Heater Metanol

HEATER
Fungsi : Memanaskan ACH masuk reaktor hidrolisis dari suhu 30°C menjadi 130°C
T1 = 30 °C
t2 = 155 °C
Umpan
Komponen BM (kg/kmol) kmol/jam
CH3OH 32 0
H2O 18 8.6082935242
C5H8O2 100 0
C4H7NO 85 89.3237045688
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 97.9319980931
massa umpan = 7747.4641717875

= 17080.2144624062
T1 = 30
T2 = 130
Ta = 80
Panas masuk
T = 30
Tref = 25
Cp= A+B.T+C.T2+D.T3 (Cp=Joule/mol.K)
CH3OH 32 0
H2O 18 8.6082935242
C5H8O2 100 0
C4H7NO 85 89.3237045688
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 97.9319980931
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 8.6082935242
C5H8O2 100 0
C4H7NO 85 89.3237045688
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 97.9319980931
Beban steam (Qs) =

=
=
Neraca Panas
Komponen Masuk (kJ/jam) Keluar (kJ/jam)
CH3OH - -
H2 O 3249.6549 68215.3753
C5 H 8 O 2 0.0000 0.0000
C4H7NO 109710.9964 2425519.7332
C4H7NOH2SO4 0.0000 0.0000
H2SO4 0.0000 0.0000
NH4HSO4 0.0000 0.0000
Beban steam (Qs) 2380774.4571 -
Total 2493735.1085 2493735.1085
Media Pemanas
Medium pemanas yang digunakan adalah steam jenuh (saturated steam) pada suhu
P = 80
λs = 901.1
= 2095.9586
massa steam = Qs / λs
= 1135.888112077
t1 = 155.5722222222
t2 = 155.5722222222
ta = 155.5722222222
∆T LMTD
Hot fluid
°C F
155.5722 312.0300 Higher Temp.
155.5722 312.0300 Lower Temp.
0 Difference
(Thin Tcout)  (Thout  Tcin)

TLMTD 
Thin Tcout
ln
Thout  Tcin
∆T LMTD = 113.109776502
Menentukan Koefisien Perpindahan Panas

Hot fluid = steam
Cold fluid = heavy liquid
Menentukan viskositas umpan log vis =A+B/T+CT+DT2

T = 353
Komponen kmol/jam xi
CH3OH 0 0
H2O 8.6082935242 0.0879007239
C5H8O2 0 0
C4H7NO 89.3237045688 0.9120992761
C4H7NOH2SO4 0 0
H2SO4 0 0
NH4HSO4 0 0
Total 97.9319980931 1
Heavy organic
UD = 6 sampai 60
Dipilih UD =
luas transfer massa dan jumlah pipa :

Dari persamaan 5.15 (Kern, p-86) :
Q
UDasumsi .T
Q
A= = 398.9997
UDasumsi .T
ukuran pipa
Panjang tabung standart, 6 ft, 8 ft,10 ft, 12 ft, 16 ft, 24 ft
Dipilih
Panjang (L) = 16
Kern D.Q, „‟Process Heat Transfer‟‟ table 10, hal : 843

Dipilih :
L = 16
OD = 1
BWG = 16
Wall thickness = 0.065
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 95.2539457908
Kern D.Q, „‟Process Heat Transfer‟‟, table 9, halaman 841

Tipe pitch = triangular pitch
SHELL
ID shell = 17 1/4
Baffle space = 13
Pass = 1
Shell Side = hot fluid (steam)

Tube Side = cold fluid (produk reaktor hidrolisis)
Koreksi luas tranfer panas (A)

A = L.a".Nt
= 435.6352
Koefisien Perpindahan Panas Ud terkoreksi :
Ud = Q/(A.∆T LMTD)
= 45.7951662456
Menghitung koefisien hi, hio, ho dan Uc
SHELL (Steam)
Baffle space (B) = 13
Pitch = 1 1/4
Clearence (C') = Pitch - OD
= 0.25
ID S  C ' B
aS 
144  PT
Flow area (as) = 0.31
Mass velocity (Gs) = Ws/as

= 8079.0878677969
De  G S
Re S 

Pada, ta = 312.03
μ = 0.0348484049
De = 0.99
= 0.0825
Re shell (Res) = Gs.De/μ
= 19126.4062299911
Menghitung koefisien perpindahan konveksi (ho)
Dari fig. 28 Kern
jH = 65
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho = 1500
Clean Overall coefficient (Uc)
hio.ho
Uc 
hio  ho
Uc = 58.4698395385
Dirt Factor (Rd)

𝑅𝑑=(𝑈𝑐 −𝑈𝑑)/(𝑈𝑐
∗𝑈𝑑)
Rd = 0.0047335311
Required surface
Q
A
UD  ΔTLMTD
A= 435.6352
Dari tabel 11, Kern, untuk IPS inner pipe = 1.00
Required length = �/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒 =

𝑜𝑢𝑡𝑠𝑖𝑑𝑒)
Menentukan Pressure Drop

SHELL (Steam)
Re shell (Res) = 19126.4062299911
f = 0.002
ρ = 55.9960718946
s = 0.8959371503
N+1 = 12 L/B
= 14.84
2
f  G S  D S  (N  1)
ΔP S 
10
5,2  10  De  s
∆Ps = 0.00054
lisis dari suhu 30°C menjadi 130°C
HEATER
kg/jam
0
154.9492834358
0
7592.5148883518
0
0
0
7747.4641717875
kg/jam
lb/jam
°C = 86 °F
°C = 266 °F
°C = 176 °F
°C = 86 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qkeluar - Qmasuk
2380774.45714557 kJ/jam
2256538.50364834 Btu/jam
m) pada suhu 281.01

psi
Btu/lb
kJ/kg
kg/jam = 2504.2016496472 lb/jam

°C = 312.03 °F
°C = 312.03 °F
°C = 312.03 °F
Cold fluid
Difference
°C F
130.00 266.00 46.03
30.00 86.00 226.03
180.00 180.00
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
Btu/jam.ft2.ºF (Kern, tabel 8, p.840)
50 Btu/jam.ft2.ºF
ft2 < 200 ft2 double pipe
> 200 ft2 shell and tube
(Towler dan Sinnott, Chemical Engineering Design Principles, Mc Graw Hill New York, 2008, halaman 805)
ft
ft
in
in
in
in2 luas penampang
ft /ft
2
luas permukaan per linear pipa
≈ 104 buah
SHELL
in 1.08 ft
in (0.2-1 )ID
k reaktor hidrolisis)
ft2
Btu/jam.ft2.ºF
L (Steam)
in Flow area
in a't
in Nt at'
at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
in (Kern, Fig.28) L/D
ft
jH
((𝑐 .
𝜇)/𝑘)^(1/3
)
Btu/jam ft2 F (Kern, p.164)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
hio = hi x 𝐼𝐷/𝑂𝐷
hio
Btu/jam ft2 F
> Rdmin = 0.003 (Tabel 8, Kern hal 840)
ft2
in maka surface outside = 0.34 ft2/lin ft (eksternal surface per foot length)
1266.3813953488 lin ft
L (Steam) TUBE (Produk

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5,22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
ΔP T  ΔP t  ΔP R
∆PT
T2 = 130 °C
t1 = 155 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒

𝐶𝑝=�+𝐵𝑇+𝐶𝑇^2+𝐷𝑇^3
𝐶𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/
= 303 K
= 403 K
= 353 K
= 303 K
= 298 K
∫ Cp dT, kJ/kmol Q masuk (kJ/jam)

400.6492104551 0
377.502799167 3249.6549014402
920.3422313084 0
1228.2405547246 109710.996449696
894.8399090023 0
701.5448205724 0
429.5656554184 0
112960.651351136
= 403 K
= 298 K
∫ Cp dT, kJ/kmol Q keluar (kJ/jam)

9015.8629395818 0
7924.3784045467 68215.3753032361
20598.9074617384 0
27154.2671108546 2425519.73319347
20252.9181859856 0
15390.0174252458 0
8870.8780543627 0
2493735.1084967
°F
= 428.5722222222 K
= 428.5722222222 K
= 428.5722222222 K
μ, Cp μ . Xi, Cp
0.2916935743 0
0.3522551926 0.0309634864
0.3211174142 0
3.1790975532 2.899652577
3.1790975532 0
5.7068088989 0
60.7800292936 0
2.9306160634
ork, 2008, halaman 805)
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 6
TUBE (ACH)
= 0.594 in2
= 0.0715 ft2
= w/at
= 238884.118355332 lb/ft2 jam
= 176 °F
= 0.0725 ft
= 7.0894181516 lb/ft jam
= 2442.9506357905
= 220.6896551724
= 10 (Kern, Fig.24)
= 3.1455854935 kJ/kg K
= 0.7513101876 Btu/lb ° F
= 0.1564272236 Btu/ft hr F
= 3.2412001067
𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
𝑤 )^0.14
= 69.9326805188 Btu/jam ft2 F

x 𝐼𝐷/𝑂𝐷
= 60.8414320514 Btu/jam ft2 F
rnal surface per foot length)
TUBE (Produk reaktor hidrolisis)

= 2442.9506357905
= 0.0004 (Fig.26, Kern)

= 55.2474986683 lb/ft3
= 0.8839599787
= 0.6550352435 psi
= 238884.118355332 lb/ft2 jam

= 0.003 (Fig.27 Kern)
= 0.0814516514
 ΔP t  ΔP R
= 0.7364868948 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝐶𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
Viskositas steam
micropoise
�_𝑔𝑎𝑠=�+𝐵𝑇+𝐶𝑇^2
T = 428.5722222222 K
Komponen BM (kg/kmol) A B
H2O 18 -36.826 4.29E-01
HEAT CAPACITY OF LIQUID
T = 353 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
Thermal conductivity of liquid
T = 353 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 428.5722222222 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 353 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
C n (micropoise) n (cP)
-1.62E-05 144.0559621088 0.0144055962
Cp=Joule/mol.K)
Cp (kJ/kmol K) BM (kg/kmol) xi
D
1.46E-06 85.7214471246 32 0
5.35E-07 75.1727504621 18 0.0879007239
3.78E-06 196.0826705543 100 0
3.62E-06 258.9318513113 85 0.9120992761
2.77E-06 194.0827031865 183 0
1.03E-06 147.1267112134 98 0
5.51E-09 84.4074534274 115 0
1
k liquid (W/mK) xi k liquid (BTU/ft h F) k.x

0.1837695335 0 0.1062511305 0
0.6620142881 0.0879007239 0.3827607611 0.033644948
0.1245654409 0 0.0720207461 0
0.2328270955 0.9120992761 0.1346150346 0.1227822756
0.1628373822 0 0.0941486633 0
0.3727524478 0 0.2155165125 0
5.72087277 0 3.3076712317 0
1 4.3129840799 0.1564272236
 T n
 1 
 TC 
  AB
Tc density ρ (g/ml) ρ (kg/m3)

647.13 0.89697 896.9704602842
Tc density ρ (g/ml) xi ρ (kg/m3)
512.58 0.73349 0.00000 733.4852419511
647.13 0.97564 0.08790 975.6407155442
553 0.86454 0.00000 864.5406131536
647 0.87624 0.91210 876.2422806685
741 0.86010 0.00000 860.1007882603
925 1.76469 0.00000 1764.6882004046
882 2.13559 0.00000 2135.5914695664
1.00000 8210.28931
Cp (kJ/kg K) Cp.xi
2.6787952226 0
4.1762639146 0.367096621
1.9608267055 0
3.0462570743 2.778488872
1.0605612196 0
1.5012929716 0
0.7339778559 0
15.1579749641 3.145585494
xi.ρ (kg/m3)
0
85.7595251513
0
799.2199498962
0
0
0
884.97948
HEATER
Fungsi : Memanaskan H2SO4 masuk reaktor hidrolisis dari suhu 30°C menjadi 130
T1 = 30 °C
t2 = 155 °C
Umpan
CH3OH 32 0
H2O 18 10.1532451347
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 91.3792062125
NH4HSO4 115 0
Total 101.5324513472
massa umpan = 9137.9206212522

= 20145.642560025
T1 = 30
T2 = 130
Ta = 80
Panas masuk
T = 30
Tref = 25
CH3OH 32 0
H2O 18 10.1532451347
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 91.3792062125
NH4HSO4 115 0
Total 101.5324513472
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 10.1532451347
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 91.3792062125
NH4HSO4 115 0
Total 101.5324513472
Beban steam (Qs) =

=
=
Neraca Panas
CH3OH - -
H2 O 3832.8785 80458.1565
C5 H 8 O 2 0.0000 0.0000
C4H7NO 0.0000 0.0000
C4H7NOH2SO4 0.0000 0.0000
H2SO4 64106.6088 1406327.5759
NH4HSO4 0.0000 0.0000
Beban steam (Qs) 1418846.2451 -
Total 1486785.7324 1486785.7324
Media Pemanas
P = 80
λs = 901.1
= 2095.9586
= 676.9438313868
t1 = 155.5722222222
t2 = 155.5722222222
ta = 155.5722222222
∆T LMTD
Hot fluid
°C F
155.5722 312.0300 Higher Temp.
155.5722 312.0300 Lower Temp.
0 Difference
(ThinTcout)  (Thout Tcin)

TLMTD 
Thin Tcout
ln
ThoutTcin
∆T LMTD = 113.109776502

Hot fluid = steam

T = 353
CH3OH 0 0
H2O 10.1532451347 0.1
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0 0
H2SO4 91.3792062125 0.9
NH4HSO4 0 0
Total 101.5324513472 1
Heavy organic
UD = 6 sampai 60
Dipilih UD =

Q
UDasumsi .T
Q
A= = 264.2087
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 1
BWG = 16
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 63.0750416864

Tipe pitch = tringular pitch
SHELL
ID shell = 15 1/4
Baffle space = 11
Pass = 1


A = L.a".Nt
= 309.9712
= 38.3564442688
SHELL (Steam)
Pitch = 1 1/4
= 0.25
ID S  C ' B
aS 
144  PT

= 6160.5278287337
De  G S
Re S 

Pada, ta = 312.03
μ = 0.0348484049
De = 0.99
= 0.0825
= 14584.4134599884
Dari fig. 28 Kern
jH = 40
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho = 1500
hio.ho
Uc 
hio  ho
Uc = 45.9340271597
Dirt Factor (Rd) 𝑅𝑑=(𝑈𝑐 −𝑈𝑑)/(𝑈𝑐

∗𝑈𝑑)
Rd = 0.004300885
Required surface
Q
A
UD  ΔTLMTD
A= 309.9712


SHELL (Steam)
Re shell (Res) = 14584.4134599884
f = 0.002
ρ = 55.9960718946
s = 0.8959371503
N+1
2 = 12 L/B
Gt = L 16.79  n
1 2 0
10 f  G S  D S  (N  1)  Ds
ΔP S 
10
5,2  10  De  s
∆Ps = 0.00031
drolisis dari suhu 30°C menjadi 130°C
HEATER
kg/jam
0
182.758412425
0
0
0
8955.1622088272
0
9137.9206212522
kg/jam
lb/jam
°C = 86 °F
°C = 266 °F
°C = 176 °F
°C = 86 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qkeluar - Qmasuk
1418846.24511212 kJ/jam
1344806.59150343 Btu/jam
m) pada suhu 281.01

psi
Btu/lb
kJ/kg
kg/jam = 1492.403909552 lb/jam

°C = 312.03 °F
°C = 312.03 °F
°C = 312.03 °F
Cold fluid
Difference
°C F
130.00 266.00 46.03
30.00 86.00 226.03
180.00 180.00
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
45 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
ft /ft
2
≈ 74 buah
SHELL
in 0.95 ft
in (0.2-1 )ID
ft2
Btu/jam.ft2.ºF
L (Steam)
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
𝜇)/𝑘)^(1/3
)
Btu/jam ft2 F (Kern, p.164) hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
hio
Btu/jam ft2 F
ft2
901.0790697674 lin ft

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s

 n
Ds 
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 130 °C
t1 = 155 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

𝐶𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇
= 303 K
= 403 K
= 353 K
= 303 K
= 298 K

400.6492104551 0
377.502799167 3832.8784589878
920.3422313084 0
1228.2405547246 0
894.8399090023 0
701.5448205724 64106.6088264135
429.5656554184 0
67939.4872854012
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 80458.156481681
20598.9074617384 0
27154.2671108546 0
20252.9181859856 0
15390.0174252458 1406327.57591584
8870.8780543627 0
1486785.73239752
°F
= 428.5722222222 K
= 428.5722222222 K
= 428.5722222222 K
μ, Cp μ . Xi, Cp
0.2916935743 0
0.3522551926 0.0352255193
0.3211174142 0
3.1790975532 0
3.1790975532 0
5.7068088989 5.136128009
60.7800292936 0
5.1713535282
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 6
TUBE (ACH)
= 0.594 in2
= 0.050875 ft2
= w/at
= 395983.146142997 lb/ft2 jam
= 176 °F
= 0.0725 ft
= 12.5099592639 lb/ft jam
= 2294.8738273004
= 220.6896551724
= 6 (Kern, Fig.24)
= 1.7687900659 kJ/kg K
= 0.4224682492 Btu/lb ° F
= 0.2322409374 Btu/ft hr F
= 2.8338078448
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 54.4656157496 Btu/jam ft2 F

= 47.3850857021 Btu/jam ft2 F

= 2294.8738273004
= 0.0004 (Fig.26, Kern)

= 105.2400893364 lb/ft3
= 1.6838414294
= 0.9448762389 psi
= 395983.146142997 lb/ft2 jam

= 0.02 (Fig.27 Kern)
= 0.2850624718
 ΔP t  ΔP R
= 1.2299387107 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝=�+𝐵𝑇+𝐶𝑇^2+𝐷𝑇^3
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
Viskositas steam
�_𝑔𝑎𝑠=�+𝐵𝑇+𝐶𝑇^2 micropoise
T = 428.5722222222 K
H2O 18 -36.826 4.29E-01
T = 353 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 353 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 428.5722222222 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 353 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
-1.62E-05 144.0559621088 0.0144055962
Cp=Joule/mol.K)
D
1.46E-06 85.7214471246 32 0
5.35E-07 75.1727504621 18 0.1
3.78E-06 196.0826705543 100 0
3.62E-06 258.9318513113 85 0
2.77E-06 194.0827031865 183 0
1.03E-06 147.1267112134 98 0.9
5.51E-09 84.4074534274 115 0
1

0.1837695335 0 0.1062511305 0
0.6620142881 0.1 0.3827607611 0.0382760761
0.1245654409 0 0.0720207461 0
0.2328270955 0 0.1346150346 0
0.1628373822 0 0.0941486633 0
0.3727524478 0.9 0.2155165125 0.1939648613
5.72087277 0 3.3076712317 0
1 4.3129840799 0.2322409374
 T n
 1 
 TC 
  AB

