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NOILVTILLSIG SNONNILNODSnulton of Unit Operations with HYSYS
Product Specifications
‘You must specify ane characteristic (eg, flow, composition) foreach
product from the column. Specify composition (component mole oF
‘mass Traction) or component recovery instead of component flow,
Specify the composition or recovery (Loss ofthe impurity. Forexample
‘use 001 ofthe heavy key in the distilate instead of 0.99 of the ight
‘ey. This is so important for mlt-component mixtures that it a
good idea to get into the habit by specifying even binary mixtures
this way (fr binaries it would net make any diference). Specity the
heavy-key composition or recovery in the distillate and the lightkey
composition or recovery in the bottom product, and make sre that
the Keys ae next to cach other inthe ist of components, The list must
be in order of boiling points,
Note: you can also specify compositions or recoveries of groups
‘ofcomponents, whatever case you ate making group of components
fs your key, do not select the flow rate of both products for the
variables This is Because the sum ofthe two prodict rates mast be
‘equal to the feed rate (the mass talance constraint
Condenser
Specify a Total condenser if you want a total condenser or a Partial
(Condenser if that is what you want If the column feed contains very
Tight components (eg, hydrogen, methane, ethane, nitrogen) you
‘must use a Partial Condenser. I you dat, the condenser temperature
‘ill be too low. In HYSYS select the Full Reflux option if you only
hhave a vapor distillate stream, The Partial Condenser option gives
you to distilate product streams, one vapor and one liquid and
feajuites one adlittonal specification,
Column Pressure
‘Specify the column pressure at the top and atthe bottom (The Boom
resure ut higher ha the top pressures tht the tapers con lo om
fhe bottom tothe fp). Although you can specify a condenser and a
reboiler pressure drop, these are normally zero. The column pressure
‘You specify determines, n order of importance: The temperstaes ia
the condenser and the reboller: the lower the pressure the lower the
column temperatures,
‘The density of the vapors in the column: the density Is
proportional to the pressure, and the required column diameter ie
Continous Distiaion
‘inversely proportional tothe density to the 025 power. This i only
"Significant at very Tow pressures (<1 pa).
"The ease of separation: the lovee the pressure the easier it 8 to
separate, that i, ess numberof stages oF lower Feflux ato. So, the
pressure should be as low as posible, although vacuum (P < 147
psa) should be avokded if possible. The most important consideration
Insolecting the pressure isthe Colunm Temperature. The condenser
temperature should be high enough o that cooling water canbe used
inthe condenser, that is grester than the water exit temperature plus
‘he minimum allowed temperature approach,
IF this roquizes too high a pressure, then arefrigorated condenser
should be considered, At the other end ofthe column, the rebolle
temperature should be low enough so thatthe lowest possible steam
pressure can be used inthe rebolr. This is because the annual steam
{oat is lower the lower the seam pressure. However, only tvo oF
tee steam pressure levels are available in a plant. The maximum
boiler temperature that allows the use ofa particular steam pressure
levels equal tothe maxima steam condensing temperature for that
level 35°F. This isto insure nucleate boiling in the rebole,
"To check if you have selected the correct pressure, check the
results by opening Performance tab in the eoluran block and locking
at the condenser and reboier (RK) tomperatures. If you don't you may
tealize your pressure i to high orto low when you are sizing the
condenser and rebole, and then it may be to late to make another
Solving Convergence Problems
When the column does not converge, check you specifications fis.
‘You may, for example, have specified the heavy key to go tothe top
andthe light key to go to the bottom, There is no way thiscan happen
fd the simulator knows bat it wil ony tel you by not converging
‘Oe season for failure to converge Is that you may not have enough
stages, You may prevent this by fist running with the specifications
‘of Ref Ratio and Distillate Rate. Then add the product specifications
you want and see how close they are (under "Current Valuo” In the
Monitor window) tothe values you want. fthey are far, yeu probably
need more (or fewer) stages.
the reflax ratio you need to achieve your specifications is to
high, you should ad stages. Itmay be that your fed tay location is
00 high or too low. One way to tell isto Took atthe temperatire
profile graphic in the Monitor window If there i a discontinuty atSan of Unt Operating with HYSYS
the feed tray instead of a smooth transition, the fed tray should be
‘moved. Note that the optimum feed tray location changes when you
‘ange the pressure inthe column Look aso atthe messages window.
Te usally tells you why itis nat converging, Whatever you do, fo not
hage igs at naar st omnes comer I you have been te for
{Dihouts, tis probably becnuse you have been changing ening at
random
‘Shortcut Distillation Method
Example
‘The following example builds 4 Shortcut column as a typical
depropanizer, having the stream Feed asthe tower feed. The fed at
{405+ 100 pala enters the column at 1272 Tomo with the following
‘ompostion in ole faction Ethane QO1S, propane 0.7315, butane
0681, butane 0.1462, LPentane 00173, nepentane Q.015, n-hexane
(0.0071 Heavy key in Distillte is butane O02 mole Faction ight
key tte ropa 005 me rato for refx ais of 3
late the minimsm reflux ratio and column performance?
1. Star the SYS program select new case press the components
{nba addall the component tate invalved inthe problem,
By clicking on the ld package tab sclct te sultable fad
posing Cvs he int an lk on ve he Stn
Envirenment button, then from the object plete scect the
shortcut dalton shone fn gue St cick ay pace ede
the sumaton area, you wl Figure 62.
fee Figure 62 shorteut
‘EL Figure 6.1 object pallet aistlltion icon
2. Double click on the ion that foks like Figure 6.2, to enter the
Giferent specifications, While the Desiga tap i pressed click
Connections and fil F for feed, D for Distt 8 for Bottom, Qe
{or condenser std Qr for Reboier as shown in Figure 63.
CConinsoos Dission
Figure 63 Distillation connection page
Close the above window to return to graph environment click
fon the feed stream and enter feed specification by typing
“Temperature pressure, low rate and feed compositions as shown
Jn Figure 64. Close the windovr you vill notice thatthe fed
stem changed color. This because we have specified all the
Independent variables we care for on that stream and the
dependant variables were automatically calculated by HYSYS.
Figure 64 Feed steam conditions