Certificate of Analysis 1.00456.2510 Nitric acid 65% for analysis EMSURE® ISO Batch K43039156 Assay (alkalimetric) Chloride (C1 Phosphate (PO4) Sulphate (S04) Ag (Silver) AL(Aluminium) As (Arsenic) Au Gold) Ba (Barium) Be Beryllium) Bi (Bismuth) Ca (Calcium) Cd (Cadmium) Co (Cobalt) Cr(Chromium) Cu (Copper) Fe (Iron) Ga Gallium) Ge (Germanium) In (indium K (Potassium) Li (Lithium) Mg (Magnesium) ‘Mn (Manganese) Mo (Molybdenum) ‘Na (Soutium) 1Ni(Niekel) Ph (Lead) Pe (Platinum) Sr (Strontium) Ti Titanium) ‘TI (Thallium) V (Vanadium) Zn (Zine) Zr Zirconium) Residue on ignition (as SQ4) Tested by the dithizone Spee. Values 2650 <02 $02 <0s 50.010 0.050 $0010 0.050 50.010 0.010 0.020 0.100 0.010 0.010 50.020 0.010 0.100 0.050 50.020 0.020 0.100 0.010 50.050 <0.010 0.010 <0.200 50.020 <0.010 50.100 0.010 50.020 0.020 0.010 0.020 0.020 <3 passes test Ppm pm Ppm ppm Ppm 333 Ppm 333 Batch Values 653 <02 <01 <0s < 0.005 <0.010 <0.002 0.00 < 0.005 < 0.008 <0010 0.050 < 0.005 < 0.008 < 0.005 0.008 0.023 <0.010 <0.010 0.010 <0010 <0.010 <0.010 0.005 1005 <0.200 <0.010 0.010 <0.010 <0.010 <0.010 0.020 <0.010 <0.010 <0.020 <3 passes test Merck KGaA, Frankfurter Strate 250, 64293 Darmstadt (Germany): +49 6151 72-0 EMD Millipore Corporation -a subsidiary of Merck KGaA, Darmstadt, Germany 290 Concord Road, Bilerica, MA 01821, USA, Phone: (978) 715-4321 % pm em ppm pm ppm ppm em ppm em ppm em ppm pm ppm em pom em ppm em pom om Pom em pom om ppm ppm ppm em ppm om ppm em Page 1 of 2Certificate of Analysis 1.00456.2510 Nitric acid 65% for analysis EMSURE® ISO Batch K43039156 Date of release (DD.MMYVYY): 13.12.2011 Date of expiry: see product label 1SO-reagent Dr. Reiner Vogt responsible laboratory manager quality contol This document has been produced electronically and is valid without a signature Merck KGaA, Frankfurter Strafe 250, 64293 Darmstadt (Germany): +49 6151 72.0 EMD Millipore Corporation - a subsidiary of Merck KGaA, Darmstadt, Germany 200 Concord Road, Bilrica, MA 01821, USA, Phone: (978) 715-4321 Page 2 of 2