647.13 0.89697 896.9704602842
512.58 0.73349 0.00000 733.4852419511
647.13 0.97564 0.10000 975.6407155442
553 0.86454 0.00000 864.5406131536
647 0.87624 0.00000 876.2422806685
741 0.86010 0.00000 860.1007882603
925 1.76469 0.90000 1764.6882004046
882 2.13559 0.00000 2135.5914695664
1.00000 8210.28931
Cp (kJ/kg K) Cp.xi
2.6787952226 0
4.1762639146 0.417626391
1.9608267055 0
3.0462570743 0
1.0605612196 0
1.5012929716 1.351163674
0.7339778559 0
15.1579749641 1.768790066
xi.ρ (kg/m3)
0
97.5640715544
0
0
0
1588.2193803641
0
1685.78345
HEATER
Fungsi : Memanaskan metanol masuk reaktor esterifikasi dari suhu 30°C menjadi
T1 = 30 °C
t2 = 155 °C
Umpan
CH3OH 32 90.5702070778
H2O 18 3.2859939076
Total 93.8562009854
massa umpan = 2957.3945168265
= 6519.931099686
T1 = 30
T2 = 150
Ta = 90
Panas masuk
T = 30
Tref = 25
CH3OH 32 90.5702070778
H2O 18 3.2859939076
Total 93.8562009854
Panas keluar
T = 150
Tref = 25
CH3OH 32 90.5702070778
H2O 18 3.2859939076
Total 93.8562009854
Beban steam (Qs) =

=
=
Neraca Panas
CH3OH 36286.8820 989921.7886
H2 O 1240.4719 31115.5652
Beban steam (Qs) 983509.9999 -
Total 1021037.3538 1021037.3538
Media Pemanas
P = 80
λs = 901.1
= 2095.9586
= 469.2411385988
t1 = 155.5722222222
t2 = 155.5722222222
ta = 155.5722222222
∆T LMTD
Hot fluid
°C F
155.5722 312.0300 Higher Temp.
155.5722 312.0300 Lower Temp.
0 Difference
(Thin  Tcout)  (Thout  Tcin)

TLMTD 
Thin  Tcout
ln
∆T LMTD = 69.3399545045

Hot fluid = steam
Cold fluid = metanol

T = 363
CH3OH 90.5702070778 0.9649890591
H2O 3.2859939076 0.0350109409
Total 93.8562009854 1
UD = 200-700
Dipilih UD =
luas transfer panas dan jumlah pipa :

Q
A= = 67.2186
UDasumsi .T
Memilih tipe hairpin

Dari tabel 6.2 Kern, p.110
Dipilih type hairpin 2 x 1 1/4
Dari Kern, table 11, p.844
ANULUS
Normal pipe size (NPS) = 2
Schedule number = 40
Outside diameter (OD) = 2.38
Inside Diameter (ID) = 2.067
Flow area (ao) = 3.35
Inside surface area (Ai) = 0.542
Outside surface area (Ao) = 0.622
Inner pipe side = cold fluid (metanol)

Annulus = hot fluid (steam)
Menghitung panjang total (L)
Panjang pipa (L) = A/Ao inner pipe
= 154.525610804
Menghitung banyaknya hairpin (Nh)
Dipilih panjang pipa standart

Lt = 20
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 3.8631402701
Menghitung Ud terkoreksi
Ud terkoreksi = Q/(2.Lt.Ao inner pipe. Nh. TLMTD)
= 154.525610804

ANNULUS (Hot fluid)
Flow area (Aa) = (π(IDn2-ODp2)/4
= 0.0082691518
Diameter ekivalen (Dea) = (IDn2-ODp2)/ODp

= 0.0761490462
Mass velocity (Ga) = Wa/Aa

= 125103.326067722
Pada, ta = 312.03
μ = 0.0348484049
Re annulus (Ren) = Ga.Dea/μ

= 273369.727385302

Dari fig. 24 Kern, 834
jH = 600
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho = 1500
hio.ho
Uc 
hio  ho
Uc = 289.3323890776
Design overall coefficient (Ud)

1 1
  Rd
UD Uc
Rd = 0.001 (Tabel 8, Kern hal 840)
1/Ud = 0.0045
Ud = 224.40 Btu/jam.ft2.ºF
Required surface
Q
A
UD  ΔTLMTD
A= 59.91


Lt = 15
untuk 1 hairpin Le =
Banyak hairpin (Nh)
Nh = 5.151
Panjang pipa total (L) = 150
A terkoreksi
A = 65.25
UD terkoreksi
𝑈_𝐷=𝑄/(� .
∆𝑇𝐿𝑀𝑇𝐷) = 206.03
Dirt Factor :
𝑅𝑑=(𝑈𝑐 −𝑈𝑑)/
(𝑈𝑐 ∗𝑈𝑑) = 0.0014

ANNULUS (Hot Fluid)
Re annulus (Ren) = 273369.727385302
De' = (ID-Odi)
= 0.0339166667
Ren' = De'.Ga/μ
= 121758.451156319
Friction factor (f) = 0.0035+(0.264/(Ren'^0.42))
f = 0.0054306089
ρ = 55.9960718946
L = 150
g = 418000000
∆ Fa = 0.5735917846
V = 0.6205957442
g' = 32.2
Ft = 0.0179412614
∆ Pa = 0.2300244929
fikasi dari suhu 30°C menjadi 150°C
HEATER
kg/jam
2898.24662649
59.1478903365
2957.3945168265
kg/jam
lb/jam
°C = 86 °F
°C = 302 °F
°C = 194 °F
°C = 86 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
°C = 302 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
Qkeluar - Qmasuk
983509.999920032 kJ/jam
932187.497594205 Btu/jam
312
psi
Btu/lb
kJ/kg
kg/jam = 1034.4983989778 lb/jam
°C = 312.03 °F
°C = 312.03 °F
°C = 312.03 °F
Cold fluid
Difference
°C F
150.00 302.00 10.03
30.00 86.00 226.03
216.00 216.00
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
200 Btu/jam.ft2.ºF

in =
=
in = 0.1983333333 ft
in = 0.17225 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pe. Nh. TLMTD)

Btu/jam.ft2.F
(Hot fluid)
D
ft 2
Flow area (Ap)
ft Mass velocity (Gp)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)
L/D
jH
k
Btu/jam ft F2
(Kern, p.164)
((𝑐 .
𝜇)/𝑘)^(1/3
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
hio
Btu/jam ft2 F
ft2
154.53 lin ft
ft
30 ft
buah ≈ 5 buah
ft
ft2
Btu/jam.ft2.F
> Rd min = 0.0010
(Hot Fluid) INNER PIP

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft3
ρ
ft
g
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 150 °C
t1 = 155 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 303 K
= 423 K
= 363 K
= 303 K
= 298 K

400.6492104551 36286.8819564784
377.502799167 1240.4718981592
778.1520096221 37527.3538546376
= 423 K
= 298 K

10929.8832421271 989921.788575747
9469.1487793387 31115.5651989225
20399.0320214657 1021037.35377467
°F
= 428.5722222222 K
= 428.5722222222 K
= 428.5722222222 K
μ, Cp μ . Xi, Cp
0.2644519031 0.2551931932
0.3117685405 0.01091531
0.2661085031
INNER PIPE
Normal pipe size (NPS) = 1 1/4 in
Outside diameter (OD) = 1.66 in
Inside Diameter (ID) = 1.38 in
Flow area (ao) = 1.5 in2
Inside surface area (Ai) = 0.362 ft2/ft
Outside surface area (Ao) = 0.435 ft2/ft
(Kern, table 6.1, p.103)
INNER PIPE
= 0.115 ft
= πD /4
2
= 0.010381625 ft2
= Wc/Ap
= 628026.065253368 lb/ft2 jam
= 194 °F
= 0.6437398866 lb/ft jam
= (Gp.ID)/μ
= 112192.826655856
= 173.9130434783
= 280
= 2.7721990366 kJ/kg K
= 0.6621283645 Btu/lb ° F
= 0.1141621114 Btu/ft hr F
= 1.5513514876
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 431.2135408092 Btu/jam ft2 F
= 358.4787266968 Btu/jam ft2 F

INNER PIPE (Cold fluid)

= 112192.826655856
= 0.0054981063
= 45.4184274877 lb/ft3
= 418000000
= 150 ft
= 0.115 ft
= 6.5607186689
= 2.069288369 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1383333333 ft
= 0.115 ft
Viskositas steam
T = 428.5722222222 K
Komponen BM (kg/kmol) A B C
H2O 18 -36.826 4.29E-01 -1.62E-05
T = 363 K
Komponen
A B C D
CH3OH 40.152 3.10E-01 -1.03E-03 1.46E-06
H2O 92.053 -4.00E-02 -2.11E-04 5.35E-07
Total
T = 363 K
Komponen A B C k liquid (W/mK)
CH3OH -1.1793 6.19E-01 5.13E+02 0.180362947
H2O -0.2758 4.61E-03 -5.54E-06 0.6684743321
Total
Densitas
ta = 428.5722222222 K
Komponen A B n Tc
H2O 0.3471 0.274 0.28571 647.13
Ta = 363 K
Komponen A B n Tc
CH3OH 0.27197 0.27192 0.2331 512.58
H2O 0.3471 0.274 0.28571 647.13
Total
n (micropoise) n (cP)
144.0559621088 0.0144055962
Cp (kJ/kmol K) BM (kg/kmol) xi Cp (kJ/kg K) Cp.xi
87.0708702906 32 0.964989059 2.7209646966 2.625701162

75.3182196094 18 0.035010941 4.1843455339 0.146497874
2.772199037
xi k liquid (BTU/ft h F) k.x

0.9649890591 0.104281524 0.10063053
0.0350109409 0.3864958034 0.013531582
0.114162111
 T n
 1 

  AB  TC 
density ρ (g/ml) ρ (kg/m3)

0.89697 896.9704602842
density ρ (g/ml) xi xi.ρ (kg/m3) ρ (kg/m3)

0.72267 0.98000 722.6708708 708.2174533704
0.96578 0.02000 965.77522 19.3155044008
727.5329577711
HEATER
Fungsi : Memanaskan produk reaktor hidrolisis masuk reaktor esterifikasi dari suh
T1 = 130 °C
t2 = 155 °C
Umpan
CH3OH 32 0
H2O 18 18.7615386589
C5H8O2 100 1.8214458517
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 97.0117899291
H2SO4 98 74.6792799209
NH4HSO4 115 1.1728803012
Total 195.2683805136
massa umpan = 25881.2834023448

= 57058.3950144773
T1 = 130
T2 = 150
Ta = 140
Panas masuk
T = 130
Tref = 25
CH3OH 32 0
H2O 18 18.7615386589
C5H8O2 100 1.8214458517
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 97.0117899291
H2SO4 98 74.6792799209
NH4HSO4 115 1.1728803012
Total 195.2683805136
Panas keluar
T = 150
Tref = 25
CH3OH 32 0
H2O 18 18.7615386589
C5H8O2 100 1.8214458517
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 97.0117899291
H2SO4 98 74.6792799209
NH4HSO4 115 1.1728803012
Total 195.2683805136
Beban steam (Qs) =

=
=
Neraca Panas
CH3OH - -
H2 O 148673.5318 177655.8009
C5 H 8 O 2 37519.7945 45379.3293
C4H7NO 49460.0272 59550.5075
C4H7NOH2SO4 1964771.8445 2367226.5547
H2SO4 1149315.4193 1377843.1944
NH4HSO4 10404.4781 12345.2001
Total 4040000.5868 4040000.5868
Media Pemanas
P = 80
λs = 901.1
= 2095.9586
= 324.364942803
t1 = 155.5722222222
t2 = 155.5722222222
ta = 155.5722222222
∆T LMTD
Hot fluid
°C F
155.5722 312.0300 Higher Temp.
155.5722 312.0300 Lower Temp.
0 Difference

TLMTD 
ln
∆T LMTD = 23.6265003766

Hot fluid = steam

T = 413
CH3OH 0 0
H2O 18.7615386589 0.0960807818
C5H8O2 1.8214458517 0.0093279099
C4H7NO 1.8214458517 0.0093279099
C4H7NOH2SO4 97.0117899291 0.4968125903
H2SO4 74.6792799209 0.3824443042
NH4HSO4 1.1728803012 0.006006504
Total 195.2683805136 1
Heavy organic
UD = 6 sampai 60
Dipilih UD =

Q
UDasumsi .T
Q
A= = 454.5592
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 1
BWG = 16
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 108.51776261

Tipe pitch = square pitch
SHELL
ID shell = 17 1/4
Baffle space = 13
Pass = 1


A = L.a".Nt
= 469.1456
= 58.134515684
SHELL (Steam)
Pitch = 1 1/4
= 0.25
ID S  C ' B
aS 
144  PT

= 2307.0695487313
De  G S
Re S 

Pada, ta = 312.03
μ = 0.0348484049
De = 0.99
= 0.0825
= 5461.748914226
Dari fig. 28 Kern
jH = 42
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho = 1500
hio.ho
Uc 
hio  ho
Uc = 72.5108813295

∗𝑈𝑑)
Rd = 0.0034104514
Required surface
Q
A
UD  ΔTLMTD
A= 469.1456


SHELL (Steam)
Re shell (Res) = 5461.748914226
f = 0.0023
ρ = 55.9960718946
s = 0.8959371503
N+1 = 12 L/B
= 14.84
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 0.00005
masuk reaktor esterifikasi dari suhu 130°C menjadi 150°C
HEATER
kg/jam
0
337.7076958608
182.144585173
154.8228973971
17753.1575570259
7318.5694322516
134.8812346364
25881.2834023448
kg/jam
lb/jam
°C = 266 °F
°C = 302 °F
°C = 284 °F
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 302 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qkeluar - Qmasuk
679855.491406542 kJ/jam
644378.592298474 Btu/jam
m) pada suhu 312

psi
Btu/lb
kJ/kg
kg/jam = 715.1014402024 lb/jam

°C = 312.03 °F
°C = 312.03 °F
°C = 312.03 °F
Cold fluid
Difference
°C F
150.00 302.00 10.03
130.00 266.00 46.03
36.00 36.00
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
60 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
ft /ft
2
≈ 112 buah
SHELL
in 1.08 ft
in (0.2-1 )ID
ft2
Btu/jam.ft2.ºF
L (Steam) TUBE
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
𝜇)/𝑘)^(1/3
)
Btu/jam ft2 F (Kern, p.164) hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
hio
Btu/jam ft2 F
ft2
1363.7953488372 lin ft

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5, 22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 150 °C
t1 = 155 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 403 K
= 423 K
= 413 K
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 148673.531784917
20598.9074617384 37519.7945463558
27154.2671108546 49460.0271858375
20252.9181859856 1964771.84451016
15390.0174252458 1149315.41928799
8870.8780543627 10404.4781241857
3360145.09543944
= 423 K
= 298 K

10929.8832421271 0
9469.1487793387 177655.80089075
24913.9052005844 45379.3292780016
32694.0861072406 59550.5075161405
24401.4315831823 2367226.55471707
18450.1403310604 1377843.19436378
10525.5413257018 12345.2000802354
4040000.58684598
°F
= 428.5722222222 K
= 428.5722222222 K
= 428.5722222222 K
μ, Cp μ . Xi, Cp
0.1621547788 0
0.1960770054 0.018839232
0.1988008158 0.0018543961
1.1756357147 0.010966224
1.1756357147 0.5840706247
3.3126233643 1.2668939377
25.1776956218 0.1512299285
2.0338543429
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 2
= 0.594 in2
= 0.231 ft2
= w/at
= 247006.039023711 lb/ft2 jam
= 284 °F
= 0.0725 ft
= 4.9200726347 lb/ft jam
= 3639.7710275519
= 220.6896551724
= 15 (Kern, Fig.24)
= 1.6272918943 kJ/kg K
= 0.3886719916 Btu/lb ° F
= 0.1991573399 Btu/ft hr F
= 2.1254594036
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 87.5794843392 Btu/jam ft2 F

= 76.1941513751 Btu/jam ft2 F

= 3639.7710275519
= 0.00038 (Fig.26, Kern)

= 72.7922741938 lb/ft3
= 1.1646763871
2
f  Gt  L  n
Pt 
10
5, 22  10  Ds  
= 0.1683196958 psi
= 247006.039023711 lb/ft2 jam

= 0.009 (Fig.27 Kern)
= 0.0618197474
 ΔP t  ΔP R
= 0.2301394432 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
Viskositas steam
T = 428.5722222222 K
H2O 18 -36.826 4.29E-01
T = 413 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 413 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 428.5722222222 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 413 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
-1.62E-05 144.0559621088 0.0144055962
Cp=Joule/mol.K)
D
1.46E-06 95.6750287206 32 0
5.35E-07 77.2234703759 18 0.0960807818
3.78E-06 215.6991122723 100 0.0093279099
3.62E-06 276.9561118493 85 0.0093279099
2.77E-06 207.4290996765 183 0.4968125903
1.03E-06 153.0096194974 98 0.3824443042
5.51E-09 82.7329036749 115 0.006006504
1

0.1615692378 0 0.0934154527 0
0.6841572521 0.0960807818 0.3955632911 0.0380060303
0.1013676213 0.0093279099 0.058608324 0.0005466932
0.2074021829 0.0093279099 0.1199149608 0.0011185559
0.1485299751 0.4968125903 0.0858764642 0.0426645086
0.3778510798 0.3824443042 0.2184644191 0.0835504728
9.58043157 0.006006504 5.539175431 0.0332710792
1 6.5110183428 0.1991573399
 T n
 1 
 TC 
  AB

647.13 0.89697 896.9704602842
512.58 0.66151 0.00000 661.5122146115
647.13 0.91404 0.09608 914.0426106982
553 0.78273 0.00933 782.7265616548
647 0.81541 0.00933 815.4107716981
741 0.81612 0.49681 816.1157161282
925 1.68770 0.38244 1687.6961933949
882 2.06178 0.00601 2061.7771763936
1.00000 7739.28124
Cp (kJ/kg K) Cp.xi
2.9898446475 0
4.2901927987 0.412205078
2.1569911227 0.020120219
3.2583071982 0.030393196
1.133492348 0.563133269
1.5613226479 0.597118954
0.7194165537 0.004321178
16.1095673167 1.627291894
xi.ρ (kg/m3)
0
87.8219286267
7.3012028113
7.6060781764
405.4565629244
645.4497964111
12.3840727785
1166.01964
HEATER
Fungsi : Memanaskan recycle MD-03 masuk reaktor esterifikasi dari suhu 89°C m
T1 = 89 °C
t2 = 155 °C
Umpan
CH3OH 32 64.6486568088
H2O 18 5.7465472719
Total 70.3952040806
massa umpan = 2172.1948687742
= 4788.8642515969
T1 = 85.1985896376
T2 = 150
Ta = 117.5992948188
Panas masuk
T = 85.1985896376
Tref = 25
CH3OH 32 64.6486568088
H2O 18 5.7465472719
Total 70.3952040806
Panas keluar
T = 150
Tref = 25
CH3OH 32 64.6486568088
H2O 18 5.7465472719
Total 70.3952040806
Beban steam (Qs) =

