1.

Uji Kadar Air

Kode KM1 Berat Sampel KM2 X Y Z

Sampel
--------------------------------------------- g ---------------------------------------------
U1 0,2447 1,0016 0,2466 8,9994 0,9997 9,8570
U2 0,2309 1,0003 0,2313 8,9868 0,9999 9,8453
Keterangan : KM : Kertas Minyak
Y : Sampel Sesungguhnya
X : Botol Timbang
Z : Botol Timbang Setelah Oven

U 1 = (KM 1 + Sampel) - KM 2 = (0,2447 + 1,0016) - 0,2466

= 0,9997 g

U 2 = (KM 1 + Sampel) - KM 2 = (0,2309 + 1,0003) - 0,2313

= 0,9999 g

(X + Y) - Z (8,9994 + 0,9997) - 9,8570

Kadar Air U1 = × 100% = × 100%
Y 0,9997

= 14,2142%

(X + Y) - Z (8,9868 + 0,9999) - 9,8453

Kadar Air U2 = × 100% = × 100%
Y 0,9999

= 14,1414 %

U1+U2 14,2142 + 14,1414

Rata-rata Kadar Air = = = 14, 1778%
2 2

Kadar Bahan Kering (BK)

Kadar BK U1 = 100% - Kadar Air U1 = 100% - 14,2142% = 85,7858%

Kadar BK U2 = 100% - Kadar Air U2 = 100% - 14,1414% = 85,8586%

U1+U2 85,7858+ 85,8586

Rata-rata Kadar BK = = = 85,8222%
2 2
2. Uji Kadar Abu

Kode KM1 Berat Sampel KM2 Y X Z

Sampel
--------------------------------------------- g ---------------------------------------------
U1 0,2283 1,0011 0,2299 0,9995 13,8151 13,8898
U2 0,2255 1,0012 0,2279 0,9988 14,3528 14,4240
Keterangan : KM : Kertas Minyak
Y : Sampel Sesungguhnya
X : Crusible Porselin
Z : Crusible Porselin Setelah Tanur

U 1 = (KM 1 + Sampel) - KM 2 = (0,2283 + 1,0011) - 0,2299

= 0,9995 g

U 2 = (KM 1 + Sampel) - KM 2 = (0,2255 + 1,0012) - 0,2279

= 0,9988 g

Z-X 13,8898 - 13,8151

Kadar Abu U1 = × 100% = × 100%
Y 0,9995

= 7,4737%

Z-X 14,4240 - 14,3528

Kadar Abu U2 = × 100% = × 100%
Y 0,9988

= 7,1285%

U1 + U2 7,4737 + 7,1285
Rata-rata Kadar Abu = = = 7,3011%
2 2

Konversi Kadar Abu (100% BK)

100 100
Kadar Abu U1 = × kadar Abu U1 = × 7,4737%
BK 85,7858

= 8,7120%

100 100
Kadar Abu U2 = × kadar Abu U2 = × 7,1285%
BK 85,8586
 = 8,3026%

8,7120 + 8,3026
Rata-rata Kadar Abu = = 8,5073%
2
3. Uji Kadar Serat Kasar

Kode KM1 Berat Sampel KM2 X a Y Z

Sampel
--------------------------------------------- g ---------------------------------------------
U1 0,2546 1,0010 0,2867 0,9689 1,0192 23,9995 22,4277
U2 0,2737 1,0011 0,3006 0,9742 1,0160 22,8730 21,3289
Keterangan : KM : Kertas Minyak
X : Sampel Sesungguhnya
Y : Crusible Porselin + Sampel Setelah Oven
Z : Crusible Porselin + Sampel Setelah Tanur
a : Berat Kertas Saring

U 1 = (KM 1 + Sampel) - KM 2 = (0,2546 + 1,0010) - 0,2867

= 0,9689g

U 2 = (KM 1 + Sampel) - KM 2 = (0,2737 + 1,0011) - 0,3006

= 0,9742g

Y-Z-a 23,9995 - 22,4277 - 1,0192

Kadar Serat Kasar U1 = × 100% = × 100%
X 0,9689

= 57,0337%

Y–Z-a 22,8730 – 21,3289 - 1,0160

Kadar Serat Kasar U2 = × 100% = × 100%
X 0,3006

= 54,2085%

U1 + U2 57,0337% + 54,2085%
Rata-rata Kadar Serat Kasar = = = 55,6211%
2 2

Konversi Kadar Serat Kasar (100% BK)

