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A mold. The clay-sawdust mixture lacks plasticity, so using a mold to shape the
pots is best.
If the sawdust is well sieved with at least a #30 sieve, more sawdust will increase
the speed while not negatively impacting the filtration significantly up to about
20% clay and 80% sawdust by volume. If the sawdust is not well sieved or is
sieved by a mesh larger than #30, more sawdust will negatively affect the results
of the filter, and so a slower ratio of 50/50 clay to sawdust by volume is
recommended.
The other main factors when determining the proportions of clay and sawdust is
the plasticity of the clay during working and the strength of the pot after firing.
More sawdust will reduce both plasticity and strength. At 50/50, the clay is not
too difficult to work with and will come out of the kiln strong enough to be easily
handled, though still not nearly as strong as clay alone. At 20/80, the clay cracks
significantly during even simple working, which can lead to air bubbles in the clay
that may impact filtration, and will come out weak and possibly even crumbly.
Mold:
Form your workable clay into/around your mold. We used small plastic balls for
our molds, although larger ones can be used. Adding water to the clay at this
point may be necessary to increase its plasticity and to help reform cracks that
may occur. Wall width should be around 0.5 - 1 cm.
Once you have the clay in the proper shape, let it dry until it can be safely
removed. Then remove it and let dry until bone dry. Larger pieces may need to
be covered in plastic or another waterproof material, allowing them to dry slowly
and evenly.
Firing:
Once the pieces are bone dry, they are ready for firing. We used an electric
programmable furnace, although a more traditional kiln and cones can certainly
be used.
As with most any clays, the furnace should be brought slowly up to about 100 or
120 degrees Celsius to allow the pore water in the clay to boil off and escape.
We used a time of 2 hours to reach 100 degrees.
Then the furnace should be brought up to about 890 degrees Celsius, or ^012, in
about an hour. It should be then held there for 8 to 9 hours, then allowed to
slowly cool off down to room temperature in 2 hours or more.
There is a lot that happens to the clay between 120 and 890 degrees Celsius.
Understanding the way this firing process affects the microstructure, and thus the
porosity, is crucial to understanding the filter.
The most significant process as the piece fires is the ceramic change. This
begins at about 350 degrees, peaks at 600 degrees, and ends by 700 degrees
Celsius. At this point, the water chemically bound to the clay is driven off,
converting the clay into a hard ceramic. At this point the clay is no longer held
together by water, but by a process that occurs called sintering, where small
points of contact between clay crystals are welded together.
Thus by 700 degrees the clay is extremely porous, with crystals being held
together only by small welds at points of contact. While good for the purpose of
filtration, this makes the ceramic extremely weak.
At 700 degrees the burning out process, where carbon, sulfur, and organic
molecules combust, begins. This is crucial in the filter making process as that
pores left over from the burnt off sawdust contributes significantly to the filtering
process. The burning out reaches a peak around 800 degrees, and is pretty
much completed by 900 degrees Celsius.
The final process to take place during firing is vitrification. Vitrification starts at
800 degrees C and involves a glass of metal oxides and silica filling in the pores
between clay crystals, strengthening the ceramic but also reducing porosity.