=
=
Neraca Panas
CH3OH 322683.8654 706602.2707
H2 O 26016.8336 54414.9111
Total 761017.1818 761017.1818
Media Pemanas
P = 80
λs = 901.1
= 2095.9586
= 196.7197647661
t1 = 155.5722222222
t2 = 155.5722222222
ta = 155.5722222222
∆T LMTD
Hot fluid
°C F
155.5722 312.0300 Higher Temp.
155.5722 312.0300 Lower Temp.
0 Difference

TLMTD 
Thin Tcout
ln
∆T LMTD = 45.9942435846

Hot fluid = steam
Cold fluid = metanol

T = 390.5992948188
CH3OH 64.6486568088 0.9183673469
H2O 5.7465472719 0.0816326531
Total 70.3952040806 1
UD = 200-700
Dipilih UD =

Q
A= = 42.4836
UDasumsi .T

Dipilih type hairpin 2 x 1 1/4
ANULUS
Inner pipe side = cold fluid (metanol)

Annulus = hot fluid (steam)
= 97.6635388374

Lt = 20
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 2.4415884709
= 97.6635388374

ANNULUS (Hot fluid)
Flow area (Aa) = (π(IDn2-ODp2)/4
= 0.0082691518

= 0.0761490462

= 52447.0146607081
Pada, ta = 312.03
μ = 0.0348484049

= 114604.67559599

jH = 290
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho = 1500
hio.ho
Uc 
hio  ho
Uc = 301.8279768371

1 1
  Rd
UD Uc
1/Ud = 0.0043
Required surface
Q
A
UD  ΔTLMTD
A= 36.65


Lt = 15
Banyak hairpin (Nh)
Nh = 2.808
A terkoreksi
A = 39.15
UD terkoreksi
𝑈_𝐷=𝑄/(� .
∆𝑇𝐿𝑀𝑇𝐷) = 217.03
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.00129

ANNULUS (Hot Fluid)
Re annulus (Ren) = 114604.67559599
De' = (ID-Odi)
= 0.0339166667
Ren' = De'.Ga/μ
= 51044.744161348

f = 0.0062814067
ρ = 55.9960718946
L = 90
g = 418000000
∆ Fa = 0.0699626728
V = 0.2601720923
g' = 32.2
Ft = 0.0031532384
∆ Pa = 0.028431971
sterifikasi dari suhu 89°C menjadi 150°C
HEATER
kg/jam
2068.7570178802
103.437850894
2172.1948687742
kg/jam
lb/jam
°C = 185.3574613476 °F
°C = 302 °F
°C = 243.6787306738 °F
°C = 185.3574613476 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
°C = 302 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
Qkeluar - Qmasuk
412316.482751514 kJ/jam
390800.571732091 Btu/jam
312
psi
Btu/lb
kJ/kg
kg/jam = 433.6923277987 lb/jam
°C = 312.03 °F
°C = 312.03 °F
°C = 312.03 °F
Cold fluid
Difference
°C F
150.00 302.00 10.03
85.20 185.36 126.67
116.64 116.64
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
200 Btu/jam.ft2.ºF

in =
=
in = 0.1983333333 ft
in = 0.17225 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)
L/D
jH
k
Btu/jam ft F2
(Kern, p.164)
((𝑐 .
𝜇)/𝑘)^(1/3
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
hio
Btu/jam ft2 F
ft2
84.25 lin ft
ft
30 ft
buah ≈ 3 buah
ft
ft2
Btu/jam.ft2.F
> Rd min = 0.0010
Hot Fluid) INNER PIP

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft 3
ρ
ft
g
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 150 °C
t1 = 155 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 358.1985896376 K
= 423 K
= 390.5992948188 K
= 358.1985896376 K
= 298 K

4991.3467869949 322683.865445915
4527.3852866213 26016.8335676254
9518.7320736162 348700.699013541
= 423 K
= 298 K

10929.8832421271 706602.270680032
9469.1487793387 54414.9110850223
20399.0320214657 761017.181765054
°F
= 428.5722222222 K
= 428.5722222222 K
= 428.5722222222 K
μ, Cp μ . Xi, Cp
0.2024912323 0.1859613358
0.2352575052 0.0192046943
0.2051660301
INNER PIPE
Normal pipe size (NPS) = 1 1/4 in
INNER PIPE
= 0.115 ft
= πD /4
2
= 0.010381625 ft2
= Wc/Ap
= 461282.72323426 lb/ft2 jam
= 243.6787306738 °F
= 0.4963146813 lb/ft jam
= (Gp.ID)/μ
= 106882.820851222
= 173.9130434783
= 300
= 2.9683817728 kJ/kg K
= 0.708985806 Btu/lb ° F
= 0.1226050658 Btu/ft hr F
= 1.4211134483
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 454.5279336607 Btu/jam ft2 F
= 377.8605713564 Btu/jam ft2 F


= 106882.820851222
= 0.0055392131
= 43.8481791071 lb/ft3
= 418000000
= 90 ft
= 0.115 ft
= 2.2955021597
= 0.6989832628 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1383333333 ft
= 0.115 ft
Viskositas steam
T = 428.5722222222 K
Komponen BM (kg/kmol) A B C
H2O 18 -36.826 4.29E-01 -1.62E-05
T = 390.5992948188 K
Komponen
A B C D
CH3OH 40.152 3.10E-01 -1.03E-03 1.46E-06
H2O 92.053 -4.00E-02 -2.11E-04 5.35E-07
Total
T = 390.5992948188 K
Komponen A B C k liquid (W/mK)
CH3OH -1.1793 6.19E-01 5.13E+02 0.1704104234
H2O -0.2758 4.61E-03 -5.54E-06 0.6805555962
Total
Densitas
ta = 428.5722222222 K
Komponen A B n Tc
H2O 0.3471 0.274 0.28571 647.13
Ta = 390.5992948188 K
Komponen A B n Tc
CH3OH 0.27197 0.27192 0.2331 512.58
H2O 0.3471 0.274 0.28571 647.13
Total
n (micropoise) n (cP)
144.0559621088 0.0144055962
Cp (kJ/kmol K) BM (kg/kmol) xi Cp (kJ/kg K) Cp.xi
91.4036089669 32 0.918367347 2.8563627802 2.623190308

76.1147179032 18 0.081632653 4.2285954391 0.345191464
2.968381773
xi k liquid (BTU/ft h F) k.x

0.9183673469 0.0985272139 0.090484176
0.0816326531 0.3934809002 0.03212089
0.122605066
 T n
 1 
 TC 
  AB
density ρ (g/ml) ρ (kg/m3)

0.89697 896.9704602842
density ρ (g/ml) xi xi.ρ (kg/m3) ρ (kg/m3)

0.69061 0.95238 690.6113204 657.7250670629
0.93775 0.04762 937.7537488 44.6549404193
702.3800074821
COOLER
Fungsi : Menurunkan suhu produk reaktor esterifikasi masuk MD-01 dari suhu 15
T1 = 150 °C
t2 = 45 °C
Umpan
CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797
massa umpan = 31010.8727879454

= 68367.1903657602
T1 = 134.6564983
T2 = 125
Ta = 129.82824915
Panas masuk
T = 134.6564983
Tref = 25
CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797
Panas keluar
T = 125
Tref = 25
CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797
Beban pendingin (Qc) =

=
=
Neraca Panas
CH3OH 623673.5668 564016.5706
H2 O 230189.8965 209612.3297
C5 H 8 O 2 1966184.5715 1779966.1307
C4H7NO 51786.7896 46976.1388
C4H7NOH2SO4 164620.5250 149233.4282
H2SO4 1202286.2529 1092600.1957
NH4HSO4 837062.1056 764577.0187
Beban pendingin (Qc) - 468821.8956
Total 5075803.7079 5075803.7079
Media Pendindin
Media pendingi yang digunakan adalah air pada suhu 30 °C
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5
massa pendingin = Qc / Cp(t2-t1)

= 7465.0790678374
∆T LMTD
Hot fluid
°C F
134.6565 274.3817 Higher Temp.
125.0000 257.0000 Lower Temp.
17.38169694 Difference

TLMTD 
Thin Tcout
ln
∆T LMTD = 166.1444497956

Hot fluid = heavy organic
Cold fluid = water

T = 402.82824915
CH3OH 65.9680171518 0.1834892537
H2O 27.7940798384 0.0773089019
C5H8O2 91.0722925865 0.2533164967
C4H7NO 1.8214458517 0.0050663299
C4H7NOH2SO4 7.7609431943 0.021586971
H2SO4 74.6792799209 0.2077195273
NH4HSO4 90.423727036 0.2515125194
Total 359.5197855797 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 445.7540
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 1
BWG = 16
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 106.415690492

Tipe pitch = square pitch
SHELL
ID shell = 17 1/4
Baffle space = 13
Pass = 1
Shell Side = cold fluid (water)

Tube Side = hot fluid (produk reaktor esterifikasi)

A = L.a".Nt
= 469.1456
= 5.7008405621
SHELL (water)
Pitch = 1 1/4
= 1/4
ID S  C ' B
aS 
144  PT
Flow area (as) = 1/3

= 53095.9247551498
De  G S
Re S 

Pada, ta = 99.5
μ = 1.6912416261
De = 0.99
= 0.0825
= 2590.0579341316
Dari fig. 28 Kern
jH = 26
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, ta = 99.5
k = 0.3597410869
c = 4.1837937877
= 0.9992819785
μ = 1.6912
((𝑐 . = 1.6748190447
𝜇)/𝑘)^(1/3
)
((𝑐 .
𝜇)/𝑘)^(1/3
)
ho = 189.8791734524
hio.ho
Uc 
hio  ho
Uc = 66.4251483885

∗𝑈𝑑)
Rd = 0.1603581897
Required surface
Q
A
UD  ΔTLMTD
A= 469.15


SHELL (water)
Re shell (Res) = 2590.0579341316
f = 0.0027
ρ = 63.4328916168
s = 1.0149262659
N+1 = 12 L/B
= 14.84
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 0.02786424
si masuk MD-01 dari suhu 150°C menjadi 125°C
COOLER
HEATER
kg/jam
2110.9765488573
500.2934370913
9107.2292586505
154.8228973971
1420.2526045621
7318.5694322516
10398.7286091355
31010.8727879454
kg/jam
lb/jam
°C = 274.38169694 °F
°C = 257 °F
°C = 265.69084847 °F
°C = 274.38169694 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 257 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
468821.895618324 kJ/jam
444357.362639273 Btu/jam
atm
kkal/kg°C = 4.1868 kJ/kg K
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 16457.6626145357 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 161.38
30.00 86.00 171.00
27.00 9.62
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
6 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
ft2/ft luas permukaan per linear pipa
≈ 112 buah
SHELL
in 1.078125 ft
in (0.2-1 )ID
reaktor esterifikasi)
ft2
Btu/jam.ft2.ºF
(water) TUBE (
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
°F 𝜇)/𝑘)^(1/3
Btu/ft hr F )
kJ/kg K hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
Btu/lb ° F
(𝜇/𝜇_𝑤 )^0.14
lb/ft jam
hi
Btu/jam ft2 F
hio
Btu/jam ft2 F
ft2
1363.7953488372 lin ft
(water) TUBE (Produk r

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5, 22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 125 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 407.6564983 K
= 398 K
= 402.82824915 K
= 407.6564983 K
= 298 K

9454.1808848393 623673.566767209
8281.9757971752 230189.896526445
21589.2728256531 1966184.57150776
28431.6931918211 51786.7896219058
21211.4070264413 164620.525003987
16099.3284104924 1202286.25290621
9257.1068794024 837062.105605802
5075803.70793932
= 398 K
= 298 K

8549.8487748267 564016.57062298
7541.6178867147 209612.329654108
19544.54071728 1779966.13067299
25790.57662448 46976.1388063866
19228.7747037333 149233.428172211
14630.5668299733 1092600.19569752
8455.4910946187 764577.018694805
4606981.812321
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.1795829388 0.0329515394
0.2120763122 0.0163953868
0.2153424221 0.054549788
1.3655179282 0.0069181644
1.3655179282 0.0294773959
3.4567706236 0.71803876
28.6996248251 7.2183149449
8.0766459793
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 2
TUBE (Produk reaktor esterifikasi)
= 0.594 in2
= 0.231 ft2
= w/at
= 295961.863055239 lb/ft2 jam
= 265.69084847 °F
= 0.0725 ft
= 19.5381173689 lb/ft jam
= 1098.2242898016
= 220.6896551724
= 3.3 (Kern, Fig.24)
= 1.9470675623 kJ/kg K
= 0.4650490977 Btu/lb ° F
= 1.3747488926 Btu/ft hr F
= 1.8766619441
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 117.4317029972 Btu/jam ft2 F

= 102.1655816076 Btu/jam ft2 F

= 1098.2242898016
= 0.0005 (Fig.26, Kern)

= 80.8118758441 lb/ft3
= 1.2929900135
2
f  Gt  L  n
10
22  10  Ds  
= 0.2864097561 psi
= 295961.863055239 lb/ft2 jam

= 0.5 (Fig.27 Kern)
= 3.0936047133
 ΔP t  ΔP R
= 3.3800144694 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06
Menghitung viskositas log vis =A+B/T+CT+DT2

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 402.82824915 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 402.82824915 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 402.82824915 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
Cp (kJ/kmol K) BM (kg/kmol) Cp (kJ/kg K)
D
5.35E-07 75.3082881783 18 4.1837937877
k liquid (W/mK) k liquid (BTU/ft h F)

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 93.644396341 32 0.1834892537
5.35E-07 76.6660166123 18 0.0773089019
3.78E-06 211.7358063845 100 0.2533164967
3.62E-06 273.4993931234 85 0.0050663299
2.77E-06 205.3173246716 183 0.021586971
1.03E-06 152.1019031793 98 0.2077195273
5.51E-09 83.0130330324 115 0.2515125194
1

0.165684618 0.1834892537 0.0957948667 0.0175773286
0.683210814 0.0773089019 0.3950160833 0.0305382596
0.1053593347 0.2533164967 0.0609162368 0.0154310877
0.211801214 0.0050663299 0.1224583749 0.0006204145
0.1509847947 0.021586971 0.0872957819 0.0018844515
0.3776384085 0.2077195273 0.2183414576 0.0453537844
8.687640051 0.2515125194 5.0229848178 1.2633435663
1 6.002807619 1.3747488926
 T n
 1 

 TC
  AB 

647.13 1.01610 1016.0968093939
512.58 0.67513 0.18349 675.1329452115
647.13 0.92493 0.07731 924.9261696705
553 0.79755 0.25332 797.5469320761
647 0.82613 0.00507 826.1292853856
741 0.82379 0.02159 823.7854012052
925 1.70094 0.20772 1700.9396155139
882 2.07456 0.25151 2074.5605330536
1.00000 7823.02088
Cp (kJ/kg K) Cp.xi
2.9263873857 0.536960637
4.2592231451 0.329275864
2.1173580638 0.536361727
3.2176399191 0.016301625
1.1219525938 0.024219558
1.5520602365 0.322393219
0.7218524612 0.181554931
15.9164738052 1.947067562
xi.ρ (kg/m3)
123.8796402753
71.5050265259
202.0317948076
4.1854435283
17.7830315869
353.3183729256
521.7779462623
1294.48126
COOLER
Fungsi : Menurunkan suhu recycle MD-02 ke reaktor hidrolisis dari suhu 203.7°C
T1 = 203.7 °C
t2 = 45 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 1.8214458517
C4H7NO 85 1.7485880177
C4H7NOH2SO4 183 7.3728960346
H2SO4 98 3.733963996
NH4HSO4 115 0
Total 14.6768939
massa umpan = 2045.9430126207

= 4510.5268844839
T1 = 203.76
T2 = 130
Ta = 166.88
Panas masuk
T = 203.76
Tref = 25
Cp= A+B.T+C.T +D.T (Cp=Joule/mol.K)
2 3

CH3OH 32 0
H2O 18 0
C5H8O2 100 1.8214458517
C4H7NO 85 1.7485880177
C4H7NOH2SO4 183 7.3728960346
H2SO4 98 3.733963996
NH4HSO4 115 0
Total 14.6768939
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 1.8214458517
C4H7NO 85 1.7485880177
C4H7NOH2SO4 183 7.3728960346
H2SO4 98 3.733963996
NH4HSO4 115 0
Total 14.6768939

=
=
Neraca Panas
CH3OH - -
H2 O - -
C5 H 8 O 2 68229.6373339042 37519.7945463558
C4H7NO 84600.6254586809 47481.626098404
C4H7NOH2SO4 265161.794471685 149322.660182772
H2SO4 100241.454144192 57465.7709643993
NH4HSO4 - -
Total 518233.511408462 518233.511408462
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 3605.6759277815
∆T LMTD
Hot fluid
°C F
203.7600 398.7680 Higher Temp.
130.0000 266.0000 Lower Temp.
132.768 Difference

TLMTD 
Thin Tcout
ln
∆T LMTD = 228.8243961819

Cold fluid = water

T = 439.88
CH3OH 0 0
H2O 0 0
C5H8O2 1.8214458517 0.1241029515
C4H7NO 1.7485880177 0.1191388334
C4H7NOH2SO4 7.3728960346 0.5023471645
H2SO4 3.733963996 0.2544110506
NH4HSO4 0 0
Total 14.6768939 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 188
UDasumsi .T

Dipilih type hairpin 3x2
ANULUS
Inner pipe side = cold fluid (water)

Annulus = hot fluid (recycle)

= 301.5934774871

Lt = 15
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 10.0531159162
= 10.0531159162

ANNULUS (Hot fluid)
Flow area (Aa) = (π(IDn -ODp2)/4
2
= 0.0204330267

= 0.1312403361

= 220746.879944231
Pada, Ta = 332.384
μ = 3.2285100633

= 8973.4565346028
jH = 35
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 332.384
k = 0.1166840582
c = 1.6729767925
= 0.399583642
μ = 3.2285
((𝑐 . = 2.2277482275
𝜇)/𝑘)^(1/3
)
ho = 69.3231585556
hio.ho
Uc 
hio  ho
Uc = 57.4126335887

1 1
  Rd
UD Uc
1/Ud = 0.02
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 19.15


Lt = 15
Banyak hairpin (Nh)
Nh = 10.053
A terkoreksi
A = 186.60
UD terkoreksi
𝑈_𝐷=𝑄/(� .
∆𝑇𝐿𝑀𝑇𝐷) = 5.03 Btu/jam.ft2.F
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.18153

