Scribd Logo
Upload

Welcome to Scribd!

  • General Chapter 561 USP 41 Articles of Botanical Origin

    Uploaded by

    Social Service (V)
    187 views14 pages
    Articles of Botanical Origin USP 41

    Original Title

    General Chapter 561 USP 41 Articles of Botanical Origin

    Copyright

    © © All Rights Reserved

    Available Formats

    PDF or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    Articles of Botanical Origin USP 41

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    187 views14 pages

    General Chapter 561 USP 41 Articles of Botanical Origin

    Uploaded by

    Social Service (V)
    Articles of Botanical Origin USP 41

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    of 14
    wean ‘Chemical Tests 561) 6279 Mo =wight of vamin€Plretyene Gc! Succinate alent prepare th Sample sting) ‘ADOTMONAL REQUIREMENTS ‘Osean Tcophercl ts Use Ape Tecophen Acetate RS Usp pa Tecophe A cnt RS Usp resco (561) ARTICLES OF BOTANICAL ORIGIN SAMPLING Fo ede the tet of sampling bis in quate ad quintalive eu it neces oer tte composition of ‘ie samp used be representative othe bleh dug en exaned Malo apg proces se We es consid apa t ngetabledagy Some aces ot sae te ay eq ate ore pace meng ore cntanes beng sated or mate snes po cota Gross Sample Wher ese eainaion of conkers, makings, and abs inate that the Bh can be considered to be omooe wou, tak inva herb of anon Scced containers hae ows, Whee te bate caer be ‘uridred ote hameeneus, de tino sub batches tha aes somegerees ws pose het Sane sees oes tnmageneos bach recommended io ese samples om the fin leat roa oe ie Nao lumen tH) 11 or more, and each conta ne bch urate tied er Ne oan to BeSompied +) —{__ngienienet (Pounding ws alee 87 ent highest whole manber) Samples ate on ro the upper, me and ewer secon sch cote. the cde mateo of compo ‘et pas tat ae cm ress ay emerson, andi he eae of 3 powdeed or gon mala rant le Liman aang cei tat moves coe om the tpt he ton lhe cotanes, NUT cares ban hen ‘rom feet sgl For mately compere pats > em in ay ies, ws y an. large bles pas. ample shold be ae om a depth Tem, ecdue te rare conte he setae ge ay Ieee tom that of tenner yes Prepare the os sample by coming an ising the ni! sampe tke Hon each opened Conta, aking eae ot increase the degre of tragentaon a gaa af the ote one For asin cntaes lng «1 ho, ms the canter av wow gays for he es, Fr ates incon. Lins holding betwee Tan Sig, thro ual potns rom the apps mee, ter prs econ, ea «the samp bing sient ery ou the tess. Throughy mix the sap, and woo amount inet ay ‘au the es. For conairersnlding mae tan witha hee spc ach ging NET 2303 rom he spre ‘te and ower pars ofthe conse, Thorough mi the samples, sod wan «poo lee sear ut et Laboratory Sample Prepare the Labratry Samp by vepeted cueing of the oss amp [Nert—Quartering canst of placing the saps ne sieve ane quae shaped ep and ng Sager et for equal pars He two oppeste pan tthe ae an cacy Med. The ce epee ees Sp uni he equred quote obained “ne Labret Sag shuld be of Se sticen for peroming all te neces t- 5 Test Sample ssa ‘Unless othe ected in he nil manera a tet procedure ow, peae the Tet ae a ols 6280 (S61) / Chemie Tess usr al Decrease the sie fe Labratny Samp by aren, aking cet eas witha parton ress eprsanae, In theeaeof ground ar anpowdered das ind te withdrawn samples tt wilpas hugh a No 20 andar ‘Siang ne renting poder trail cannot be grand ede to sr fne a tates possible by ‘ot ton paper a sampling cat spend aun sth ye, aed witha tbe porto srl. METHODS OF ANALYSIS. Foreign Organic Matter Unies others spec n the nil many sph igh the folowing quanti fhe Lobster Samp ting care thatthe thse potion representa (quoi neces). Toss Ror a - a lane one iba Spread the smple out in in et, ad separate the foreign ganic ate by hard as complete as pose Wight and etre the pera of fag opie matin te weg ug kes, Total Ash Accurately weigh aunty of the Tex Sample, presenting 244g of the rie mate na aed cle an noe ie gory st Spd ad Inerene te trperatire to 75225" unl ee om carbo, an deere he west then caine con be blind sw, xtc the hare ssw hu wat cea te sil ‘hls on nase paper, nemerate the ede ater paper al hah wea ea 0, the a he se, ‘Sorat tyes ane te le os temperature 1698125" arb ee sh canna beatae in) ‘Seis 13 mf oho best up the ash wah gas od tart hel and aor eat he whole to ‘emporio 67325" cool ma deceatar, weigh he aah, an skate he peceniage al ah fom the weap ‘Aci Insoluble Ash Bo she ash obtain Tt Ath th 25 mn 3 Wyant he inoluble mater 1 eating cr ai er mh hot gon we Ot een of ai Water-Soluble Ash the ah bain 5 ect Tot ah wth 25 ml of wate fr Sin Calet he sabe mater in ast nae oo anes iter oper Wash eth hat water, dig for 15min at terpertre net exceng 150 Sh tract he wea tthe eae mg, stained Totty abate he pacetage of water soba th leh {oie weit of pe termine Toa Ah Alcohol-Soluble Extractives MeTWOD 1 (HOT EXTRACTION METHOD) Traner shout 4g lithe, corey powered mates acetate igh oa topped Con ask Al rival cto snd eight is Stake, a low to sander tach ax condense t the fa ol gent ‘land igh Rast ote erga weght ith leah Stake, an Wer py ecugh 3 yer. 25 ‘hetite os tredttbestomed dy and evaporate ona water bath ores: By a 183 fr 6, colin 3 does 1dr ar nigh thot dey, Clete econo, ng lesol-eaactae mater nthe est specimen Meron 2 (COLD EXTRACTION METHOD) Taner abou 4 of iced, comes powered mate cca weighs oa ls topped coil ase Ad 1 ino aesolsetstpper state fits and mace for 24h,sokng equa ng te rsh and hen ale {Gstaad Ftd nrg precautions gant es of kona Eaporate 25 ma teat to yes ed 7 uspar Chemie Tess ($61) 6281 boomed, salon dy and oy at 15" costant weight. Clete the conten, bmg, of akchotxtacabe mater i Water-Soluble Extractives ‘MeHoD 7 (HoT DetRACTION METHOD) Proceed a rected n Method 3 (et xacton Mead) a Ach Sle Ett, excep se wae in place flo METHOD 2 (COLD EXTRACTION METHOD) Proceed as ced n Method 2 (Cal Carton Met) in Ako xt, xcept we water in peo eo ‘Crude Fiber [oust wid quantity the Tes Some representing aout 29 othe dr. wth ete Al 200m fb te sul (978) he ether esas more SOD ft sd canret fight fehun condenser Ree ‘mature fo 30 nin acute ne than ass ough» her ot Raden pape rad wash he reo te ie sth boiling wae nt the vert washing na ong ac. awe he ete knoe sk wth 200 me oan Sedum hykosde esto, add to 1.23% bytitton ane om sour caters Again elu ems Fr 30 min accurtly tne then pips sro red iter wash he reac wth song ate ane Lat washing ‘evil and dy a 110 to constant weigher the diel edu, eto tans weg cutie ea and righ he sh he diene tee the wight oan by yng a 110 anh te sees he eg the Nore The bong with acid an alta should cane or 30 accurate tn, om the time Ha the gud ahh ‘eoied blow the bling pot by beng aed to tel sh) san Ae the olston he bon rouse bang Uhehea shuld red ow enough hist o mata bling the bing, teh Ss be ey tte ene ‘me to tine owas down any pares at may aero the wal othe hes Asoc la voce tee “lau ring the bling operation ain preventing ences thing | Starch Content The folowing general procedure fra educing sugar an yb uo desi the rch content in botanic otc ‘Malt extract Ue conn barley mat of inn elec, and gin jt bfoe we, Prepare mal ete ja eto For evry BO mt fm extact neded cigs 9 feud ma wth 100. owner at room emperor 2h oe Man elec mine ue the mate or 20 rin | Tarte ava 9 erecta sg ocean an mth ‘Test alton: tre about $9 ol he fey fund et specimen wh fhe YO potions ote, sing fe tat ‘il completly retain the salt arch gral low the eer to evaporate om Wefan ash 250 P| oye Carey wan tex pet 3h ht 00M ‘interest to abov owen posse gelatinsng sar, and ala t sande abot Tm sting heey ste complete sno ugar Trans to widen bite, mse te bese hale wars ae ano Adan ‘ual volute of acco mon alto andor NLT ‘Centre ante precpate cosy pach on the bate of te bt, and cant the apematan. Wash the prc: tate wth ces Sem potion aot soon (50 100) by cnting ae decane s ata fe os ey ae Te re rene ra eo soa ted sd 074 drops 20% saluton a naphtha lah prepared by dching 20g of Vrain | ok et and 2m of wale. Shae the ts tbe wel oll wifes ring alls 2-4 Ml safe ad eo sown hs sibs 1 est ube andthe fest tube upright. sas presen tbe inttace othe sh cle ae te se et nd on tain, the whale ston bores lo kt) “Trae the reste