100 100
Kadar Serat Kasar U1 = × kadar serat U1 = × 57,0337%
BK 85,7858

= 66,4838%
 100 100
Kadar Serat Kasar U2 = × kadar serat U2 = × 54,2085%
BK 85,8586

= 63, 1369%

U1 + U2 66,4838 + 63,1369
Rata-rata Kadar Serat Kasar = =
2 2

= 64,8103%
4. Uji Kadar Lemak Kasar

Kode KM1 Berat Sampel KM2 A B X

Sampel
------------------------------------ g ---------------------------------------
U1 0,8790 1,0016 0,7029 1,7045 1,6912 1,1777
U2 0,8811 1,0007 0,7068 1,7075 1,7037 1,1750
Keterangan : KM : Kertas Minyak
X : Sampel Sesungguhnya
a : Oven 1 sebelum disokhlet
b : Oven 2 setelah disokhlet

a-b 1,7045 - 1,6912

Kadar Lemak Kasar U1 = × 100% = × 100%
X × BK/100 1,0016 × 85,7858/100

= 1,5481%

a-b 1,7075 - 1,7037

Kadar Lemak Kasar U2 = × 100% = × 100%
X × BK/100 1,0007 × 85,8586/100

= 0,4423%

U1 + U2 1,5481 + 0,4423
Rata-rata Kadar Lemak Kasar = =
2 2

= 0,9952%
5. Uji Kadar Protein Kasar

Kode KM1 Berat Sampel KM2 X Titran Titran

Sampel Sampel blanko
---------------------------- g ------------------------ -------- mL -------
U1 0,2308 1,0018 0,2322 1,0004 16 0,2
U2 0,2469 1,0016 0,2487 0,9998 15 0,2
Keterangan : KM : Kertas Minyak
X : Sampel Sesungguhnya

U 1 = (KM 1 + Sampel) - KM 2 = (0,2308 + 1,0018) - 0,2322

= 1,0004 g

U 2 = (KM 1 + Sampel) - KM 2 = (0,2469 + 1,0016) - 0,2487

= 0,9998 g

(titran sampel-titran blangko) × N HCl × 0,014 × 6,25

Kadar Protein Kasar U1 = × 100%
X

(16 - 0,2) × 0,1 × 0,014 × 6,25

= × 100%
1,0004

= 13,8194%

(titran sampel-titran blangko) × N HCl × 0,014 × 6,25

Kadar Protein Kasar U2 = × 100%
X

(15 - 0,2) × 0,1 × 0,014 × 6,25

= × 100%
1,0016

= 12,9293%

U1 + U2 13,8194 + 12,9293
Rata-rata Kadar Protein Kasar = =
2 2

= 13,3743%

Konversi Kadar Protein Kasar (100% BK)

100
Kadar Protein Kasar U1 = × 13,8194% = 16,1091%
85,7858
 100
Kadar Protein Kasar U2 = × 12,9293% = 15,0588%
85,7858

U1 + U2 16,1091 + 15,0588
Rata-rata Kadar Protein Kasar = = = 15,5839%
2 2
6. Bahan Ekstrak Tanpa Nitrogen (BETN)

Kadar BETN U1 = 100% - (kadar abu + serat kasar + lemak kasar + protein kasar)

= 100% - (8,71 + 66,48 + 1,53 + 16,10)

= 100% - 92,82

= 7,18%

Kadar BETN U2 = 100% - (kadar abu + serat kasar + lemak kasar + protein kasar)

= 100% - (8,30 + 63,13 + 0,43 + 15,05)

= 100% - 86,91

= 13,09%

U1 + U2 7,18 + 13,09
Rata-rata Kadar BETN = =
2 2

= 20,27%