ANNULUS (Hot Fluid)
Re annulus (Ren) = 8973.4565346028
De' = (ID-Odi)
= 0.0573333333
Ren' = De'.Ga/μ
= 3920.1223480827

f = 0.0116736886
ρ = 62.773252634
L = 300
g = 418000000
∆ Fa = 3.6142297962
V = 0.9768265175
g' = 32.2
Ft = 0.0444498468
∆ Pa = 1.5949112607
aktor hidrolisis dari suhu 203.7°C menjadi 130°C
COOLER
HEATER
kg/jam
0
0
182.144585173
148.6299815012
1349.239974334
365.9284716126
0
2045.9430126207
kg/jam
lb/jam
°C = 398.768 °F
°C = 266 °F
°C = 332.384 °F
°C = 398.768 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
226443.659616531 kJ/jam
214627.150126762 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 7949.1452639056 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 285.77
30.00 86.00 180.00
27.00 -105.77
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
5 Btu/jam.ft2.ºF
in =
=
in = 0.2916666667 ft
in = 0.2556666667 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
US (Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
301.59 lin ft
ft
30 ft
buah ≈ 10 buah
ft
ft2
US (Hot Fluid) INNER PIP

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft3
ρ
ft
g
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 130 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 476.76 K
= 403 K
= 439.88 K
= 476.76 K
= 298 K

16557.7309322673 0
13779.39940182 0
37459.0533498956 68229.6373339042
48382.2516248576 84600.6254586809
35964.4016715942 265161.794471685
26845.8544994867 100241.454144192
14919.5095811528 0
518233.511408462
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 0
20598.9074617384 37519.7945463558
27154.2671108546 47481.626098404
20252.9181859856 149322.660182772
15390.0174252458 57465.7709643993
8870.8780543627 0
291789.851791931
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.1220097868 0
0.1637643798 0
0.1604693189 0.0199147161
0.8151459381 0.0971155361
0.8151459381 0.4094862507
3.1762831006 0.8080815205
18.3405757686 0
1.3345980234
INNER PIPE
Normal pipe size (NPS) = 2 in
INNER PIPE
= 0.17225 ft
= πD /4
2
= 0.0232909991 ft2
= Wc/Ap
= 341296.877930161 lb/ft2 jam
= 99.5 °F
= 1.6912416261 lb/ft jam
= (Gp.ID)/μ
= 34760.4897579792
= 87.0827285922
= 110
= 4.1837937877 kJ/kg K
= 0.9992819785 Btu/lb ° F
= 0.3597410869 Btu/ft hr F
= 1.6748190447
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 384.7613038028 Btu/jam ft2 F
= 334.1603424203 Btu/jam ft2 F


= 34760.4897579792
= 0.0067684952
= 63.4328916168 lb/ft3
= 418000000
= 300 ft
= 0.17225 ft
= 1.6328394216
= 0.7192758754 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1983333333 ft
= 0.17225 ft
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 439.88 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 439.88 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 439.88 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 101.8419316655 32 0
5.35E-07 79.1551254574 18 0
3.78E-06 227.7525013659 100 0.1241029515
3.62E-06 287.1919761201 85 0.1191388334
2.77E-06 212.9533949977 183 0.5023471645
1.03E-06 155.3217678604 98 0.2544110506
5.51E-09 82.0004871314 115 0
1

0.1496345307 0 0.0865150918 0
0.6811416492 0 0.3938197419 0
0.0906362318 0.1241029515 0.0524036923 0.0065034529
0.1955600509 0.1191388334 0.1130681245 0.0134708044
0.1419743122 0.5023471645 0.0820861374 0.0412357384
0.377132494 0.2544110506 0.21804895 0.0554740625
12.4083588076 0 7.1742150386 0
1 8.1201567765 0.1166840582
n
 T
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.62121 0.00000 621.2141855209
647.13 0.88423 0.00000 884.2336818045
553 0.74102 0.12410 741.0157064727
647 0.78612 0.11914 786.1207784224
741 0.79537 0.50235 795.3673539124
925 1.65229 0.25441 1652.2872277601
882 2.02741 0.00000 2027.4116387946
1.00000 7507.65057
Cp (kJ/kg K) Cp.xi
3.1825603645 0
4.3975069699 0
2.2775250137 0.282647576
3.3787291308 0.402537847
1.1636797541 0.584571225
1.5849159986 0.403220144
0.7130477142 0
16.6979649457 1.672976793
xi.ρ (kg/m3)
0
0
91.9622362751
93.6575124781
399.5505349875
420.3601294388
0
1005.53041
COOLER
Fungsi : Menurunkan suhu recycle MD-04 masuk reaktor hidrolisis dari suhu 284°
T1 = 284 °C
t2 = 45 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
massa umpan = 6949.9555966843

= 15322.0111075622
T1 = 284
T2 = 130
Ta = 207
Panas masuk
T = 284
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908

=
=
Neraca Panas
CH3OH - -
H2 O - -
C5 H 8 O 2 - -
C4H7NO - -
C4H7NOH2SO4 21156.7843 7859.0874
H2SO4 2743705.8090 1059094.1589
NH4HSO4 25025.4608 10404.4781
Total 2789888.0540 2789888.0540
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 27268.7228059437
∆T LMTD
Hot fluid
°C F
284.0000 543.2000 Higher Temp.
130.0000 266.0000 Lower Temp.
277.2 Difference

TLMTD 
Thin Tcout
ln
∆T LMTD = 287.1593079664

Cold fluid = water

T = 480
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0.3880471597 0.0055137657
H2SO4 68.8169564471 0.9778207673
NH4HSO4 1.1728803012 0.016665467
Total 70.377883908 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 113
UDasumsi .T

ANULUS


= 123.2822430851

Lt = 20
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 3.0820560771
= 30.8205607713

ANNULUS (Hot fluid)
2
= 0.0215802824

= 0.0942541905

= 710000.492633652
Pada, Ta = 404.6
μ = 8.6387545542

= 7746.5474046314
jH = 28
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 404.6
k = 0.3834921823
c = 1.6024113919
= 0.3827293857
μ = 8.6388
((𝑐 . = 2.0505111856
𝜇)/𝑘)^(1/3
)
ho = 233.601712056
hio.ho
Uc 
hio  ho
Uc = 80.9781619762

1 1
  Rd
UD Uc
1/Ud = 0.02
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 86.76


Lt = 15
Banyak hairpin (Nh)
Nh = 4.109

A terkoreksi
A = 110.04
UD terkoreksi
𝑈_𝐷=𝑄/(� .
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.007

ANNULUS (Hot Fluid)
Re annulus (Ren) = 7746.5474046314
De' = (ID-Odi)
= 0.0438333333
Ren' = De'.Ga/μ
= 3602.5665580933

f = 0.0119688976
ρ = 99.8777216707
L = 120
g = 418000000
∆ Fa = 7.9225439847
V = 1.9746381452
g' = 32.2
Ft = 0.1816395561
∆ Pa = 5.6210235282
aktor hidrolisis dari suhu 284°C menjadi 130°C
COOLER
HEATER
kg/jam
0
0
0
0
71.0126302281
6744.0617318198
134.8812346364
6949.9555966843
kg/jam
lb/jam
°C = 543.2 °F
°C = 266 °F
°C = 404.6 °F
°C = 543.2 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
1712530.32965887 kJ/jam
1623165.35946629 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 60117.1716724395 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 430.20
30.00 86.00 180.00
27.00 -250.20
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
50 Btu/jam.ft2.ºF
in =
=
in = 0.375 ft
in = 0.3355 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
(Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
123.28 lin ft
ft
30 ft
buah ≈ 4 buah
ft
ft2
(Hot Fluid) INNER PIP

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft3
ρ
ft
g
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 130 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 557 K
= 403 K
= 480 K
= 557 K
= 298 K

26823.0355509124 0
20936.0391930526 0
59915.2110772504 0
74847.1517730466 0
54521.167720479 21156.7842783541
39869.6186324351 2743705.80899241
21336.7559664106 25025.460764217
2789888.05403498
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 0
20598.9074617384 0
27154.2671108546 0
20252.9181859856 7859.0873780406
15390.0174252458 1059094.15887388
8870.8780543627 10404.4781241857
1077357.7243761
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.0754052296 0
0.1314596888 0
0.1144733696 0
0.5040775239 0
0.5040775239 0.0027793653
3.4411436298 3.3648217046
12.2095595703 0.203478012
3.5710790819
INNER PIPE
INNER PIPE
= 0.2556666667 ft
= πD /4
2
= 0.0513118739 ft2
= Wc/Ap
= 1171603.51232967 lb/ft2 jam
= 99.5 °F
= 1.6912416261 lb/ft jam
= (Gp.ID)/μ
= 177112.459877865
= 78.2268578879
= 60
= 4.1837937877 kJ/kg K
= 0.9992819785 Btu/lb ° F
= 0.3597410869 Btu/ft hr F
= 1.6748190447
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 141.3953327534 Btu/jam ft2 F
= 123.943108825 Btu/jam ft2 F


= 177112.459877865
= 0.0051494505
= 63.4328916168 lb/ft3
= 418000000
= 120 ft
= 0.2556666667 ft
= 3.9450640035
= 1.7378251205 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.2916666667 ft
= 0.2556666667 ft
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 480 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 480 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 480 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 113.5103616 32 0
5.35E-07 83.38668448 18 0
3.78E-06 250.7902928 100 0
3.62E-06 306.1917248 85 0
2.77E-06 221.622304 183 0.0055137657
1.03E-06 158.7536064 98 0.9778207673
5.51E-09 80.9296607232 115 0.016665467
1

0.1265954839 0 0.0731944682 0
0.66175136 0 0.3826087424 0
0.07383382 0 0.0426889414 0
0.1771506698 0 0.1024242625 0
0.1319705864 0.0055137657 0.0763022234 0.0004207126
0.37260368 0.9778207673 0.2154304986 0.2106524154
17.894012 0.016665467 10.34588796 0.1724190543
1 11.2385370965 0.3834921823
n
 T
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.53955 0.00000 539.5488703662
647.13 0.83629 0.00000 836.2853469907
553 0.66878 0.00000 668.7837139012
647 0.73922 0.00000 739.218598237
741 0.76291 0.00551 762.91052967
925 1.59822 0.97782 1598.2233875376
882 1.97439 0.01667 1974.387339695
1.00000 7119.35779
Cp (kJ/kg K) Cp.xi
3.5471988 0
4.6325935822 0
2.507902928 0
3.6022555859 0
1.2110508415 0.006677451
1.6199347592 1.584005849
0.7037361802 0.011728092
17.824672677 1.602411392
xi.ρ (kg/m3)
0
0
0
0
4.2065098823
1562.7760191922
32.9040870377
1599.88662
COOLER
Fungsi : Menurunkan suhu produk MD-04 dari suhu 338.8194°C menjadi 45°C
T1 = 338.8194 °C
t2 = 40 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125
massa umpan = 10472.4266033183

= 23087.7211382076
T1 = 338.8194
T2 = 45
Ta = 191.9097
Panas masuk
T = 338.8194
Tref = 25
2 3

CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125
Panas keluar
T = 45
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125

=
=
Neraca Panas
CH3OH - 0
H2 O 0 0
C5 H 8 O 2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0 0
H2SO4 104733.6108 6019.0619
NH4HSO4 2287348.2267 152969.0085
Beban pendingin (Qc) 2233093.7672
Total 2392081.8376 2392081.8376
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 40
ta = 35
massa steam = Qc / Cp(t2-t1)

= 53336.5283084514
∆T LMTD
Hot fluid
°C F
338.8194 641.8749 Higher Temp.
45.0000 113.0000 Lower Temp.

TLMTD 
Thin Tcout
ln
∆T LMTD = 170.7589973339

Cold fluid = water

T = 464.9097
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0 0
H2SO4 2.1283594777 0.0232915076
NH4HSO4 89.2508467348 0.9767084924
Total 91.3792062125 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 413.1679
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 1
BWG = 16
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 98.6363465264

SHELL
ID shell = 17 1/4
Baffle space = 13
Pass = 1

Tube Side = hot fluid (produk reaktor esterifikasi)

A = L.a".Nt
= 435.6352
= 28.4527922672
SHELL (water)
Pitch = 1 1/4
= 0.25
ID S  C ' B
aS 
144  PT

= 379359.986415637
De  G S
Re S 

Pada, ta = 95
μ = 1.7793839869
De = 0.72
= 0.06
= 12791.8422062237
Dari fig. 28 Kern
jH = 70
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, ta = 95
k = 0.3580266988
c = 4.1861643547
= 0.9998481787
μ = 1.7794
((𝑐 . = 1.7064599811
𝜇)/𝑘)^(1/3
)
((𝑐 .
𝜇)/𝑘)^(1/3
)
ho = 712.7846058573
hio.ho
Uc 
hio  ho
Uc = 174.4222417811

∗𝑈𝑑)
Rd = 0.0294127217
Required surface
Q
A
UD  ΔTLMTD
A= 435.64


SHELL (water)
Re shell (Res) = 12791.8422062237
f = 0.002
ρ = 63.5772431591
s = 1.0172358905
N+1 = 12 L/B
= 14.84
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 1.44547
suhu 338.8194°C menjadi 45°C
COOLER
HEATER
kg/jam
0
0
0
0
0
208.5792288192
10263.8473744992
10472.4266033183
kg/jam
lb/jam
°C = 641.87492 °F
°C = 113 °F
°C = 377.43746 °F
°C = 641.87492 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 113 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
2233093.76721824 kJ/jam
2116564.23516349 Btu/jam
atm
°C = 86 °F
°C = 104 °F
°C = 95 °F
kg/jam = 117586.777039378 lb/jam
Cold fluid
Difference
°C F
40.00 104.00 537.87
30.00 86.00 27.00
18.00 -510.87
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
30 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
≈ 104 buah
SHELL
in 1.078125 ft
in (0.2-1 )ID
reaktor esterifikasi)
ft2
Btu/jam.ft2.ºF
LL (water) TUBE (
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
°F 𝜇)/𝑘)^(1/3
Btu/ft hr F )
Btu/lb ° F
(𝜇/𝜇_𝑤 )^0.14
lb/ft jam
hi
Btu/jam ft2 F
hio
Btu/jam ft2 F
ft2
1266.3813953488 lin ft
LL (water) TUBE (Produk

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5,22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 45 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 611.8194 K
= 318 K
= 464.9097 K
= 611.8194 K
= 298 K

35696.5543274654 0
26611.7116486667 0
79086.355337383 0
96041.2013354596 0
68449.0536426269 0
49208.6096883161 104733.610816862
25628.3084185969 2287348.22673974
2392081.8375566
= 318 K
= 298 K

1616.2479200853 0
1507.2078500789 0
3712.699808416 0
4950.579460256 0
3627.8219535467 0
2828.0287944747 6019.0618880606
1713.9222096668 152969.008450297
158988.070338358
= 303 K
= 313 K
= 308 K
μ, Cp μ . Xi, Cp
0.0912167204 0
0.1420885498 0
0.1304172297 0
0.5990593382 0
0.5990593382 0
3.2854501934 0.0765230882
14.1119965205 13.783306846
13.8598299342
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 6
= 0.594 in2
= 0.0715 ft2
= w/at
= 322905.190744163 lb/ft2 jam
= 377.43746 °F
= 0.0725 ft
= 33.5281482758 lb/ft jam
= 698.2379741448
= 220.6896551724
= 2.5 (Kern, Fig.24)
= 0.7281580372 kJ/kg K
= 0.1739175593 Btu/lb ° F
= 8.8444298928 Btu/ft hr F
= 0.8703509057
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 265.4399161143 Btu/jam ft2 F

= 230.9327270194 Btu/jam ft2 F

= 698.2379741448
= 0.0007 (Fig.26, Kern)

= 123.9718062139 lb/ft3
= 1.9835488994
= 0.9334002329 psi
= 322905.190744163 lb/ft2 jam

= 0.014 (Fig.27 Kern)
= 0.1693933535
 ΔP t  ΔP R
= 1.1027935865 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
T = 308 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 308 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 308 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 308 K
H2O 18 -36.826 4.29E-01
T = 464.9097 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 464.9097 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 308 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 464.9097 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3509583853 18 4.1861643547

0.6192348176 0.3580266988
D μ, Cp
-1.26E-05 0.7355598419
-1.62E-05 93.7692032 0.0093769203
Cp=Joule/mol.K)
D
1.46E-06 108.746684239 32 0
5.35E-07 81.5951133412 18 0
3.78E-06 241.3418501178 100 0
3.62E-06 298.4514444502 85 0
2.77E-06 218.2477592847 183 0
1.03E-06 157.4452100018 98 0.0232915076
5.51E-09 81.3291813289 115 0.9767084924
1

0.1363897283 0 0.0788572651 0
0.6711367618 0 0.3880351563 0
0.0803022255 0 0.0464288181 0
0.1841951403 0 0.1064972061 0
0.1357677338 0 0.0784976428 0
0.3747927527 0.0232915076 0.2166961679 0.0050471804
15.6529762779 0.9767084924 9.0501749307 8.8393827123
1 9.965187187 8.8444298928
 T n
 1 
 TC 
  AB

647.13 1.01841 1018.409097827
512.58 0.57495 0.00000 574.952820672
647.13 0.85488 0.00000 854.8779380414
553 0.69777 0.00000 697.7730391772
647 0.75737 0.00000 757.3739917032
741 0.77535 0.00000 775.3484195679
925 1.61874 0.02329 1618.7394699506
882 1.99459 0.97671 1994.5907255494
1.00000 7273.65640
Cp (kJ/kg K) Cp.xi
3.3983338825 0
4.5330618523 0
2.4134185012 0
3.5111934641 0
1.1926107065 0
1.6065837755 0.037419758
0.7072102724 0.690738279
17.3624124545 0.728158037
xi.ρ (kg/m3)
0
0
0
0
0
37.7028826981
1948.1337004679
1985.83658
COOLER
Fungsi : Menurunkan suhu produk MD-03 ke dekanter dari suhu 117°C menjadi 4
T1 = 117.82 °C
t2 = 40 °C
Umpan
CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784
massa umpan = 9370.3527065479

= 20658.0669839096
T1 = 117.82
T2 = 45
Ta = 81.41
Panas masuk
T = 117.82
Tref = 25
CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784
Panas keluar
T = 45
Tref = 25
CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784

=
=
Neraca Panas
CH3OH 10408.0355 2132.4134
H2 O 154199.6804 33230.2142
C5 H 8 O 2 1610638.4992 331361.6016
C4H7NO 1737.3904 360.6885
C4H7NOH2SO4 0.0000 0.0000
H2SO4 0.0000 0.0000
NH4HSO4 0.0000 0.0000
Total 1776983.6056 1776983.6056
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 40
ta = 35

= 33674.8516270461
∆T LMTD
Hot fluid
°C F
117.8200 244.0760 Higher Temp.
45.0000 113.0000 Lower Temp.
131.076 Difference

