5.57557362 in
LEBAR BAFFLE (Wb) 8.36336043 in
JARAK PENGADUK DARI
DASA MIXER (Zi) 36.24122853 in
TINGGI CAIRAN DALAM
MIXER (ZL)
Vh 28.66411391 in3 (EQ. 5.11 BROWNELL)
Vhead 11015.72432 in3 0.180515379 m3
Vmixer 7.375793025 m3
Vcairan 5.845635221 m3
V cairan dalam shell 5.665119842 m3
H cairan dalam shell 1.598417257 m 62.92984723 in
H cairan dalam mixer 76.25942299 in 1.936988298 m
JAM DENGAN ASAM FOSFAT SEBANYAK 2000 KG/JAM
ZL Zr
L
H
Zi
Di
Dt
ft
ft
ABEL 5.7 BROWNELL)

OD
ic r b
OA
B A
sf
r
ID
t
a
C
Q. 5.11 BROWNELL)
Belt Conveyor (BC-01)
Fungsi : mengangkut KOH ke hopper

Jenis : horizontal belt conveyor
Bahan: reinforced belt
Kondisi operasi : T = 30 C, P = 1 atm
Massa : 800 kg/jam

Densitas : 2.12 g/cm3 (www.hapman.com)
2120 kg/m3
132.3469 lb/cuft
Overdesign massa
960 kg/jam 0.96 ton/jam
Digunakan 1 belt conveyor dengan width 14 in
Q: 0.3774 m3/jam 13.3263 ft3/jam

Dari Tabel 21-7 diperoleh
Kapasitas : 32 ton/jam
Speed : 30.5 m/menit 100 fpm
Speed asli : 0.9150 m/menit 3.0020 fpm

L: 5m 16.40419948 ft
W: 14 in
F: 0.03 (antifriction)
Lo : 150 (antifriction)
delta Z : 3m 9.8425 ft
Power required (Brown) Power required

1. Empty belt 1. Empty belt
ℎ�=(𝐹(𝐿+𝐿_𝑂)(0.03𝑊𝑆))/990 2. Material (excluding belt)
3. Elevating material (exclude belt)
TOTAL HP
2. Material (excluding belt)
Elevasi 30.9638 derajat
ℎ�=(𝐹(𝐿+𝐿_𝑂)𝑇)/990
3. Elevating material (exclude belt)
ℎ�=(𝑇.�𝑒��𝑎⁡𝑍)/990
kalau turun elevasinya, nilainya turun
TOTAL HP
ℎ�=(𝐹(𝐿+𝐿_𝑂)(0.03𝑊𝑆))/990+(𝐹(𝐿+𝐿_𝑂⁡𝑇)/990+(𝑇.�𝑒��𝑎⁡𝑍)/990
0.0064 hp
0.0048 hp
0.0095 hp
0.0207 hp Standar 1.5 hp
NAMA CP-06
TUGAS MENGALIRKAN GLYCEROL KELUARAN ST-01 KE RDC-01 SEBANYAK 10423.309 KG/JAM
JENIS SENTRIFUGAL, SINGLE STAGE
SIFAT FISIS
KOMPONEN RHO, kg/m3 Massa, kg/jam Fraksi

GLYCEROL 1260 10677.6 1
TOTAL 10677.6
DATA PERHITUNGAN
POMPA
DATA TITIK 1 TITIK 2 KETERANGAN

Suhu (T), C
o
27 27
Tekanan (P), atm 1 1
Tinggi (Z), m 1 14.5 PASTIKAN KETINGGIAN LETAK PLATE FEED RDC-0
Flow rate (Fv), kg/j 10677.6 10677.6
(Fv)design, kg/j 12813.12 12813.12 OVER DESIGN 120%
Rho (r), kg/m3 1260 1260
viskositas(µ) cP 660 660 DARI DATA
Q, m3/j 10.1691428571 10.1691428571
G, kg/s 3.5592 3.5592
Dopt hit., in 1.5310223628 1.5310223628 Dopt = 282G0.52rho-0.37
Dipilih pipa standard STAINLESS STEEL STAINLESS STEEL KOROSIF
NPS, in 1.5 1.5 TABEL 11 KERN
Schedule Number 40 40 TABEL 11 KERN
Di, in 1.61 1.61 TABEL 11 KERN
V pipa, m/s 2.1506650669 2.1506650669 V = Q / (π/4 (Di)2)
Re pipa 167.9032038345 167.9032038345 Re = (ρ V Di)/µ
PERHITUNGAN HEAD 0.0176218116
Pressure head m 0 DP = (P2 - P1) / ρ / g

Static Head : m 13.5 DH = z2 - z1
Velocity head : m 0 DV = (V22-V12) / (2g)
Friction head : SUCTION DISCHARGE
f 0.095 0.095 FIG 125 BROWN
Panj. lin. pipa (L), m 3 15 data
elbow 1 3 fig. 127, Brown (Le=9ft)
Standard Tee 0 0 fig. 127, Brown
Gate valve fully open 1 1 fig. 127, Brown (Le=0,9ft)
Globe valve 0 1 fig. 127, Brown (Le=40ft)
L + Le, m 5.86512 35.69592
L+Le overdesign 8.79768 53.54388
Fs 4.8230488916 29.3537331533 F = f(L+Le)V2/(2gD)
Fs total, m 34.1767820449 Fs tot.=Fs suction+Fs discharge
Total Head : m 47.6767820449 Tot Head = DP+DH+DV+Fs
(-Ws), m 47.6767820449 (-Ws) = Tot. Head + Q
SPEK POMPA
TOTAL HEAD 47.6767820449 m

156.4198885989 ft
Q 10.1691428571 m3/jam
44.7782600491 gpm
0.4392712802 ft3/s
SPEK POMPA SENTRIFUGAL SINGLE STAGE STAGE 3500 rpm
SPEK MOTOR
PENGGERAK
PENGGERAK MOTOR
KUTUB 2
FREKUENSI 50 Hz
60.f
Kecept. sinkron   3000 rpm
P/2
SLIP 2%
ACTUAL SPEED 2940 rpm
PUTARAN SPESIFIK
POMPA
n.Q 1/2
Ns  444.7971115227 rpm (COULSON EQ 5.2)
H3/4
POWER POMPA
(-Ws).Q.
P 9.8264632944 Hp
550
EFFICIENCY POMPA 65%

EFFICIENCY MOTOR 90%
POWER MOTOR 16.7973731529 Hp

EBANYAK 10423.309 KG/JAM
RHO.FRAKSI
1260
1260
komponen A B C D
glycerol -18.2152 4.23E+03 2.87E-02 -1.86E-05
viskositas 660 cp
NGGIAN LETAK PLATE FEED RDC-01
RULE OF THUMB 1-3 m/s

LAMINAR
n+Fs discharge
T log miu = A + B/T + CT + DT^2
300 K
NAMA CP-08
TUGAS MENGALIRKAN ASAM ASETAT KE RDC-01
SIFAT FISIS

Asam Asetat 1050 96098.8 1
TOTAL 96098.8
DATA PERHITUNGAN
POMPA

Suhu (T), C
o
27 27
Tinggi (Z), m 1 1 PASTIKAN KETINGGIAN LETAK PLATE FEED RDC-0
Flow rate (Fv), kg/j 96098.8 96098.8
Rho (r), kg/m3 1050 1050
viskositas(µ) cP 1.037 1.037 DARI DATA
Q, m3/j 109.8272 109.8272
G, kg/s 32.0329333333 32.0329333333
Dipilih pipa standard STAINLESS STEEL STAINLESS STEEL KOROSIF : asam asetat
V pipa, m/s 1.636773126 1.636773126 V = Q / (π/4 (Di)2)
Re pipa 255307.486673706 255307.486673706 Re = (ρ V Di)/µ
PERHITUNGAN HEAD

Static Head : m 0 DH = z2 - z1
f 0.029 0.029 FIG 125 BROWN
elbow 1 3 fig. 127, Brown (Le=9ft)
L + Le, m 6.01752 35.69592
Fs 0.2322539868 1.3777303164 F = f(L+Le)V2/(2gD)
(-Ws), m 1.6099843033 (-Ws) = Tot. Head + Q
SPEK POMPA
TOTAL HEAD 1.6099843033 m

5.2821007325 ft
Q 109.8272 m3/jam
483.6072214883 gpm
4.7441495728 ft3/s
SPEK MOTOR
PENGGERAK
PENGGERAK MOTOR
KUTUB 2
FREKUENSI 50 Hz
60.f
P/2
SLIP 2%
PUTARAN SPESIFIK
POMPA
n.Q 1/2
Ns  18556.1856854466 rpm (COULSON EQ 5.2)
H3/4
POWER POMPA
(-Ws).Q.
P 2.9864569608 Hp
550


RHO.FRAKSI
1050
1050
asam asetat -3.8937 7.85E+02 6.67E-03

1.10005
NGGIAN LETAK PLATE FEED RDC-01

LAMINAR
n+Fs discharge
-7.56E-06 300
NAMA CP-09
TUGAS MENGALIRKAN KOMPONEN BOTTOM DARI RDC-01 KE TDC-01
rho flowrate X
GLYCEROL 1260 8149.961 0.0842143033
AIR 1000 5.54333 5.72797432833894E-05
MONOACETIN 1220 8.646592 0.000089346
DIACETIN 1170 0.371379 3.8374936691198E-06
TRIACETIN 1160 5974.314 0.0617331409
Asam Asetat 1050 82637.61 0.8539020925
TOTAL 96776.446301 1
DATA PERHITUNGAN
POMPA

