CEM Continuous Stirred Tank Reactor - Run 1 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 10:16:29 00:00:00 0.050 0.050 0.0 0.0 0.20 30 18.7
2 10:16:39 00:00:10 0.050 0.050 0.0 0.0 0.20 30 18.4
3 10:16:49 00:00:20 0.050 0.050 0.0 0.0 0.20 30 18.2
4 10:16:59 00:00:30 0.050 0.050 0.0 0.0 0.20 30 18.1
5 10:17:09 00:00:40 0.050 0.050 0.0 0.0 0.20 30 18.2
6 10:17:19 00:00:50 0.050 0.050 0.0 0.0 0.19 30 18.6
7 10:17:29 00:01:00 0.050 0.050 0.0 0.0 0.19 30 18.8
8 10:17:39 00:01:10 0.050 0.050 0.0 0.0 0.20 30 19.4
9 10:17:49 00:01:20 0.050 0.050 0.0 0.0 0.19 30 20.1
10 10:17:59 00:01:30 0.050 0.050 0.0 0.0 0.19 30 20.8
11 10:18:09 00:01:40 0.050 0.050 0.0 0.0 0.20 30 21.6
12 10:18:19 00:01:50 0.050 0.050 0.0 0.0 0.20 30 22.5
13 10:18:29 00:02:00 0.050 0.050 0.0 0.0 0.20 30 23.3
14 10:18:39 00:02:10 0.050 0.050 0.0 0.0 0.20 30 24.3
15 10:18:49 00:02:20 0.050 0.050 0.0 0.0 0.20 30 25.3
16 10:18:59 00:02:30 0.050 0.050 0.0 0.0 0.20 30 26.4
17 10:19:09 00:02:40 0.050 0.050 0.0 0.0 0.20 30 27.4
18 10:19:19 00:02:50 0.050 0.050 0.0 0.0 0.20 30 28.5
19 10:19:29 00:03:00 0.050 0.050 0.0 0.0 0.19 30 29.5
20 10:19:39 00:03:10 0.050 0.050 0.0 0.0 0.19 30 30.5
21 10:19:49 00:03:20 0.050 0.050 0.0 0.0 0.20 30 31.3
22 10:19:59 00:03:30 0.050 0.050 0.0 0.0 0.19 30 32.1
23 10:20:09 00:03:40 0.050 0.050 0.0 0.0 0.20 30 32.9
24 10:20:19 00:03:50 0.050 0.050 0.0 0.0 0.20 30 33.6
25 10:20:29 00:04:01 0.050 0.050 0.0 0.0 0.19 30 34.3
26 10:20:39 00:04:10 0.050 0.050 0.0 0.0 0.19 30 34.8
27 10:20:49 00:04:20 0.050 0.050 0.0 0.0 0.20 30 35.4
28 10:20:59 00:04:30 0.050 0.050 0.0 0.0 0.20 30 35.8
29 10:21:09 00:04:40 0.050 0.050 0.0 0.0 0.20 30 36.3
30 10:21:19 00:04:50 0.050 0.050 0.0 0.0 0.20 30 36.7
31 10:21:29 00:05:00 0.050 0.050 0.0 0.0 0.20 30 37.0

Page 1
 CEM Continuous Stirred Tank Reactor - Run 1 Results

32 10:21:39 00:05:10 0.050 0.050 0.0 0.0 0.20 30 37.4

33 10:21:49 00:05:20 0.050 0.050 0.0 0.0 0.20 30 37.7
34 10:21:59 00:05:30 0.050 0.050 0.0 0.0 0.19 30 38.0
35 10:22:09 00:05:40 0.050 0.050 0.0 0.0 0.20 30 38.3
36 10:22:19 00:05:50 0.050 0.050 0.0 0.0 0.20 30 38.6
37 10:22:29 00:06:00 0.050 0.050 0.0 0.0 0.20 30 38.8
38 10:22:39 00:06:10 0.050 0.050 0.0 0.0 0.20 30 39.1
39 10:22:49 00:06:20 0.050 0.050 0.0 0.0 0.20 30 39.2
40 10:22:59 00:06:30 0.050 0.050 0.0 0.0 0.20 30 39.4
41 10:23:09 00:06:40 0.050 0.050 0.0 0.0 0.20 30 39.6
42 10:23:19 00:06:50 0.050 0.050 0.0 0.0 0.20 30 39.6
43 10:23:29 00:07:00 0.050 0.050 0.0 0.0 0.20 30 39.8
44 10:23:39 00:07:10 0.050 0.050 0.0 0.0 0.20 30 39.9
45 10:23:49 00:07:20 0.050 0.050 0.0 0.0 0.19 30 40.1
46 10:23:59 00:07:30 0.050 0.050 0.0 0.0 0.20 30 40.1
47 10:24:09 00:07:40 0.050 0.050 0.0 0.0 0.20 30 40.3

Page 2
 CEM Continuous Stirred Tank Reactor - Run 1 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 3
 CEM Continuous Stirred Tank Reactor - Run 1 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 4
 CEM Continuous Stirred Tank Reactor - Run 1 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 5
 CEM Continuous Stirred Tank Reactor - Run 1 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 6
 CEM Continuous Stirred Tank Reactor - Run 1 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
14.65 199.90
15.82 199.90
18.85 199.90
21.39 199.90
23.54 199.90
25.59 199.90
26.95 199.90
29.00 199.90
30.76 199.90
31.84 199.90
33.20 199.90
34.57 199.90
35.84 199.90
36.91 199.90
38.57 199.90
39.55 199.90
40.82 199.90
41.50 199.90
41.11 199.90
40.33 199.90
40.63 199.90
41.50 199.90
41.31 199.90
40.92 199.90
41.02 199.90
41.31 199.90
41.41 199.90
41.70 199.90
41.70 199.90
41.21 199.90
41.11 199.90

Page 7
 CEM Continuous Stirred Tank Reactor - Run 1 Results

41.50 199.90
41.50 199.90
41.70 199.90
41.60 199.90
41.89 199.90
41.80 199.90
41.70 199.90
41.70 199.90
41.99 199.90
41.89 199.90
41.89 199.90
41.99 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.89 199.90

Page 8
 CEM Continuous Stirred Tank Reactor - Run 2 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 10:33:29 00:00:00 0.050 0.050 0.0 0.0 0.20 30 23.4
2 10:33:39 00:00:10 0.050 0.050 0.0 0.0 0.20 30 22.8
3 10:35:38 00:02:09 0.050 0.050 0.0 0.0 0.20 30 18.5

Page 9
 CEM Continuous Stirred Tank Reactor - Run 2 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 10
 CEM Continuous Stirred Tank Reactor - Run 2 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 11
 CEM Continuous Stirred Tank Reactor - Run 2 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
12.79 199.90
12.99 199.90
16.60 199.90

Page 12
 CEM Continuous Stirred Tank Reactor - Run 3 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 10:35:42 00:00:00 0.050 0.050 0.0 0.0 0.20 30 18.4
2 10:35:51 00:00:10 0.050 0.050 0.0 0.0 0.20 30 18.3
3 10:36:02 00:00:20 0.050 0.050 0.0 0.0 0.20 30 18.3
4 10:36:11 00:00:30 0.050 0.050 0.0 0.0 0.19 30 18.5
5 10:36:22 00:00:40 0.050 0.050 0.0 0.0 0.19 30 18.8
6 10:36:31 00:00:50 0.050 0.050 0.0 0.0 0.20 30 19.1
7 10:36:42 00:01:00 0.050 0.050 0.0 0.0 0.19 30 19.6
8 10:36:51 00:01:10 0.050 0.050 0.0 0.0 0.20 30 20.2
9 10:37:02 00:01:20 0.050 0.050 0.0 0.0 0.20 30 21.0
10 10:37:11 00:01:30 0.050 0.050 0.0 0.0 0.20 30 21.8
11 10:37:22 00:01:40 0.050 0.050 0.0 0.0 0.19 30 22.6
12 10:37:31 00:01:50 0.050 0.050 0.0 0.0 0.20 30 23.4
13 10:37:42 00:02:00 0.050 0.050 0.0 0.0 0.20 30 24.4
14 10:37:51 00:02:10 0.050 0.050 0.0 0.0 0.19 30 25.4
15 10:38:02 00:02:20 0.050 0.050 0.0 0.0 0.20 30 26.4
16 10:38:12 00:02:30 0.050 0.050 0.0 0.0 0.20 30 27.3
17 10:38:21 00:02:40 0.050 0.050 0.0 0.0 0.20 30 28.3
18 10:38:32 00:02:50 0.050 0.050 0.0 0.0 0.20 30 29.4
19 10:38:41 00:03:00 0.050 0.050 0.0 0.0 0.19 30 30.4
20 10:38:52 00:03:10 0.050 0.050 0.0 0.0 0.20 30 31.2
21 10:39:01 00:03:20 0.050 0.050 0.0 0.0 0.19 30 31.9
22 10:39:12 00:03:30 0.050 0.050 0.0 0.0 0.20 30 32.6
23 10:39:21 00:03:40 0.050 0.050 0.0 0.0 0.19 30 33.3
24 10:39:32 00:03:50 0.050 0.050 0.0 0.0 0.19 30 34.0
25 10:39:41 00:04:00 0.050 0.050 0.0 0.0 0.20 30 34.6
26 10:39:52 00:04:10 0.050 0.050 0.0 0.0 0.20 30 35.1
27 10:40:01 00:04:20 0.050 0.050 0.0 0.0 0.19 30 35.5
28 10:40:12 00:04:30 0.050 0.050 0.0 0.0 0.19 30 36.0
29 10:40:21 00:04:40 0.050 0.050 0.0 0.0 0.19 30 36.4
30 10:40:32 00:04:50 0.050 0.050 0.0 0.0 0.20 30 36.8
31 10:40:42 00:05:00 0.050 0.050 0.0 0.0 0.20 30 37.1