TLMTD 
ThinTcout
ln
∆T LMTD = 68.6829161873

Hot fluid = light organic
Cold fluid = water

T = 354.41
CH3OH 1.319360343 0.0117078121
H2O 22.0475325665 0.1956466028
C5H8O2 89.2508467348 0.7919990552
C4H7NO 0.0728578341 0.0006465298
C4H7NOH2SO4 0 0
H2SO4 0 0
NH4HSO4 0 0
Total 112.6905974784 1
light organic
UD = 75 sampai 150
Dipilih UD =

Q
UDasumsi .T
Q
A= = 243.2057
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 1
BWG = 16
ID = 0.87
a't = 0.594
a" = 0.2618
Jumlah tube
Nt = A/(a".L)
= 58.0609398982

SHELL
ID shell = 13 1/4
Baffle space = 10
Pass = 1

Tube Side = hot fluid (produk MD-03)

A = L.a".Nt
= 242.9504
= 80.0840550321
SHELL (water)
Pitch = 1 1/4
= 0.25
ID S  C ' B
aS 
144  PT
Flow area (as) = 0.1828776042

= 405955.949238918
De  G S
Re S 

Pada, ta = 95
μ = 1.7793839869
De = 0.72
= 0.06
= 13688.6456961554
Dari fig. 28 Kern
jH = 65
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, ta = 95
k = 0.3580266988
c = 4.1861643547
= 0.9998481787
μ = 1.7794
((𝑐 .
= 1.7064599811
𝜇)/𝑘)^(1/3
)
((𝑐 .
𝜇)/𝑘)^(1/3
)
ho = 661.8714197246

hio.ho
Uc 
hio  ho
Uc = 182.4733552069

∗𝑈𝑑)
Rd = 0.007006628
Required surface
Q
A
UD  ΔTLMTD
A= 242.95

�/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒
Required length = 𝑜𝑢𝑡𝑠𝑖𝑑𝑒) =

SHELL (Water)
Re shell (Res) = 13688.6456961554
f = 0.002
ρ = 63.5772431591
s = 1.0172358905
N+1 = 12 L/B
= 19.32
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 1.65525
nter dari suhu 117°C menjadi 45°C
COOLER
HEATER
kg/jam
42.2195309771
396.8555861973
8925.0846734775
6.1929158959
0
0
0
9370.3527065479
kg/jam
lb/jam
°C = 244.076 °F
°C = 113 °F
°C = 178.538 °F
°C = 244.076 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 113 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
1409898.68792116 kJ/jam
1336325.94468937 Btu/jam
atm
°C = 86 °F
°C = 104 °F
°C = 95 °F
kg/jam = 74240.2513940183 lb/jam
Cold fluid
Difference
°C F
40.00 104.00 140.08
30.00 86.00 27.00
18.00 -113.08
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
80 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
≈ 58 buah
SHELL
in 0.828125 ft
in (0.2-1 )ID
ft2
Btu/jam.ft2.ºF
(water) T
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
°F 𝜇)/𝑘)^(1/3
Btu/ft hr F )
Btu/lb ° F (𝜇/𝜇_𝑤 )^0.14
lb/ft jam
hi
Btu/jam ft2 F
hio
Btu/jam ft2 F
ft2
706.2511627907 lin ft
(Water) TUBE (Pro

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5,22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 45 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 390.82 K
= 318 K
= 354.41 K
= 390.82 K
= 298 K

7888.6981868019 10408.0355458449
6993.9654219913 154199.680410455
18046.1985310567 1610638.49924067
23846.3081674601 1737.3903636279
17767.3582238511 0
13544.0245666 0
7857.7841067437 0
1776983.60556059
= 318 K
= 298 K

1616.2479200853 2132.4134102747
1507.2078500789 33230.2141591269
3712.699808416 331361.601573166
4950.579460256 360.6884968617
3627.8219535467 0
2828.0287944747 0
1713.9222096668 0
367084.917639429
= 303 K
= 313 K
= 308 K
μ, Cp μ . Xi, Cp
0.2876561425 0.0033678241
0.3459838174 0.0676905585
0.3173454944 0.2513373318
3.0947073594 0.0020008207
3.0947073594 0
5.5803066664 0
59.3306975737 0
0.324396535
TUBE
OD tube = 1 in
ID tube = 0.87 in
BWG = 16
a't = 0.594 in2
a" = 0.2618 ft2/ft
L = 16 ft
Pitch = 1 1/4 in
Passes = 4
TUBE (Produk MD-03)
= 0.594 in2
= 0.0598125 ft2
= w/at
= 345380.430243002 lb/ft2 jam
= 178.538 °F
= 0.0725 ft
= 0.7847437651 lb/ft jam
= 31908.6080167564
= 220.6896551724
= 105 (Kern, Fig.24)
= 2.406569885 kJ/kg K
= 0.574799342 Btu/lb ° F
= 0.1331181669 Btu/ft hr F
= 1.5019965525
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 289.5726609299 Btu/jam ft2 F

= 251.928215009 Btu/jam ft2 F
TUBE (Produk MD-03)

= 31908.6080167564
= 0.00021 (Fig.26, Kern)

= 55.1266656017 lb/ft3
= 0.8820266496
= 0.4802910616 psi
= 345380.430243002 lb/ft2 jam

= 0.016 (Fig.27 Kern)
= 0.2902406635
 ΔP t  ΔP R
= 0.7705317251 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0833 ft
= 0.0725 ft
T = 308 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 308 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 308 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 308 K
H2O 18 -36.826 4.29E-01
T = 354.41 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 354.41 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 308 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 354.41 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3509583853 18 4.1861643547

0.6192348176 0.3580266988
D μ, Cp
-1.26E-05 0.7355598419
-1.62E-05 93.7692032 0.0093769203
Cp=Joule/mol.K)
D
1.46E-06 85.9052542799 32 0.0117078121
5.35E-07 75.1888854913 18 0.1956466028
3.78E-06 196.4548114613 100 0.7919990552
3.62E-06 259.3045150783 85 0.0006465298
2.77E-06 194.4320254387 183 0
1.03E-06 147.2837018832 98 0
5.51E-09 84.3675113997 115 0
1

0.1832948096 0.0117078121 0.1059766565 0.0012407548
0.6629922433 0.1956466028 0.3833261913 0.0749964671
0.1240277165 0.7919990552 0.0717098468 0.0567941309
0.2322424989 0.0006465298 0.1342770349 8.6814109991413E-05
0.1625055032 0 0.0939567789 0
0.372978488 0 0.2156472036 0
5.7727010245 0 3.3376370836 0
1 4.3425307956 0.1331181669
 T n
 1 
 TC 
  AB

647.13 1.01841 1018.409097827
512.58 0.73198 0.01171 731.9829024428
647.13 0.97426 0.19565 974.2583116973
553 0.86275 0.79200 862.7510767456
647 0.87487 0.00065 874.8726831268
741 0.85910 0.00000 859.0994107999
925 1.76291 0.00000 1762.9085126714
882 2.13390 0.00000 2133.8985587143
1.00000 8199.77146
Cp (kJ/kg K) Cp.xi
2.6845391962 0.031430081
4.1771603051 0.817247223
1.9645481146 1.555920251
3.0506413539 0.001972331
1.0624700844 0
1.5028949172 0
0.7336305339 0
15.1758845052 2.406569885
xi.ρ (kg/m3)
8.5699182973
190.6103289537
683.2980376703
0.5656312967
0
0
0
883.04392
HEATER-01
Fungsi : untuk menaikkan suhu dari tangki penyimpanan H2SO4 ke Reaktor Hidrolisis (R-01)
T ref = 25 °C
T masuk tangki= 30.00 °C
T masuk reaktor= 130 °C
Input HE
Komponen n (kmol/jam) A B
H2SO4 91.37921 26.004 7.03E-01
H2O 10.15325 92.053 -4.00E-02
Total
Output HE
H2SO4 91.37921 26.004 7.03E-01
H2O 10.15325 92.053 -4.00E-02
Total
Neraca Panas disekitar HE-01

Komponen input (kJ/jam) output (kJ/jam)
H2SO4 64106.6088264135 1406327.57591584
H2O 3832.8784589878 80458.156481681
Sub Total 67939.4872854012 1486785.73239752

beban Pemanas 1418846.24511212
Total 1486785.73239752 1486785.73239752
1. Neraca Massa
T= 30.00 C 303.15
T keluar = 130.00 C 403.15
Komponen massa Kg/jam fraksi BM

H2SO4 8955.1622088272 0.98 98
H2O 182.758412425 0.02 18
Total 9137.9206212522 1 116
beban panas = 1418846.24511212 kJ/jam

2. Menghitung kebutuhan steam
digunakan pemanas steam jenuh pada P =
T= 147.76 C= 297.97
λ= 2149.224 kJ/kg 924.00
Steam = Saturated Steam
P= 50.00 Psi
Qr = 1418846.24511212
Kebutuhan Steam 
λ 2149.224
= 660.17 kg/jam
= 1455.394092242 lb/jam
3. Kondisi Operasi
*Fluida dingin T in = 30.00
T out = 130.00
Massa in = 9137.9206212522
= 20145.3276482632
*Fluida panas T in = 147.76

T out = 147.76
Massa steam = 660.17
= 1455.4168429624
Beban panas (Q) = 1418846.24511212

= 1344806.59150343
Menentukan spesifikasi Alat

Fluida panas oF Fluida dingin oF Dt
297.97 T1 - t2 266.00 31.97
297.97 T2 - t1 86.00 211.97
T1  T2
R= = -
t 2  t1
t 2 - t 1
DTLMTD = = 95.16 oF
 t 2 
ln 
 t 

 1 
Tavg =(𝑇_1+ 297.97 oF

𝑇_2)/
2
tavg = ta = t1  t 2
= 176.00 oF
2
5. Menghitung densitas
Densitas = A. B –(1-T/Tc) ^ n
Komponen A B n
H2SO4 0.42169 0.19356 0.2857
H2O 0.3471 0.274 0.28571
# Fluida dingin
T= 353.00 K
Komponen Fraksi massa ρ, kg/m3 x/ρ, kg/m3
H2SO4 0.980 563.63 2E-03
H2O 0.020 410.65 5E-05
Total 1.00 559.46
ρ fluida dingin = 559.46 kg/m3
# Fluida panas
T= 420.76
Komponen ρ, kg/m3
H2O 395.05
ρ fluida panas = 395.05 kg/m3
6. Menghitung viskositas
Log μ = A + B/T + CT + DT2
μ = cp
Komponen A B C
H2SO4 -18.7045 3.50E+03 3.31E-02
H2O -10.2158 1.79E+03 1.77E-02
# Fluida dingin
T= 353.00 K
Komponen Fraksi mol μ, cP μ.x
H2SO4 0.9000 5.71 5.1361
H2O 0.1000 0.35 0.0352
Total 1.00 5.17
viscosity > 0,5 maka termasuk heavy organic
# Fluida panas
T= 420.76 K
Komponen μ, cP
H2O 0.19
7. Menghitung spesific heat

Cp = A + BT + CT2 + DT3 (cair)
Cp = J/mol K
Komponen A B C
H2SO4 26.004 7.03E-01 -1.39E-03
H2O 92.053 -4.00E-02 -2.11E-04
# Fluida dingin
Tref = 298.15 K
T= 353.00 K
Komponen Fraksi mol Cp (j/mol.K) Cp (j/kg.K)
H2SO4 0.9000 147.13 1,501.29
H2O 0.1000 75.17 4,176.26
Total 1.00
# Fluida panas
T= 420.76 K
Komponen Cp (j/mol.K) Cp (j/kg.K)
H2O 34.47 1,915.18
8. Menghitung konduktivitas termal

log10 Kliq = A+B(1-T/C)^2/7 (cair) k = A+BT+CT2
K = W/(m.K)
Komponen A B C
H2SO4 0.1553 1.07E-03 -1.29E-06
H2O -0.2758 4.61E-03 -5.54E-06
# Fluida dingin
T= 353.00 K
Komponen Fraksi mol k (W/m.K) k (Btu/hr.ft.F)
C4H7NO 0.9000 2.70 1.56
H2O 0.1000 0.66 0.38
Total 1.00 1.94
# Fluida panas
T= 420.76 K
Komponen k (W/m.K) k (Btu/hr.ft.F)
H2O 0.03 0.02
9. Jenis heaters yang digunakan

Untuk heaters fluida panas steam dan fluida dingin heavy organic
UD = 6-60 Btu/ft2.oF.jam (tabel 8. Kern hal 840)
diambil Ud = 10.00 Btu/ft2.h.F
A = 𝑄/(𝑈_𝑑. 〖∆ (Kern, hal 87)

𝑇〗 _𝐿𝑀𝑇𝐷 )
= 1344806.59150343
951.5518475579
= 1413.2772638242 ft2 >200 ft2 maka digunakan jenis shell and tube (Kern, 103)
ukuran pipa
Dipilih
Panjang (L) =

Dipilih :
L =
OD =
BWG =
Wall thickness =
ID =
a't =
a" =
Jumlah tube
Nt =
=

Tipe pitch =
ID shell
Baffle space
Pass
Shell Side =
Tube Side =

A =
=
Ud =
=
SHE
Baffle space (B) =
Pitch =
Clearence (C') =
=
ID S  C ' B
aS 
144  PT
Flow area (as) =
Mass velocity (Gs) =

=
De  G S
Re S 

Pada, ta =
μ =
De =
=
Re shell (Res) =
=
Dari fig. 28 Kern
jH =
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho =
hio.ho
Uc 
hio  ho
Uc =

∗𝑈𝑑)
Rd =
Required surface
Q
A
UD  ΔTLMTD
A=
Dari tabel 11, Kern, untuk IPS inner pipe =
Required length = �/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒


SHELL (Steam)
Re shell (Res) = 194.44
f = 0.004
ρ = 24.66
s = 0.39
N+1 = 12 L/B
= 99.10
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 0.001314
C
Steam =
P=
K
K
C
-1.39E-03
-2.11E-04
-1.39E-03
-2.11E-04
298 K
303.00 K
403 K
Beban Panas =
λ=
Kebutuhan Steam 
Kmol
91.38
10.15
101.5324513472
D
 D
1.03E-06
5.35E-07
1.03E-06
5.35E-07
ʃ Cp dT (J/mol.K)
701.5448205724
377.502799167
ʃ Cp dT (J/mol.K)
1418846.24511212 kj/jam
Digunakan pemanas steam jenuh pada suhu 132 C
T=
saturated steam
Qr
λ
=
Fraksi
0.9
0.1
1
132 C =
#REF! kJ/kg
5505.8 kPa
15390.0174
7924.3784
ʃ Cp dT (kJ/kmol.K)
#REF! kg/jam
701.5448205724
377.502799167
1079.0476197395
ʃ Cp dT (kJ/kmol.K)
15390.0174252457
7924.3784045467
23314.3958297925
1344750.49295054
269.6
#REF!
50.00 psi
F
Btu/lb
°C 303.00 K 86.00
°C 403.00 K 266.00
kg/jam
lb/jam
°C 420.76 K 297.97
°C 420.76 K 297.97
kg/jam
lb/jam
kJ/jam
btu/jam
(pers 5.14, Kern)
35.09 C = 308.09 K
147.76 C = 420.76 K
80.00 C = 353.00 K
Tc
925
647.13
D
-1.70E-05 A B
-1.26E-05 -36.826 4.29E-01
D
1.03E-06 Komponen A
5.35E-07 H2O 33.933
Cp.x
1,351.16
417.63
1,768.79
(liquid n solid u/inorganic)
Komponen A B
H2O 0.00053 4.71E-05
k.x
1E+00
4E-02
1.44
nis shell and tube (Kern, 103)
ft,10 ft, 12 ft, 16 ft, 24 ft (Towler dan Sinnott, Chemical Engineering Design Principles, Mc Graw Hill New York, 2008, halaman 80
16 ft
er‟‟ table 10, hal : 843
16 ft
1 in
16
0.065 in
0.87 in
0.594 in2 luas penampang
0.2618 ft /ft
2
A/(a".L)
337.3943047709 ≈ 472 buah
er‟‟, table 9, halaman 841

square pitch
SHELL
= 31 in
= 23 in (0.2-1 )ID
1.94 ft
= 1
hot fluid (steam)

cold fluid (produk reaktor hidrolisis)
L.a".Nt
1977.1136 ft2
d terkoreksi :
Q/(A.∆T LMTD)
7.1482 Btu/jam.ft2.ºF
SHELL (steam)
23 in
1 1/4 in
Pitch - OD
1/4 in
1.00 ft2
Ws/as
1453.902361336 lb/ft2 jam
297.97 °F
0.45 lb/ft jam
0.72 in (Kern, Fig.28)
0.06 ft
Gs.De/μ
194.44
han konveksi (ho)
𝜇)/𝑘)^(1/3)
1500 Btu/jam ft2 F (Kern, p.164)

31.35 Btu/jam ft2 F
−𝑈𝑑)/(𝑈𝑐
0.1079932512 > Rdmin = 0.003 (Tabel 8, Kern hal 840)
1977.1136 ft2
1.00 in maka surface outsi 0.34 ft2/lin ft (eksternal surface
�/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒 = 5747.423255814 lin ft

SHELL (Steam) T
Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5,22  10  Ds  
∆Pt
psi < 10 psi Gt
V2/2g'
∆Pr
∆PT
Q= n ʃ Cp dT (kJ/jam)
64106.6088264135
3832.8784589878
67939.4872854012
Q= n ʃ Cp dT (kJ/jam)
1406327.57591584
80458.156481681
1486785.73239752
Btu/jam
F
Btu/lb
°F
°F
°F
°F
C
-1.62E-05
B C D
-8.42E-03 2.99E-05 -1.78E-08 3.69E-12
C
4.96E-08
Mc Graw Hill New York, 2008, halaman 805)
1 1 1/4
16 16
0.065 0.065
0.87 1.12
0.594 0.985
0.2618 0.3271
TUBE
1.94 ft OD tube =
ID tube =
BWG =
a't =
a" =
L =
Pitch =
Passes =
TUBE (heavy organic)
Flow area
a't = 0.594 in2
Nt at'
at  = 1.947 ft2
144  n
Mass velocity (Gt) = w/at
= 10346.86 lb/ft2 jam
D G t
Re 

Pada Ta = 176.00 °F
D = 0.0725 ft
μ = 12.51 lb/ft jam
Ret = 59.96
L/D = 220.6896551724
jH = 1.2
c = 0.422741 Btu/lbF
k = 1.44 Btu/ft hr F
((𝑐 . = 1.542311957
𝜇)/𝑘)^(1/3
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi = 36.80 Btu/jam ft2 F
hio = 32.0146035344 Btu/jam ft2 F

ft2/lin ft (eksternal surface per foot length)

= 59.96
= 0.005 (Fig.26, Kern)

= 34.93 lb/ft3
= 0.56
= 0.00405 psi
= 10346.8554947423 lb/ft2 jam
= 0.001 (Fig.27 Kern)

