1H-RMN Bencilo en CDCl3 Current Data Parameters

NAME ls.130203
EXPNO 1
PROCNO 1

8.0130
8.0057
7.9960
7.9924
7.9877
7.9845
7.6962
7.6934
7.6904
7.6790
7.6747
7.6709
7.6592
7.6561
7.6533
7.5490
7.5455
7.5170
7.5147
7.5099
7.2791
F2 - Acquisition Parameters
Date_ 20030213
Time 18.46
INSTRUM spect
PROBHD 5 mm QXI 1H/3
PULPROG zg30
TD 16384
SOLVENT CDCl3
NS 8
DS 2
SWH 5995.204 Hz
FIDRES 0.365918 Hz
AQ 1.3664756 sec
RG 64
DW 83.400 usec
DE 6.70 usec
TE 300.0 K
D1 1.00000000 sec

============ CHANNEL f1 =============

NUC1 1H
P1 9.50 usec
PL1 2.00 dB
SFO1 400.1328151 MHz

F2 - Processing parameters
SI 32768
SF 400.1300000 MHz
WDW no
SSB 0
LB 0.00 Hz
GB 0
PC 1.00
1.9500

1.0000

2.0486

8.9 8.8 8.7 8.6 8.5 8.4 8.3 8.2 8.1 8.0 7.9 7.8 7.7 7.6 7.5 7.4 7.3 7.2 7.1 7.0 6.9 6.8 6.7 6.6 6.5 6.4 6.3 ppm
13C-RMN Bencilo en CDCl3 Current Data Parameters
NAME ls.130203
EXPNO 2
PROCNO 1

F2 - Acquisition Parameters
Date_ 20030213

194.50

134.80
133.00
129.84
128.96
Time 18.58

77.29
76.97
76.65
INSTRUM spect
PROBHD 5 mm QXI 1H/3
PULPROG zgpg30
TD 65536
SOLVENT CDCl3
NS 340
DS 2
SWH 22222.223 Hz
FIDRES 0.339084 Hz
AQ 1.4746100 sec
RG 2048
DW 22.500 usec
DE 15.00 usec
TE 300.0 K
D1 0.50000000 sec
D11 0.03000000 sec
D12 0.00002000 sec

============ CHANNEL f1 =============

NUC1 13C
P1 16.00 usec
PL1 -6.00 dB
SFO1 100.6232933 MHz

============ CHANNEL f2 =============

CPDPRG2 waltz16
NUC2 1H
PCPD2 90.00 usec
PL2 2.00 dB
PL12 18.00 dB
PL13 24.00 dB
SFO2 400.1316005 MHz

F2 - Processing parameters
SI 32768
SF 100.6127743 MHz
WDW EM
SSB 0
LB 1.00 Hz
GB 0
PC 1.40

210 200 190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 ppm