CAIRO UNIVERSITY FOURTH YEAR FACULTY OF ENGINEERING (MASS TRANSFER CHEMICAL ENGINEERING DEPARTMENT ‘SHEET 1: DIFFUSION J+ Calculate the mass diffusivity of a mixture of CO and Oz at 25°C 1 atm. using Gilliland correlation, Vo2 =25.6, Veo =34 em? /gmole 2 Caleulate the diffusion coefficient of Methanol in Water at 30°C knowing that: Vu = 14.9 cm? /gmole and Vy = 8 em? /gmole 3. Determine the diffusivity of COz (1), O2 @) and Na (3) in a gas mixture having the next composition (Mole Basis): 28.5% CO2, 15% O2 and 56.5% No ‘The gas mixture is at 273K and 1 atm, the binary diffusivities are given as follows: Diz = 0.1874 m*/see, Dy3 = 0.1945 m°/see, Dza = 0.1834 m/sec 4- Consider the case in which liquid (A) evaporates and diffuses through stagnant gas (B) as shown in the figure. Assuming the process is carried out isothermally at 25 °C and the total pressure is 1 atm, Calculate the molar flux when the level of liquid (A) is 0.05 m below the top of the container. ‘Assume that Dan = 1.0B-5 m? /seé. The mole fraction of A in the gas phase at the gas-liquid interface is 0.2 and at the top of the container is 0.001 B 5- An open cylindrical tank 20 fi in diameter contains benzene at 22 °C which is exposed to the atmosphere in such a manner that the liquid is covered with a stagnant air film estimated to be 5 mm thick. The concentration of benzene beyond the stagnant film is negligible. The vapour pressure of benzene at 22°C is 100 mmHg. If benzene is worth 30 cents per gallon, what is the value of the loss of benzene from this tank, in dollars per day? Given that the specific gravity of benzene is 0.88 and diffusivity of benzene in air at 22 °C is 1.0132E-4 fi/seeMASS TRANSFER Sheet 1 & Ifa floating roof is used to decrease the losses, what diameter of the roof will be needed to reduce the losses by 95%? Note: 1 gellon~0.1337 #0 6- By what percentage would the rate of absorption be increased or decreased by increasing the total pressure from 100 to 200 KN/m? in the following cases: 8) The absorption of ammonia from a mixture of ammonia and air containing 10% of ammonia by volume, using pure water as solvent, Assume that all the resistance to ‘mass transfer lies within the gas phase. ns as (a) but the absorbing solution exerts a partial vapour pressure b) The same condi ‘of ammonia of 5 KN/n?. ‘The diffusivity can be assumed to be inversely proportional to the absolute pressure. = Ammonia is absorbed with water ftom ammonia-air mixture using a column operating at 1 atm and 25°C. Resistance to mass transfer can be considered only through a thin film of 1 mm within the gas phase. Ata point in the column, the partial pressure of ammonia is ‘50 mmFig; the backpressure of ammonia at the interface is negligible, Jf the diffusivity of NH in air at these conditions is 0.236 em’/see, what is the transfer rate per unit area at that point in the colurnn? If the total pressure is 2 atm, how the transfer would be related? & A simple rectifying tower consists of a tube arranged vertically and supplied at the bottom with » vapour mixture of Benzene and Toluene. At the top of the column