= 0.0071580103
ΔP t  ΔP R
= 0.01 psi < 10 psi

TUBE
1 in = 0.0833333333 ft
0.87 in = 0.0725 ft
16
0.594 in2
0.2618 ft2/ft
16 ft
1 1/4 in
1
(Kern, Fig.24)
HEATER-01
Fungsi : untuk menaikkan suhu dari tangki penyimpanan ACH ke Reaktor Hidrolisis (R-01)
T ref = 25 °C
T masuk tangki= 30.00 °C
T masuk reaktor= 130 °C
Input HE
C4H7NO 89.32 55.844 1.34E+00
H2O 8.61 92.053 -4.00E-02
Total
Output HE
C4H7NO 89.32 55.844 1.34E+00
H2O 8.61 92.053 -4.00E-02
Total
Neraca Panas disekitar HE-01

Komponen input (kJ/jam) output (kJ/jam)
C4H7NO 109710.996449696 2425519.73319347
H2O 3249.6549014402 68215.3753032361
Sub Total 112960.651351136 2493735.1084967

beban Pemanas 2380774.45714557
Total 2493735.1084967 2493735.1084967
1. Neraca Massa
T= 30.00 C 303.15
T keluar = 130.00 C 403.15
Komponen massa Kg/jam fraksi BM

C4H7NO 7592.5148883518 0.98 85
H2O 154.9492834358 0.02 18
Total 7747.4641717875 1 103
beban panas = 2380774.46 kJ/jam

2. Menghitung kebutuhan steam
digunakan pemanas steam jenuh pada P =
T= 138.34 C= 281.01
λ= 2149.22 kJ/kg 924.00
Steam = Saturated Steam
P= 50.00 Psi
Qr = 2380774.46
Kebutuhan Steam 
λ 2149.22
= 1107.74 kg/jam
= 2442.10 lb/jam
3. Kondisi Operasi
*Fluida dingin T in = 30.00
T out = 130.00
Massa in = 7747.46
= 17079.95
*Fluida panas T in = 138

T out = 138
Massa steam = 1107.74
= 2442.14
Beban panas (Q) = 2380774.46

= 2256538.50
Menentukan spesifikasi Alat

Fluida panas oF Fluida dingin oF Dt
281.01 T1 - t2 266.00 15.01
281.01 T2 - t1 86.00 195.01
T1  T2
R= = -
t 2  t1
 t 2 - t 1
DTLMTD = = 70.19 oF
 t 2 
ln 
 t  
 1 
Tavg = (𝑇_1+ 281.01 oF

𝑇_2)/
2
tavg = ta = t1  t 2
= 176.00 oF
2
5. Menghitung densitas
Densitas = A. B –(1-T/Tc) ^ n
Komponen A B n
C4H7NO 0.28033 0.23985 0.2857
H2O 0.3471 0.274 0.28571
# Fluida dingin
T= 353.00 K
Komponen Fraksi massa ρ, kg/m3 x/ρ, kg/m3
C4H7NO 0.980 337.42 3E-03
H2O 0.020 410.65 5E-05
Total 1.00 338.63
ρ fluida dingin = 338.63 kg/m3
# Fluida panas
T= 411.34
Komponen ρ, kg/m3
H2O 397.18
ρ fluida panas = 397.18 kg/m3
6. Menghitung viskositas
Log μ = A + B/T + CT + DT2
μ = cp
Komponen A B C
C4H7NO -2.3289 1.00E+03 2.83E-04
H2O -10.2158 1.79E+03 1.77E-02
# Fluida dingin
T= 353.00 K
Komponen Fraksi mol μ, cP μ.x
C4H7NO 0.9121 3.18 2.8997
H2O 0.0879 0.35 0.0310
Total 1.00 2.93
viscosity > 0,5 maka termasuk heavy organic
# Fluida panas
T= 411.34 K
Komponen μ, cP
H2O 0.20
7. Menghitung spesific heat

Cp = A + BT + CT2 + DT3 (cair)
Cp = J/mol K
Komponen A B C
C4H7NO 55.844 1.34E+00 -3.44E-03
H2O 92.053 -4.00E-02 -2.11E-04
# Fluida dingin
Tref = 298.15 K
T= 353.00 K
Komponen Fraksi mol Cp (j/mol.K) Cp (j/kg.K)
C4H7NO 0.9121 258.93 3,046.26
H2O 0.0879 75.17 4,176.26
Total 1.00 7,222.52
# Fluida panas
T= 411.34 K
Komponen Cp (j/mol.K) Cp (j/kg.K)
H2O 34.40 1,910.85
8. Menghitung konduktivitas termal

log10 Kliq = A+B(1-T/C)^2/7 (cair) k = A+BT+CT2
K = W/(m.K)
Komponen A B C
C4H7NO -1.4284 9.97E-01 6.47E+02
H2O -0.2758 4.61E-03 -5.54E-06
# Fluida dingin
T= 353.00 K
Komponen Fraksi mol k (W/m.K) k (Btu/hr.ft.F)
C4H7NO 0.9121 0.23 0.13
H2O 0.0879 0.66 0.38
Total 1.00 0.52
# Fluida panas
T= 411.34 K
Komponen k (W/m.K) k (Btu/hr.ft.F)
H2O 0.03 0.02
9. Jenis heaters yang digunakan

Untuk heaters fluida panas steam dan fluida dingin heavy organic
UD = 6-60 Btu/ft2.oF.jam (tabel 8. Kern hal 840)
diambil Ud = 20.00 Btu/ft2.h.F
A = 𝑄/(𝑈_𝑑. 〖∆ (Kern, hal 87)

𝑇〗 _𝐿𝑀𝑇𝐷 )
= 2256538.50
1403.87
= 1607.37 ft2 > 200 ft2 maka digunakan jenis shell n tube (Kern, 103)
ukuran pipa
Dipilih
Panjang (L) =

Dipilih :
L =
OD =
BWG =
Wall thickness =
ID =
a't =
a" =
Jumlah tube
Nt =
=

Tipe pitch =
ID shell =
Baffle space =
Pass =
Shell Side =
Tube Side =

A =
=
Ud =
=
Baffle space (B) =

Pitch =
Clearence (C') =
=
ID S  C 'B
aS 
144  PT
Flow area (as) =
Mass velocity (Gs) =

=
De  G S
Re S 

Pada, ta =
μ =
De =
=
Re shell (Res) =
=
Dari fig. 28 Kern
jH =
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
untuk steam
ho =
hio.ho
Uc 
hio  ho
Uc =

∗𝑈𝑑)
Rd =
Required surface
Q
A
UD  ΔTLMTD
A=
Dari tabel 11, Kern, untuk IPS inner pipe =
Required length = �/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒

Surface actual = #DIV/0!

= #DIV/0!
Ud koreksi =
𝑈_𝐷=𝑄/(� .
∆𝑇𝐿𝑀𝑇𝐷)
= #DIV/0!
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) =

SHELL (Steam)
Re shell (Res) = 213.96
f = 0.0023
ρ = 21.14
s = 0.34
N+1 = 12 L/B
= 83.03
2
f  G S  D S  (N  1)
ΔP S 
10
5,22  10  De  s
∆Ps = 0.00
C
C
-3.44E-03
-2.11E-04
-3.44E-03
-2.11E-04
298 K
303 K
403 K
Beban Panas =
D
D
 3.62E-06
5.35E-07
3.62E-06
5.35E-07
Digunakan pemanas steam jenuh pada suhu 132 C
Steam =
P=
K
K
Kebutuhan Steam 
Kmol
89.32
8.61
97.9319980931
T=
λ=
saturated steam
Qr
λ
=
Fraksi
0.9120992761
0.0879007239
1
ʃ Cp dT (J/mol.K
2,380,774.46 kj/jam
132 C =
2,149.22 kJ/kg
5505.8 kPa
1228.2406
377.5028
ʃ Cp dT (J/mol.K
27154.2671
7924.3784
1,107.74
50.00 psi
F
Btu/lb
°C 303.00 K
°C 403.00 K
kg/jam
lb/jam
°C 411.34 K
°C 411.34 K
kg/jam
lb/jam
kJ/jam
btu/jam
(pers 5.14, Kern)
21.22 C = 294.22
138.34 C = 411.34
80.00 C = 353.00
Tc
647
647.13
D
-8.15E-07 A
-1.26E-05 -36.826
D
3.62E-06 Komponen
5.35E-07 H2O
Cp.x
2,778.49
367.10
3,145.59
(liquid n solid u/inorganic)
Komponen A
H2O 0.00053
k.x
1E-01
3E-02
0.16
*Ud koreksi :
*A
Ud A(ft2)
60.00 535.79
- #DIV/0!
200.00 160.74
(Kern, 103)
(Towler dan Sinnott, Chemical Engineering Design Principles, Mc Graw Hill New York, 2008, halaman
16 ft
16 ft
1 1/2 in
16
0.065 in
1.37 in
1.47 in2 luas penampang
0.3925 ft /ft
2
A/(a".L)
255.9500550338 ≈ 260
triangular pitch
SHELL
37 in
28 in (0.2-1 )ID
2.31 ft
1
heavy organics
hot fluid (steam)
L.a".Nt
1632.8 ft2
Q/(A.∆T LMTD)
20 Btu/jam.ft2.ºF
SHELL (steam)
28 in
1 7/8 in
Pitch - OD
3/8 in
1.43 in2 0.0099030671
Ws/as
1712.529654974 lb/ft2 jam
281.01 °F
0.48 lb/ft jam
0.72 in (Kern, Fig.28)
0.06 ft
Gs.De/μ
213.96
1500 Btu/jam ft2 F (Kern, p.164)

12.07 Btu/jam ft2 F
(0.03) > Rdmin = 0.003
#DIV/0! ft2
- in maka surface outside = 0.34
= #DIV/0! lin ft
x ft2/lin ft (eksternal surface per foot length)

ft2
Btu/jam.ft2.F
#DIV/0! Rd min = 0.0030

SHELL (Steam)
(Kern fig. 29, p.839)

lb/ft3
psi < 10 psi

ʃ Cp dT (kJ/kmol.K) Q= n ʃ Cp dT (kJ/jam)
1228.2405547246 109710.996449696
377.502799167 3249.6549014402
1605.7433538917 112960.651351136
ʃ Cp dT (kJ/kmol.K) Q= n ʃ Cp dT (kJ/jam)
27154.2671108546 2425519.73319347
7924.3784045467 68215.3753032361
35078.6455154013 2493735.1084967
2,256,538.50 Btu/jam
269.6 F
923.9513976 Btu/lb
kg/jam
86.00 °F
266.00 °F
281.01 °F
281.01 °F
K
B C
4.29E-01 -1.62E-05
A B C
33.933 -8.42E-03 2.99E-05
B C
4.71E-05 4.96E-08
ering Design Principles, Mc Graw Hill New York, 2008, halaman 805)
penampang
permukaan per linear pipa
buah
2.31 ft OD tube
ID tube
BWG
a't
a"
L
Pitch
Passes
Flow area
a't =
Nt at'
at  =
144  n
Mass velocity (Gt) =
=
ft2
D G t
Re 

Pada Ta =
D =
μ =
Ret =
L/D =
jH =
c =
k =
((𝑐 . =
𝜇)/𝑘)^(1/3
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi =
hio =
(Tabel 8, Kern hal 840)
ft2/lin ft (eksternal surface per foot length ft2/lin ft (eksternal surface per foot length)
Ret = 414.52
f = 0.0001
ρ = 24.80
s = 0.40
2
 Gf t  nL
Pt 
10
5,2 10  Ds
∆Pt = 0.00
Gt = 25,740.58
V2/2g' = 0.097
∆Pr = 3.9120653679
∆PT = 3.91
D E
-1.78E-08 3.69E-12
TUBE
= 1 1/2 in = 0.1250 ft
= 1.37 in = 0.114167 ft
= 16
= 1.47 in2
= 0.3925 ft2/ft
= 16 ft
= 1 7/8 in
= 4
1.47 in2
0.6635416667 ft2
w/at
25740.58 lb/ft2 jam
176.00 °F
0.1141666667 ft
7.09 lb/ft jam
414.52
140.1459854015
3 (Kern, Fig.24)
0.751795 Btu/lbF
0.16 Btu/ft hr F
3.2422260146
13.32 Btu/jam ft2 F
12.1684330405 Btu/jam ft2 F

s)
(Fig.26, Kern)
lb/ft3
psi
lb/ft2 jam
(Fig.27 Kern)
psi < 10 psi

COOLER
T1 = 284 °C
t2 = 45 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
massa umpan = 6949.9555966843

= 15322.0111075622
T1 = 284
T2 = 130
Ta = 207
Panas masuk
T = 284
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908

=
=
Neraca Panas
Komponen Q masuk (kJ/jam) Q keluar (kJ/jam)
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 21156.7842783541 7859.0873780406
H2SO4 2743705.80899241 1059094.15887388
NH4HSO4 25025.460764217 10404.4781241857
Total 2789888.05403498 2789888.05403498
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 27268.7228059437
∆T LMTD
Hot fluid
°C F
284.0000 543.2000 Higher Temp.
130.0000 266.0000 Lower Temp.
277.2 Difference

TLMTD 
Thin Tcout
ln
Thout Tcin
∆T LMTD = 287.1593079664

Cold fluid = water

T = 480
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0.3880471597 0.0055137657
H2SO4 68.8169564471 0.9778207673
NH4HSO4 1.1728803012 0.016665467
Total 70.377883908 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 942.0818
UDasumsi .T
ukuran pipa
Dipilih
Panjang (L) = 16

Dipilih :
L = 16
OD = 3/4
BWG = 16
ID = 0.62
a't = 0.302
a" = 0.1963
Jumlah tube
Nt = A/(a".L)
= 299.9496330793

SHELL
ID shell = 21 1/4
Baffle space = 16
Pass = 1

Tube Side = hot fluid (produk MD-04)

A = L.a".Nt
= 948.5216
= 5.9592642334
SHELL (water)
Pitch = 1
= 1/4
ID S  C ' B
aS 
144  PT

= 102244.955780061
De  G S
Re S 

Pada, ta = 99.5
μ = 1.6912416261
De = 0.99
= 0.0825
= 4987.5835135049
Dari fig. 28 Kern
jH = 35
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, ta = 99.5
k = 0.3597410869
c = 4.1837937877
= 0.9992819785
μ = 1.6912
((𝑐 . = 1.6748190447
𝜇)/𝑘)^(1/3
)
((𝑐 .
𝜇)/𝑘)^(1/3
)
ho = 255.6065796475
hio.ho
Uc 
hio  ho
Uc = 35.7177235358

∗𝑈𝑑)
Rd = 0.1398086457
Required surface
Q
A
UD  ΔTLMTD
A= 948.52


SHELL (water)
Re shell (Res) = 4987.5835135049
f = 0.0027
ρ = 63.4328916168
s = 1.0149262659
N+1 = 12 L/B
= 12.05
2
f  G S  D S  (N  1)
ΔP S 
10
5,2  10  De  s
∆Ps = 0.10332575
k reaktor hidrolisis dari suhu 284°C menjadi 130°C
COOLER
HEATER
kg/jam
0
0
0
0
71.0126302281
6744.0617318198
134.8812346364
6949.9555966843
kg/jam
lb/jam
°C = 543.2 °F
°C = 266 °F
°C = 404.6 °F
°C = 543.2 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
1712530.32965887 kJ/jam
1623165.35946629 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 60117.1716724395 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 430.20
30.00 86.00 180.00
27.00 -250.20
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
6 Btu/jam.ft2.ºF
ft
ft
in
in
in
in2 luas penampang
≈ 302 buah
SHELL
in 1.328125 ft
in (0.2-1 )ID
ft2
Btu/jam.ft2.ºF
LL (water) T
in Flow area
in a't
Nt at'
in at 
144  n
Mass velocity (Gt)
ft2
D G t
Re 

lb/ft2 jam Pada Ta
D
μ
Ret
°F
lb/ft jam
ft
jH
((𝑐 .
°F 𝜇)/𝑘)^(1/3
Btu/ft hr F )
Btu/lb ° F
(𝜇/𝜇_𝑤 )^0.14
lb/ft jam
hi
Btu/jam ft2 F
hio
Btu/jam ft2 F
ft2
2757.3302325581 lin ft
LL (water) TUBE (Produk r

Ret
(Kern fig. 29, p.839) f

lb/ft3 ρ
s
2
f  Gt  L  n
Pt 
10
5,22  10  Ds  
∆Pt
psi < 10 psi Gt

V2/2g'
∆Pr
∆PT
T2 = 130 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 557 K
= 403 K
= 480 K
= 557 K
= 298 K

26823.0355509124 0
20936.0391930526 0
59915.2110772504 0
74847.1517730466 0
54521.167720479 21156.7842783541
39869.6186324351 2743705.80899241
21336.7559664106 25025.460764217
2789888.05403498
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 0
20598.9074617384 0
27154.2671108546 0
20252.9181859856 7859.0873780406
15390.0174252458 1059094.15887388
8870.8780543627 10404.4781241857
1077357.7243761
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.0754052296 0
0.1314596888 0
0.1144733696 0
0.5040775239 0
0.5040775239 0.0027793653
3.4411436298 3.3648217046
12.2095595703 0.203478012
3.5710790819
TUBE
OD tube = 3/4 in
ID tube = 0.62 in
BWG = 16
a't = 0.302 in2
a" = 0.1963 ft2/ft
L = 16 ft
Pitch = 1 in
Passes = 2
TUBE (Produk MD-04)
= 0.302 in2
= 0.3166805556 ft2
= w/at
= 48383.1761652769 lb/ft2 jam
= 404.6 °F
= 0.0516666667 ft
= 8.6387545542 lb/ft jam
= 289.3701192145
= 309.6774193548
= 3.3 (Kern, Fig.24)
= 1.6024113919 kJ/kg K
= 0.3827293857 Btu/lb ° F
= 0.3834921823 Btu/ft hr F
= 2.0505111856
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 50.2252554402 Btu/jam ft2 F

= 41.5195444972 Btu/jam ft2 F

= 289.3701192145
= 0.0005 (Fig.26, Kern)

= 99.8777216707 lb/ft3
= 1.5980435467
= 0.0086903882 psi
= 48383.1761652769 lb/ft2 jam

= 0.5 (Fig.27 Kern)
= 2.5030607008
 ΔP t  ΔP R
= 2.511751089 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.0625 ft
= 0.0516666667 ft
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 480 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 480 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 480 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 113.5103616 32 0
5.35E-07 83.38668448 18 0
3.78E-06 250.7902928 100 0
3.62E-06 306.1917248 85 0
2.77E-06 221.622304 183 0.0055137657
1.03E-06 158.7536064 98 0.9778207673
5.51E-09 80.9296607232 115 0.016665467
1