Suhu (T), C
o
121.055 27
Tinggi (Z), m 1 7
Flow rate (Fv), kg/j 96776.446301 96776.446301
Rho (r), kg/m3 1074.4884345334 1074.4884345334
viskositas(µ) cP 0.4806261314 2.0196773245
Q, m3/j 108.0809544606 108.0809544606
G, kg/s 32.2588154337 32.2588154337
Dipilih pipa standard STAINLESS STEEL STAINLESS STEEL KOROSIF : asam asetat
NPS, in 6 6 TABEL 11 KERN
V pipa, m/s 1.7852276532 1.7852276532 V = Q / (π/4 (Di)2)
Re pipa 584009.031120084 138977.646528715 Re = (ρ V Di)/µ
PERHITUNGAN HEAD

f 0.0182 0.021 FIG 125 BROWN
elbow 1 3 fig. 127, Brown (Le=7,5ft)
L + Le, m 6.3528 68.6448
Fs 0.1927202622 2.4028006763 F = f(L+Le)V2/(2gD)
(-Ws), m 8.5955209384 (-Ws) = Tot. Head + Q
SPEK POMPA

28.2005280132 ft
Q 108.0809544606 m3/jam
475.9178972283 gpm
4.6687178944 ft3/s
SPEK MOTOR
PENGGERAK
PENGGERAK MOTOR
KUTUB 2
FREKUENSI 50 Hz
60.f
P/2
SLIP 2%
PUTARAN SPESIFIK
POMPA
n.Q 1/2
Ns  5241.0755368212 rpm (COULSON EQ 5.2)
H3/4
POWER POMPA
(-Ws).Q.
P 16.0567825855 Hp
550


komponen A B C D
glycerol -18.2152 4.23E+03 2.87E-02 -1.86E-05
triacetin -12.8264 2.33E+03 2.37E-02 -1.70E-05
asam asetat -3.8937 7.85E+02 6.67E-03 -7.56E-06
106.1100221 menghitung viskositas dianggap hanya mengandung glycerol, triacetin dan asam a
0.057279743 Komponen miu, Cp x ln(miu) x log miu = A +
0.109002166 glycerol 8.6360 0.084214303 0.181560545
0.004489868 triacetin 0.61433 0.061733141 -0.03007819
71.6104435 asam asetat 0.35508 0.853902092 -0.88414794
896.5971971 total -0.73266558
1074.488435 miu mix suhu 0.480626131 cp
miu mix suhu 2.019677324 cp

LAMINAR
n+Fs discharge
T
394.055 K
300 K
glycerol, triacetin dan asam asetat

miu, Cp x ln(miu) x
660.156 0.084214303 0.546759375
3.357 0.061733141 0.074753534
1.100 0.853902092 0.081424849
0.702937758
NAMA CP-10
TUGAS MENGALIRKAN TRIACETIN KE ST-06
SIFAT FISIS

TRIACETIN 1160 5257 1
TOTAL 5257
DATA PERHITUNGAN
POMPA

Suhu (T), C
o
177 27
Tinggi (Z), m 1 1
Flow rate (Fv), kg/j 5257 5257
Rho (r), kg/m3 1160 1160
viskositas(µ) cP 0.375707 3.356552 DARI DATA
Q, m3/j 5.4382758621 5.4382758621
G, kg/s 1.7523333333 1.7523333333
Dipilih pipa standard carbon steel carbon steel NONKOROSIF
V pipa, m/s 1.5654645796 1.5654645796 V = Q / (π/4 (Di)2)
Re pipa 169420.183979906 18963.5964380488 Re = (ρ V Di)/µ
PERHITUNGAN HEAD

f 0.0142 0.0135 FIG 125 BROWN
elbow 1 3 fig. 127, Brown (Le=3.5ft)
L + Le, m 6.286256 34.087856
L+Le overdesign 9.429384 51.131784
Fs 0.4776274556 2.4623077447 F = f(L+Le)V2/(2gD)
(-Ws), m 2.9399352003 (-Ws) = Tot. Head + Q
SPEK POMPA

9.6454566938 ft
Q 5.4382758621 m3/jam
23.9466132192 gpm
0.2349144302 ft3/s
SPEK MOTOR
PENGGERAK
PENGGERAK MOTOR
KUTUB 2
FREKUENSI 50 Hz
60.f
P/2
SLIP 2%
PUTARAN SPESIFIK
POMPA
n.Q 1/2
Ns  2628.6168265331 rpm (COULSON EQ 5.2)
H3/4
POWER POMPA
(-Ws).Q.
P 0.298326882 Hp
550


RHO.FRAKSI
1160
1160
viskositas tria A B C D viskositas pad

Triacetin -12.8264 2.33E+03 2.37E-02 -1.70E-05 0.375707
viskositas pad
3.356552

TURBULEN
n+Fs discharge
450 K
300 K
NAMA HE-02
TUGAS MENDINGINKAN TRIACETIN
JENIS SHELL AND TUBE
PENDINGIN AIR
HEAT CAPACITY
KOMPONEN A B C D
TRIACETIN 92.681 1.9216 -0.0045 0.000004363
AIR 92.053 -0.039953 -0.0002110 0.000000535
VISKOSITAS
KOMPONEN A B C D T
TRIACETIN -12.8264 2.33E+03 2.37E-02 -1.70E-05 450
300
THERMAL CONDUCTIVITY
KOMPONEN A B C
TRIACETIN -1.7907 9.84E-01 7.04E+02
PANAS YANG
DIBUTUHKAN/DIHILANG
KAN
Tin 177 C 450 K

Tout 30 C 303 K
Tavg 103.5 C 376.5 K
KOMPONEN F, kg/jam Cpin, kJ/kmol/Cpout, kJ/kmoBM, kg/kmol F, kmol/jam
triacetin 5257.2 4.39E+02 3.81E+02 218.21 24.09238807

Q DIBUTUHKAN -1978462.35 kJ/jam menghasilkan panas
-1875220.25 BTU/jam exotermis
KEBUTUHAN
PEMANAS/PENDINGIN
PENDINGIN AIR
BM 18 kg/kmol
Tin 27 C 300 K
Tout 90 C 363 K
CpdT 4737.75555 kJ/kmol
Q DIBUTUHKAN -1978462.35 kJ/jam
MASSA PENDINGIN 7516.707435 kg/jam
BEBAN HE
SPLIT 1
HOT FLUID TRIACETIN HASIL ATAS VDC02

MASSA 5257.2 kg/jam 11590.02312 lb/jam
TEKANAN 1 atm 14.7 psi
Tin 177 C 350.6 F
Tout 30 C 86 F
Tavg 103.5 C 218.3 F 376.5
BEBAN PANAS -1978462.35 kJ/jam -1875220.25 BTU/jam
COLD FLUID Air

MASSA 7516.707435 kg/jam 16571.33321 lb/jam
TEKANAN 1 atm 14.7 psi
Tin 27 C 80.6 F
Tout 90 C 194 F
Tavg 58.5 C 137.3 F 331.5
LMTD
HOT FLUID COLD FLUID DIFFERENCE

HIGHER TEMP 350.6 194 156.6
LOWER TEMP 86 80.6 5.4
DIFFERENCE 264.6 113.4 151.2
LMTD 44.9024997 F
S 0.42
R 1.75
FT 1
DELTA T 44.9024997 F
EQUIPMENTS
light ORGANIC-WATER Q
A
U D t
(DARI KERN TABEL 8) light-heavy organics
UD 40 BTU/jam.ft2.F
TRIAL UD 40 BTU/jam.ft2.F
A 1044.051147 ft2 96.99552548 m2
SPECIFICATION
OD 0.75 in
BWG 16
(DARI KERN TABEL 10)

di 0.62 in 0.051666667 ft
a' 0.1963 ft2/ft
a" 0.302 in2
L 16 ft
Nt 332.4156734
(DARI KERN TABEL 9)

PITCH 1 in triangular pitch
Nt STANDART 342
ID SHELL STANDART 23.25
n 6 pass
B 17.4375 in
C' 0.25 in
A CORRECTED 1074.1536 ft2

UD CORRECTED 38.87902613 BTU/ft2.F
DIRT FACTOR
MENINJAU TUBES SIDE COLD FLUID
at'=a" 0.302 in2

at = Nt.at"/144.n 0.119541667 ft2
G = m / at 138649.0615 lb/jam.ft2
miu 0.7 lb/ft.jam
Re = D.G/miu 10233.62121
jH 28 (KERN FIG.24)
v = G/rho.3600 0.531882726 ft/s
Tavg 137.3 F
hi 390 BTU/jam.ft2.F (KERN FIG.25)
CORRECTION FACTOR 0.98 (KERN FIG.25)
hi 382.2 BTU/jam.ft2.F
OD 0.75 in
hio 315.952 BTU/jam.ft2.F
MENINJAU SHELL SIDE HOT STREAM
as = ID*C'B/144Pt 0.703857422 ft2