a condenser returns some of the product as a liquid reflux flowing in a thin film down the inner wall of the tube, At one point in thé column the Benzene concentration in the ‘vapour is 70 mol% and the adjacent liquid contains 60% by mol Benzene. ‘The temperature at this point is 365K. Assuming the diffusional resistance in the vapour phase is to be equivalent to a stagnant vapour layer of 0.2 min thick, Calculate the rate of exchange of Benzene between vapours and liquid if the diffusivity of the vapour is 0.081 em’/sec. Constants of Antoine equation for toluene are: A=16.0137, B=3096.52 & C=-53.67MASS TRANSFER Sheet 1 9- Hp gas at 2 atm and 25°C flows through a pipe of rubber of 25 mm ID and 50 mm OD. ‘The solubility of Hp is reported to be 0.053 (em? Hy at STP/cm? of rubber. atm), and the diffusivity of Hz through rubber is 1.8BE-6 om?/sec. Estimate the rate of loss by diffusion of Hz atthe outer surface = zero, per meter of pipe tength, knowing that the concentra 10-During a summer storm, a house owner forgot to close the windows. When the storm was over, a 1.235 m? water with uniform thickness of 0.3 om was spread over the floor. Water ‘evaporating from this slop does so as if it were diffusing across an air film, which is 0.1 cm thick. The diffusion coefficient of water in 30°C air is about 0.28 cm*/sec. If the air outside the film is 55% saturated, how long will it take until the floor is dry again’? 8.3036, BH3816.44 & C=-46.13 Constants of Antoine equation for water are: 1-An open cylindrical tank is filled with pure methanol within 2 ft from the top. The tank is plotted shown in the figure below. The air within the tank is stationary but circulation of air immediately above the tank is adequate to assume a negligible concentration of methanol at 77°F and 1 atm. Calculate the rate of loss of methanol from the tank at steady state, Diffusivity of methanol in air at 77°F and 1 atm is 0.62 £7 Constants of Antoine equation for methanol are: A=18,5875, B=3626.55 & C=-34.29 20 Methanol +6 « 12-A sintered solid of Sitica 4 mm thick is porous with # porosity of 0.4 and tortusity of 3. ‘The pores of the Silica are filled with water at 25°C, At one face of the solid Silica the concentration of KCI is held at 0.1 gmole/lit and pure water flows rapidly by the other face. Calculate the diffusion flux of KC! at steady state given that the diffusivity of KCI in water at 25°C is 1.87E-9 m* /sec.MASS TRANSFER, Sheet 1 Past 1+ Mid-Term exam {A laboratory beaker measures 10 em in diameter and 20 em in height is filled to 90% of its height with anitine. How long would it take to evaporate half of the amount of aniline ions Proble it the temperature in the laboratory is 35 °C and the thickness of the thin film is equal (0 0.2 m? (Sp. Gr. of aniline=1.022, Diffusivity of aniline at 26 °C is equal to 0.74E-05 is given by the following equation: 385752 T-T345 Where P, is the vapour pressure in mmHg, and T is the temperature in Kelvin. m’/sec). Vapour pressure of anilin In(P,) =1667~ 2+ Mid-Term Exam, November 2001 ‘A drop of liquid toluene is kept at « uniform temperature of 