0.1265954839 0 0.0731944682 0
0.66175136 0 0.3826087424 0
0.07383382 0 0.0426889414 0
0.1771506698 0 0.1024242625 0
0.1319705864 0.0055137657 0.0763022234 0.0004207126
0.37260368 0.9778207673 0.2154304986 0.2106524154
17.894012 0.016665467 10.34588796 0.1724190543
1 11.2385370965 0.3834921823
 T n
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.53955 0.00000 539.5488703662
647.13 0.83629 0.00000 836.2853469907
553 0.66878 0.00000 668.7837139012
647 0.73922 0.00000 739.218598237
741 0.76291 0.00551 762.91052967
925 1.59822 0.97782 1598.2233875376
882 1.97439 0.01667 1974.387339695
1.00000 7119.35779
Cp (kJ/kg K) Cp.xi
3.5471988 0
4.6325935822 0
2.507902928 0
3.6022555859 0
1.2110508415 0.006677451
1.6199347592 1.584005849
0.7037361802 0.011728092
17.824672677 1.602411392
xi.ρ (kg/m3)
0
0
0
0
4.2065098823
1562.7760191922
32.9040870377
1599.88662
COOLER
T1 = 284 °C
t2 = 45 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
massa umpan = 6949.9555966843

= 15322.0111075622
T1 = 284
T2 = 130
Ta = 207
Panas masuk
T = 284
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908
Panas keluar
T = 130
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0.3880471597
H2SO4 98 68.8169564471
NH4HSO4 115 1.1728803012
Total 70.377883908

=
=
Neraca Panas
CH3OH - -
H2 O - -
C5 H 8 O 2 - -
C4H7NO - -
C4H7NOH2SO4 21156.7842783541 7859.0873780406
H2SO4 2743705.80899241 1059094.15887388
NH4HSO4 25025.460764217 10404.4781241857
Total 2789888.05403498 2789888.05403498
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 27268.7228059437
∆T LMTD
Hot fluid
°C F
284.0000 543.2000 Higher Temp.
130.0000 266.0000 Lower Temp.
277.2 Difference
(ThinTcout)  (ThoutTcin)
TLMTD 
ThinTcout
ln 
ThoutTcin
∆T LMTD = 287.1593079664

Cold fluid = water

T = 480
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0.3880471597 0.0055137657
H2SO4 68.8169564471 0.9778207673
NH4HSO4 1.1728803012 0.016665467
Total 70.377883908 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 1130
UDasumsi .T

ANULUS


= 1817.5211721711

Lt = 15
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 60.5840390724
= 60.5840390724

ANNULUS (Hot fluid)
2
= 0.0204330267

= 0.1312403361

= 749864.978767815
Pada, Ta = 404.6
μ = 8.6387545542

= 11391.9814773991
jH = 35
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 404.6
k = 0.3834921823
c = 1.6024113919
= 0.3827293857
μ = 8.6388
((𝑐 . = 2.0505111856
𝜇)/𝑘)^(1/3
)
ho = 209.7101100184
hio.ho
Uc 
hio  ho
Uc = 128.8483348535

1 1
  Rd
UD Uc
1/Ud = 0.01
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 60.83


Lt = 12
Banyak hairpin (Nh)
Nh = 75.730
A terkoreksi
A = 179.14
UD terkoreksi
𝑈_𝐷=𝑄/(� .
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.02393

ANNULUS (Hot Fluid)
Re annulus (Ren) = 11391.9814773991
De' = (ID-Odi)
= 0.0573333333
Ren' = De'.Ga/μ
= 4976.6732592162

f = 0.0108941711
ρ = 99.8777216707
L = 288
g = 418000000
∆ Fa = 14.7591751772
V = 2.0855083992
g' = 32.2
Ft = 0.2026092523
∆ Pa = 10.377423201
k reaktor hidrolisis dari suhu 284°C menjadi 130°C
COOLER
HEATER
kg/jam
0
0
0
0
71.0126302281
6744.0617318198
134.8812346364
6949.9555966843
kg/jam
lb/jam
°C = 543.2 °F
°C = 266 °F
°C = 404.6 °F
°C = 543.2 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 266 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
1712530.32965887 kJ/jam
1623165.35946629 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 60117.1716724395 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 430.20
30.00 86.00 180.00
27.00 -250.20
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
5 Btu/jam.ft2.ºF
in =
=
in = 0.2916666667 ft
in = 0.2556666667 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
US (Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
1,817.52 lin ft
ft
24 ft
buah ≈ 12 buah
ft
ft2

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft3
ρ
ft
g
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 130 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 557 K
= 403 K
= 480 K
= 557 K
= 298 K

26823.0355509124 0
20936.0391930526 0
59915.2110772504 0
74847.1517730466 0
54521.167720479 21156.7842783541
39869.6186324351 2743705.80899241
21336.7559664106 25025.460764217
2789888.05403498
= 403 K
= 298 K

9015.8629395818 0
7924.3784045467 0
20598.9074617384 0
27154.2671108546 0
20252.9181859856 7859.0873780406
15390.0174252458 1059094.15887388
8870.8780543627 10404.4781241857
1077357.7243761
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.0754052296 0
0.1314596888 0
0.1144733696 0
0.5040775239 0
0.5040775239 0.0027793653
3.4411436298 3.3648217046
12.2095595703 0.203478012
3.5710790819
INNER PIPE
INNER PIPE
= 0.17225 ft
= πD /4
2
= 0.0232909991 ft2
= Wc/Ap
= 2581133.23138774 lb/ft2 jam
= 99.5 °F
= 1.6912416261 lb/ft jam
= (Gp.ID)/μ
= 262883.902711799
= 87.0827285922
= 110
= 4.1837937877 kJ/kg K
= 0.9992819785 Btu/lb ° F
= 0.3597410869 Btu/ft hr F
= 1.6748190447
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 384.7613038028 Btu/jam ft2 F
= 334.1603424203 Btu/jam ft2 F


= 262883.902711799
= 0.0048973431
= 63.4328916168 lb/ft3
= 418000000
= 288 ft
= 0.17225 ft
= 64.8693171726
= 28.5753358713 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1983333333 ft
= 0.17225 ft
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 480 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 480 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 480 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 113.5103616 32 0
5.35E-07 83.38668448 18 0
3.78E-06 250.7902928 100 0
3.62E-06 306.1917248 85 0
2.77E-06 221.622304 183 0.0055137657
1.03E-06 158.7536064 98 0.9778207673
5.51E-09 80.9296607232 115 0.016665467
1

0.1265954839 0 0.0731944682 0
0.66175136 0 0.3826087424 0
0.07383382 0 0.0426889414 0
0.1771506698 0 0.1024242625 0
0.1319705864 0.0055137657 0.0763022234 0.0004207126
0.37260368 0.9778207673 0.2154304986 0.2106524154
17.894012 0.016665467 10.34588796 0.1724190543
1 11.2385370965 0.3834921823
n
 T
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.53955 0.00000 539.5488703662
647.13 0.83629 0.00000 836.2853469907
553 0.66878 0.00000 668.7837139012
647 0.73922 0.00000 739.218598237
741 0.76291 0.00551 762.91052967
925 1.59822 0.97782 1598.2233875376
882 1.97439 0.01667 1974.387339695
1.00000 7119.35779
Cp (kJ/kg K) Cp.xi
3.5471988 0
4.6325935822 0
2.507902928 0
3.6022555859 0
1.2110508415 0.006677451
1.6199347592 1.584005849
0.7037361802 0.011728092
17.824672677 1.602411392
xi.ρ (kg/m3)
0
0
0
0
4.2065098823
1562.7760191922
32.9040870377
1599.88662
COOLER
Fungsi : Menurunkan suhu produk MD-03 ke dekanter dari suhu 124°C menjadi 3
T1 = 124 °C
t2 = 45 °C
Umpan
CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784
massa umpan = 9370.3527065479

= 20658.0669839096
T1 = 124.3663328742
T2 = 35
Ta = 79.6831664371
Panas masuk
T = 124.3663328742
Tref = 25
2 3

CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784
Panas keluar
T = 35
Tref = 25
CH3OH 32 1.319360343
H2O 18 22.0475325665
C5H8O2 100 89.2508467348
C4H7NO 85 0.0728578341
C4H7NOH2SO4 183 0
H2SO4 98 0
NH4HSO4 115 0
Total 112.6905974784

=
=
Neraca Panas
CH3OH 11202.8511837735 1060.1340330662
H2O 165206.437770208 16634.6767439833
C5H8O2 1732499.03534128 164743.94300318
C4H7NO 1866.495992438 179.4319865661
C4H7NOH2SO4 0 0
H2SO4 0 0
NH4HSO4 0 0
Total 1910774.8202877 1910774.8202877
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 27517.5413923268
∆T LMTD
Hot fluid
°C F
124.3663 255.8594 Higher Temp.
35.0000 95.0000 Lower Temp.

TLMTD 
ln
∆T LMTD = 48.4184472704

Cold fluid = water

T = 352.6831664371
CH3OH 1.319360343 0.0117078121
H2O 22.0475325665 0.1956466028
C5H8O2 89.2508467348 0.7919990552
C4H7NO 0.0728578341 0.0006465298
C4H7NOH2SO4 0 0
H2SO4 0 0
NH4HSO4 0 0
Total 112.6905974784 1
light organic
UD = 75 sampai 150
Dipilih UD =

Q
UDasumsi .T
Q
A= = 226
UDasumsi .T

ANULUS


= 362.5893928901

Lt = 15
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 12.0863130963
= 362.5893928901

ANNULUS (Hot fluid)
2
= 0.0204330267

= 0.1312403361

= 1011013.55765419
Pada, Ta = 175.4296995867
μ = 0.7975611989

= 166364.360902501
jH = 35
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 175.4296995867
k = 0.1332880891
c = 2.4026655276
= 0.5738668022
μ = 0.7976
((𝑐 . = 1.5086711744
𝜇)/𝑘)^(1/3
)
ho = 53.6273880162
hio.ho
Uc 
hio  ho
Uc = 46.4907576146

1 1
  Rd
UD Uc
1/Ud = 0.02
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 829.15

Surface actual = 1,333.04 x

= 829.15 ft2
Ud koreksi =
𝑈_𝐷=𝑄/(� .
= 40.80 Btu/jam.ft2.F
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.003

ANNULUS (Hot Fluid)
Re annulus (Ren) = 166364.360902501
De' = (ID-Odi)
= 0.0573333333
Ren' = De'.Ga/μ
= 72677.5291754685

f = 0.005897816
ρ = 55.2570766904
L = 30
g = 418000000
∆ Fa = 4.943074402
V = 5.0823734473
g' = 32.2
Ft = 1.2032850866
∆ Pa = 2.358540678
kanter dari suhu 124°C menjadi 35°C
COOLER
HEATER
kg/jam
42.2195309771
396.8555861973
8925.0846734775
6.1929158959
0
0
0
9370.3527065479
kg/jam
lb/jam
°C = 255.8593991735 °F
°C = 95 °F
°C = 175.4296995867 °F
°C = 255.8593991735 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 95 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
1728156.63452091 kJ/jam
1637976.2368617 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 60665.7221043514 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 142.86
30.00 86.00 9.00
27.00 -133.86
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
150 Btu/jam.ft2.ºF
in =
=
in = 0.2916666667 ft
in = 0.2556666667 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
US (Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
1,333.04 lin ft Dipilih panjang pipa standart

Lt
untuk 1 hairpin
0.62 Banyak hairpin (Nh)
Nh
Panjang pipa total (L)
Rd min = 0.0030

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft 3
ρ
ft
g
D
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 35 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 397.3663328742 K
= 308 K
= 352.6831664371 K
= 397.3663328742 K
= 298 K

8491.1231741255 11202.8511837735
7493.1939559121 165206.437770208
19411.5697354638 1732499.03534128
25618.3293983885 1866.495992438
19099.3574096192 0
14534.4823215045 0
8402.7982944609 0
1910774.8202877
= 308 K
= 298 K

803.5212204627 1060.1340330662
754.4915374905 16634.6767439833
1845.852997818 164743.94300318
2462.768607638 179.4319865661
1797.9214153233 0
1406.8035394173 0
858.406902179 0
182618.185766795
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.2926103749 0.0034258273
0.353692442 0.0691987247
0.321973286 0.2550025383
3.1984629028 0.0020679017
3.1984629028 0
5.7360764412 0
61.1121647236 0
0.3296949921
INNER PIPE
INNER PIPE
= 0.17225 ft
= πD /4
2
= 0.0232909991 ft2
= Wc/Ap
= 2604685.26668 lb/ft2 jam
= 99.5 °F
= 1.6912416261 lb/ft jam
= (Gp.ID)/μ
= 265282.636290966
= 87.0827285922
= 115
= 4.1837937877 kJ/kg K
= 0.9992819785 Btu/lb ° F
= 0.3597410869 Btu/ft hr F
= 1.6748190447
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 402.2504539756 Btu/jam ft2 F
= 349.349448894 Btu/jam ft2 F

pipa standart
= 15 ft
Le = 30 ft
= 44.435 buah ≈
= 30 ft

= 265282.636290966
= 0.0048920224
= 63.4328916168 lb/ft3
= 418000000
= 30 ft
= 0.17225 ft
= 6.873622267
= 3.0278731686 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1983333333 ft
= 0.17225 ft
1 buah
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 352.6831664371 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 352.6831664371 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 352.6831664371 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 85.6804284408 32 0.0117078121
5.35E-07 75.169319506 18 0.1956466028
3.78E-06 195.9995125561 100 0.7919990552
3.62E-06 258.8483298095 85 0.0006465298
2.77E-06 194.0038809778 183 0
1.03E-06 147.0912764241 98 0
5.51E-09 84.4164323132 115 0
1

0.1838759619 0.0117078121 0.1063126648 0.0012446887
0.6617915065 0.1956466028 0.3826319541 0.074860642
0.124686236 0.7919990552 0.072090587 0.0570956768
0.2329583833 0.0006465298 0.134690942 8.7081713325875E-05
0.1629119314 0 0.0941917659 0
0.372700952 0 0.2154867389 0
5.7094841558 0 3.3010866085 0
1 4.3064912613 0.1332880891
n
 T
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.73382 0.01171 733.8218449344
647.13 0.97595 0.19565 975.9509656566
553 0.86494 0.79200 864.9419981832
647 0.87655 0.00065 876.5496839213
741 0.86033 0.00000 860.3256070684
925 1.76509 0.00000 1765.0879200811
882 2.13597 0.00000 2135.9716154308
1.00000 8212.64964
Cp (kJ/kg K) Cp.xi
2.6775133888 0.031347824
4.1760733059 0.817034555
1.9599951256 1.552314288
3.0452744683 0.001968861
1.0601304971 0
1.5009313921 0
0.7340559332 0
15.153974111 2.402665528
xi.ρ (kg/m3)
8.5914482905
190.9414909506
685.0332453789
0.5667155278
0
0
0
885.13290
COOLER
Fungsi : Menurunkan suhu produk MD-04 dari suhu 361°C menjadi 35°C
T1 = 297 °C
t2 = 45 °C
Umpan
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125
massa umpan = 10472.4266033183

= 23087.7211382076
T1 = 361
T2 = 35
Ta = 198
Panas masuk
T = 361
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125
Panas keluar
T = 35
Tref = 25
CH3OH 32 0
H2O 18 0
C5H8O2 100 0
C4H7NO 85 0
C4H7NOH2SO4 183 0
H2SO4 98 2.1283594777
NH4HSO4 115 89.2508467348
Total 91.3792062125

=
=
Neraca Panas
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0 0
H2SO4 113065.502080042 2994.1836464464
NH4HSO4 2440499.92389258 76613.542862454
Total 2553565.42597263 2553565.42597263
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 39392.9763297941
∆T LMTD
Hot fluid
°C F
361.0000 681.8000 Higher Temp.
35.0000 95.0000 Lower Temp.
586.8 Difference
(ThinTcout)  (ThoutTcin)
TLMTD 
ThinTcout
ln 
ThoutTcin
∆T LMTD = 135.0117983006

Cold fluid = water

T = 471
CH3OH 0 0
H2O 0 0
C5H8O2 0 0
C4H7NO 0 0
C4H7NOH2SO4 0 0
H2SO4 2.1283594777 0.0232915076
NH4HSO4 89.2508467348 0.9767084924
Total 91.3792062125 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 232
UDasumsi .T

ANULUS


= 372.3003063314

Lt = 20
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 9.3075076583
= 139.6126148743

ANNULUS (Hot fluid)
2
= 0.0204330267

= 0.1312403361

= 1129921.74457794
Pada, Ta = 388.4
μ = 31.6033558366

= 4692.2646547719
jH = 42
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 388.4
k = 9.3406118361
c = 0.7269089773
= 0.1736192265
μ = 31.6034
((𝑐 . = 0.8375008011
𝜇)/𝑘)^(1/3
)
ho = 2503.4706957089
hio.ho
Uc 
hio  ho
Uc = 1034.1231151088

1 1
  Rd
UD Uc
1/Ud = 0.00
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 68.90

Surface actual = 110.77 x

= 68.90 ft2
Ud koreksi =
𝑈_𝐷=𝑄/(� .
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.003

ANNULUS (Hot Fluid)
Re annulus (Ren) = 4692.2646547719
De' = (ID-Odi)
= 0.0573333333
Ren' = De'.Ga/μ
= 2049.8512992579

f = 0.0142319969
ρ = 123.4650195702
L = 60
g = 418000000
∆ Fa = 5.9686001412
V = 2.542154469
g' = 32.2
Ft = 0.3010504353
∆ Pa = 5.3755731329
suhu 361°C menjadi 35°C
COOLER
HEATER
kg/jam
0
0
0
0
0
208.5792288192
10263.8473744992
10472.4266033183
kg/jam
lb/jam
°C = 681.8 °F
°C = 95 °F
°C = 388.4 °F
°C = 681.8 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 95 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
2473957.69946373 kJ/jam
2344859.16483261 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 86846.5434761906 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 568.80
30.00 86.00 9.00
27.00 -559.80
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
75 Btu/jam.ft2.ºF
in =
=
in = 0.2916666667 ft
in = 0.2556666667 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
US (Hot fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
110.77 lin ft Dipilih panjang pipa standart

Lt
untuk 1 hairpin
0.62 Banyak hairpin (Nh)
Nh
Rd min = 0.0030

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft 3
ρ
ft
g
D
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 130 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 634 K
= 308 K
= 471 K
= 634 K
= 298 K

39847.320234624 0
29152.4826718272 0
88022.008358592 0
105580.721182272 0
74480.49217056 0
53123.310823296 113065.502080042
27344.2775410856 2440499.92389258
2553565.42597263
= 308 K
= 298 K