Page 13
 CEM Continuous Stirred Tank Reactor - Run 3 Results

32 10:40:51 00:05:10 0.050 0.050 0.0 0.0 0.20 30 37.4

33 10:41:02 00:05:20 0.050 0.050 0.0 0.0 0.20 30 37.7
34 10:41:11 00:05:30 0.050 0.050 0.0 0.0 0.19 30 38.0
35 10:41:22 00:05:40 0.050 0.050 0.0 0.0 0.19 30 38.3
36 10:41:31 00:05:50 0.050 0.050 0.0 0.0 0.19 30 38.5
37 10:41:42 00:06:00 0.050 0.050 0.0 0.0 0.20 30 38.7
38 10:41:51 00:06:10 0.050 0.050 0.0 0.0 0.20 30 38.9
39 10:42:02 00:06:20 0.050 0.050 0.0 0.0 0.20 30 39.1
40 10:42:11 00:06:30 0.050 0.050 0.0 0.0 0.19 30 39.2
41 10:42:21 00:06:40 0.050 0.050 0.0 0.0 0.19 30 39.4
42 10:42:32 00:06:50 0.050 0.050 0.0 0.0 0.20 30 39.6
43 10:42:41 00:07:00 0.050 0.050 0.0 0.0 0.19 30 39.6
44 10:42:52 00:07:10 0.050 0.050 0.0 0.0 0.20 30 39.7
45 10:43:01 00:07:20 0.050 0.050 0.0 0.0 0.20 30 39.9
46 10:43:12 00:07:30 0.050 0.050 0.0 0.0 0.19 30 40.0
47 10:43:21 00:07:40 0.050 0.050 0.0 0.0 0.19 30 40.1
48 10:43:32 00:07:50 0.050 0.050 0.0 0.0 0.20 30 40.2
49 10:43:41 00:08:00 0.050 0.050 0.0 0.0 0.19 30 40.2
50 10:55:58 00:20:17 0.050 0.050 0.0 0.0 0.20 30 19.6

Page 14
 CEM Continuous Stirred Tank Reactor - Run 3 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 15
 CEM Continuous Stirred Tank Reactor - Run 3 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 16
 CEM Continuous Stirred Tank Reactor - Run 3 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 17
 CEM Continuous Stirred Tank Reactor - Run 3 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 18
 CEM Continuous Stirred Tank Reactor - Run 3 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
16.89 199.90
19.24 199.90
21.97 199.90
24.22 199.90
25.68 199.90
27.34 199.90
29.20 199.90
30.86 199.90
32.03 199.90
33.50 199.90
35.25 199.90
36.52 199.90
37.21 199.90
38.67 199.90
39.84 199.90
40.92 199.90
41.89 199.90
41.70 199.90
40.53 199.90
41.02 199.90
40.82 199.90
41.89 199.90
42.29 199.90
41.21 199.90
41.11 199.90
41.50 199.90
41.70 199.90
41.41 199.90
41.31 199.90
41.11 199.90
41.89 199.90

Page 19
 CEM Continuous Stirred Tank Reactor - Run 3 Results

41.70 199.90
41.89 199.90
41.70 199.90
41.70 199.90
41.41 199.90
41.70 199.90
41.60 199.90
41.80 199.90
41.80 199.90
41.89 199.90
41.89 199.90
41.60 199.90
41.80 199.90
41.99 199.90
41.99 199.90
41.80 199.90
41.89 199.90
41.89 199.90
18.75 199.90

Page 20
 CEM Continuous Stirred Tank Reactor - Run 4 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 10:56:01 00:00:00 0.050 0.050 0.0 0.0 0.20 30 19.6
2 10:56:11 00:00:10 0.050 0.050 0.0 0.0 0.19 30 19.5
3 10:56:21 00:00:20 0.050 0.050 0.0 0.0 0.20 30 19.7
4 10:56:31 00:00:30 0.050 0.050 0.0 0.0 0.20 30 19.8
5 10:56:41 00:00:40 0.050 0.050 0.0 0.0 0.20 30 20.1
6 10:56:51 00:00:50 0.050 0.050 0.0 0.0 0.20 30 20.6
7 10:57:01 00:01:00 0.050 0.050 0.0 0.0 0.20 30 21.2
8 10:57:11 00:01:10 0.050 0.050 0.0 0.0 0.20 30 21.8
9 10:57:21 00:01:20 0.050 0.050 0.0 0.0 0.20 30 22.5
10 10:57:31 00:01:30 0.050 0.050 0.0 0.0 0.20 30 23.2
11 10:57:41 00:01:41 0.050 0.050 0.0 0.0 0.20 30 24.0
12 10:57:51 00:01:50 0.050 0.050 0.0 0.0 0.19 30 24.9
13 10:58:01 00:02:00 0.050 0.050 0.0 0.0 0.19 30 25.9
14 10:58:11 00:02:10 0.050 0.050 0.0 0.0 0.19 30 26.9
15 10:58:21 00:02:20 0.050 0.050 0.0 0.0 0.20 30 27.7
16 10:58:31 00:02:30 0.050 0.050 0.0 0.0 0.20 30 28.7
17 10:58:41 00:02:40 0.050 0.050 0.0 0.0 0.20 30 29.7
18 10:58:51 00:02:50 0.050 0.050 0.0 0.0 0.20 30 30.7
19 10:59:01 00:03:00 0.050 0.050 0.0 0.0 0.19 30 31.3
20 10:59:11 00:03:10 0.050 0.050 0.0 0.0 0.19 30 32.1
21 10:59:21 00:03:20 0.050 0.050 0.0 0.0 0.20 30 32.7
22 10:59:31 00:03:30 0.050 0.050 0.0 0.0 0.19 30 33.4
23 10:59:41 00:03:40 0.050 0.050 0.0 0.0 0.20 30 34.1
24 10:59:51 00:03:50 0.050 0.050 0.0 0.0 0.19 30 34.6
25 11:00:01 00:04:00 0.050 0.050 0.0 0.0 0.20 30 35.1
26 11:00:11 00:04:10 0.050 0.050 0.0 0.0 0.20 30 35.5
27 11:00:21 00:04:20 0.050 0.050 0.0 0.0 0.19 30 35.9
28 11:00:31 00:04:30 0.050 0.050 0.0 0.0 0.19 30 36.3
29 11:00:41 00:04:40 0.050 0.050 0.0 0.0 0.20 30 36.7
30 11:00:51 00:04:50 0.050 0.050 0.0 0.0 0.20 30 37.0
31 11:01:01 00:05:00 0.050 0.050 0.0 0.0 0.19 30 37.3