26 °C and is suspended by & fine wire in a Sarge room full of stagnant air. The drop can be considered as a sphere of diameter 4 mom, Calculate the time in seconds for complete evaporation of the drop. ‘The following data for toluene at 26 °C are available: 1 (viscosity) at 26 °C =0.5-0P = Liquid specific gravity at 26 °C =0.866 = Surface tension at 26 °C =13.4 dyne/em ~ Vapour pressure at 26 °C=29 mmHg - Diffusivity in air at 45 °C is 0.0943 om*/see 3- Mid-Term exam, November 2000 {A flag plug 30 mom thick having an area of 4 em? and made of valeanized rubber is used for closing an opening in a container, The gas CO2 at 25°C and 2 atm is inside the container. Calculate the total leakage of CO. to the outside at steady state, Assume the partial pressure of CO? outside is zero. The solubility of COp gas in vuleanized rubber is 0.9 m? gas (at STP) per m? rubber per atm pressure of CO2. The diffusivity is 0.11E-9 m/sec.‘CAIRO UNIVERSITY FOURTH YEAR FACULTY OF ENCINEERING 8 MASS TRANSFER ‘CHEMICAL ENGINEERING DEPARTMENT — SHEET? 1. Calculate the gas film coefficient Ke for the absorption of sulphur dioxide from a dilute mixture ‘with air in a wetted wall column using the experimental data below: Inside diameter= 25 mm Gas velocity = 2.2 m/sec Gas temperature = 293 °K Gas viscosity = 1, 788-5 Pas Diffusivity = 12.2*10B-6 m/sec Gas content ~ 8314 ki/kgmol. K ‘Total pressure = I atm. Using the relation: Sh=0.023 Re" Sch? 2. Sulphur dioxide is stripped from water using air in a wetted-wall column 2" ID. Gas flows at 3 flsec, At one point in the column SO» concentration in the air is 0.1 mole fraction. At the same point the concentration of SOs in the water at the interface is 0.00 mole fraction. The column is operating at 10 atm & 25 °C. Calculate the mass transfer coefficient and flux at that point of the column, Given that; H =1640 atm/mole fraction lig O°C is 0.16 em*isec, “The relation in the previous problem can be used as both systems are the same. | #=1,78E-5 Pa and Diffusivity of $O2 in air at 3, Inn experimental study of the absorption of NHy by water in a wetted-wall column, the value of K, was found to be 0.205 Tbmole NHyhr.f?.atm, At one point in the column the gas contained 8 mole%NHy and the liquid phase concentration was 0.004 Ibmole NH /A* solution, ‘The temperature was 68 °F, and the total pressure was 1 atim and 85% of the total resistance to the mass transfer was found to be in the gas phase. If Henry's constant at 1 atm is 0.15 atm/Ibmole NH per ft? of solution. Calculate the interfacial film coefficients and the interfacial compositions.MASS TRANSFER, Sheet 2 4. Vivian studied the absorption of SO; in water in a packed column with 1" ceramic rings. ‘The result shows that the mass transfer coefficients in liquid! and gas phase respectively follow the next relations: K,= 0.006 Go K,= 0.0004 G,"7 G9 Where G_= liquid rate, Toff? Gg= gas rate, Ib/ar.t? K,= liquid phase mass transfer coefficient, Tbmole/he.ft7. (Ibmole/ft") ‘Kg = gas phase mass transfer coefficient, Ibmole/h.f atm An air-SOz mixture is to be contacted counter currently in @ packed tower