Gt = m / as 16466.4359 lb/jam.ft2
miu 1.624669564 lb/ft.jam
De 0.060833333 ft (KERN FIG.28)
Re 616.5611804
jH 14
k 0.1001 W/m.K 6.94E-01 BTU/ft2.jam.F
Cp 410 j/mol.K 9.80E+01 BTU/lb.F
ho =
jH*k/De*(cp*miu/k)^1/3*
(miu/miu w)^-0.14 977.5443498 BTU/jam.ft2.F dikarenakan nilai ho diatas batas nilai h organ
300 BTU/jam.ft2.F
CLEAN OVERALL
COEFFICIENT
h io  h o
UC 
h io  h o
153.8847183 BTU/jam.ft2.F
DIRT FACTOR
(U C  U D )
Rd 
UC  UD
0.019222438 CEK
Rdmin > 0.003 (MENINJAU FLUIDA DI TUBE, KERN TABEL 12)
PRESSURED DROP
Re 10233.62121
f 0.0003 ft2/in2 (KERN FIG.26)
sg 1 (KERN TABEL 6)
rho 62.5 lb/ft3
g 32.2 ft/s2
dPt=(f.Gt^2.L.n)/
(5.22.10^10.D.sg) 0.205279419 psi
dPr=3(4n/sg)*((v^2)/2g) 0.316284858 psi

dPT=dPt+dPr 0.521564277 psi SYARAT dPT<10 psi
Tout miu 450K 0.3757
300 miu 300K 3.3566
logk = A+ B(1-C/T)^2/7
Hin, kJ/jam Hout, kJ/jam
4.76E+06 2.78E+06
K
o diatas batas nilai h organic compunds, maka digunakan ho sebesar batas maksimum yaitu 300
A DI TUBE, KERN TABEL 12)
REBOILER PADA MD-01 (Kern, hal 465)
Tugas : Memanaskan produk bawah RDC-01 sebanyak 96776.50 kg/jam
dengan menggunakan steam sebanyak 27459.89 kg/jam
Alat : Kettel
Fluida Dingin : Hasil Bawah Menara Distilasi

T= 392.0 K 119.0 C P= 1.0133
246.2 F 14.89
T out Reboiler = 121.06 C 394.06 K

249.9 F
Fluida panas : Steam Saturated
P= 140.000 Psia 9.52 atm (Tabel 7)
T= 353.02 F
H= 868.20 Btu/lb
(1) Duty
Neraca panas di sekitar Reboiler : Rin-Rout =Racc
F*HF + Qr = Qc + D*HD + B*HB
Qr = Qc + D*HD + B*HB - F*HF 18379376.84
Beban Reboiler Qr = 18379376836.63 J/jam 18379376.8 KJ/JAM
= 17504168.4158 Btu/jam 18379376.8 KJ/JAM
T1 T2
tw2 tw1
Hot fluid Cold fluid Difference

K F K F
451.3 353.02 Higher Temp 394.06 249.90 103.12
451.3 353.02 Lower Tem 392.00 246.20 106.82
0 Difference 3.70 3.70
m steam = 20161.45 lb/jam - Laju alir fluida dingin, Wc = 96776.50

9153.30 kg/jam 20161.44715024 213355.41
t 2  t1
LMTD   104.96 F
2.3 log t 2
t1
(2) Trial UD
UD = 50 - 100 untuk medium organics-steam (Miu<2 cp)
Diambil UD = 100 (Kern, 1950)
(3) delt = weighted delt = delt LMTD Tc = Ta = 353.02 F

= 104.96 F tc = ta = 248.05 F
(4) Luas transfer panas Qr

A A= 1667.7047 ft2 154.93484
U D  Δt
(5) Jenis HE : Shell & Tube Heat Exchanger hal.230 kern
(6) Trial Lay Out HE
TRIAL AWAL : L, ft = 12 a" = 0.1963
OD, in = 0.75 3/4 in
pass = 2 Triangular pitch
A
Nt 
L    OD
= 707.97 tubes 728 pada IDs =
Diambil : Shell Tube
ID, in 31 Nt 728
Pass, n 1 OD, in 0.75
L, ft 12 Pt, in 1
Clearance(C'),in 0.3800 ga usah ah… 1.0000
Baffle Space,in 6.2000 ID,in 0.62
Koreksi UD :
A= 1714.8768 ft2 Check maximum flux : Q/A = 10207.2455
UD = 97.2492 harus mendekati UD trial. (batasan untuk organic`s reboiler
70.000 to 125.000 Btu/jam ft2)
HOT FLUID : TUBE SIDE, steam COLD FLUID : SHELL SIDE, liquid from MD
DIRT FACTOR
(7) Flow area : (7) Asumsikan ho sistem komponen terbanyak air..jd, an
at'= 0.302 in2 [Table 10] ho = 300
tc = 248.05
Nt at'
at 
144  n ho  (TV  ta )
= 0.7634 ft2 tw  ta 
m hio  ho
(8).
G t  = 265.544583
at
= 26410.4540 lb/jam ft2 dtw = 19.34
emang asumsinya udah benar???

Dari Fig 15.11 diperoleh :
D G
(9) Hitung Re  t
ho = >900
 hence use ho trial.
Pd Ta= 353.02 F
miu = 0.0363 lb/ft jam (Fig 15)
D=IDt= 0.62 in [Table 10]
= 0.0517 ft
Re = 37590.6
(10) steam condensing :
hio = 1500 Btu/jam ft2 F
(12) Clean overall coeficient

h io  h o
UC  = 250.0000 Btu/hr ft2 F
h io  h o
h io  h o
UC 
(13) Dirt factor h io  h o
(U C  U D )
Rd 
UC  UD
= 0.0063 > Rd min = 0.003
PRESSURE DROP
(1) Re = 37590.64 diperoleh Reboiler sejajar bottom
f= 0.0003 [Fig 26]
(2) s= 0.3106 hydrostatic head <<<
2
f Gt Ln
 Pt  fluid velocity <<
5, 22  10 10  D  s  
= 0.0060 psi DP <<
(3). 2
 4n  V
 Pr    negligible
 s  2g '
dgn (V^2)/2g' = 2.50E-02 [Fig 27]
Pr  0.6440 psi
(4).P
T  Pt  Pr
= 0.6500 psi < 2 psi
Oke !
SUMMARY :
Lay Out : SHELL TUBE

IDshell, in 31 Nt 728
IDbundle, in 31 OD, in 0.75
circle supp. plates = 31 Pt, in 1 Triangular
BWG 16
Operation Condition
HOT fluid fluid COLD fluid
1500 houtside 300.0000
UC 250.0000
UD 97.2492
Rd calc. 0.0063
Rd req'd. 0.003
0.6500 Calc dP 0
2 Allow. dP 2
Ada = 1 reboiler
harga pembuatan steam lebih besar dari harga alat ya??
atm
psi
klo 5 reboiler :
dTw= 28.446
P= 70.000 Psia
T= 302.92 F
H= 907.90 Btu/lb
1197.24 tubes 1200
steam total yg dibutuhkan :

R-01 27459.89 kg/jam T= 353.02 F P=
R-02 #REF! kg/jam T= 292.71 F P=
R-03 #REF! kg/jam T= 417.33 F P=
18379376837 J/jam 17504168 Btu/jam
121.06
119.00
kg/jam
lb/j
m2
31 in
BWG 16
n 2
Triangular pitch
De, ft 0.0592
Btu/jam ft2 < 125.000 < Heat flux maximum untuk natural circulation (12500)
(batasan untuk organic`s reboiler ??? kern
70.000 to 125.000 Btu/jam ft2)
HELL SIDE, liquid from MD
istem komponen terbanyak air..jd, anggap ho asam asetat! T= 392.0000 K

Komponen A B miu, mNs/m2
F H2O 658.2500 283.1600 0.2262
C6H12O6 0.0000
H2SO4 0.0000
Yeast 0.0000
F C2H5OH 686.6400 300.8800 0.2948
yup!!
k(cµ/k)^1/3 0.37
btu/(ft2.j. oF) De 0.710721868 in
0.059226822 ft
at 0.51 ft2
Gs 420658.0134 lb/ jam. ft2
Re #DIV/0!
jh 100
ho 624.7169529
er sejajar bottom
static head <<<
d velocity <<
140.000 Psia
60.000 Psia
300.000 Psia
xi,f wi/miui
#DIV/0! #DIV/0!
#DIV/0! 0.0000
#DIV/0! 0.0000
#DIV/0! 0.0000
#DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0!
RUNGE KUTTA
Persamaan 1 b
Persamaan 2 a
Trial
FA 156808.93
FB 470426.78
FD 5659
W=rho.A.dz
Persamaan 3 c
Komponen A B C D
Amonia 33.573 -0.012581 8.891E-05 -7.18E-08
Fenol 4.408 0.36338 -6.04E-05 -1.28E-07
Air 33.933 -0.008419 2.991E-05 -1.78E-08
Anilin -22.062 0.57313 -0.000457 1.841E-07
DPA -119.401 1.306 -0.00122 5.876E-07
CEK PATEN
FA0 ### BM C 93.13

X1 #NUM! BM E 169.23
X2 #NUM! FA #NUM!
FC #NUM!
FE #NUM!
FC (wt) #NUM!
FE (wt) #NUM!
Total #NUM!
Selektibvity
wt/wt
A #NUM!
E #NUM!
conv #NUM!
PRESSURE DROP
DATA ITERASI
FA0
FB0
FT
h
P
delH
Area
rho cat
berat katali
TEBEL ITERASI
meter kelvin atm atm