Page 21
 CEM Continuous Stirred Tank Reactor - Run 4 Results

32 11:01:11 00:05:10 0.050 0.050 0.0 0.0 0.19 30 37.7

33 11:01:21 00:05:20 0.050 0.050 0.0 0.0 0.19 30 37.9
34 11:01:31 00:05:30 0.050 0.050 0.0 0.0 0.20 30 38.2
35 11:01:41 00:05:40 0.050 0.050 0.0 0.0 0.19 30 38.4
36 11:01:51 00:05:50 0.050 0.050 0.0 0.0 0.19 30 38.6
37 11:02:01 00:06:00 0.050 0.050 0.0 0.0 0.19 30 38.8
38 11:02:11 00:06:10 0.050 0.050 0.0 0.0 0.20 30 39.0
39 11:02:21 00:06:20 0.050 0.050 0.0 0.0 0.19 30 39.2
40 11:02:31 00:06:30 0.050 0.050 0.0 0.0 0.19 30 39.4
41 11:02:41 00:06:40 0.050 0.050 0.0 0.0 0.19 30 39.5
42 11:02:51 00:06:50 0.050 0.050 0.0 0.0 0.19 30 39.6
43 11:03:01 00:07:00 0.050 0.050 0.0 0.0 0.19 30 39.7
44 11:03:11 00:07:10 0.050 0.050 0.0 0.0 0.19 30 39.8
45 11:03:21 00:07:20 0.050 0.050 0.0 0.0 0.19 30 40.0
46 11:03:31 00:07:30 0.050 0.050 0.0 0.0 0.20 30 40.1
47 11:03:41 00:07:41 0.050 0.050 0.0 0.0 0.20 30 40.2
48 11:03:51 00:07:50 0.050 0.050 0.0 0.0 0.19 30 40.3
49 11:04:01 00:08:00 0.050 0.050 0.0 0.0 0.20 30 40.4
50 11:04:11 00:08:10 0.050 0.050 0.0 0.0 0.20 30 40.4

Page 22
 CEM Continuous Stirred Tank Reactor - Run 4 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 23
 CEM Continuous Stirred Tank Reactor - Run 4 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 24
 CEM Continuous Stirred Tank Reactor - Run 4 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 25
 CEM Continuous Stirred Tank Reactor - Run 4 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 26
 CEM Continuous Stirred Tank Reactor - Run 4 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
18.85 199.90
20.41 199.90
23.14 199.90
25.39 199.90
27.15 199.90
29.10 199.90
30.27 199.90
31.93 199.90
33.40 199.90
35.55 199.90
36.04 199.90
37.50 199.90
38.57 199.90
40.04 199.90
40.82 199.90
42.09 199.90
41.70 199.90
41.02 199.90
40.72 199.90
40.82 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.50 199.90
41.41 199.90
41.70 199.90
41.41 199.90
41.21 199.90
41.60 199.90
41.80 199.90
41.80 199.90

Page 27
 CEM Continuous Stirred Tank Reactor - Run 4 Results

41.89 199.90
41.70 199.90
41.80 199.90
41.70 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.60 199.90
41.60 199.90
41.80 199.90
41.99 199.90
41.99 199.90
41.89 199.90
41.70 199.90
41.99 199.90
41.89 199.90
41.89 199.90
41.89 199.90

Page 28
 CEM Continuous Stirred Tank Reactor - Run 5 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 11:19:31 00:00:00 0.050 0.050 0.0 0.0 0.20 30 19.8
2 11:19:41 00:00:10 0.050 0.050 0.0 0.0 0.20 30 19.7
3 11:19:51 00:00:20 0.050 0.050 0.0 0.0 0.19 30 19.9
4 11:20:01 00:00:30 0.050 0.050 0.0 0.0 0.20 30 20.1
5 11:20:11 00:00:40 0.050 0.050 0.0 0.0 0.19 30 20.5
6 11:20:21 00:00:50 0.050 0.050 0.0 0.0 0.19 30 21.0
7 11:20:31 00:01:00 0.050 0.050 0.0 0.0 0.19 30 21.6
8 11:20:41 00:01:10 0.050 0.050 0.0 0.0 0.19 30 22.3
9 11:20:51 00:01:20 0.050 0.050 0.0 0.0 0.19 30 23.0
10 11:21:01 00:01:30 0.050 0.050 0.0 0.0 0.19 30 23.8
11 11:21:11 00:01:40 0.050 0.050 0.0 0.0 0.20 30 24.7
12 11:21:21 00:01:50 0.050 0.050 0.0 0.0 0.19 30 25.6
13 11:21:31 00:02:00 0.050 0.050 0.0 0.0 0.19 30 26.5
14 11:21:41 00:02:11 0.050 0.050 0.0 0.0 0.19 30 27.4
15 11:21:51 00:02:20 0.050 0.050 0.0 0.0 0.19 30 28.5
16 11:22:01 00:02:30 0.050 0.050 0.0 0.0 0.20 30 29.4
17 11:22:11 00:02:40 0.050 0.050 0.0 0.0 0.19 30 30.3
18 11:22:21 00:02:50 0.050 0.050 0.0 0.0 0.19 30 31.1
19 11:22:31 00:03:00 0.050 0.050 0.0 0.0 0.19 30 31.8
20 11:22:41 00:03:10 0.050 0.050 0.0 0.0 0.19 30 32.4
21 11:22:51 00:03:20 0.050 0.050 0.0 0.0 0.20 30 33.2
22 11:23:01 00:03:30 0.050 0.050 0.0 0.0 0.19 30 33.8
23 11:23:11 00:03:40 0.050 0.050 0.0 0.0 0.20 30 34.3
24 11:23:21 00:03:50 0.050 0.050 0.0 0.0 0.19 30 34.8
25 11:23:31 00:04:00 0.050 0.050 0.0 0.0 0.20 30 35.3
26 11:23:41 00:04:10 0.050 0.050 0.0 0.0 0.19 30 35.7
27 11:23:51 00:04:20 0.050 0.050 0.0 0.0 0.19 30 36.2
28 11:24:01 00:04:30 0.050 0.050 0.0 0.0 0.19 30 36.5
29 11:24:11 00:04:40 0.050 0.050 0.0 0.0 0.19 30 36.9
30 11:24:21 00:04:50 0.050 0.050 0.0 0.0 0.19 30 37.2
31 11:24:31 00:05:00 0.050 0.050 0.0 0.0 0.19 30 37.6

Page 29
 CEM Continuous Stirred Tank Reactor - Run 5 Results

32 11:24:41 00:05:10 0.050 0.050 0.0 0.0 0.19 30 37.9

33 11:24:51 00:05:20 0.050 0.050 0.0 0.0 0.19 30 38.2
34 11:25:01 00:05:30 0.050 0.050 0.0 0.0 0.19 30 38.4
35 11:25:11 00:05:40 0.050 0.050 0.0 0.0 0.19 30 38.6
36 11:25:21 00:05:50 0.050 0.050 0.0 0.0 0.20 30 38.8
37 11:25:31 00:06:00 0.050 0.050 0.0 0.0 0.19 30 39.1
38 11:25:41 00:06:10 0.050 0.050 0.0 0.0 0.19 30 39.2
39 11:25:51 00:06:20 0.050 0.050 0.0 0.0 0.19 30 39.4
40 11:26:01 00:06:30 0.050 0.050 0.0 0.0 0.19 30 39.5
41 11:26:11 00:06:40 0.050 0.050 0.0 0.0 0.19 30 39.6
42 11:26:21 00:06:50 0.050 0.050 0.0 0.0 0.19 30 39.7
43 11:26:31 00:07:00 0.050 0.050 0.0 0.0 0.19 30 39.8
44 11:26:41 00:07:10 0.050 0.050 0.0 0.0 0.19 30 39.9
45 11:26:51 00:07:20 0.050 0.050 0.0 0.0 0.19 30 40.0
46 11:27:01 00:07:30 0.050 0.050 0.0 0.0 0.20 30 40.1
47 11:27:11 00:07:40 0.050 0.050 0.0 0.0 0.19 30 40.3
48 11:27:21 00:07:50 0.050 0.050 0.0 0.0 0.19 30 40.3

Page 30
 CEM Continuous Stirred Tank Reactor - Run 5 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 31
 CEM Continuous Stirred Tank Reactor - Run 5 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 32
 CEM Continuous Stirred Tank Reactor - Run 5 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 33
 CEM Continuous Stirred Tank Reactor - Run 5 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 34
 CEM Continuous Stirred Tank Reactor - Run 5 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
19.53 199.90
21.09 199.90
24.12 199.90
26.46 199.90
27.93 199.90
29.49 199.90
31.74 199.90
33.30 199.90
34.57 199.90
35.94 199.90
36.82 199.90
38.87 199.90
39.94 199.90
40.92 199.90
41.99 199.90
41.80 199.90
40.82 199.90
40.33 199.90
40.92 199.90
42.29 199.90
41.70 199.90
41.21 199.90
41.21 199.90
41.70 199.90
41.80 199.90
41.41 199.90
41.80 199.90
41.89 199.90
41.50 199.90
41.41 199.90
41.89 199.90

