King Fahd Unvesity of Petroleum and Minerals, College of engineering sciences and applied engineering Department of Chemical Engineering CHE 495; Integrated Design Course Final Report Production of Phthalic Anhydride from O-Xylene Prepared by: Group: 2 . Hassan Al-Haraz 200969070 . MAl-Abdrabalnabi 200971250 Mohammad Al-Bakshi 200986590 . Aeel Al-Brahim 200985730 . Mujtaba Al-Nasser 200964010 FewNEContents 4 2. a 5 6. 2 8 SUMMARY OF THE PROJECT PROBLEM INFORMATION. PHYSICAL & CHEMICAL PROPERITIES. LUTERATURE REVIEW OF PRODUCTION PROCESS. KINETIC DATA FOR THE PROBLEM, SAFETY & ENVIRONMENT PRECAUTIONS PRELIMINARY COSTS OF MATERIALS [MASS AND ENERGY BALANCES 2 6. A. Materia Balance around the mixing point 1B. Material Galance around the Reactor: (©. Material Balance around the Switch Condenser . Materal Balnee around the Fest Distiaton Column: , Material fatance around the Second Dstilation Column ENERGY BALANCE: ‘A. Energy Balance around the reactor: Eneray Balance around Heat Exchangers and Heater: Energy balance around mining points 1. Energy balance around Pumps and compressor: Energy balance for first distillation eolum 701, PROCESS SIMULATION 4 IntraoucTion A. Fow Fate Spreadsheets 5. Energy Spreadsheets Discussion of Mass Balance: 10 2 « 18 16 19 20 2 2 25 26 2 2 36 a7 2 2 so s6 7REACTOR DESIGN EQUATIONS. MOLE BALANCE NET RATE LAWS, RATE LAWS, STOICHIOMETRY. PRESSURE OROP. ENERGY BALANCES. Catalyst information. 4. Calculation and Recut K. Reactor instrumentation and Control. L conclusion i HAZOP ANALYSIS Distltion cola (7-701) INTRODUCTION. PREUMINARY CALCULATIONS, A. Material Balance. B. Physical Properties. Relative Volt. UL Minimum Ref 1. Column Diameter \V._ TRAY SPECIFICATIONS. Vk TRAY LAYOUT AND HYDROUUCS (TOP VIL TRAY LAYOUT AND HYDROVUCS (BOTTOM) Vl. DESIGN FLOWSHEET. 1X Design simulation. X DESIGN OF CONDENSER Xi, DESIGN OF vessel XL Control Stem 6 70 n n 2 % ” * 96 98 9 100 100 100 100 202 203 106 07 0 au a9 aa a2 aa 9