No W X1 X2 T PA PB
1 0 0 0 573.15 3.7165 11.149409
2 64.353 0.0683 1E-05 578.86 3.4626 10.895623
3 128.71 0.1555 0.0001 586.09 3.1382 10.571445
4 193.06 0.2722 0.0005 595.68 2.7033 10.137686
5 257.41 0.4368 0.0024 609.04 2.0881 9.5261583
6 321.76 0.6707 0.0144 627.84 1.2061 8.6567268
7 386.12 0.9087 0.1124 647.1 0.3011 7.7721629
8 450.47 0.9665 0.3307 652.22 0.0834 7.5574813
9 514.82 0.9413 0.1034 650.69 0.1955 7.6509499
10 579.18 0.9646 0.3049 653.16 0.0916 7.564675
11 643.53 0.9416 0.1731 651.84 0.1796 7.6500831
12 707.88 0.9606 0.3656 653.94 0.093 7.5794864
13 772.23 0.9379 0.1933 652.61 0.1861 7.6636697
14 836.59 0.9619 0.3896 655.13 0.0864 7.574548
15 900.94 0.9341 0.0337 653.43 0.2367 7.6778461
16 965.29 0.9817 0.2403 658.13 0.0517 7.5010298
17 1029.6 0.9156 1.2436 653.82 -0.0764 7.7467437
18 1094 0.8867 4.7409 651.74 -1.5746 7.8538586
19 1158.4 7E+20 -6E+29 3E+17 -2E+51 -2.56E+21
20 1222.7 #NUM! #NUM! #NUM! 3.7165 11.149409
21 1287.1 #NUM! #NUM! #NUM! 3.7165 11.149409
22 1351.4 #NUM! #NUM! #NUM! 3.7165 11.149409
23 1415.8 #NUM! #NUM! #NUM! 3.7165 11.149409
24 1480.1 #NUM! #NUM! #NUM! 3.7165 11.149409
25 1544.5 #NUM! #NUM! #NUM! 3.7165 11.149409
26 1608.8 #NUM! #NUM! #NUM! 3.7165 11.149409
27 1673.2 #NUM! #NUM! #NUM! 3.7165 11.149409
28 1737.5 #NUM! #NUM! #NUM! 3.7165 11.149409
29 1801.9 #NUM! #NUM! #NUM! 3.7165 11.149409
30 1866.2 #NUM! #NUM! #NUM! 3.7165 11.149409
31 1930.6 #NUM! #NUM! #NUM! 3.7165 11.149409
32 1994.9 #NUM! #NUM! #NUM! 3.7165 11.149409
33 2059.3 #NUM! #NUM! #NUM! 3.7165 11.149409
34 2123.6 #NUM! #NUM! #NUM! 3.7165 11.149409
35 2188 #NUM! #NUM! #NUM! 3.7165 11.149409
36 2252.3 #NUM! #NUM! #NUM! 3.7165 11.149409
37 2316.7 #NUM! #NUM! #NUM! 3.7165 11.149409
38 2381.1 #NUM! #NUM! #NUM! 3.7165 11.149409
39 2445.4 #NUM! #NUM! #NUM! 3.7165 11.149409
40 2509.8 #NUM! #NUM! #NUM! 3.7165 11.149409
41 2574.1 #NUM! #NUM! #NUM! 3.7165 11.149409
42 2638.5 #NUM! #NUM! #NUM! 3.7165 11.149409
43 2702.8 #NUM! #NUM! #NUM! 3.7165 11.149409
44 2767.2 #NUM! #NUM! #NUM! 3.7165 11.149409
45 2831.5 #NUM! #NUM! #NUM! 3.7165 11.149409
46 2895.9 #NUM! #NUM! #NUM! 3.7165 11.149409
47 2960.2 #NUM! #NUM! #NUM! 3.7165 11.149409
48 3024.6 #NUM! #NUM! #NUM! 3.7165 11.149409
49 3088.9 #NUM! #NUM! #NUM! 3.7165 11.149409
50 3153.3 #NUM! #NUM! #NUM! 3.7165 11.149409
51 3217.6 #NUM! #NUM! #NUM! 3.7165 11.149409
52 3282 #NUM! #NUM! #NUM! 3.7165 11.149409
53 3346.3 #NUM! #NUM! #NUM! 3.7165 11.149409
54 3410.7 #NUM! #NUM! #NUM! 3.7165 11.149409
55 3475.1 #NUM! #NUM! #NUM! 3.7165 11.149409
56 3539.4 #NUM! #NUM! #NUM! 3.7165 11.149409
57 3603.8 #NUM! #NUM! #NUM! 3.7165 11.149409
58 3668.1 #NUM! #NUM! #NUM! 3.7165 11.149409
59 3732.5 #NUM! #NUM! #NUM! 3.7165 11.149409
60 3796.8 #NUM! #NUM! #NUM! 3.7165 11.149409
61 3861.2 #NUM! #NUM! #NUM! 3.7165 11.149409
62 3925.5 #NUM! #NUM! #NUM! 3.7165 11.149409
63 3989.9 #NUM! #NUM! #NUM! 3.7165 11.149409
64 4054.2 #NUM! #NUM! #NUM! 3.7165 11.149409
65 4118.6 #NUM! #NUM! #NUM! 3.7165 11.149409
66 4182.9 #NUM! #NUM! #NUM! 3.7165 11.149409
67 4247.3 #NUM! #NUM! #NUM! 3.7165 11.149409
68 4311.6 #NUM! #NUM! #NUM! 3.7165 11.149409
69 4376 #NUM! #NUM! #NUM! 3.7165 11.149409
70 4440.3 #NUM! #NUM! #NUM! 3.7165 11.149409
71 4504.7 #NUM! #NUM! #NUM! 3.7165 11.149409
72 4569 #NUM! #NUM! #NUM! 3.7165 11.149409
73 4633.4 #NUM! #NUM! #NUM! 3.7165 11.149409
74 4697.8 #NUM! #NUM! #NUM! 3.7165 11.149409
75 4762.1 #NUM! #NUM! #NUM! 3.7165 11.149409
76 4826.5 #NUM! #NUM! #NUM! 3.7165 11.149409
77 4890.8 #NUM! #NUM! #NUM! 3.7165 11.149409
78 4955.2 #NUM! #NUM! #NUM! 3.7165 11.149409
79 5019.5 #NUM! #NUM! #NUM! 3.7165 11.149409
80 5083.9 #NUM! #NUM! #NUM! 3.7165 11.149409
81 5148.2 #NUM! #NUM! #NUM! 3.7165 11.149409
82 5212.6 #NUM! #NUM! #NUM! 3.7165 11.149409
83 5276.9 #NUM! #NUM! #NUM! 3.7165 11.149409
84 5341.3 #NUM! #NUM! #NUM! 3.7165 11.149409
85 5405.6 #NUM! #NUM! #NUM! 3.7165 11.149409
86 5470 #NUM! #NUM! #NUM! 3.7165 11.149409
87 5534.3 #NUM! #NUM! #NUM! 3.7165 11.149409
88 5598.7 #NUM! #NUM! #NUM! 3.7165 11.149409
89 5663 #NUM! #NUM! #NUM! 3.7165 11.149409
90 5727.4 #NUM! #NUM! #NUM! 3.7165 11.149409
91 5791.8 #NUM! #NUM! #NUM! 3.7165 11.149409
92 5856.1 #NUM! #NUM! #NUM! 3.7165 11.149409
93 5920.5 #NUM! #NUM! #NUM! 3.7165 11.149409
94 5984.8 #NUM! #NUM! #NUM! 3.7165 11.149409
95 6049.2 #NUM! #NUM! #NUM! 3.7165 11.149409
96 6113.5 #NUM! #NUM! #NUM! 3.7165 11.149409
97 6177.9 #NUM! #NUM! #NUM! 3.7165 11.149409
98 6242.2 #NUM! #NUM! #NUM! 3.7165 11.149409
99 6306.6 #NUM! #NUM! #NUM! 3.7165 11.149409
100 6370.9 #NUM! #NUM! #NUM! 3.7165 11.149409
101 6435.3 #NUM! #NUM! #NUM! 3.7165 11.149409
102 6499.6 #NUM! #NUM! #NUM! 3.7165 11.149409
103 6564 #NUM! #NUM! #NUM! 3.7165 11.149409
104 6628.3 #NUM! #NUM! #NUM! 3.7165 11.149409
105 6692.7 #NUM! #NUM! #NUM! 3.7165 11.149409
106 6757 #NUM! #NUM! #NUM! 3.7165 11.149409
107 6821.4 #NUM! #NUM! #NUM! 3.7165 11.149409
108 6885.7 #NUM! #NUM! #NUM! 3.7165 11.149409
109 6950.1 #NUM! #NUM! #NUM! 3.7165 11.149409
110 7014.5 #NUM! #NUM! #NUM! 3.7165 11.149409
111 7078.8 #NUM! #NUM! #NUM! 3.7165 11.149409
112 7143.2 #NUM! #NUM! #NUM! 3.7165 11.149409
113 7207.5 #NUM! #NUM! #NUM! 3.7165 11.149409
114 7271.9 #NUM! #NUM! #NUM! 3.7165 11.149409
115 7336.2 #NUM! #NUM! #NUM! 3.7165 11.149409
116 7400.6 #NUM! #NUM! #NUM! 3.7165 11.149409
117 7464.9 #NUM! #NUM! #NUM! 3.7165 11.149409
118 7529.3 #NUM! #NUM! #NUM! 3.7165 11.149409
119 7593.6 #NUM! #NUM! #NUM! 3.7165 11.149409
120 7658 #NUM! #NUM! #NUM! 3.7165 11.149409
121 7722.3 #NUM! #NUM! #NUM! 3.7165 11.149409
122 7786.7 #NUM! #NUM! #NUM! 3.7165 11.149409
123 7851 #NUM! #NUM! #NUM! 3.7165 11.149409
124 7915.4 #NUM! #NUM! #NUM! 3.7165 11.149409
125 7979.7 #NUM! #NUM! #NUM! 3.7165 11.149409
126 8044.1 #NUM! #NUM! #NUM! 3.7165 11.149409
127 8108.5 #NUM! #NUM! #NUM! 3.7165 11.149409
128 8172.8 #NUM! #NUM! #NUM! 3.7165 11.149409
129 8237.2 #NUM! #NUM! #NUM! 3.7165 11.149409
130 8301.5 #NUM! #NUM! #NUM! 3.7165 11.149409
131 8365.9 #NUM! #NUM! #NUM! 3.7165 11.149409
132 8430.2 #NUM! #NUM! #NUM! 3.7165 11.149409
133 8494.6 #NUM! #NUM! #NUM! 3.7165 11.149409
134 8558.9 #NUM! #NUM! #NUM! 3.7165 11.149409
135 8623.3 #NUM! #NUM! #NUM! 3.7165 11.149409
136 8687.6 #NUM! #NUM! #NUM! 3.7165 11.149409
137 8752 #NUM! #NUM! #NUM! 3.7165 11.149409
138 8816.3 #NUM! #NUM! #NUM! 3.7165 11.149409
139 8880.7 #NUM! #NUM! #NUM! 3.7165 11.149409
140 8945 #NUM! #NUM! #NUM! 3.7165 11.149409
141 9009.4 #NUM! #NUM! #NUM! 3.7165 11.149409
142 9073.7 #NUM! #NUM! #NUM! 3.7165 11.149409
143 9138.1 #NUM! #NUM! #NUM! 3.7165 11.149409
144 9202.5 #NUM! #NUM! #NUM! 3.7165 11.149409
145 9266.8 #NUM! #NUM! #NUM! 3.7165 11.149409
146 9331.2 #NUM! #NUM! #NUM! 3.7165 11.149409
147 9395.5 #NUM! #NUM! #NUM! 3.7165 11.149409
148 9459.9 #NUM! #NUM! #NUM! 3.7165 11.149409
149 9524.2 #NUM! #NUM! #NUM! 3.7165 11.149409
150 9588.6 #NUM! #NUM! #NUM! 3.7165 11.149409
151 9652.9 #NUM! #NUM! #NUM! 3.7165 11.149409
152 9717.3 #NUM! #NUM! #NUM! 3.7165 11.149409
153 9781.6 #NUM! #NUM! #NUM! 3.7165 11.149409
154 9846 #NUM! #NUM! #NUM! 3.7165 11.149409
155 9910.3 #NUM! #NUM! #NUM! 3.7165 11.149409
156 9974.7 #NUM! #NUM! #NUM! 3.7165 11.149409
157 10039 #NUM! #NUM! #NUM! 3.7165 11.149409
158 10103 #NUM! #NUM! #NUM! 3.7165 11.149409
159 10168 #NUM! #NUM! #NUM! 3.7165 11.149409
160 10232 #NUM! #NUM! #NUM! 3.7165 11.149409
161 10296 #NUM! #NUM! #NUM! 3.7165 11.149409
162 10361 #NUM! #NUM! #NUM! 3.7165 11.149409
163 10425 #NUM! #NUM! #NUM! 3.7165 11.149409
164 10490 #NUM! #NUM! #NUM! 3.7165 11.149409
165 10554 #NUM! #NUM! #NUM! 3.7165 11.149409
166 10618 #NUM! #NUM! #NUM! 3.7165 11.149409
167
168
169
170
171
172
173
174
175
176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198
199
200
201
202
203
204
205
206
207
208
209
210
156808.93 mol/jam FD0 5659 A--k1 6.7945E+14
470426.78 mol/jam A-k2 8.9454E+21
632894.71 mol/jam
64.3528 kg
15 atm
12.00808 joule/mol 530.95 BERAT DATA 8880.6864
2.04266456 m2 Z 4.29604645
1012 kg/m3
53095.0158 kg
1
atm atm atm mol/jam/kg.cat/atm2
PC PD PE K1 K2 k1 k2
0 0 0 16.666 3.20815 3.714070422 0.07792223
0.25374034 0.2538 5E-05 16.232 3.01214 5.134522513 0.13154384
0.57761781 0.578 0.0003 15.71 2.78578 7.670136958 0.25170481
1.01031005 1.0117 0.0014 15.062 2.51915 12.86052037 0.58049853