om he ble se arene ite beaker wth about 30 of wate. mete te braer in bo ing wate an constant for 5 min rua of re sachs gee. Col th bea to 38 ad 20 ot Hak ‘xx ad at ths temperature for Th eat aan to baling tra fow min coo So ad 20 fl of Ma exe sd Fold ths temperate fr run the reas when ested wh dine TS shows be tinge un mls ca tion. Col dt ith ater 0 250m ie [General procedure: Tae 200 Mo! he Tex sno 3 ak ited th 9 fu cones, 420m ye «aaa eat bang waterbath lor 25% Col ety estas th sam house TS compe neces {6282 (361) | Chemie! Tests useat ‘on th ad cabonate Sate wih yater wo SOD rn a ite. Tevolame of squot akan depend on the ‘arch content he specimen under et Ge Tae The ages conta between 100 and 200mg a eos. Taner 0 ml ofthe ate to 400i salvesstanc ss bake, SO mo hai cuprates, cover the Dak “ruth Bate and het Ajit he aren he Bue so tha te cone of th as bg tol inh and ‘omine botng or eacy 2m, Fr he No slg a once though stad ie Was he pcp of ip ‘Snide horougiy with water about 0 ten with TO Mot akahol, and nay wi 10 mL of er pagent get For ston of educng sas of compara high puriy, proced as drecedin Metiod 14 to determine te aroun of reduced copper obtained by weighing the ded caprou xe Fer soon mung sugars contaning Large mous ‘nga mpurties, ing soe, proesed ms droted in Mad 1Bto deere the aoa af feed copper eained Upton ty ode toate etd 4b the propia btainedin Gee pedi fo 30min at on at 11022, coo to oom temperate ln adescesto and wig Retro Table? to fn he quant fetes, ne caresperng tthe weg of upreus ‘ute ound etemine the pecarage dents an hn he content of Stab the talon aul Percentage of dextos = (otf deatrosin mg «0.1» SOO. ample ig abgut ml) Cte of sch = deste «08 opel hen Gu waged rei S poe feat eee Pees alr fe ‘mis’ | cee. | “Seas | eat = |S eh as So | Sy | fae [oe [ae | ave {60[ tor] nis[ ae es a [oes [ies eae a use Chomicl Tests (S61) 6283 care] SEs [erg | ewe | Be lemme | S| SS ome = sor | de [sar] dee oe | S| | oer mote toe arte atta ff asf itd 8 St oss sono: Trane 399 of sou tint, acutely bed to 210ml ask ‘een ands th ete to volume, rid Toran ones san Ossove 429 ot potssien iodide 100 mt of wate, Sunt ct sumone Oss 5 29 fad aette 10m of Water {onmsoumore Tranter abet 03.9 pure elroy toppey seat weighed, to a 280. fk 39 Smo rica ode the cops, ai abet 25m of mae, rt expel ares A outs of ome TS 88d ‘sun the bromine cmp removed. Ceo a 10 rl oS ee an ey 0 mo aan ‘ide luton, ad rate wth Sx toate seo to «bgt yelow coun Ad enough sch 5 to rode a raked te cola contin the tation As he endpoint eats, ad29 ofptatiam theyre se sua copltcy os ‘oie Comte van ont the prepa hemp we, Gre mot aaa oars een souk {mg of copper. (Nort s ese hatte concentation of ats ae soon be sey eed th on ona es than 320 9 of coppe a he campo rato sd 42996 pomsa lode tomas tea len Wo greater amounts of copper ate presen a tno le stat sey, wah constant agian, her he tel ‘namin proportionately grater "octoue: Wah the pected cupous oie obtained in Gna prodre wth ater, cover is et witha watch ss, and dole he crow onde wth 8 mL ie acl eect under te wth dss wi pte, Cec the te inva 35cm fs, wath he watch sad thee with water, Colet al he wah te fe oe cote te Maso expel ed fumes. A tout Sm of bre 1, ad ta ute brome completly ese CO ad proceed | drected in Copper Sion begining wth “ad 10 mit Sas tat sara” Fete Sos tens ‘olan cosine cane west ope, mg, ad lily he weight of cpr ty 11239 fo obtain the wes tng, ot aprons anide om Tobie? the quant of Sexo mg: conepansn toe weigh ol eereun on The net of tachi quoter toe weight, mg arne tne tenes 09, Cast tank Stermaton, in SD ‘no ate cupric arate Ts and SD mt Mal exo? the eg ol he cps oie so ean eee 0 ‘exc the sl ve determination according. (Nhe aie cup: aate Ts dette’ on star. an he ‘gant of cpus once ebtaned i the Bn eer tenses] suaidey, he foloming methods specie or deste lcs, ap because os exten may account fr erences ote betwee ales eine om te same specimen ups determinations dnt ary more a 2 65284 (361) | Chemica Tests use ‘lucoomylase solution: reparation of gucourasein wale contain 30 ternational Unis (U/mL Ue gi

    You might also like