s BEC em sern-WE 23)" 19 1 - 2.60 CAG 2 ‘ (P22 Q. P. Code: 24241 ‘Time: 3 Hours ‘Total Marks: 80 NB. (1) Question No.1 is compulsory, (2) Atempr any Three out of remaining questions, (3) Assume nny suitable data il) hecessary and! indicate it clearly, (4) Draw neat sketehes wherever required, Subequestions of wn individual question should be grovped andl (5) Answer to the ©. one below the other, written together QI. (@) Explain in brie the purpose of cach of the following process enginecting (04) aetivitie (1) To conduct Mass balance around the process flow sheet (2) Deciding equipment specifications (3) To carry HAZOP study of the process (4) Interact with market analysers (b) What are the common characteristics of PFDs? (04) (©) Explain that, when the vapour recovery system (VRS) should be installed (04) Gn Purge stream, when on gas recycle stream ail when on flash vapour stream, ey r (@) Fite hazard is one of the major accidéits fi*¢hemical process industries, (04) What are the various types / classes of fire? What is the conecpt of fire triangle? (©) In liquid phase catalytic reduction process, what precautions should be (04) taken when Ha is used as reducing agent? : AE. (a) Discuss the common featurs of Nitration process, (05) (b) Draw PPS (block) diagram) for manufacture of monochloro benzene (05) (MCB) from benzene using Clz as chlorinating agent (©) With a suitable extmiple, describe the “Fault Tree Analysis” (FTA), a (10) safety redundangy technique. Q3. (a) Consider thedfeed to distillation column, whose composition and other (14) related data is given below. Feed temperature is 340 K and Pressure is 11250°mm Hg. The key component to be recovered in distillate js Propylene tnd that in residue is trans-2-butene. The recovery of propylene ‘in distillate is 99.5% and that of trans-2-butene in residue is 99%, Then “carryout the mass balance and calculate molar composition of distillate Bnd residue, Component | Composition in Antoine Constants ] feed (gmoVs) Rae ReB Cc Propylene 90 15.893 [1875.3 | -22.91_| Trons-2-butene 20 15.821 | 2213.6 | -33.11 30. 15.816 _|_2209.8 | -36.21 12 15.897] 2189.4 | ~30.52 10 15.833 = 1431 8 15.725 =25.10 Page 1of 3 S9LASICABIBACDSATAIF52499E38EBB -QP, Cog, c% is absorption column to recover acetone ) ha Ser Tatig 100 gpl a air, 10 gmol/s of acetone and 3 forvateayde If water is to be Used as solvent for this opera estimate solvent flow rate at each of the following cond ions and how solvent flow rate changes for different operating conditions: from t, BMol/s ¢ tion, then CONCludg Condition No. 18.3036 QA (a) The shell and tube hheat exchanger is used to heat 7060 kg/h of liquid ‘A’ (19) from 75 to 120K by coating liquid “B° from/160 to'120 K. The overall Viquid *A* and “W* are 2010 IEK and. 2386 IkgK espe: ly. Then calculate heat transfer area required, flowrate of Niquid "B* and bare exchanger in Present year. Data: Cy = Rs, \ MF = 3.29; Clin present Years 1125; CL in hase year = 389 (b) The pump is used to prumy = Thevinlet and exit pressures for the pump are 200 and $00 KPa respectively, The efficiency of pump and associated of the pump and its bare module Data: Co = Rs. 42,2508, = 2000 watts a = 936; P= 1; Fy= 1s; ME Cl in base year = 389 heat transfer coefficient is 255 Wink. The Specific heat capacities of module cost of heat 1000; Sa = 37,m5a=0.65; Fy = 3,1; Fo 0.1; iP the chemical at the rate 0600 m/day, Density (19) of chemical is 1100 ky/mnoahie: Motor are 70% and 90%, Tespect * break horse power cost i =3.38; CI in present year» 1125; QS. fa) Considerthe Pro€css system where there are multiple hot and cold streams (12) are involved:n order to design heat exchanger network for this system, craluale Quoe, Qc and pinch temperature at Apes 25°C. Process stream data is as below: Process: agent, why it is required to © boiling point Pogezof3 CPLASSCABIBACDIATATES WEATHERSted ae rte 4 a nod QP. Code: 24241 : See q Write short notes on the following; cach camry equal marks: (20) Sa} Batch v/s Continuous process Major utilities used in chemical process industries (c) Different types of Flexibilities that may be involved in process and their effect on process (d) Reaction information that must be known while synthesizing any Oo chemical manufacturing process ey