Page 35
 CEM Continuous Stirred Tank Reactor - Run 5 Results

41.70 199.90
41.60 199.90
41.50 199.90
41.70 199.90
41.80 199.90
41.80 199.90
41.60 199.90
41.60 199.90
41.99 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.89 199.90
41.89 199.90
41.89 199.90
41.99 199.90

Page 36
 CEM Continuous Stirred Tank Reactor - Run 6 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 11:37:49 00:00:00 0.050 0.050 0.0 0.0 0.20 50 19.4
2 11:37:59 00:00:10 0.050 0.050 0.0 0.0 0.20 50 19.2
3 11:38:09 00:00:20 0.050 0.050 0.0 0.0 0.20 50 19.0
4 11:38:19 00:00:30 0.050 0.050 0.0 0.0 0.19 50 19.0
5 11:38:29 00:00:40 0.050 0.050 0.0 0.0 0.20 50 19.0
6 11:38:39 00:00:50 0.050 0.050 0.0 0.0 0.20 50 19.4
7 11:38:49 00:01:00 0.050 0.050 0.0 0.0 0.19 50 19.8
8 11:38:59 00:01:10 0.050 0.050 0.0 0.0 0.19 40 20.2
9 11:39:09 00:01:20 0.050 0.050 0.0 0.0 0.19 30 20.9
10 11:39:19 00:01:30 0.050 0.050 0.0 0.0 0.19 30 21.6
11 11:39:29 00:01:40 0.050 0.050 0.0 0.0 0.19 30 22.4
12 11:39:39 00:01:50 0.050 0.050 0.0 0.0 0.19 30 23.1
13 11:39:49 00:02:00 0.050 0.050 0.0 0.0 0.20 30 24.0
14 11:39:59 00:02:10 0.050 0.050 0.0 0.0 0.19 50 25.0
15 11:40:09 00:02:20 0.050 0.050 0.0 0.0 0.20 50 25.9
16 11:40:19 00:02:30 0.050 0.050 0.0 0.0 0.20 50 26.9
17 11:40:29 00:02:40 0.050 0.050 0.0 0.0 0.19 50 27.8
18 11:40:39 00:02:50 0.050 0.050 0.0 0.0 0.19 50 28.9
19 11:40:49 00:03:00 0.050 0.050 0.0 0.0 0.19 50 29.9
20 11:40:59 00:03:11 0.050 0.050 0.0 0.0 0.19 50 30.8
21 11:41:09 00:03:20 0.050 0.050 0.0 0.0 0.19 50 31.4
22 11:41:19 00:03:30 0.050 0.050 0.0 0.0 0.20 50 32.1
23 11:41:29 00:03:40 0.050 0.050 0.0 0.0 0.20 50 32.9
24 11:41:39 00:03:50 0.050 0.050 0.0 0.0 0.19 50 33.7
25 11:41:49 00:04:00 0.050 0.050 0.0 0.0 0.19 50 34.2
26 11:41:59 00:04:10 0.050 0.050 0.0 0.0 0.19 50 34.7
27 11:42:09 00:04:20 0.050 0.050 0.0 0.0 0.19 50 35.2
28 11:42:19 00:04:30 0.050 0.050 0.0 0.0 0.20 50 35.6
29 11:42:29 00:04:40 0.050 0.050 0.0 0.0 0.20 50 36.0
30 11:42:39 00:04:50 0.050 0.050 0.0 0.0 0.19 50 36.4
31 11:42:49 00:05:00 0.050 0.050 0.0 0.0 0.19 50 36.8

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 CEM Continuous Stirred Tank Reactor - Run 6 Results

32 11:42:59 00:05:10 0.050 0.050 0.0 0.0 0.19 50 37.1

33 11:43:09 00:05:21 0.050 0.050 0.0 0.0 0.20 50 37.5
34 11:43:19 00:05:30 0.050 0.050 0.0 0.0 0.20 50 37.8
35 11:43:29 00:05:40 0.050 0.050 0.0 0.0 0.19 50 38.1
36 11:43:39 00:05:50 0.050 0.050 0.0 0.0 0.19 50 38.3
37 11:43:49 00:06:00 0.050 0.050 0.0 0.0 0.20 50 38.5
38 11:43:59 00:06:10 0.050 0.050 0.0 0.0 0.19 50 38.8
39 11:44:09 00:06:20 0.050 0.050 0.0 0.0 0.19 50 38.9
40 11:44:19 00:06:30 0.050 0.050 0.0 0.0 0.19 50 39.1
41 11:44:29 00:06:41 0.050 0.050 0.0 0.0 0.20 50 39.3
42 11:44:39 00:06:50 0.050 0.050 0.0 0.0 0.20 50 39.4
43 11:44:49 00:07:00 0.050 0.050 0.0 0.0 0.19 50 39.6
44 11:44:59 00:07:10 0.050 0.050 0.0 0.0 0.19 50 39.6
45 11:45:09 00:07:21 0.050 0.050 0.0 0.0 0.19 50 39.7
46 11:45:19 00:07:30 0.050 0.050 0.0 0.0 0.19 50 39.8
47 11:45:29 00:07:40 0.050 0.050 0.0 0.0 0.19 50 40.0
48 11:45:39 00:07:50 0.050 0.050 0.0 0.0 0.19 50 40.0
49 11:45:49 00:08:00 0.050 0.050 0.0 0.0 0.20 50 40.2
50 11:45:59 00:08:10 0.050 0.050 0.0 0.0 0.19 50 40.2
51 11:46:09 00:08:20 0.050 0.050 0.0 0.0 0.19 50 40.3

Page 38
 CEM Continuous Stirred Tank Reactor - Run 6 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 39
 CEM Continuous Stirred Tank Reactor - Run 6 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

Page 40
 CEM Continuous Stirred Tank Reactor - Run 6 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 41
 CEM Continuous Stirred Tank Reactor - Run 6 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

Page 42
 CEM Continuous Stirred Tank Reactor - Run 6 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
15.23 199.90
16.50 199.90
19.53 199.90
21.68 199.90
23.73 199.90
26.46 199.90
27.73 199.90
29.30 199.90
31.15 199.90
32.91 199.90
34.77 199.90
34.96 199.90
36.91 199.90
38.09 199.90
39.06 199.90
40.23 199.90
41.31 199.90
41.89 199.90
40.72 199.90
40.33 199.90
40.63 199.90
41.70 199.90
42.38 199.90
41.50 199.90
40.82 199.90
41.02 199.90
41.60 199.90
41.31 199.90
41.11 199.90
41.11 199.90
41.31 199.90

Page 43
 CEM Continuous Stirred Tank Reactor - Run 6 Results

41.70 199.90
41.50 199.90
41.41 199.90
41.50 199.90
41.60 199.90
41.89 199.90
41.50 199.90
41.89 199.90
41.70 199.90
41.80 199.90
41.70 199.90
41.60 199.90
41.80 199.90
41.70 199.90
41.89 199.90
41.70 199.90
41.89 199.90
41.80 199.90
41.99 199.90
41.80 199.90

Page 44
 CEM Continuous Stirred Tank Reactor - Run 7 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 12:05:51 00:00:00 0.050 0.050 0.0 0.0 0.19 50 19.7
2 12:06:01 00:00:10 0.050 0.050 0.0 0.0 0.19 50 19.7
3 12:06:11 00:00:20 0.050 0.050 0.0 0.0 0.19 50 19.8
4 12:06:21 00:00:30 0.050 0.050 0.0 0.0 0.19 50 20.0
5 12:06:31 00:00:40 0.050 0.050 0.0 0.0 0.20 50 20.3
6 12:06:41 00:00:50 0.050 0.050 0.0 0.0 0.19 50 20.7
7 12:06:51 00:01:00 0.050 0.050 0.0 0.0 0.19 50 21.3
8 12:07:01 00:01:10 0.050 0.050 0.0 0.0 0.19 50 21.8
9 12:07:11 00:01:20 0.050 0.050 0.0 0.0 0.19 50 22.5
10 12:07:21 00:01:30 0.050 0.050 0.0 0.0 0.20 50 23.3
11 12:07:31 00:01:40 0.050 0.050 0.0 0.0 0.20 50 24.0
12 12:07:41 00:01:50 0.050 0.050 0.0 0.0 0.19 50 24.9
13 12:07:51 00:02:00 0.050 0.050 0.0 0.0 0.20 50 25.8
14 12:08:01 00:02:10 0.050 0.050 0.0 0.0 0.19 50 26.7
15 12:08:11 00:02:20 0.050 0.050 0.0 0.0 0.19 50 27.6
16 12:08:21 00:02:30 0.050 0.050 0.0 0.0 0.19 50 28.6
17 12:08:31 00:02:40 0.050 0.050 0.0 0.0 0.19 50 29.5
18 12:08:41 00:02:50 0.050 0.050 0.0 0.0 0.19 50 30.4
19 12:08:51 00:03:00 0.050 0.050 0.0 0.0 0.19 50 31.2
20 12:09:01 00:03:10 0.050 0.050 0.0 0.0 0.19 50 31.8
21 12:09:11 00:03:20 0.050 0.050 0.0 0.0 0.20 50 32.6
22 12:09:21 00:03:30 0.050 0.050 0.0 0.0 0.19 50 33.3
23 12:09:31 00:03:40 0.050 0.050 0.0 0.0 0.20 50 34.0
24 12:09:41 00:03:50 0.050 0.050 0.0 0.0 0.19 50 34.5
25 12:09:51 00:04:00 0.050 0.050 0.0 0.0 0.20 50 35.0
26 12:10:01 00:04:10 0.050 0.050 0.0 0.0 0.20 50 35.4
27 12:10:11 00:04:20 0.050 0.050 0.0 0.0 0.19 50 35.9
28 12:10:21 00:04:30 0.050 0.050 0.0 0.0 0.19 50 36.3
29 12:10:31 00:04:40 0.050 0.050 0.0 0.0 0.19 50 36.7
30 12:10:41 00:04:50 0.050 0.050 0.0 0.0 0.20 50 37.0
31 12:10:51 00:05:00 0.050 0.050 0.0 0.0 0.19 50 37.3