1.61818036 1.6233 0.0051 14.235 2.20116 25.72258948 1.780583
2.47500815 2.4927 0.0177 13.201 1.83828 64.90115099 7.95120902
3.33912686 3.3772 0.0381 12.276 1.5452 158.3937103 33.6462902
3.55074247 3.5919 0.0412 12.05 1.47802 199.0274223 48.6729601
3.47592272 3.4985 0.0225 12.116 1.49767 185.9692624 43.6150636
3.54456267 3.5847 0.0402 12.009 1.46616 207.4356379 52.0407078
3.4617428 3.4993 0.0376 12.066 1.48294 195.6614641 47.3489974
3.51633956 3.5699 0.0536 11.975 1.45636 214.7114637 55.0237737
3.44113884 3.4857 0.0446 12.033 1.47304 202.5097267 50.0572978
3.51969658 3.5749 0.0552 11.924 1.44155 226.2808575 59.8966378
3.46331228 3.4716 0.0083 11.997 1.46267 209.9922709 53.0816862
3.63201793 3.6484 0.0164 11.798 1.40537 257.8465792 73.9774698
3.01242118 3.4027 0.3902 11.98 1.45783 213.6013728 54.5645455
1.30001621 3.2956 1.9955 12.07 1.48411 194.8656316 47.0380047
-1.5E+51 7E+66 2E+51 1.1482 0.00537 6.79448E+14 8.9454E+21
0 0 0 #NUM! #NUM! #NUM! #NUM!
meter
1
mol/jam mol/jam Joule/mol/K
FA FB FC FD FE r1 r2 CpA CpB
156809 470427 0 5659 0 153.897849 0 168.74 42.053
146099 459719 10706 16367 1.9037 193.692892 0.1156 169.69 42.158
132408 446041 24371 30045 14.571 254.293019 0.4562 170.87 42.287
114062 427739 42628 48347 59.616 351.576835 1.5851 172.39 42.453
88105 401937 68276 74149 213.92 506.928357 6.0099 174.41 42.672
50890 365253 104428 110833 745.7 647.302357 23.545 177.07 42.954
12705 327931 140888 148155 1608.3 225.172056 31.026 179.58 43.209
3517.1 318873 149816 157213 1737.7 -85.281308 9.5347 180.21 43.271
8247.7 322816 146660 153269 950.86 91.4849927 27.339 180.03 43.253
3863.4 319176 149556 156910 1694.9 -75.797941 11.779 180.33 43.282
7576.2 322780 146061 153306 1585.7 72.3415623 25.233 180.17 43.267
3922.5 319801 148365 156285 2260.8 -73.778622 10.76 180.42 43.291
7853.4 323353 145192 152733 1881.8 86.992452 26.779 180.26 43.276
3647.4 319593 148506 156493 2327.5 -90.606139 10.03 180.56 43.305
9985.3 323951 146127 152135 348.1 171.110622 42.467 180.36 43.285
2182.6 316491 153246 159595 690.31 -189.548 10.757 180.92 43.339
-3225 326858 127103 149228 16466 -309.23926 -62.265 180.41 43.29
-66438 331378 54852 144709 84198 -2479.0299 -304.72 180.16 43.266
-6E+55 -1E+26 -6E+55 3E+71 6E+55 5.846E+132 ### -3E+45 -2E+45
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
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156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
156809 470427 0 5659 0 #NUM! #NUM! #NUM! #NUM!
CpC CpD CpE a1 b1 c1 zi+h/2 xi+h*a1/2
191.13 35.576 339 0.001 2E-19 0.08225257 32.176 0.031579
192.44 35.623 341.77 0.0012 8E-07 0.10275976 96.529 0.108032
194.1 35.683 345.27 0.0016 4E-06 0.13370779 160.88 0.207694
196.27 35.762 349.87 0.0022 2E-05 0.18287215 225.23 0.344369
199.25 35.872 356.23 0.0032 8E-05 0.26060386 289.59 0.540791
203.39 36.025 365.09 0.0041 0.0006 0.33168982 353.94 0.803535
207.54 36.178 374.08 0.0014 0.0039 0.12312235 418.29 0.954928
208.63 36.218 376.46 -0.0005 -0.0036 -0.0361336 482.65 0.94899
208.3 36.206 375.75 0.0006 0.004 0.05682698 547 0.960112
208.83 36.226 376.9 0 -0.002 -0.0305217 611.35 0.949
208.55 36.215 376.28 0.0005 0.0041 0.04663227 675.7 0.956417
208.99 36.232 377.26 0 -0.0026 -0.0300394 740.06 0.945429
208.71 36.222 376.64 0.0006 0.0045 0.05435895 804.41 0.955767
209.25 36.241 377.81 -0.0006 -0.0042 -0.0383724 868.76 0.943305
208.89 36.228 377.03 0.0011 0.0047 0.10197343 933.12 0.969213
209.88 36.265 379.2 -0.0012 -0.0121 -0.0848197 997.47 0.942784
208.97 36.231 377.21 -0.002 -0.0337 -0.1782129 1061.8 0.852109
208.53 36.215 376.24 -0.0158 -0.6789 -1.3622562 1126.2 0.378058
5E+45 -5E+44 2E+46 4E+127 3E+136 3.1312E+30 1190.5 1E+129
#NUM! #NUM! #NUM! #NUM! #NUM! #NUM! 1254.9 0
#NUM! #NUM! #NUM! #NUM! #NUM! #NUM! 1641 0
x2+h*b1/2T+h*c1/PA PB PC PD PE K1 K2
6.98E-18 575.8 3.5991 11.032 0.1174 0.1174 3E-17 16.462 3.1153
3.9E-05 582.16 3.3148 10.748 0.4014 0.4015 0.0001 15.989 2.9058
0.000228 590.39 2.9439 10.378 0.7712 0.7719 0.0007 15.413 2.6617
0.001021 601.56 2.4341 9.8696 1.2773 1.2798 0.0025 14.687 2.3721
0.005059 617.43 1.698 9.1396 2.0012 2.0098 0.0086 13.757 2.0285
0.034939 638.51 0.7046 8.1631 2.9608 2.9863 0.0255 12.673 1.6674
0.239001 651.06 0.1275 7.6004 3.5089 3.549 0.04 12.1 1.4929
0.216387 651.06 0.1486 7.6225 3.4859 3.5269 0.041 12.1 1.4929
0.232081 652.52 0.1138 7.5812 3.5338 3.5682 0.0344 12.037 1.4742
0.239321 652.18 0.1442 7.6225 3.4816 3.5269 0.0454 12.052 1.4786
0.305665 653.34 0.1125 7.5949 3.505 3.5545 0.0495 12.001 1.4639
0.281249 652.97 0.1458 7.6358 3.4566 3.5137 0.057 12.017 1.4685
0.337385 654.36 0.1089 7.5973 3.4966 3.5521 0.0555 11.957 1.4511
0.253491 653.9 0.1573 7.6436 3.4524 3.5058 0.0534 11.977 1.4569
0.183872 656.72 0.0934 7.5474 3.581 3.6021 0.021 11.857 1.4223
-0.14933 655.4 0.2444 7.6456 3.5356 3.5038 -0.0318 11.913 1.4383
0.15771 648.09 0.4629 7.9826 3.0802 3.1668 0.0867 12.232 1.5319
-17.1043 607.91 41.847 9.7444 40.941 1.4049 -39.535 14.302 2.2259
1E+138 1E+32 5E+267 ### 5E+267 #NUM! ### 1.1482 0.0054
#NUM! #NUM! 3.7165 11.149 0 #NUM! 0 #NUM! #NUM!
2
k1 k2 FA FB FC FD FE r1 r2
4.3192 0.0995 151857 465475 4951.9 10611 1E-12 171.49 0.042
6.176 0.1773 139863 453486 16935 22599 5.4604 219.97 0.2359
9.6926 0.3675 124212 437859 32540 38227 28.289 295.74 0.8342
17.518 0.9568 102704 416427 53895 59659 104.98 418.91 2.9737
39.138 3.5098 71644 385626 84437 90460 364.28 595.94 11.897
107.12 17.877 29731 344425 124925 131661 1076.4 541.43 36.48
189.06 44.794 5378.5 320685 148052 155400 1689.2 -11.404 15.773
189.03 44.782 6268 321617 147079 154469 1730.9 21.99 18.85
201.67 49.723 4803.2 319873 149102 156213 1451.6 -37.219 15.862
198.63 48.515 6083.3 321615 146898 154471 1913.9 15.911 19.103
209.08 52.708 4745.3 320452 147886 155634 2089 -38.454 14.441
205.76 51.361 6150.5 322175 145845 153911 2406.7 21.066 18.87
218.74 56.702 4596 320554 147533 155532 2340.1 -46.191 13.898
214.33 54.867 6636.7 322508 145665 153578 2253.6 41.102 22.742
242.5 66.989 3940 318445 151094 157640 887.67 -92.898 18.831
228.9 61.02 10312 322590 149177 153496 -1340 189.68 57.446
165.57 36.145 19533 336808 129961 139277 3657.4 479.83 45.065
24.288 1.6227 2E+06 411144 2E+06 64938 -2E+06 9806.1 2820.6
7E+14 9E+21 2E+272 ### 2E+272 #NUM! ### #NUM! #NUM!
#NUM! #NUM! 156809 470427 0 #NUM! 0 #NUM! #NUM!
CpA CpB CpC CpD CpE a2 b2 c2
169.19 42.102 191.74 35.598 340.29 0.00109364 2.7666E-07 0.091340752
170.24 42.217 193.2 35.651 343.37 0.00140281 1.7481E-06 0.116218089
171.56 42.363 195.07 35.719 347.34 0.00188598 7.2566E-06 0.154719699
173.29 42.551 197.59 35.811 352.67 0.00267144 3.3085E-05 0.21664004
175.62 42.802 201.11 35.94 360.19 0.00380041 0.00020708 0.305114536
178.49 43.1 205.7 36.11 370.08 0.00345282 0.00179819 0.281279103
180.07 43.257 208.38 36.209 375.92 -7.2726E-05 0.00184606 0.00208736
180.07 43.257 208.38 36.209 375.92 0.00014024 0.00295149 0.019520689
180.25 43.275 208.69 36.221 376.6 -0.0002374 0.00115502 -0.010189138
180.21 43.271 208.62 36.218 376.44 0.00010147 0.0028649 0.016723051
180.35 43.284 208.87 36.227 376.98 -0.0002452 0.00039313 -0.011454067
180.31 43.28 208.79 36.224 376.81 0.00013434 0.00289749 0.019068987
180.47 43.296 209.08 36.235 377.46 -0.0002946 -0.000243 -0.015393211
180.42 43.291 208.98 36.232 377.24 0.00026212 0.00373008 0.030468109
180.75 43.323 209.58 36.254 378.55 -0.0005924 0.0003625 -0.035203958
180.6 43.308 209.3 36.243 377.94 0.00120961 0.00324584 0.117711791
179.71 43.222 207.75 36.186 374.54 0.00305997 0.00520636 0.253112963
174.24 42.654 199 35.863 355.69 0.06253518 -1.6908878 4.021520407
-1E+89 -7E+88 2E+89 -2E+88 6E+89 #NUM! #NUM! #NUM!
#NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM!
zi+h/2 xi+h*a2/2 x2+h*b2/2 T+h*c2/PA PB PC PD PE
32.176 0.0351896 8.9019E-06 576.09 3.5857 11.019 0.1307 0.1308 3E-05
32.245 0.113424 6.9276E-05 582.6 3.2947 10.728 0.4213 0.4215 0.0002
32.332 0.216198 0.0003435 591.07 2.912 10.346 0.8025 0.8035 0.001
32.449 0.3581843 0.001587 602.65 2.3815 9.8182 1.3274 1.3312 0.0038
32.613 0.5590557 0.0090851 618.86 1.6239 9.0717 2.0628 2.0777 0.0149
32.847 0.7818117 0.0723011 636.89 0.7523 8.2438 2.847 2.9056 0.0586
33.085 0.9063841 0.1717702 647.17 0.2882 7.7809 3.3088 3.3685 0.0598