of 1 ft? area with water at 20 °C and 1 atm total pressure. Under these conditions Vivian relation are valid ‘The ges flow is to be 200 Ife and the liquid rate is to be 6000 Tb/hr. ‘At one point in the colunm the gas phase analysis is 0,1 mole fraction and the liquid phase is 0.022 mole fraction, Determine: a- The interfacial concentration b- The instantaneous rate of transfer. The percent of differential resistance in each phase. Equilibrium data: P.P SO; atm 0.121 0,078 0.051 0,034 0.018 | 0.004 SO; cone., Tbmole/ft? water 1.46 0.975 0.682 0.487 10.292 | 0.098 5. Weited wall column 5 cm diameter, 1 meter length used for humidification of air, operates at 25 °C and 1 atm, air velocity= 3 m/sec based on dry air. Inlet air humidity is 70% and outlet airis 98%, Calculate: 1- Rate of evaporation 2+ Mean mass transfer coefficient 3- Thickness of film using film theory 4- Mean time of contact using penetration theory Given that: 70% lnumidity=0,014 gm water/gm dry air 98% humidity=0.0195 gm water/em dry ait Paie=0.0012 gmvom® =0.185 cP Diffusivity of water in air at 0°C=0.256 cm’/sec‘MASS TRANSFER Sheet 2 Past Examinations Problems: November 2001 Ammonia is to be scrubbed from 5% ammonia-air mixture by counter current contact with large excess of pure water in a wetted wall column 5 cm in diameter and 2m high. In one ‘experiment, Temperature 20 €, air velocity 510 cm/sec and air leaving contains 4% NH3. Calculate: i+ Rate and flux of ammonia transferred from air to water. Thickness of liquid film coefficient. ~ Thickness of gas film coefficient, Given that: Dyyisi0.2 cm*/see, Dsrpaycie=2E-5 m/sec Consider the system is controlled by gas phase. November 2002 A Carbon disulphide-Nitrogen (CS2-N2) mixture is to be scrubbed with absorbent hydrocarbon oil in order to remove CS2. At some point in the mass transfer apparatus the partial pressure of the CS, in the CS;-N; mixture is equal to 152 mmElg. The concentration of CS2 in the hydrocarbon oil at this same location is equal to 15 mol % The individual mass transfer coefficients are given as ky-1.2E-3 Kgmoli(m?.sec) and k,=2.08-3 Kgmol(m?.sec) at this location. The total system pressure is 760 mmlg, Solutions of hydrocarbon oil and CS2 obey Raoults law. The vapour pressure of CS2 at the scrubber operating temperature is 346 mmHg, The scrubber operated at 24 °C and 1 atmosphere tatal pressure. ~ What ate the interfacial compositions (in mole fraction) of CS2? = What is the molar flux of CS? ~ What fraction of the resistance to mass transfer isin the gas phase? = Draw the concentration profile ofthe liquid and vapour phases. ‘November 2003, A tubular absorber composed of 100 vertical tubes (5 m long and 3 cm inside diameter) is used to absorb ammonia from its mixture with CO2 by pure water flowing countercurrent to the gas flow. Concentration of feed gas is 1.5% NH (by volume) and at outlet is 0.5%. Gas velocity in tubes is 1 m/sec, pressure is 1 atma, and temperature is 25 °C. Large excess of water is used, ‘The system is known to be gas phase controlled, CO> is insoluble in water. Diffusivity of NH in gas is 0.2 cm’/sec and in water is 2E-5 em”/see.MASS TRANSFER Sheet 2 Calculate: i- Rate and flux of NHs transferred from gas to liquid, ii- Mass transfer coefficient6s in the gas and liquid phases iii- Thickness of gas film and liquid film using film theory iv- Mean time of contact using penetration theory. Novem! 