803.5212204627 0
754.4915374905 0
1845.852997818 0
2462.768607638 0
1797.9214153233 0
1406.8035394173 2994.1836464464
858.406902179 76613.542862454
79607.7265089004
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.0845949723 0
0.1376223004 0
0.1237992461 0
0.5581293172 0
0.5581293172 0
3.3405640133 0.0778067722
13.2960393316 12.9863545302
13.0641613023
INNER PIPE
INNER PIPE
= 0.17225 ft
= πD /4
2
= 0.0232909991 ft2
= Wc/Ap
= 3728759.90605397 lb/ft2 jam
= 99.5 °F
= 1.6912416261 lb/ft jam
= (Gp.ID)/μ
= 379767.671214604
= 116.1103047896
= 580
= 4.1837937877 kJ/kg K
= 0.9992819785 Btu/lb ° F
= 0.3597410869 Btu/ft hr F
= 1.6748190447
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 2028.7414200511 Btu/jam ft2 F
= 1761.9363509435 Btu/jam ft2 F

pipa standart
= 15 ft
Le = 30 ft
= 3.692 buah ≈
= 60 ft

= 379767.671214604
= 0.0046973093
= 63.4328916168 lb/ft3
= 418000000
= 60 ft
= 0.17225 ft
= 27.0517096081
= 11.9164455807 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1983333333 ft
= 0.17225 ft
2 buah
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 471 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 471 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 471 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 110.6123715378 32 0
5.35E-07 82.2882441506 18 0
3.78E-06 245.0350433249 100 0
3.62E-06 301.4829875759 85 0
2.77E-06 219.5884289695 183 0
1.03E-06 157.9689505962 98 0.0232915076
5.51E-09 81.1674578465 115 0.9767084924
1

0.1326636457 0 0.0767029336 0
0.6676525169 0 0.3860206496 0
0.0777178118 0 0.0449345722 0
0.1813712848 0 0.1048645207 0
0.1342406062 0 0.0776146943 0
0.3739797422 0.0232915076 0.2162261047 0.005036232
16.53164573 0.9767084924 9.558200504 9.3355756042
1 10.4645639791 9.3406118361
n
 T
1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.56161 0.00000 561.6124357436
647.13 0.84746 0.00000 847.4626846683
553 0.68639 0.00000 686.3898881655
647 0.75013 0.00000 750.1282593901
741 0.77036 0.00000 770.3640287071
925 1.61049 0.02329 1610.4866492409
882 1.98648 0.97671 1986.4760039221
1.00000 7212.91995
Cp (kJ/kg K) Cp.xi
3.4566366106 0
4.5715691195 0
2.4503504332 0
3.5468586774 0
1.1999367703 0
1.6119280673 0.037544235
0.7058039813 0.689364742
17.5430836596 0.726908977
xi.ρ (kg/m3)
0
0
0
0
0
37.5106620616
1940.2079829412
1977.71865
COOLER
Fungsi : Menurunkan suhu produk reaktor esterifikasi masuk MD-01 dari suhu 13
T1 = 135 °C
t2 = 45 °C
Umpan
CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797
massa umpan = 31010.8727879454

= 68367.1903657602
T1 = 134.6564982889
T2 = 125
Ta = 129.8282491445
Panas masuk
T = 134.6564982889
Tref = 25
2 3

CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797
Panas keluar
T = 125
Tref = 25
CH3OH 32 65.9680171518
H2O 18 27.7940798384
C5H8O2 100 91.0722925865
C4H7NO 85 1.8214458517
C4H7NOH2SO4 183 7.7609431943
H2SO4 98 74.6792799209
NH4HSO4 115 90.423727036
Total 359.5197855797

=
=
Neraca Panas
CH3OH 623673.5667 564016.5706
H2 O 230189.8965 209612.3297
C5 H 8 O 2 1966184.5713 1779966.1307
C4H7NO 51786.7896 46976.1388
C4H7NOH2SO4 164620.5250 149233.4282
H2SO4 1202286.2528 1092600.1957
NH4HSO4 837062.1055 764577.0187
Total 5075803.7074 5075803.7074
Media Pendindin
P = 1
Cp = 1
t1 = 30
t2 = 45
ta = 37.5

= 7465.0790592411
∆T LMTD
Hot fluid
°C F
134.6565 274.3817 Higher Temp.
125.0000 257.0000 Lower Temp.

TLMTD 
Thin Tcout
ln
∆T LMTD = 166.1444497854

Cold fluid = water

T = 402.8282491445
CH3OH 65.9680171518 0.1834892537
H2O 27.7940798384 0.0773089019
C5H8O2 91.0722925865 0.2533164967
C4H7NO 1.8214458517 0.0050663299
C4H7NOH2SO4 7.7609431943 0.021586971
H2SO4 74.6792799209 0.2077195273
NH4HSO4 90.423727036 0.2515125194
Total 359.5197855797 1
Heavy organic
UD = 5 sampai 75
Dipilih UD =

Q
UDasumsi .T
Q
A= = 178
UDasumsi .T

ANULUS
Inner pipe side = hot fluid (recycle)

Annulus = cold fluid (water)

= 286.6585490978

Lt = 15
Banyak hairpin (Nh)

Nh = L/(2.Lt)
= 9.5552849699
= 28.6658549098

ANNULUS (Cold fluid)
2
= 0.0204330267

= 0.1312403361

= 805444.189158338
Pada, Ta = 99.5
μ = 1.6912416261

= 62502.4623857969
jH = 95
ho = jH.𝑘/𝐷𝑒 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
Pada, Ta = 99.5
k = 0.3597410869
c = 4.1837937877
= 0.9992819785
μ = 1.6912
((𝑐 . = 1.6748190447
𝜇)/𝑘)^(1/3
)
ho = 436.1282355264
hio.ho
Uc 
hio  ho
Uc = 312.7621562579

1 1
  Rd
UD Uc
1/Ud = 0.01
Required surface
Q
A
UD  ΔTLMTD
Q
A
UD  ΔTLMTD
A= 16.57

Ud koreksi =
𝑈_𝐷=𝑄/(� .
Dirt Factor :
(𝑈𝑐 ∗𝑈𝑑) = 0.0061

ANNULUS (Cold fluid)
Re annulus (Ren) = 62502.4623857969
De' = (ID-Odi)
= 0.0573333333
Ren' = De'.Ga/μ
= 27304.6733623709

f = 0.0071172989
ρ = 63.4328916168
L = 40
g = 418000000
∆ Fa = 3.8305717624
V = 3.5271054383
g' = 32.2
Ft = 0.5795251292
∆ Pa = 1.9426749871
asi masuk MD-01 dari suhu 135°C menjadi 125°C
COOLER
HEATER
kg/jam
2110.9765488573
500.2934370913
9107.2292586505
154.8228973971
1420.2526045621
7318.5694322516
10398.7286091355
31010.8727879454 134.6564983
kg/jam
lb/jam
°C = 274.3816969201 °F
°C = 257 °F
°C = 265.69084846 °F
°C = 274.3816969201 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
°C = 257 °F
°C = 77 °F
A B C D
40.152 3.10E-01 -1.03E-03 1.46E-06
92.053 -4.00E-02 -2.11E-04 5.35E-07
42.365 1.08E+00 -3.16E-03 3.78E-06
55.844 1.34E+00 -3.44E-03 3.62E-06
-90.764 1.71E+00 -3.54E-03 2.77E-06
26.004 7.03E-01 -1.39E-03 1.03E-06
95.016 -3.11E-02 9.68E-07 5.51E-09
Qmasuk-Qkeluar
468821.895078457 kJ/jam
444357.362127578 Btu/jam
atm
°C = 86 °F
°C = 113 °F
°C = 99.5 °F
kg/jam = 16457.662595584 lb/jam
Cold fluid
Difference
°C F
45.00 113.00 161.38
30.00 86.00 171.00
27.00 9.62
°F
K
A B C D
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-4.7825 7.35E+02 1.03E-02 -1.13E-05
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-2.3289 1.00E+03 2.83E-04 -8.15E-07
-18.7045 3.50E+03 3.31E-02 -1.70E-05
-0.8508 9.30E+02 -4.76E-12 1.78E-15
15 Btu/jam.ft2.ºF
in =
=
in = 0.2916666667 ft
in = 0.2556666667 ft
in2 =
ft2/ft =
ft2/ft =
ft
ft
≈ 5 buah
pipe. Nh. TLMTD)

Btu/jam.ft2.F
(Cold fluid)
D
ft 2
Flow area (Ap)
lb/ft2 jam Pada Ta

°F
lb/ft jam μ
Re inner pipe (Rep)

L/D
jH
°F k
Btu/ft hr F
kJ/kg K ((𝑐 .
Btu/lb ° F 𝜇)/𝑘)^(1/3
lb/ft jam
)
hi = jH.𝑘/𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
(𝜇/𝜇_𝑤 )^0.14
hi
Btu/jam ft F 2
hio
Btu/jam ft2 F
ft2
26.65 lin ft Dipilih panjang pipa standart

Lt
untuk 1 hairpin
Banyak hairpin (Nh)
Nh
Rd min = 0.0030
(Cold fluid) INNER PIP

Rep
(Eq. (6.4))
ft
(Eq. (3.47b)
f
lb/ft 3
ρ
ft
g
D
ft
∆ Fp
fps
∆Pp
ft
psi < 10 psi

T2 = 125 °C
t1 = 30 °C
〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

= 407.6564982889 K
= 398 K
= 402.8282491445 K
= 407.6564982889 K
= 298 K

9454.1808837933 623673.566698202
8281.9757963246 230189.896502802
21589.2728232911 1966184.57129265
28431.6931887786 51786.789616364
21211.4070241596 164620.524986278
16099.3284088055 1202286.25278023
9257.1068784858 837062.105522922
5075803.70739946
= 398 K
= 298 K

8549.8487748267 564016.57062298
7541.6178867147 209612.329654108
19544.54071728 1779966.13067299
25790.57662448 46976.1388063866
19228.7747037333 149233.428172211
14630.5668299733 1092600.19569752
8455.4910946187 764577.018694805
4606981.812321
= 303 K
= 318 K
= 310.5 K
μ, Cp μ . Xi, Cp
0.1795829388 0.0329515394
0.2120763122 0.0163953868
0.2153424221 0.054549788
1.3655179283 0.0069181644
1.3655179283 0.029477396
3.4567706237 0.71803876
28.6996248272 7.2183149454
8.0766459799
INNER PIPE
INNER PIPE
= 0.17225 ft
= πD /4
2
= 0.0232909991 ft2
= Wc/Ap
= 2935348.12234979 lb/ft2 jam
= 265.69084846 °F
= 19.5381173702 lb/ft jam
= (Gp.ID)/μ
= 25878.3231001164
= 87.0827285922
= 85
= 1.9470675622 kJ/kg K
= 0.4650490977 Btu/lb ° F
= 1.3747488926 Btu/ft hr F
= 1.8766619441
𝐷 ((𝑐.𝜇)/𝑘)^(1/3)
^0.14
= 1273.119355609 Btu/jam ft2 F
= 1105.6881126235 Btu/jam ft2 F

pipa standart
= 20 ft
Le = 40 ft
= 0.666 buah ≈
= 40 ft
= 24.88 ft2
INNER PIPE (Hot fluid)

= 25878.3231001164
= 0.0071997361
= 80.8118758445 lb/ft3
= 418000000
= 40 ft
= 0.17225 ft
= 10.5545545346
= 5.9231482684 psi < 10 psi

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^𝑇𝑖�▒ 〖𝐶𝑝𝑖 𝑑𝑇〗〗
𝑝 𝑑𝑇=�𝑇+𝐵/2 𝑇^2+𝐶/3 𝑇^3+𝐷/4 𝑇^4
= 0.1983333333 ft
= 0.17225 ft
1 buah
T = 310.5 K
Komponen
A B C
H2O 92.053 -4.00E-02 -2.11E-04

T = 310.5 K
Komponen A B C
H2O -0.2758 4.61E-03 -5.54E-06

T = 310.5 K
Komponen A B C
H2O -10.2158 1.79E+03 1.77E-02
Viskositas steam
T = 310.5 K
H2O 18 -36.826 4.29E-01
T = 402.8282491445 K
Komponen
A B C
CH3OH 40.152 3.10E-01 -1.03E-03
H2O 92.053 -4.00E-02 -2.11E-04
C5H8O2 42.365 1.08E+00 -3.16E-03
C4H7NO 55.844 1.34E+00 -3.44E-03
C4H7NOH2SO4 -90.764 1.71E+00 -3.54E-03
H2SO4 26.004 7.03E-01 -1.39E-03
NH4HSO4 95.016 -3.11E-02 9.68E-07
Total
T = 402.8282491445 K
Komponen A B C
CH3OH -1.1793 6.19E-01 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
C5H8O2 -1.8863 1.30E+00 5.64E+02
C4H7NO -1.4284 9.97E-01 6.47E+02
C4H7NOH2SO4 -1.6405 1.03E+00 7.41E+02
H2SO4 0.1553 1.07E-03 -1.29E-06
NH4HSO4 51.6119 -2.96E-01 4.71E-04
Total
Densitas
ta = 310.5 K
Komponen A B n
H2O 0.3471 0.274 0.28571
Ta = 402.8282491445 K
Komponen A B n
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
C5H8O2 0.30985 0.25357 0.28571
C4H7NO 0.28033 0.23985 0.2857
C4H7NOH2SO4 0.28517 0.264 0.29
H2SO4 0.42169 0.19356 0.2857
NH4HSO4 0.75456 0.3 0.28571
Total
Cp=Joule/mol.K)
D
5.35E-07 75.3082881783 18 4.1837937877

0.6221999842 0.3597410869
D μ, Cp
-1.26E-05 0.6991236475
-1.62E-05 94.81665395 0.0094816654
Cp=Joule/mol.K)
D
1.46E-06 93.64439634 32 0.1834892537
5.35E-07 76.666016612 18 0.0773089019
3.78E-06 211.7358063824 100 0.2533164967
3.62E-06 273.4993931216 85 0.0050663299
2.77E-06 205.3173246705 183 0.021586971
1.03E-06 152.1019031788 98 0.2077195273
5.51E-09 83.0130330326 115 0.2515125194
1

0.165684618 0.1834892537 0.0957948667 0.0175773286
0.683210814 0.0773089019 0.3950160833 0.0305382596
0.1053593347 0.2533164967 0.0609162368 0.0154310877
0.2118012141 0.0050663299 0.1224583749 0.0006204145
0.1509847947 0.021586971 0.0872957819 0.0018844515
0.3776384085 0.2077195273 0.2183414576 0.0453537844
8.6876400506 0.2515125194 5.0229848175 1.2633435662
1 6.0028076188 1.3747488926
n
 T
 1 
 TC 
  AB

647.13 1.01610 1016.0968093939
512.58 0.67513 0.18349 675.1329452187
647.13 0.92493 0.07731 924.9261696764
553 0.79755 0.25332 797.546932084
647 0.82613 0.00507 826.1292853913
741 0.82379 0.02159 823.7854012093
925 1.70094 0.20772 1700.9396155211
882 2.07456 0.25151 2074.5605330605
1.00000 7823.02088
Cp (kJ/kg K) Cp.xi
2.9263873856 0.536960637
4.2592231451 0.329275864
2.1173580638 0.536361727
3.2176399191 0.016301625
1.1219525938 0.024219558
1.5520602365 0.322393219
0.7218524612 0.181554931
15.9164738051 1.947067562
xi.ρ (kg/m3)
123.8796402766
71.5050265263
202.0317948096
4.1854435284
17.783031587
353.3183729271
521.777946264
1294.48126

Heater Metanol

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Heater Metanol

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HEATER

massa umpan = 7747.4641717875

Beban steam (Qs) =

(Thin Tcout)  (Thout  Tcin)

Menentukan Koefisien Perpindahan Panas

Menentukan viskositas umpan log vis =A+B/T+CT+DT2

luas transfer massa dan jumlah pipa :

Panjang tabung standart, 6 ft, 8 ft,10 ft, 12 ft, 16 ft, 24 ft

Kern D.Q, „‟Process Heat Transfer‟‟ table 10, hal : 843

Kern D.Q, „‟Process Heat Transfer‟‟, table 9, halaman 841

Shell Side = hot fluid (steam)

Koreksi luas tranfer panas (A)

Mass velocity (Gs) = Ws/as

Dirt Factor (Rd)

Dari tabel 11, Kern, untuk IPS inner pipe = 1.00

Required length = �/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒 =

Menentukan Pressure Drop

m) pada suhu 281.01

kg/jam = 2504.2016496472 lb/jam

Btu/jam.ft2.ºF (Kern, tabel 8, p.840)

> Rdmin = 0.003 (Tabel 8, Kern hal 840)

L (Steam) TUBE (Produk

(Kern fig. 29, p.839) f

psi < 10 psi Gt

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒

∫ Cp dT, kJ/kmol Q masuk (kJ/jam)

∫ Cp dT, kJ/kmol Q keluar (kJ/jam)

= 69.9326805188 Btu/jam ft2 F

= 60.8414320514 Btu/jam ft2 F

rnal surface per foot length)

TUBE (Produk reaktor hidrolisis)

= 0.0004 (Fig.26, Kern)

= 238884.118355332 lb/ft2 jam

= 0.7364868948 psi < 10 psi

HEAT CAPACITY OF LIQUID

Thermal conductivity of liquid

k liquid (W/mK) xi k liquid (BTU/ft h F) k.x

Tc density ρ (g/ml) ρ (kg/m3)

massa umpan = 9137.9206212522

Beban steam (Qs) =

(ThinTcout)  (Thout Tcin)

Menentukan Koefisien Perpindahan Panas

Menentukan viskositas umpan log vis =A+B/T+CT+DT2

luas transfer massa dan jumlah pipa :

Panjang tabung standart, 6 ft, 8 ft,10 ft, 12 ft, 16 ft, 24 ft

Kern D.Q, „‟Process Heat Transfer‟‟ table 10, hal : 843

Kern D.Q, „‟Process Heat Transfer‟‟, table 9, halaman 841

Shell Side = hot fluid (steam)

Koreksi luas tranfer panas (A)

Mass velocity (Gs) = Ws/as

Dirt Factor (Rd) 𝑅𝑑=(𝑈𝑐 −𝑈𝑑)/(𝑈𝑐

Dari tabel 11, Kern, untuk IPS inner pipe = 1.00

Required length = �/(𝑠𝑢𝑟𝑓𝑎𝑐𝑒 =

Menentukan Pressure Drop

m) pada suhu 281.01

kg/jam = 1492.403909552 lb/jam

Btu/jam.ft2.ºF (Kern, tabel 8, p.840)

> Rdmin = 0.003 (Tabel 8, Kern hal 840)

L (Steam) TUBE (Produk

(Kern fig. 29, p.839) f

psi < 10 psi Gt

〖∆𝐻〗 _ =∑▒ 〖� _𝑖 ∫_𝑇𝑟𝑒𝑓^

∫ Cp dT, kJ/kmol Q masuk (kJ/jam)

∫ Cp dT, kJ/kmol Q keluar (kJ/jam)