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

32 12:11:01 00:05:10 0.050 0.050 0.0 0.0 0.19 50 37.6

33 12:11:11 00:05:20 0.050 0.050 0.0 0.0 0.19 50 37.9
34 12:11:21 00:05:30 0.050 0.050 0.0 0.0 0.19 37 38.2
35 12:11:31 00:05:40 0.050 0.050 0.0 0.0 0.19 30 38.4
36 12:11:41 00:05:50 0.050 0.050 0.0 0.0 0.19 30 38.7
37 12:11:51 00:06:00 0.050 0.050 0.0 0.0 0.20 30 38.9
38 12:12:01 00:06:10 0.050 0.050 0.0 0.0 0.19 30 39.0
39 12:12:11 00:06:20 0.050 0.050 0.0 0.0 0.20 30 39.2

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
19.43 199.90
20.61 199.90
22.95 199.90
25.49 199.90
26.95 199.90
28.71 199.90
30.47 199.90
32.13 199.90
33.50 199.90
34.77 199.90
35.64 199.90
37.11 199.90
38.48 199.90
40.23 199.90
40.72 199.90
41.70 199.90
41.70 199.90
40.63 199.90
40.43 199.90
40.82 199.90
42.19 199.90
42.09 199.90
41.50 199.90
40.92 199.90
41.11 199.90
41.70 199.90
41.89 199.90
41.80 199.90
41.31 199.90
41.31 199.90
41.60 199.90

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 CEM Continuous Stirred Tank Reactor - Run 7 Results

41.80 199.90
41.80 199.90
41.60 199.90
41.70 199.90
41.60 199.90
41.50 199.90
41.70 199.90
41.89 199.90

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 12:23:24 00:00:00 0.050 0.050 0.0 0.0 0.18 50 19.5
2 12:23:34 00:00:10 0.050 0.050 0.0 0.0 0.18 50 19.6
3 12:23:44 00:00:20 0.050 0.050 0.0 0.0 0.19 50 19.6
4 12:23:51 00:00:27 0.050 0.050 0.0 0.0 0.19 50 19.7
5 12:24:01 00:00:37 0.050 0.050 0.0 0.0 0.19 50 19.6
6 12:24:11 00:00:47 0.050 0.050 0.0 0.0 0.19 50 19.7
7 12:24:21 00:00:57 0.050 0.050 0.0 0.0 0.19 50 19.8
8 12:24:31 00:01:07 0.050 0.050 0.0 0.0 0.19 45 20.1
9 12:24:41 00:01:17 0.050 0.050 0.0 0.0 0.19 50 20.6
10 12:24:51 00:01:27 0.050 0.050 0.0 0.0 0.19 60 21.1
11 12:25:01 00:01:37 0.050 0.050 0.0 0.0 0.19 60 21.7
12 12:25:11 00:01:47 0.050 0.050 0.0 0.0 0.20 50 22.4
13 12:25:21 00:01:57 0.050 0.050 0.0 0.0 0.19 50 23.1
14 12:25:31 00:02:07 0.050 0.050 0.0 0.0 0.20 50 23.9
15 12:25:41 00:02:17 0.050 0.050 0.0 0.0 0.20 50 24.7
16 12:25:51 00:02:27 0.050 0.050 0.0 0.0 0.19 50 25.7
17 12:26:01 00:02:37 0.050 0.050 0.0 0.0 0.19 50 26.6
18 12:26:11 00:02:47 0.050 0.050 0.0 0.0 0.19 50 27.5
19 12:26:21 00:02:57 0.050 0.050 0.0 0.0 0.19 30 28.5
20 12:26:31 00:03:07 0.050 0.050 0.0 0.0 0.19 20 29.4
21 12:26:41 00:03:17 0.050 0.050 0.0 0.0 0.19 64 30.3
22 12:26:51 00:03:27 0.050 0.050 0.0 0.0 0.19 65 31.1
23 12:27:01 00:03:37 0.050 0.050 0.0 0.0 0.19 65 31.8
24 12:27:11 00:03:47 0.050 0.050 0.0 0.0 0.19 65 32.4
25 12:29:12 00:05:48 0.050 0.050 0.0 0.0 0.19 50 32.8
26 12:29:23 00:05:59 0.050 0.050 0.0 0.0 0.20 50 32.9
27 12:29:32 00:06:09 0.050 0.050 0.0 0.0 0.19 50 33.5
28 12:29:42 00:06:18 0.050 0.050 0.0 0.0 0.19 50 33.9
29 12:29:53 00:06:29 0.050 0.050 0.0 0.0 0.19 50 34.5
30 12:30:02 00:06:38 0.050 0.050 0.0 0.0 0.19 50 35.0
31 12:30:13 00:06:49 0.050 0.050 0.0 0.0 0.19 50 35.4

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

32 12:30:22 00:06:58 0.050 0.050 0.0 0.0 0.19 50 35.9

33 12:30:33 00:07:09 0.050 0.050 0.0 0.0 0.19 50 36.3
34 12:30:42 00:07:18 0.050 0.050 0.0 0.0 0.19 50 36.7
35 12:30:53 00:07:29 0.050 0.050 0.0 0.0 0.19 50 37.0
36 12:31:02 00:07:38 0.050 0.050 0.0 0.0 0.19 50 37.3
37 12:31:13 00:07:49 0.050 0.050 0.0 0.0 0.19 50 37.7
38 12:31:22 00:07:58 0.050 0.050 0.0 0.0 0.19 50 37.9
39 12:31:32 00:08:09 0.050 0.050 0.0 0.0 0.19 50 38.2
40 12:31:43 00:08:19 0.050 0.050 0.0 0.0 0.19 50 38.4
41 12:31:52 00:08:28 0.050 0.050 0.0 0.0 0.20 50 38.7
42 12:32:03 00:08:39 0.050 0.050 0.0 0.0 0.19 50 38.8
43 12:32:12 00:08:48 0.050 0.050 0.0 0.0 0.19 50 39.0
44 12:32:23 00:08:59 0.050 0.050 0.0 0.0 0.19 50 39.2
45 12:32:32 00:09:08 0.050 0.050 0.0 0.0 0.19 50 39.3
46 12:32:43 00:09:19 0.050 0.050 0.0 0.0 0.19 50 39.5
47 12:32:52 00:09:28 0.050 0.050 0.0 0.0 0.19 50 39.6
48 12:33:03 00:09:39 0.050 0.050 0.0 0.0 0.19 50 39.7
49 12:33:12 00:09:48 0.050 0.050 0.0 0.0 0.19 50 39.8
50 12:33:23 00:09:59 0.050 0.050 0.0 0.0 0.19 50 39.9
51 12:33:32 00:10:08 0.050 0.050 0.0 0.0 0.19 50 40.0
52 12:33:43 00:10:19 0.050 0.050 0.0 0.0 0.19 50 40.1
53 12:33:52 00:10:28 0.050 0.050 0.0 0.0 0.19 50 40.2