1004 Pur n-butyl alcohol flows at a rate of 600 grv/min as a film inside vertical tube with ID=2.5 cm and length 120 em, Air flows at a rate of 100 gavimin counter current to the liquid inside the tube, Mean temperature of the liquid and gas is 30 C and mean pressure= 1 atm. The vaporization rate of alcohol is observed to be | gnv/min, Air entering the tube is free of alechol. Calculate: i- Mass transfer coefficients (in gas, in liquid and overall) fie ‘Thickness of liquid and gas films iii Maximum possible concontrations of alcohol in air leaving the tube Given that n-butyl aleohol: Mol.wi=74, Liquid density=0.8 gm/em’, Diffusivity in air at 30°C=0.1 em*isec, Vapour pressure at 30°C=10 mmHg, November 2006 ‘A wetted wall column, D=3 cin, 2=70 cm is used to humidify air with pure water at 25°C and 1 atm, Velocity of dry air in tube-3 m/see. The inlet sir was 70% saturated and outlet 98% saturated. Calculate: i- Rate of water evaporation ii+ Mean overall mass transfer coefficient. iii- Mean mass transfer coefficient in the gas phase. Thickness of film using film theory. Given that: ‘Saturated air, % 70 OB 100 ‘am water/gm dry air o0l4a2 0.0196 0.02 ‘Air density=0,012 given’, Diflusivity of water in air=0.25 em/see Assume any missing dataMASS TRANSFER Sheet 2 November 2007 A tube 2m long and 3m intemal diameter is used to humidify air with pure water. Air enters at bottom at 1 nvsee (based on dry ges) with a concentration of water vepour-0.01 gm/gm dry air, and leaves at a concentration ~0.015 gim/gm dry air. The concentration of air saturated with ‘water vapour =0.02 gm water/gm dry air. This process occurs at temperature of 25°C and pressure of 1 aim Find Rate and flux of mass transfor, {i- Overall and individual mass transfer coefficients (mean value), iii- Maximum possible value of water vapour in air. Given that air density=0,0012 gree. Diffusivity of water vapour in air=0.25 em’, Assume any missing data215 | 475 163 | [Raster OOK ay get y 0 x [0 15 [20 [25 } 30 4] 1f1 kg of silica gel contains § w1% water is placed in ‘completely closed room 4:3°3 m containing air at 25 Cand 15 mmHg water and lef for long time. at will be the fal concentration of water in the gel and the ait? ‘When 1 kg of silica gel containing 5 w1% water is placed for long time in a Flowing ait stream containing 12 mmHg water. ‘What is the final concentration of water inthe silica gel? 2 Pure water is used to ebsorb ammonia from air-ammonia stream at 20 °C and T Sim using co-current spray column. IC 10 Kgmoviin of gas camaining 03 Kgmot 77 ammonis/Kgmol of pure air is contacted with 10 Kgmol/min of pure water A. i+ Calculate the percent ammonia absorbed considering the two phases leaving . the column are at equilibrium. i Can we obtain 9% removal of ammonia from ai? How? eu ‘The equilibrium relation: X% YD R[F reamonia BP (kay 423 | 328 [152 | mi « ») , L gm ammonia/gm water 0.05 [or 0.15 0.2 025 |cae we » fate nti seat A tte ena 68 °F and lam “oo Wilh pute water in ulti stage tower. The water rate will be'24) Ibfar and the 84s rate will be 248 fod tthe gas inlet. . Assume that the tower temperature remains constant, at this temperature the Patil pressure of NH over aqueous ammonia solution areas following: PP. commit B 18z 31. 