33.143 0.9710014 0.4256578 652.85 0.0619 7.5407 3.5628 3.6087 0.0459
33.118 0.9337021 0.1405351 650.36 0.2118 7.6793 3.4354 3.4701 0.0346
33.141 0.9678183 0.397117 653.7 0.0721 7.5525 3.5494 3.5969 0.0475
33.118 0.9336819 0.1857263 651.47 0.2007 7.6794 3.4242 3.47 0.0458
33.137 0.9648907 0.458864 654.55 0.0706 7.5634 3.5261 3.586 0.0599
33.114 0.9284386 0.1854797 652.12 0.2166 7.6989 3.4012 3.4505 0.0493
33.138 0.9703309 0.5095719 656.11 0.0541 7.5432 3.55 3.6062 0.0562
33.111 0.9150399 0.0453508 652.3 0.3014 7.7487 3.3864 3.4007 0.0143
33.158 1.0205995 0.3447185 661.91 -0.0502 7.3564 3.8194 3.793 -0.0264
33.092 1.0140224 1.4111097 661.97 0.0214 7.3808 3.8421 3.7686 -0.0735
33.063 2.898899 -49.665791 781.14 -357.56 0.3757 -339.73 10.78 350.5
7E+20 6.883E+20 #NUM! #NUM! 3.7165 11.149 0 #NUM! #NUM!
32.176 0 #NUM! #NUM! 3.7165 11.149 0 #NUM! #NUM!
32.176 0 #NUM! #NUM! 3.7165 11.149 0 #NUM! #NUM!
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3
K1 K2 k1 k2 FA FB FC FD FE
16.44 3.1052 4.3915 0.1022 151290 464909 5516.7 11177 1.3468
15.958 2.8922 6.3262 0.1843 139013 452641 17776 23445 9.631
15.367 2.6429 10.053 0.3898 122865 436525 33860 39561 42.222
14.62 2.3462 18.535 1.0482 100483 414260 56007 61825 159.72
13.678 2.0008 41.999 3.9339 68516 382762 87037 93324 628.18
12.751 1.692 99.374 15.834 31740 347832 120121 128254 2473.7
12.273 1.5443 158.87 33.811 12158 328298 139608 147788 2521.6
12.022 1.4701 204.63 50.908 2611.7 318165 150326 157921 1935.6
12.131 1.5019 183.28 42.599 8935.1 324014 144952 152072 1461
11.986 1.4594 212.42 54.075 3042.4 318664 149759 157422 2004
12.082 1.4877 192.49 46.115 8467.8 324017 144478 152069 1931.4
11.949 1.4487 220.58 57.477 2979.2 319123 148777 156962 2526.3
12.054 1.4793 198.12 48.315 9140.1 324839 143506 151246 2081.4
11.883 1.4296 236.21 64.202 2281.7 318270 149786 157816 2370.7
12.046 1.477 199.75 48.958 12718 326940 142882 149145 604.19
11.642 1.3613 303.69 96.386 -2117 310388 161153 165698 -1114
11.64 1.3607 304.39 96.742 903.96 311419 162111 164667 -3103
8.1746 0.5848 23303 107582 -2E+07 15854 -1E+07 460506 1E+07
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#NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659 0
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#NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659 0
#NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659 0
r1 r2 CpA CpB CpC CpD CpE a3 b3
173.5 0.0479 169.24 42.107 191.8 35.6 340.43 0.00110643 3.27E-07
223.53 0.2559 170.31 42.225 193.3 35.654 343.58 0.00142549 1.95E-06
302.43 0.9107 171.66 42.374 195.23 35.724 347.66 0.00192866 8.26E-06
431.14 3.3113 173.45 42.569 197.83 35.82 353.19 0.00274948 3.97E-05
605.53 13.117 175.83 42.823 201.42 35.952 360.86 0.0038616 0.000269
551.8 32.316 178.28 43.079 205.35 36.097 369.32 0.00351894 0.002111
211.93 27.83 179.59 43.21 207.55 36.179 374.11 0.0013515 0.004376
-123.33 5.494 180.29 43.279 208.76 36.223 376.75 -0.0007865 -0.01034
117.94 27.583 179.99 43.249 208.23 36.204 375.6 0.00075212 0.004248
-110.57 7.5096 180.39 43.288 208.94 36.23 377.15 -0.0007052 -0.00721
107.37 26.767 180.12 43.262 208.47 36.213 376.11 0.00068471 0.004492
-115.62 5.7921 180.5 43.298 209.12 36.237 377.54 -0.0007373 -0.00858
137.53 30.039 180.2 43.27 208.61 36.218 376.41 0.00087707 0.00495
-158.13 3.2251 180.68 43.316 209.45 36.249 378.27 -0.0010084 -0.01663
275.59 48.36 180.22 43.272 208.65 36.219 376.5 0.00175748 0.004568
-490 -11.381 181.36 43.38 210.68 36.294 380.96 -0.0031248 0.055814
-330.51 27.667 181.37 43.381 210.69 36.294 380.98 -0.0021077 0.199525
7E+06 1E+10 190.41 43.78 234.83 37.109 436.44 46.6131631 -40334.6
#NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM!
c3 zi+h/2 xi+h*a3/2x2+h*b3/T+h*c3/2 PA PB PC PD
0.0924 32.176 0.001106 3.27E-07 573.2424 3.7124 11.145 0.0041 0.0041
0.118 96.529 0.069712 1.5E-05 578.9765 3.4573 10.89 0.259 0.2591
0.1581 160.88 0.157443 0.00012 586.2507 3.131 10.564 0.5848 0.5851
0.2228 225.23 0.274976 0.00056 595.9017 2.693 10.127 1.0204 1.0219
0.3099 289.59 0.440634 0.00269 609.3501 2.0733 9.5118 1.632 1.6376
0.2851 353.94 0.674231 0.01655 628.127 1.1907 8.6436 2.4857 2.5058
0.1153 418.29 0.910076 0.11675 647.2155 0.2952 7.7671 3.3433 3.3823
-0.0562 482.65 0.965703 0.32035 652.1645 0.0866 7.5604 3.5482 3.589
0.0697 547 0.942091 0.10762 650.7603 0.1921 7.6482 3.4781 3.5013
-0.0491 611.35 0.963848 0.29772 653.1081 0.0944 7.5673 3.5421 3.5821
0.0642 675.7 0.942257 0.17757 651.8996 0.1765 7.6475 3.4638 3.5019
-0.0523 740.06 0.959831 0.35705 653.8872 0.096 7.5822 3.5139 3.5672
0.0801 804.41 0.938794 0.19825 652.6931 0.1824 7.6604 3.4439 3.489
-0.0737 868.76 0.960888 0.37292 655.0604 0.0911 7.5783 3.5169 3.5711
0.155 933.12 0.93586 0.03826 653.59 0.2293 7.6713 3.469 3.4781
-0.2365 997.47 0.978554 0.29609 657.8889 0.0561 7.5126 3.6132 3.6368
-0.1429 1061.8 0.913456 1.44311 653.6789 -0.1425 7.7546 2.9307 3.3948
1E+06 1126.2 47.49991 -40330 1317138 -7E+06 -165.38 -7E+06 2287.7
#NUM! 1190.5 #NUM! #NUM! #NUM! #NUM! 11.149 #NUM! 0
#NUM! 1641 #NUM! #NUM! #NUM! #NUM! 11.149 #NUM! 0
4
PE K1 K2 k1 k2 FA FB FC FD
1E-06 16.658 3.2048 3.7338 0.0786 156635 470253 173.45 5832.5
5E-05 16.223 3.0083 5.1687 0.133 145875 459495 10929 16590
0.0004 15.699 2.7811 7.7369 0.2553 132105 445738 24673 30347
0.0015 15.047 2.5134 13.013 0.5917 113626 427308 43055 48778
0.0056 14.217 2.1944 26.13 1.8264 87478 401331 68859 74754
0.02 13.187 1.8334 65.79 8.1281 50238 364701 104880 111384
0.039 12.271 1.5436 159.22 33.929 12455 327719 141062 148367
0.0408 12.052 1.4787 198.53 48.478 3655.2 318996 149708 157090
0.0232 12.113 1.4968 186.55 43.834 8103.4 322698 146751 153387
0.04 12.011 1.4668 206.99 51.859 3981.2 319287 149452 156799
0.0381 12.064 1.4821 196.22 47.567 7446.8 322672 146147 153413
0.0533 11.978 1.457 214.22 54.819 4049.9 319917 148261 156169
0.0451 12.029 1.472 203.23 50.345 7695 323216 145309 152870
0.0542 11.927 1.4425 225.55 59.585 3845.9 319751 148389 156335
0.0091 11.99 1.4607 211.43 53.671 9673 323676 146366 152410
0.0236 11.808 1.4082 255.21 72.758 2367.2 316981 152450 159105
0.4642 11.987 1.4596 212.26 54.012 -6013 327189 123654 148897
7E+06 1.1495 0.0054 7E+14 9E+21 -3E+11 -7E+06 -3E+11 1E+08
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
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0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
0 #NUM! #NUM! #NUM! #NUM! 156809 470427 0 5659
FE r1 r2 CpA CpB CpC CpD CpE a4
0.0512 154.49 0.0012 168.76 42.054 191.15 35.577 339.05 0.00098519
2.1856 194.59 0.1191 169.71 42.16 192.47 35.624 341.83 0.00124092
15.629 255.74 0.4673 170.9 42.29 194.13 35.684 345.34 0.00163089
63.905 354.02 1.6256 172.42 42.457 196.32 35.764 349.97 0.00225763
236.07 510.39 6.1722 174.45 42.677 199.32 35.874 356.37 0.00325484
845.55 646.02 23.834 177.11 42.958 203.45 36.027 365.22 0.0041198
1646.2 218.32 30.583 179.6 43.211 207.56 36.179 374.13 0.00139226
1722.9 -79.742 10.097 180.21 43.27 208.62 36.218 376.44 -0.0005085
977.24 86.473 26.905 180.04 43.254 208.32 36.207 375.78 0.00055145
1687.8 -70.863 12.266 180.32 43.282 208.82 36.225 376.87 -0.0004519
1607.8 67.55 24.797 180.18 43.267 208.56 36.216 376.31 0.00043078
2249 -68.278 11.335 180.42 43.291 208.98 36.232 377.24 -0.0004354
1902.7 80.92 26.239 180.27 43.277 208.73 36.222 376.68 0.00051604
2287.2 -81.698 11.104 180.56 43.304 209.23 36.241 377.78 -0.000521
384.76 159.09 41.519 180.38 43.287 208.92 36.229 377.1 0.00101454
995.75 -176.44 10.315 180.89 43.336 209.83 36.263 379.09 -0.0011252
19584 -410.77 -80.87 180.39 43.288 208.94 36.23 377.14 -0.0026196
3E+11 1E+25 4E+35 -3E+11 -2E+11 4E+11 -4E+10 1E+12 6.4172E+19
0 #NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM! #NUM!
b4 c4
7.9794E-09 0.0826
8.3625E-07 0.1032
3.766E-06 0.1344
1.6049E-05 0.1841
8.6028E-05 0.2623
0.0006759 0.3311
0.00397642 0.1196
-0.0028725 -0.0332
0.0039878 0.0542
-0.0015578 -0.0279
0.00406327 0.0441
-0.0020707 -0.0271
0.00440542 0.0512
-0.0031572 -0.0336
0.00473311 0.0958
-0.0124673 -0.0788
-0.0496404 -0.2361
-5.468E+28 3E+16
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ACCUMULATOR (ACC-rdc)
Tugas: Menampung condensat dari CD RDC 1416.7804459289