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

1.00 0.00 0.00 0.0 0.00 0.00

1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00
1.00 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
18.85 199.90
18.85 199.90
18.85 199.90
18.95 199.90
20.02 199.90
22.95 199.90
24.61 199.90
26.86 199.90
28.32 199.90
30.08 199.90
31.45 199.90
33.11 199.90
34.38 199.90
35.84 199.90
36.82 199.90
38.09 199.90
39.36 199.90
40.63 199.90
41.60 199.90
41.60 199.90
41.02 199.90
40.72 199.90
41.21 199.90
41.70 199.90
41.50 199.90
40.82 199.90
40.33 199.90
40.92 199.90
42.09 199.90
41.99 199.90
41.60 199.90

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 CEM Continuous Stirred Tank Reactor - Run 8 Results

41.31 199.90
41.80 199.90
41.60 199.90
41.80 199.90
41.50 199.90
41.89 199.90
41.70 199.90
41.80 199.90
41.89 199.90
41.99 199.90
41.70 199.90
41.70 199.90
41.60 199.90
41.70 199.90
41.70 199.90
41.89 199.90
41.89 199.90
41.80 199.90
41.60 199.90
41.80 199.90
41.80 199.90
41.89 199.90

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 12:59:35 00:00:00 0.050 0.050 0.0 0.0 0.20 70 19.3
2 12:59:45 00:00:10 0.050 0.050 0.0 0.0 0.20 70 19.3
3 12:59:55 00:00:20 0.050 0.050 0.0 0.0 0.20 70 19.3
4 13:00:05 00:00:30 0.050 0.050 0.0 0.0 0.19 70 19.5
5 13:00:15 00:00:40 0.050 0.050 0.0 0.0 0.19 70 19.7
6 13:00:25 00:00:50 0.050 0.050 0.0 0.0 0.20 71 20.2
7 13:00:35 00:01:00 0.050 0.050 0.0 0.0 0.19 75 20.7
8 13:00:45 00:01:10 0.050 0.050 0.0 0.0 0.19 75 21.3
9 13:00:55 00:01:20 0.050 0.050 0.0 0.0 0.19 75 22.0
10 13:01:05 00:01:30 0.050 0.050 0.0 0.0 0.19 75 22.6
11 13:01:15 00:01:40 0.050 0.050 0.0 0.0 0.19 75 23.3
12 13:01:25 00:01:50 0.050 0.050 0.0 0.0 0.19 75 24.0
13 13:01:35 00:02:00 0.050 0.050 0.0 0.0 0.19 75 24.8
14 13:01:45 00:02:10 0.050 0.050 0.0 0.0 0.19 75 25.7
15 13:01:55 00:02:20 0.050 0.050 0.0 0.0 0.19 75 26.5
16 13:02:05 00:02:30 0.050 0.050 0.0 0.0 0.19 75 27.3
17 13:02:15 00:02:40 0.050 0.050 0.0 0.0 0.19 75 28.2
18 13:02:25 00:02:50 0.050 0.050 0.0 0.0 0.19 75 29.1
19 13:02:35 00:03:00 0.050 0.050 0.0 0.0 0.19 75 29.9
20 13:02:45 00:03:10 0.050 0.050 0.0 0.0 0.19 75 30.7
21 13:02:55 00:03:20 0.050 0.050 0.0 0.0 0.19 75 31.3
22 13:03:05 00:03:30 0.050 0.050 0.0 0.0 0.20 75 32.0
23 13:03:15 00:03:40 0.050 0.050 0.0 0.0 0.20 75 32.6
24 13:03:25 00:03:50 0.050 0.050 0.0 0.0 0.19 75 33.2
25 13:03:35 00:04:00 0.050 0.050 0.0 0.0 0.19 75 33.7
26 13:03:45 00:04:10 0.050 0.050 0.0 0.0 0.19 75 34.2
27 13:03:55 00:04:20 0.050 0.050 0.0 0.0 0.19 75 34.7
28 13:04:05 00:04:30 0.050 0.050 0.0 0.0 0.20 75 35.1
29 13:04:15 00:04:40 0.050 0.050 0.0 0.0 0.19 75 35.4
30 13:04:25 00:04:50 0.050 0.050 0.0 0.0 0.19 75 35.9
31 13:04:35 00:05:00 0.050 0.050 0.0 0.0 0.19 75 36.1

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

32 13:04:45 00:05:10 0.050 0.050 0.0 0.0 0.19 75 36.5

33 13:04:55 00:05:20 0.050 0.050 0.0 0.0 0.19 75 36.8
34 13:05:05 00:05:30 0.050 0.050 0.0 0.0 0.19 75 37.1
35 13:05:15 00:05:40 0.050 0.050 0.0 0.0 0.19 75 37.4
36 13:05:25 00:05:50 0.050 0.050 0.0 0.0 0.19 75 37.7
37 13:05:35 00:06:00 0.050 0.050 0.0 0.0 0.19 70 37.9
38 13:05:45 00:06:10 0.050 0.050 0.0 0.0 0.19 70 38.1
39 13:05:55 00:06:20 0.050 0.050 0.0 0.0 0.19 70 38.3
40 13:06:05 00:06:30 0.050 0.050 0.0 0.0 0.19 70 38.6
41 13:06:15 00:06:40 0.050 0.050 0.0 0.0 0.19 70 38.7
42 13:06:25 00:06:51 0.050 0.050 0.0 0.0 0.19 70 38.9
43 13:06:35 00:07:00 0.050 0.050 0.0 0.0 0.19 70 39.1
44 13:06:45 00:07:10 0.050 0.050 0.0 0.0 0.19 70 39.2
45 13:06:55 00:07:20 0.050 0.050 0.0 0.0 0.19 70 39.4
46 13:07:05 00:07:30 0.050 0.050 0.0 0.0 0.19 70 39.5
47 13:07:15 00:07:40 0.050 0.050 0.0 0.0 0.18 70 39.6
48 13:07:25 00:07:50 0.050 0.050 0.0 0.0 0.19 70 39.7
49 13:07:35 00:08:00 0.050 0.050 0.0 0.0 0.20 70 39.8
50 13:07:45 00:08:10 0.050 0.050 0.0 0.0 0.19 70 39.8
51 13:07:55 00:08:20 0.050 0.050 0.0 0.0 0.19 70 39.9
52 13:08:05 00:08:30 0.050 0.050 0.0 0.0 0.20 70 40.0
53 13:08:15 00:08:40 0.050 0.050 0.0 0.0 0.20 70 40.1

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

1.50 0.00 0.00 0.0 0.00 0.00

1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
19.24 199.90
20.21 199.90
22.07 199.90
24.80 199.90
26.56 199.90
28.52 199.90
29.69 199.90
31.05 199.90
32.91 199.90
33.89 199.90
34.96 199.90
36.62 199.90
37.89 199.90
38.96 199.90
39.84 199.90
41.31 199.90
41.31 199.90
40.92 199.90
40.82 199.90
41.02 199.90
41.21 199.90
41.11 199.90
41.21 199.90
41.41 199.90
41.60 199.90
41.31 199.90
41.70 199.90
41.50 199.90
41.11 199.90
41.11 199.90
41.41 199.90

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 CEM Continuous Stirred Tank Reactor - Run 9 Results

41.99 199.90
41.89 199.90
41.50 199.90
41.50 199.90
41.60 199.90
41.60 199.90
41.70 199.90
41.89 199.90
41.70 199.90
41.50 199.90
41.70 199.90
41.70 199.90
41.80 199.90
41.70 199.90
41.70 199.90
41.89 199.90
41.80 199.90
41.99 199.90
41.89 199.90
41.89 199.90
41.80 199.90
41.89 199.90