50. 6 166 Conc Ta 100 Ib HO 2 3 3 75 10 20 For 98%, NHy; recovery finds: a How many theoretical plates are required? & Ifthe overall efficiency is 75%, how ‘Many actuat plates are required? ca a packed column is used, find the totat height of the packing ‘Hint: Tower diameter is 1 m, Ky.a= 28 To/hr.f??) ‘+ Tis desired to absorb 80% of ammonia in a2 mol¥ amnonia-ir mixture. Pure C__-—wateris used asa solvent. The gas rate is 1000 fovhr, Find the necessary amount (Ate prs the mt eee Lo ‘avilorium relation is (y =2.83 x) where y & x ar the mols faction of sxamonia v inthe gas and the liquid phase respectively: a Single stage is used with estimated 90% stage efficieney. _, bs Three stages with 90% stage. efficiency using equal amount of water it excl stage. . © Counter current multi-stage tower containing 9 plates with overall efficiency 0f 30%, Xe,\Soneer 1 - a ee ee Phe las Loos, 25°C . 2qR ~ Ate 2 NONpa Sol * 4 atm NOG ye Vas as.6 © pot Nae de Coegral Ma = 3a > Ay: 98 “TD . _9:00435 a1"5 eL = 200485 eT Pus vat) Ho Me TED = 0.16189 ontyec 2-Th30c - BOB’ \y A ed oP © 10” poise «14.4 co gr > WeR oF Haat Dp. to! + 5-664 10 ay CUP WV) “s +a 5 CO CD — 28.5 % Dye Ore wwe QO, (2) —» 15.0% “Dy: 0114S m/sec 9,0) —2 56.5% “Dy, =0:1834 m/sec ot) 1-o-aRS x : “Dania? Se, Ss “Tens ewes” = ORIG Vee D> De ORF 6.1945 . “DD .z te : bros = ONT M/se0 min ‘Be +33 O.2gS 4 OSS Wy Dy O1gsy O13 lM \-9.565 : : 0.1905 nt/e, Bomik yy Ma O.28S OAS 4 ee +S Bs. Da ONS —OIBBGeo TP RSC 2 age P21 gtm OK B.05 m De txt? wife 2 10" entisec. $2 08 » Sy eo0t ve? Set = F. 7 (2% Rr 7 oe) bx Ro Ba Sab atm Fad RAP 2 OR Ls 0-2 ofm- ‘Ra 4,Pp 2 0.0014420.001 atm 1-0-0! | ‘Rost 04, wl Re 82» aad 0.05 Fe B18 416" ae em* Sec *B- ds a6 Ft ” Te aac = atnl84392 FLCOF T= Hés+n60: S31.6°R T° L atm: et Psi bts Smm 2 0.Sem er BeBe an’ OOFCAR = OS oma A—— 20 ft —r P* . 400 mn Hg R20 @st 2 30 Gant / gpllon > 4. 24g _e <4 oy “D . 10132410 Pte. > Segre 0-88 3 i grlea = 0-£33% Pt > Soe +6262 54.019 th soda ~~ eR. xe -8 FD in = 5* = = Ra 2 %) 2 volsaxte" a, Into -T60, 10.42 459.6 o-ol64 -6 = 2.3, \ Ml s\ 48 #18 Sele Re FAs @.248415%s Ia a0", Zoesanio” el a Sec <4 R. A.06aa x10 “pmol 38 we 1 FRY 2d Gallen Yers! " Ba qa We Gasset pas xe 3600 * RY dag sec 4 ey Re 6ug.3s _Bpllon (o 6aB35 ae 7 - ¥§ 5 Z| ae1 Bee Pleatiog rook 4 lop = C98 Arene ze doy 2 006% IEx a0” O.np 2 194g BY x*- 2 2 400 K hr ?. D0 mnt @® yo oa | ee Rue | areknra 20-4 D athtoo «Rm “oma? © a ° P2048 400 = IO “Rao D.D, Fr. D 9. Ge ; a 100 +107, ioCesss-) 2 10,6364 21_ RT Dd Riso Ke Re 0.4 200 = a ER - Reo ‘D:2D, OSD, Bee Fie Be 0018, HGS Be, Ae increase in abs, a6 ton iTS coeSD Yeed De SER fmt wotey aie ammonia i) a Prtoo KR Jot x Ss . PR: O-441002 10 EN/m® ne eS knot “DD, 1 Fe > * 400 «10° ‘ In (R= te RT Fre SyeS.qg_ DO RT ox dvIP. s00 RR “RP 1 04 ¥WO 220 KR ‘Ris OE RS “DAD, osD 200-5 i * ¥ 200 41075 fn 280 -20 ) RT oo Fe 800-24 DoD, RT 2x = % increase . _ 80%: 2F- 546. 