Alat: Silinder Horizontal
Kondisi Operasi: T: 375.88
P: 0.9
Umpan masuk: 10000.0000 kg/jam

6.118453255 lb/s
komposisi kg/j MR X
Asam asetat 8524.4000 60.05 0.8524394267
AIR 1475.4600 18 0.1475459008
Mono 0.0001 134.131 1.24999915937557E-08
gliserol 0.0235 92.0938 0.00000235
Tri 0.1231 218.21 0.00001231
JUMLAH 10000.0067 53.8477 1
rho (liq)= 1045.9689020743 kg/m3

Volume umpan= 0.0026556982 m3/s 9.5605136827
Dari Fig 5-4 Evans diperoleh :
Untuk flow rate = 0.0938409274 cuft/s
Maka : L/D ratio = 1
L, shell length = 7 ft
D, drum diameter = 3.5 ft
Holding times = 5 menit
cara membaca fig 5-4 evans
PERHITUNGAN TEBAL DINDING
Code = ASME
Tebal dinding
t = ((P*R)/(S*E-0.6*P))+c
Jari-jari dalam, R
Di = 3.5 ft
R= 1.75 ft
Tekanan, P
P = Pdesign - Pudara luar
Pudara luar =
Pdes =Pudara*1.1 =
Maximal allowable stress