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 13:55:57 00:00:00 0.050 0.050 0.0 0.0 0.19 68 19.2
2 13:56:07 00:00:10 0.050 0.050 0.0 0.0 0.19 75 19.3
3 13:56:17 00:00:20 0.050 0.050 0.0 0.0 0.20 75 19.4
4 13:56:27 00:00:30 0.050 0.050 0.0 0.0 0.19 75 19.8
5 13:56:37 00:00:40 0.050 0.050 0.0 0.0 0.19 75 20.1
6 13:56:47 00:00:50 0.050 0.050 0.0 0.0 0.19 75 20.6
7 13:56:57 00:01:00 0.050 0.050 0.0 0.0 0.20 75 21.2
8 13:57:07 00:01:10 0.050 0.050 0.0 0.0 0.19 75 21.8
9 13:57:17 00:01:20 0.050 0.050 0.0 0.0 0.19 75 22.6
10 13:57:27 00:01:30 0.050 0.050 0.0 0.0 0.20 75 23.3
11 13:57:37 00:01:40 0.050 0.050 0.0 0.0 0.19 75 24.1
12 13:57:47 00:01:50 0.050 0.050 0.0 0.0 0.19 75 24.7
13 13:57:57 00:02:00 0.050 0.050 0.0 0.0 0.18 75 24.8
14 13:58:07 00:02:10 0.050 0.050 0.0 0.0 0.19 75 24.7
15 13:58:17 00:02:20 0.050 0.050 0.0 0.0 0.19 75 24.7
16 13:58:27 00:02:30 0.050 0.050 0.0 0.0 0.19 75 25.0
17 13:58:37 00:02:40 0.050 0.050 0.0 0.0 0.19 75 25.9
18 13:58:47 00:02:50 0.050 0.050 0.0 0.0 0.19 75 26.8
19 13:58:57 00:03:00 0.050 0.050 0.0 0.0 0.19 75 27.6
20 13:59:07 00:03:10 0.050 0.050 0.0 0.0 0.19 80 28.6
21 13:59:17 00:03:20 0.050 0.050 0.0 0.0 0.20 75 29.5
22 13:59:27 00:03:30 0.050 0.050 0.0 0.0 0.19 70 30.4
23 13:59:37 00:03:40 0.050 0.050 0.0 0.0 0.19 75 31.1
24 13:59:47 00:03:50 0.050 0.050 0.0 0.0 0.20 75 31.6
25 13:59:57 00:04:00 0.050 0.050 0.0 0.0 0.19 75 32.3
26 14:00:07 00:04:10 0.050 0.050 0.0 0.0 0.20 75 32.9
27 14:00:17 00:04:20 0.050 0.050 0.0 0.0 0.19 75 33.6
28 14:00:27 00:04:30 0.050 0.050 0.0 0.0 0.19 75 34.1
29 14:00:37 00:04:40 0.050 0.050 0.0 0.0 0.19 75 34.5
30 14:00:47 00:04:50 0.050 0.050 0.0 0.0 0.20 75 35.0
31 14:00:57 00:05:00 0.050 0.050 0.0 0.0 0.19 75 35.4

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

32 14:01:07 00:05:10 0.050 0.050 0.0 0.0 0.20 75 35.8

33 14:01:17 00:05:20 0.050 0.050 0.0 0.0 0.19 75 36.2
34 14:01:27 00:05:30 0.050 0.050 0.0 0.0 0.19 75 36.6
35 14:01:37 00:05:40 0.050 0.050 0.0 0.0 0.19 75 36.9
36 14:01:47 00:05:50 0.050 0.050 0.0 0.0 0.19 75 37.2
37 14:01:57 00:06:00 0.050 0.050 0.0 0.0 0.19 75 37.5
38 14:02:07 00:06:10 0.050 0.050 0.0 0.0 0.19 75 37.8
39 14:02:17 00:06:20 0.050 0.050 0.0 0.0 0.20 75 38.0
40 14:02:27 00:06:30 0.050 0.050 0.0 0.0 0.19 75 38.2
41 14:02:37 00:06:40 0.050 0.050 0.0 0.0 0.19 75 38.5
42 14:02:47 00:06:50 0.050 0.050 0.0 0.0 0.19 75 38.7
43 14:02:57 00:07:00 0.050 0.050 0.0 0.0 0.19 75 38.8
44 14:03:07 00:07:10 0.050 0.050 0.0 0.0 0.19 75 39.0
45 14:03:17 00:07:20 0.050 0.050 0.0 0.0 0.19 75 39.2
46 14:03:27 00:07:30 0.050 0.050 0.0 0.0 0.19 75 39.4
47 14:03:37 00:07:40 0.050 0.050 0.0 0.0 0.19 75 39.6
48 14:03:47 00:07:50 0.050 0.050 0.0 0.0 0.19 75 39.6
49 14:03:57 00:08:00 0.050 0.050 0.0 0.0 0.19 75 39.7
50 14:04:07 00:08:10 0.050 0.050 0.0 0.0 0.19 75 39.8
51 14:04:17 00:08:20 0.050 0.050 0.0 0.0 0.20 75 39.9
52 14:04:27 00:08:30 0.050 0.050 0.0 0.0 0.19 75 40.0
53 14:04:37 00:08:40 0.050 0.050 0.0 0.0 0.19 75 40.1
54 14:04:47 00:08:50 0.050 0.050 0.0 0.0 0.19 75 40.2

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

1.50 0.00 0.00 0.0 0.00 0.00

1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
19.82 199.90
22.66 199.90
24.12 199.90
26.56 199.90
28.22 199.90
29.88 199.90
31.74 199.90
32.81 199.90
34.18 199.90
35.84 199.90
37.60 199.90
38.48 199.90
38.57 199.90
38.96 199.90
38.87 199.90
37.99 199.90
38.77 199.90
40.14 199.90
40.92 199.90
41.99 199.90
41.70 199.90
40.63 199.90
40.33 199.90
40.82 199.90
41.89 199.90
41.41 199.90
41.02 199.90
41.02 199.90
41.60 199.90
41.80 199.90
41.99 199.90

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 CEM Continuous Stirred Tank Reactor - Run 10 Results

41.50 199.90
41.50 199.90
41.31 199.90
41.41 199.90
41.70 199.90
41.41 199.90
41.50 199.90
41.80 199.90
41.99 199.90
41.60 199.90
41.60 199.90
41.70 199.90
41.70 199.90
41.89 199.90
41.89 199.90
41.80 199.90
41.80 199.90
41.99 199.90
41.70 199.90
41.99 199.90
41.70 199.90
41.80 199.90
41.99 199.90

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 14:18:21 00:00:00 0.050 0.050 0.0 0.0 0.19 60 18.9
2 14:18:30 00:00:10 0.050 0.050 0.0 0.0 0.19 60 18.8
3 14:18:41 00:00:20 0.050 0.050 0.0 0.0 0.19 60 18.8
4 14:18:50 00:00:30 0.050 0.050 0.0 0.0 0.19 60 18.9
5 14:19:01 00:00:40 0.050 0.050 0.0 0.0 0.19 60 19.3
6 14:19:11 00:00:50 0.050 0.050 0.0 0.0 0.20 60 19.8
7 14:19:21 00:01:00 0.050 0.050 0.0 0.0 0.19 60 20.5
8 14:19:31 00:01:10 0.050 0.050 0.0 0.0 0.19 60 21.3
9 14:19:41 00:01:20 0.050 0.050 0.0 0.0 0.20 60 22.3
10 14:19:51 00:01:30 0.050 0.050 0.0 0.0 0.19 60 23.2
11 14:20:00 00:01:40 0.050 0.050 0.0 0.0 0.19 60 24.2
12 14:20:11 00:01:50 0.050 0.050 0.0 0.0 0.20 60 25.4
13 14:20:20 00:02:00 0.050 0.050 0.0 0.0 0.19 60 26.5
14 14:20:31 00:02:10 0.050 0.050 0.0 0.0 0.20 60 27.6
15 14:20:41 00:02:20 0.050 0.050 0.0 0.0 0.19 60 28.9
16 14:20:51 00:02:30 0.050 0.050 0.0 0.0 0.19 60 30.2
17 14:21:00 00:02:40 0.050 0.050 0.0 0.0 0.19 60 31.3
18 14:21:11 00:02:50 0.050 0.050 0.0 0.0 0.19 60 32.4
19 14:21:21 00:03:00 0.050 0.050 0.0 0.0 0.19 60 33.3
20 14:21:31 00:03:10 0.050 0.050 0.0 0.0 0.19 60 34.1
21 14:21:41 00:03:20 0.050 0.050 0.0 0.0 0.19 60 34.9
22 14:21:51 00:03:30 0.050 0.050 0.0 0.0 0.19 60 35.5
23 14:22:01 00:03:40 0.050 0.050 0.0 0.0 0.19 60 36.2
24 14:22:11 00:03:51 0.050 0.050 0.0 0.0 0.19 60 36.7
25 14:22:21 00:04:00 0.050 0.050 0.0 0.0 0.19 60 37.2
26 14:22:30 00:04:10 0.050 0.050 0.0 0.0 0.20 60 37.6
27 14:22:41 00:04:20 0.050 0.050 0.0 0.0 0.19 60 38.0
28 14:22:50 00:04:30 0.050 0.050 0.0 0.0 0.20 60 38.3
29 14:23:01 00:04:40 0.050 0.050 0.0 0.0 0.19 60 38.7
30 14:23:11 00:04:50 0.050 0.050 0.0 0.0 0.19 60 39.0
31 14:23:21 00:05:00 0.050 0.050 0.0 0.0 0.19 60 39.3