6g SOO Ts F406. 2 = 48.05 % F486. 634 . +- P. . a atm soster |! ek Tr ASC 2 ac | onmenia OX = 4 mm = Od cm \ 2 1 1 sy > SO momllg P \ 5 P. ° baa D= oascat pen. R-R EDP, nes) RT r ox F600 . iN Seo et = S86 as io Ge 6543 nig opel BQ 4208 ot Sent Gee. ci) Pea aden P. too am ty © Be Bn. Gem Gillon Garellation D Db: S23. ONS Cmigeo. ute 0 a F, 28 In Gea + BA aRIs ot = 6.593 x 19% Amel Cm. seooe a TH 865° \ sl OX = OR mm = 0.0m ow wate “D 2 0.05) cw Ke, R= 4 atm In e. 16.0134. 39652 _ B dye0 [aque sere T 820.8 |xprenT \ Sel gq nan e- F.-B RAR, T RT eX Teaser, odd * . . Ree O4eP Ne Roe 6.6686 Wo PRRs Hal. Ge me = 0.568 ok 2 0.4% %0- SER = O2Q2F atm “ FL 9081 T Bans6s @ os ®.8- 0.994 1 "Sag > = Gaiqsan™® See com* Sec @> OFs1L 20.4 atm Qe ie 2.051 yea? 824365 = Lo.22te 0443 atm OFF3_ 0.4 . * ——— - 6 gias si Ave! 9-0g Secw 9q- PRP aadn . \ {_ TH 28% ROB * . 1 . 1 \ \ as a C, me Wel 20.058 OP teed s| Cm rubber etn _ BE rm De 1.88 10S cert sec. he tm: tooo sek Sar aPPasion in solids AC, F.2D + SB area Gustont < . Rte. _D SE waned = - Daan wg & Cc. Rate » for = -Orant fae é & Rete 2 2011 D + C,-G) & 4) ~s 250mm ,. = 85cm + gso * Sslbilihy = a.o53 Cutts ot BrP Se Loon to get Ca? rubber .otim LC gmst fone y oF STP ned ——e Vs 88.6 Nits anasto? on? Ne? ———» Ve 0.053 Gm+ oe 0.053 41 oeawar 7 2366s 15% grt + Selubilty s 2accaic® ye te CrP rubles ten -& C= 2386410 *2 eg netaa sid art He TTetol Ressure + caf raoloor Rate, AT #100 188 HOS, (4-439 x10) as hh (gz Rates Be6h yg? Pee +>10- OX so.d em = © V2 4.935 m? . heo. po 3 cm at “Tz 36°C = 308° “D2 028 emygec. #@ 55% soturcled ar ‘hn Peg BSG 1 * 8.3036 Fae t-? Sol Ae Ve 1885 4 A AWE mie BULGE YI’ cw 0.3 x16* h P. (83036 - SB! sg une ° BOB - 46-13, eR: 31.38 pen Hy = Bohs atm : BX FDR. Ce) “ ° 3 é = #26 rain ig Feo- 173 Fr 928 4, la Cee -& ot = 2163 10% gre em Fe Re Fe 022.16306%e ance alot: 8.905 ee 8 for ne s 7a. Hasse = 6861s yr. 68-61 410° 8.905 = F405 secue —— 492, Te FFF. 344260 = 534°R Fo ahoe 14-4 Pst hP rig. _ 3626.55 18 9845 Fz 84.99 De 0.62 RYhr 2? Se r..D # Rr Pi RD, RT CR we need to get re PCx) ai ta Pe aq iM & tong: 1 i tay ee BL aR Ae Bei 99x me [FSOay) RD? ve) aT BR oer (3-06x)* * weer BRISRs Aes | a y-—2 ° tn & + 8.s8%5- 2 = 125.843 milly Taro 28.34.24 Rane [-4--+-]- 6-62 * s WFQ 4334 Re Y¥g Béas 55 =9ald” Ee) aw Romo 24-835 THe 32 + TE ease = 208% + ttn dh (Besa 185-894, * O%ce) l2- E204 Te 3° DK=> Gene = Od Om Te as’ eagsk Cys Od gmel /t# = ots? grolfon? Geo De B00 mise. REI Fem /see Fe? Sel fa porous Solid De 4S 14 mal Xe -Xy <3 3 Fe 16 eOg | GLY -o a 3 de 6.283 916" WV, ooNiOyemver gD04 Oe My,+ 600 g/min Avtodty! abeohs! Jd +35 em QAy- Ay. CO, -CH,- OW Mote L . Ro em . . 40. ; . PB BTC . 40 mmnblg me * ° Blin 7 ower D awe. ot Gut see, —T-30°C “P. 4 atm Rate - 2 9 Jenin abe in —» 0% alcohal + Liquid is pure abchol —v]s A. o Aw WDE ws 2.54 120 2 42-48 om Red grimin= FE gVmin # 2.0186 Qr~Vnin Fa Bg 2 1k 8h aI” oS F. &CR-R) RAT to mm tg = 12 atm fa sr od Ramat PG. Eps semis os EP, 70 * £0 ” paged’. 