ar Mana for Water Supply Binet by Er Sey
EXPERIMENT NO.4
DETERMINATION OF OPTIMUM pOsk OF COAGULANT (JAR TEST)
APPARATUS REQUIRED
1. Floccutator
2. Jars
3. Pippottes
4, Measuring eytinders (10m!)
5. ‘Turbidimeter
6, Colorimeter
7. ‘Thermometer
8, pl meter 7
CHEMICALS REQUIRED
1.1% Alum [AL(80,)).181 0] solution
Buller solution (ptt 4)
3. Distilled water
THEORY
Coagulants and foe
suspended and colloidal pi
micals added to the water which help in removal of fin
1s. The colloidal particles are characteristically very small ang
and to the electrical charge
ion duc to both their small siz
main in continuous suspe
between particles.
the process of binding small particles in the water together
ino larger, heavier clumps which settle out relatively quickly. Coagulants neutralize the
Isive electrical charges (lypically negative) surrounding particles allowing them
creating clumps or larger particles. Flocculants facilitate the agglomeration of the
forming larger floccules and thereby, increases gravitational setlng.
-ve a dual purpose of both coagulation and flocculation in that they create
repu
togethe
congulated particles
Some congulants s
large floes that readily settle,
‘The coagulant required for treating water, termed as dosage of coagulant, depends upon the
characteristics of water, The dose of coagulant increased the residual turbidity improved. Itis
important to note that the optimum coagulant dose is the dose which meets the specified
turbidity required on the regulatory permit, The addition of excess coagulant may reduct
is required but also could lead to the production of more sludge which
turbidity beyond what
would require disposal
‘The jar test isu ermine the optimum dose of coagulant required at the operating
conditions for water or wastewater. This method helps to predict the functioning of a le?
scale treament operation on a small scale. A jar test simulates the coagulation
that encourage the removal of suspended colloids and organic mate?
flocculation processes th
which can lead to turbidity, odor and taste problems.
12a Labs, Manual for Water Supply Engineering by ler. Sichu Shrestha
April 19, 2009
‘qhe first step of the jar test involves
ater rapidly (in the flash mix chamts
adding coagulant to the so
luree water and mixing the
he coagulant in the wate
flocculation ba
Finally, the mixer is
imentation basin), In case of
Is upon the type of source water. For
wed to perform jar tests frequently as
very'little turbidity to remove and is
water conditions. Surface water plants,
susceptible to sudden changes in water
to adjust the coagulant dosage and deal with the changing
Particles to cluster together.
ul (as in case of
vater treatment plant, frequency of jar test depen
example, plants which treat groundwater may not in
compared to surface water. Groundwater may have
unlikely to be affected by weather-related changes in
reeds (0 treat water with a high turbidity which is
J quality, especially after rains,
source Water turbidity.
rpm gauge
Flocculator used in Jar Test
ifferent sources of water need different coagulants, but the most commonly used are alum
and ferric sulfate, Aluminum Sulfate is also known as alum, filter alum, and alumina sulfate,
lum is the most widely used coagulant. Alum is available in dry form as a powder or in lump
form or liquid solution. It reacts in presence of alkalinity (optimum range of pH is 6.5 to 8.5).
The reactions obtained are as below.
ity then the reaction will be (without addition of soda ash)
Ip (SO4)3.18 H20 + 3 Ca(HCOs), —*» — 2AI(OH)3 } 3 CaSO, + 6CO2 + 18 H20.
lum ‘Natural Alkalinity Floc
Floc
13
—AI(OH)s } Na2SO4+ 18 H20apply Engineering DY ES,
ab Manat for Water St Sey
: Ait
Pmt
1
2 3. CaSO. HIB ELO.
With addition of tim AION |
Al; ($04)3.18 10 #3 Ca(OIDs Bloc ’
‘Alum Lime
Fi i Ki 4 ity of n water Sa
eae cee Temperature, Cotor and Turbidity of ve
Take sO0ml to 1000 ml of water summple (#8 P oy 4
6) , in [
Le See tg Jum is placed on measuring cylinders on side of jars, 5
. Following dose of 1 % alum is |
Tai) per 500 ml of | Concentration I
eae | (mg/l) f
«
Switch on the flocculator ;
Supply the prepared alum dose into the jars at the same time
7. ‘When stiri intially at the speed of 60-80 rpm for | 10 2minutes then at 1510 20pm for
al properties of the water sampl
best floc formation and the sample without add
so that the floc get
rom the ja
ion of coagu
c settled,
having good- better othe
nt.
OBSERVATION
Characteristic of water sample after addition of Alum
see Mee eee |
(NTU)
1
|
3
i
5
6 Loe "
“Record floc formation characteristic a Worse, Poor,
sample indicates poor coagulation, P
Good, Better Best. 0 hazy
formed and dense, with the liquid bety
roperly coagulate
ulated \ floc particles that are well-
ween the particles cle:
megenss
14