Material = Stainless steel
S= 18750
Joint Effisiensi, E=
Corrosion All., c =
Maka tebal dinding :

t = 0.1248 in
PERHITUNGAN TEBAL HEAD
Dipilih jenis Torispherical Dished Head

Code = ASME
Tebal Head :
t = (0.885PRc/(SE-0.1P))+c
diambil Rc = Dt =
t = 0.1247
Dari Tabel 5-8 B&Y, diambil sf =
OD = ID + 2t = ini od
a = ID/2 = 21
Dari Tabel 5-7 B&Y
untuk t=0.1875 in, OD=48 in maka diperoleh
AB = a-icr = 18
BC = r-icr = 45
AC = ((BC^2)-(AB^2))^0.5 =
b = r - AC = 6.7568187454
OA = t + b + sf =
kg/jam
375.88 K 102.88 C
0.90 atm
rhoi moli xi trial awal : 5 menit

1050 141.9550 0.6339376744
1022.7834403398 81.9700 0.3660586626
1050 0.0000 4.16175590282E-09
1260 0.0003 1.13954957259E-06
1160 0.0006 2.51929576871E-06
223.9259 1
0.0938409274 cuft/s
5.6304556435 cuft/men
3 28.134503161 cuft 0.7967095 cum

7 ft 6.8581034881 ft 2.0903754 m
3.5 ft 2.286034496 ft 0.6967918 m
5 menit
27.4327
-14.5673
ft = 42 in
ft = 21 in
1 atm
0.99 atm
-0.147 psig
psig
0.85
0.125
0.1875 in = 3/16 in
3.5 ft = 42 in
in
0.1875 in
2
42.375 in
in
icr = 3
r = 48
in
in
41.2431812546 in
in
8.9443 in 0.7453598954 ft
0.2271856961 m
V 1
CD-01
AC-01
Lo D
P=1 a t m
MD-01
Densitas (g/ml)
Komponen A B n Tc (K)
PO 0.31226 0.27634 0.29353 482.25
AIR 0.3471 0.274 0.28571 647.13
PG 0.31839 0.26106 0.20459 626
DPG 0.33335 0.265 0.2857 654
NO NAMA ALAT PENANGGUNGJAWAB
1 ST-01 VICTOR
2 ST-02 VICTOR
3 ST-03 VICTOR
4 ST-04 UJO udah
5 ST-05 VICTOR
6 ST-06 UJO TRIACETIN Udah
7 MX-01 UJO udah
8 MX-02 VICTOR
9 BC-01 UJO udah
10 HP-01 VICTOR
11 DC-01 VICTOR
12 DC-02 UJO udah
13 VDC-02 VICTOR
14 VDC-01 VICTOR
15 TDC-01 VICTOR
16 TDC-02 UJO UDAH naskah udah
17 HE-1 VICTOR
18 HE-2 VICTOR
19 HE-3 UJO CEK RD
20 CP-01 VICTOR
21 CP-02 VICTOR
22 CP-03 VICTOR
23 CP-04 VICTOR
24 CP-05 VICTOR
25 CP-06 VICTOR
26 CP-07 UJO udah naskah udah
27 CP-08 UJO udah
28 CP-09 UJO pastikan viskositas
29 CP-10 UJO udah
30 RB-01 VICTOR
31 RB-02 BERSAMA
32 RB-03 VICTOR
33 RB-04 UJO lagi rancang
34 CD-01 VICTOR
35 CD-02 BERSAMA
36 CD-03 VICTOR
37 CD-04 UJO lagi rancang
38 ACC-01 VICTOR
39 ACC-02 BERSAMA
40 ACC-03 VICTOR
41 ACC-04 UJO UDAH
42 RDC-01 BERSAMA
43 RB-05 UJO udah dicek lagi bagian kernnya
44 ACC-05 UJO udah cek pembacaan grafik evans
bikin naskah
tangki UDAH
belt conveyor hitung ulang
MD udah
Pompa udah
mixer UDAH
decanter plus decantar victor
reboiler plus reboiler victor
heat exchanger
akumulator
condenser udah

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Menentukan Sifat Fisis

2. Kapasitas panas gas (Cp) J/gmolK

2. Kapasitas panas liquid(Cl)

4. Kapasitas Panas Campuran Liquid

Shortcut Menara Distilasi

dari perhitungan neraca panas didapatkan suhu

Perhitungan Kondisi Umpan

Komponen Distilat(kg/jam) Distilat (kgmol/jam) xd=yi Po Ki

Komponen Feed(kg/jam) Feed (kgmol/jam) xb=xi Po Ki

Menentukan Komponen Kunci

Feed Menara Top Menara

Komponen alfa avg

Penentuan Tray Minimum

Perhitungan refluks minimum, refluk optimum, dan jumlah plate aktual

Kondisi umpan cair jenuh Teta 3.0062009192

Komponen Alfa xi,Fi alfaxi,Fi alfaxiFi/(alfa-Teta)

Komponen Alfa di xi.d alfaxi.d alfaxi.d

Penentuan feed plate

viskositas rata2 suhu distilat

Suhu Distilat 66.59644438 339.746444381 K

xi=yi/Ki Komponen Distilat(kg/jamDistilat (kgmol/j xd=yi

ositas rata2 suhu distilat 0.4378687262 cP

Distribusi komposisi (trial)

Check Feed Bubble Point

Check Top Bubble Point dan Dew Point

Check Bottom Bubble Point dan Dew Point

Menghitung nilai relative volatility

Komponen alfa feed alfa bottom alfa top alfa avg

𝐶=⁡⁡⁡log⁡〖��� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗 〗 /log⁡𝛼��⁡

Komponen BM fi, kmol/jam alfa di/bi di, kmol/jam

Menghitung Reflux Minimum

trial nilai teta 1.391387831

komponen alfa xif alfa xi alfa-teta atas/bawah

komponen alfa xid alfa xi alfa-teta atas/bawah

Menghitung Jumlah Tray Minimum

Menghitung Jumlah Tray Teoritis

Fig 11.11 Coulson and Richardson, 4th Volume 6

Menghitung viskositas pada Feed alfa LK avg 3.6352216416

miu, Cp x ln(miu) x Eo 52.3741513165

miu mix 0.249567211 cp

Mennetukan Letak Feed Plate

B= 74.7660 log(Nr/Ns) -0.723893341

Menghitung Diameter dan Tinggi MD

Menghitung Diameter Column Berdasarkan Kecepatan Uap Maksimum

L 1039.593019 kg/jam L 10332.282128 kg/jam

di, kg/jam bi, kmol/jam bi, kg/jam

Ki bulb Zi/Ki Zi*Ki

Ki bulb Zi/Ki Zi*Ki

dengan pembacaan grafik diperoleh:

eq. 11.80 Coulson Richardson

Distribusi Komposisi (TRIAL)

Check Feed Buble Point

Check Top Bubble Point dan Dew Point

Check Bottom Bubble Point dan Dew Point

Menghitung nilai relative volatility

komponen alfa feed alfa bottom alfa top alfa avg

log⁡〖⁡�� /𝑏�=𝐴+𝐶⁡log⁡〖 (𝛼�) 〗⁡〗 A -2.7624710461

Nama MW fi (kg/jam) fi (kmol/jam) alfa di/bi

Menghitung Reflux Minimum

trial nilai teta 1.2459526417

komponen alfa xif alfa*xi alfa-teta

Menghitung Jumlah Tray Minimum

Menghitung Jumlah Tray Teoritis

𝐶=⁡⁡⁡log⁡〖�� /𝑏��⁡⁡−log⁡〖�ℎ� /𝑏ℎ� 〗〗 /log⁡𝛼��⁡