4 (<2 -S ) <3 gre) * Bo ate Einoy +e a. 2 %. 4: % RT = 2.1994 WIG BAY RAR: 53-256 Kec. ie 0, =: +898 T= Mowimum @oseible Pactial Pagure af alloted in cir is Hs veQour Peeteue = 16 mn tig.Nev 200 F Liam . de Bem Pare wsater Ve A misee Ceased on tey aie) ar in = oot Weer as shy aie . wooder ar ot => 0-015 weg Saturoled air a7 0-08 wees a gt LT es BSS 2298 Pe dt adm Saez e001 Blom Ds aas eH /ec SoBbion .. papain ie Rate «ae (0.016-ool) Tig a= Bat Dade O = goots Lv Be too = 0-848 We bk Robe = oBURACOOIS- OL) 2 Ka HIS) YM fe = 2.356 410" Bre! /sec, . -* : oO t R 2 BSExl = VAS HIS amo! ast TAS *200, Gm? see F:a. Fe 4 CR -T) PeR oon gr we 2 ae oy tr 24.7% FS ye aa a Pr = Bo8Latm oo ©0878 a 9o* saa 0? 202 1B 4 eg 2. PRs $ a SSIFOSNS On deram dain 2 coins BT Ste a g an aye ar dy sie 2.0125 gm water oe Van dra cir Boas ah ot —z 8 et 24 g SOS yy See = @otF Sag «Mpa CR. WR = o.0nt alm 4 25 #19 55__ gal a A. BSNS ee Lageqa we a, 9-0818-O.019F ont and Since Pure vscter isused —» Pico %- > L086 HS ore aoe Grn Bee, ato, We Hox. Pessilele yQue af woter vapte ake ig its Vop Pressure = BOR admSheek 2 uy Dis 8Gmm 2 ooagm Viz 2Q m/sec TE a3" kk A148 a0 fas. D = avis wee. Ps 4 atm Sh. 0.083 Ro sg Se! => + PL PM teas RT eeBRa29s = 1807 YViit 21903 Kam? + Ree 30d ~ S207 429 yo.cgs a EE = BAGS V4 Bvlos -5 Sch Le FL = 8c FD is0F es agets® Bs ee : ° * Sh= o.09ae saq.g s 1A Se 23.0% 6 Jad, RBH Ry KL QB. e M2210 © o.6 “hee D 0-085 Ke VI ope,I Aig 2 242.54 eme SOB om w Vas BVeec © FUG emisec. geod : Xz 0005 Pe 1 ate TF ass 1aRlk Hs Gre adm/mal-Qackion Wiquid Pe BS? BS eeFRe15" FA VFB + “D @ we © 06 cxt/sec. Ry Re? Fe LD 2 tate | RE Bale ETE same system an problem t : . 2 theoces REY sar = 016+ Gi) fF. BY. Qe 2.08 BM/Er 3 O18RS OMfec, RAT 82 +2 a Rex SBA, CMB WHE 508% | 0 16.4 - Vea 148110" _ 9 9822 2 sen. 2 —_ 80 so OOH EF & oss oe Sh = 6.023 ¥( 3096. 4) St @08t2) = 40.4! = Be . kOe wae = mF Sm sy 4 «Ae 2 LHe _ + Gotten 3 * en e RT Be Kae » Fe ARP) & Te Hak = 1640 v0.08 = 8.2ahm RABP ea HO ob atm sec eee5 5 6-805 bmi Ne he: PEP ator Jd 2 0.08 C2 0.00% Menol sos PF sole 7. CBF. S28"e Pet alms Wet Bi 8S x J HT Rs inguphoie ~~ 4g 8, me ots ___ofm Tomat bHa/PH Selq, Yemel 1 tee, OH Sely ~~ Ae ogse lt ee = OATKAS and LL... t., —% ey Ke ™. oe6oR ——> K+ o.tors BL = “Re dR +008 aten Fe BP) KCB) nk 7G G 6 oo8=P ot H8S 0.85 @.205 o.00% - Cy z Rem . “p86 1Cooat- CO) o-0g- HSC; = a.olast okm Rama:Shwdd dag mh kay >Re wt Ag a pou. 2s Andi ff _ bey? cies (oot o-coe 6) ac a0 38 3S bey. o2 (38352 0. WS (e04- fH) feet bl] 4,K, 20.006 6% k& = O.000¢ a” 6°?" A.it Pr BT 20 = 293° P «tabs G, = 30 AOE, G, = Goon oe deot X= @or Soto eS a &- ‘ KG 2 e000 %* (a0) Cécooy ** a FL ECG) 2 1g CR -%) R BW ke a-G RP. Ody ds od afm -d tbmel S—, *G — Ke002 ———— tbe £0, Tone! Selp FH sole wee * ” 3 ne. Suet é Aaa =) Pie cosa 64 40.998418 > Ole 3 vee -osous Pr = 928. O.c064 (6000) 2 006855 Mie tome = 0865 Eran Mo 64 Hye 218 ‘ue need te Comert "Vometsol, Yate "BAP solo” to conve tt Inte cone. (9.012