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

32 14:23:30 00:05:10 0.050 0.050 0.0 0.0 0.19 60 39.5

33 14:23:41 00:05:20 0.050 0.050 0.0 0.0 0.19 60 39.6
34 14:23:51 00:05:30 0.050 0.050 0.0 0.0 0.19 60 39.7
35 14:24:01 00:05:40 0.050 0.050 0.0 0.0 0.19 60 39.9
36 14:24:11 00:05:50 0.050 0.050 0.0 0.0 0.19 60 40.1
37 14:24:21 00:06:00 0.050 0.050 0.0 0.0 0.19 60 40.2
38 14:24:31 00:06:10 0.050 0.050 0.0 0.0 0.19 60 40.3

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

Reactor NaOH EtAC Initial Final Final

Volume Feed Feed Feed NaOH NaAC
Notes
Concentration Concentration Conductivity Concentration Concentration
[dm³] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

1.50 0.00 0.00 0.0 0.00 0.00

1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00
1.50 0.00 0.00 0.0 0.00 0.00

Page 80
 CEM Continuous Stirred Tank Reactor - Run 11 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/ Measured

Final NaOH NaAC of of Rate (a - a0)) Conductivity
Conductivity Concentration Concentration NaOH NaAC Constant 0-5
[mS] [mol/dm³] [mol/dm³] [%] [%] K [mS]
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.01
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02
0.0 0.00 0.00 0.00 0.00 0.000 0.000 0.02

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
17.19 199.90
18.36 199.90
21.09 199.90
23.54 199.90
25.59 199.90
27.93 199.90
29.30 199.90
30.96 199.90
32.62 199.90
34.28 199.90
35.64 199.90
37.11 199.90
38.48 199.90
39.36 199.90
40.92 199.90
42.19 199.90
41.31 199.90
40.82 199.90
40.72 199.90
42.38 199.90
42.19 199.90
41.89 199.90
41.41 199.90
41.31 199.90
41.31 199.90
41.41 199.90
41.70 199.90
42.19 199.90
41.70 199.90
41.80 199.90
42.19 199.90

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 CEM Continuous Stirred Tank Reactor - Run 11 Results

41.70 199.90
41.80 199.90
41.60 199.90
41.80 199.90
41.80 199.90
41.70 199.90
41.70 199.90

Page 84
 CEM Continuous Stirred Tank Reactor - Run 12 Results

Sample Sample Elapsed Sodium Ethyl Flowrate Flowrate Measured Stirrer Reactor
Number Time Time Hydroxide Acetate of Sodium of Ethyl Conductivity Speed Temp.
Concentaion Concentraion Hydroxide Acetate
[mol/dm³] [mol/dm³] [cm³/min] [cm³/min] 0 - 20 [mS] [rpm] [°C]
1 14:40:46 00:00:00 0.050 0.050 0.0 0.0 0.19 60 19.5
2 14:40:56 00:00:10 0.050 0.050 0.0 0.0 0.19 60 19.4
3 14:41:06 00:00:20 0.050 0.050 0.0 0.0 0.20 60 19.4
4 14:41:16 00:00:31 0.050 0.050 0.0 0.0 0.19 60 19.6
5 14:41:26 00:00:40 0.050 0.050 0.0 0.0 0.19 60 20.0
6 14:41:36 00:00:50 0.050 0.050 0.0 0.0 0.19 60 20.6
7 14:41:46 00:01:00 0.050 0.050 0.0 0.0 0.20 60 21.4
8 14:41:56 00:01:10 0.050 0.050 0.0 0.0 0.19 60 22.2
9 14:42:06 00:01:20 0.050 0.050 0.0 0.0 0.19 60 23.1
10 14:42:16 00:01:30 0.050 0.050 0.0 0.0 0.19 60 24.1
11 14:42:26 00:01:40 0.050 0.050 0.0 0.0 0.19 60 25.2
12 14:42:36 00:01:50 0.050 0.050 0.0 0.0 0.19 60 26.4
13 14:42:46 00:02:00 0.050 0.050 0.0 0.0 0.20 60 27.5
14 14:42:56 00:02:10 0.050 0.050 0.0 0.0 0.19 60 28.6
15 14:43:06 00:02:20 0.050 0.050 0.0 0.0 0.20 60 29.9
16 14:43:16 00:02:30 0.050 0.050 0.0 0.0 0.20 60 31.1
17 14:43:26 00:02:40 0.050 0.050 0.0 0.0 0.19 60 32.3
18 14:43:36 00:02:50 0.050 0.050 0.0 0.0 0.19 60 33.3
19 14:43:46 00:03:01 0.050 0.050 0.0 0.0 0.19 60 34.2
20 14:43:56 00:03:10 0.050 0.050 0.0 0.0 0.19 60 34.9
21 14:44:06 00:03:20 0.050 0.050 0.0 0.0 0.19 60 35.4
22 14:44:16 00:03:30 0.050 0.050 0.0 0.0 0.20 60 36.1
23 14:44:26 00:03:40 0.050 0.050 0.0 0.0 0.19 60 36.7
24 14:44:36 00:03:50 0.050 0.050 0.0 0.0 0.19 60 37.2
25 14:44:46 00:04:00 0.050 0.050 0.0 0.0 0.19 60 37.7
26 14:44:56 00:04:10 0.050 0.050 0.0 0.0 0.19 60 38.1
27 14:45:06 00:04:20 0.050 0.050 0.0 0.0 0.19 60 38.4
28 14:45:16 00:04:30 0.050 0.050 0.0 0.0 0.19 60 38.8
29 14:45:26 00:04:40 0.050 0.050 0.0 0.0 0.19 60 39.1
30 14:45:36 00:04:51 0.050 0.050 0.0 0.0 0.20 60 39.3
31 14:45:46 00:05:00 0.050 0.050 0.0 0.0 0.19 60 39.5

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 CEM Continuous Stirred Tank Reactor - Run 12 Results

32 14:45:56 00:05:10 0.050 0.050 0.0 0.0 0.19 60 39.6

33 14:46:06 00:05:20 0.050 0.050 0.0 0.0 0.19 60 39.8
34 14:46:16 00:05:31 0.050 0.050 0.0 0.0 0.19 60 40.0
35 14:46:26 00:05:40 0.050 0.050 0.0 0.0 0.19 60 40.1
36 14:46:36 00:05:50 0.050 0.050 0.0 0.0 0.20 60 40.2
37 14:46:46 00:06:00 0.050 0.050 0.0 0.0 0.19 60 40.3

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 CEM Continuous Stirred Tank Reactor - Run 12 Results

Measured NaOH EtAC Initial Final Final

Conductivity Feed Feed Feed NaOH NaAC
Notes
0-5 Concentration Concentration Conductivity Concentration Concentration
[mS] [mol/dm³] [mol/dm³] [mS] [mol/dm³] [mol/dm³]
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00

Page 87
 CEM Continuous Stirred Tank Reactor - Run 12 Results

0.016889 0.00 0.00 0.0 0.00 0.00

0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00
0.019336 0.00 0.00 0.0 0.00 0.00
0.016889 0.00 0.00 0.0 0.00 0.00

Page 88
 CEM Continuous Stirred Tank Reactor - Run 12 Results

Calculated Current Current Conversion Production Specific ln ((a - a1)/

Final NaOH NaAC of of Rate (a - a0))
Conductivity Concentration Concentration NaOH NaAC Constant
[mS] [mol/dm³] [mol/dm³] [%] [%] K
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000

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 CEM Continuous Stirred Tank Reactor - Run 12 Results

0.0 0.00 0.00 0.00 0.00 #REF! 0.000

0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000
0.0 0.00 0.00 0.00 0.00 #REF! 0.000

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 CEM Continuous Stirred Tank Reactor - Run 12 Results

Optional Optional
Temperature Temperature
T2 T3
[°C] [°C]
17.77 199.90
19.04 199.90
21.68 199.90
23.93 199.90
25.98 199.90
27.83 199.90
29.49 199.90
30.86 199.90
33.30 199.90
34.57 199.90
36.13 199.90
37.50 199.90
38.87 199.90
40.23 199.90
41.11 199.90
42.77 199.90
41.89 199.90
41.41 199.90
40.92 199.90
41.02 199.90
42.09 199.90
41.99 199.90
41.70 199.90
41.60 199.90
41.70 199.90
41.70 199.90
41.70 199.90
41.70 199.90
41.89 199.90
41.99 199.90
41.89 199.90

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 CEM Continuous Stirred Tank Reactor - Run 12 Results

41.80 199.90
41.80 199.90
41.80 199.90
41.80 199.90
41.70 199.90
41.80 199.90

Page 92