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A New Rheometer For Soft-To - Uid Fresh Concrete - de Larrard Et Al. - 1997
A New Rheometer For Soft-To - Uid Fresh Concrete - de Larrard Et Al. - 1997
This paper describes the development of apparatus designed to ments in the field of concrete rheology. However, these
characterize the rheological behavior of fresh concrete, both in the rheometers seem to have room for improvement, from the
lab and on site, in the range of consistency from soft to fluid. The
viewpoint of the practitioner as well as that of the scientist:
principles that governed the design of the rheometer are first
recalled. It is a torsional rheometer, in which a sample shaped like • they are bulky, require a large quantity of concrete, can
a hollow cylinder is sheared between two horizontal planes. The be used only in the laboratory, and are not easy to use to
conduct of the tests is then described, followed by their processing, test behavior under vibration;
which yields, in particular, two physical quantities to characterize
a concrete, the shear yield stress (τ0, in Pa) and the plastic
• the characteristics indicated (g and h, respectively the
viscosity (μ, in Pa.s). These parameters may be measured with or ordinate at the origin and the slope of the experimental
without vibration, giving different values in each case. Later, the straight line relating the measured torque and the speed
results of experiments are described. They deal with the detection, of rotation of the rotating part) are still technological
with only one sample, of the phenomenon of loss of workability, quantities, not intrinsic properties of the material. They
and with the pumpability of the concrete on site, respectively. The
article concludes with a look at the prospects for industrial use of
depend on the shape of the apparatus and cannot be
the BT RHEOM rheometer. used in a flow calculation.
J. C. Sitzkar, F. Claux, M. Joly, and F. Derkx are employed by LCPC. They are
involved in the development of special laboratory facilities, both from mechanical and
electronic aspects.
DESIGN OF APPARATUS4
Response to the specifications
The logical choice was a plane/plane type of rheometer
design, in which a ring of concrete having a vertical axis is
sheared, its bottom section being fixed and its top section
rotating about the axis (see Fig. 1 and 2). The minimum
dimensions lead to a volume of concrete of the order of 7
liters, of which 6 liters are in the zone of shear: this is very
nearly the capacity of the Abrams cone, and experience has
shown that it is, statistically, sufficiently representative of
the material. The apparatus has 5 independent parts [cf. Fig.
1 and 3(a)]:
• a container (a), of which the interior volume is a hollow
cylinder, containing the sample of concrete;
• a rotating part (b) used to cause the top section of the
sample to rotate, including top blades in the shape of a
spoked wheel, coupled to a hollow shaft and a cylin-
drical external skirt. This last part serves to keep the
configuration symmetrical with respect to the hori-
zontal midplane of the sample;
• a system of blocking blades (c), at the bottom of the
container, to prevent rotation of the bottom section of
the concrete;
• a disc (d), coupled to a shaft, capable of measuring the
height of the sample;
• the body of the apparatus (e), cylindrical in shape,
covered by a plate holding the above-mentioned Fig. 1—Prototype of BT RHEOM rheometer. Body dimen-
sions: height 300 x diameter 300 mm; container dimen-
elements. The body contains the two motors of the
sions: height 240 x diameter 270 mm.
rheometer, one to turn the system of top blades and the
other to apply a vertical vibration to the plate, indepen-
dently of the rest of the body.
The tests are controlled and the measurements acquired by
a microcomputer, as in the case of the BML viscometer.2
Programs have been especially developed for various types
of tests.
Fig. 3—Photos (a) through (e) showing different stages of preparation of test.
limit upward movements of material between the skirt • Fill the rheometer with concrete so that the level of
and the inside wall of the container. material after consolidation is above the top blades
• Place the system of bottom blades in the bottom of the [Fig. 3(d)].
container. • Attach the container to the rheometer body plate.
• Fit the rotating part with the seal in the container, • Insert the shaft of the disc into the shaft of the rotating
aligning its shaft with that of the motor [Fig. 3(b)]. part [the disc then rests on the free surface of the
• Attach the container to the rheometer body plate. concrete, cf. Fig. 3(e)], then run the desired program.
• Run a no-load test [Fig. 3(c)]: moisten the seal by • Disconnect the disc, then the container, from the body
pouring water into the space between the skirt and the and remove the rotating part from the fresh concrete.
container, start the corresponding program, then • Empty the container and withdraw the worn seal.
disconnect the container from the body and empty the • Clean the four parts (container, rotating part, blocking
water in it; blades, and disc) in water.
· ∞
· hγ - i ·
∑
4i
τ ( γ ) = ------------ K F ( K h γ ⁄ R2 ) (1)
4
2πR 2 i = 0
with
F ( Ω ) = ----Γ ( Ω ) + ∂Γ (Ω)
3
---------------- (2)
Ω ∂Ω
·
γ = Ωr ⁄ h (3)
∂Γ
2h ------- silica fume. The intervals of variation of the mix design
∂Ω
μ = -------------------------- (6) parameters are: 5 to 20 mm for the maximum aggregate size,
4 4
π ( R2 – R1 ) 350 to 600 kg/m3 for the proportion of cement, 0.26 to 0.66
for the water/cement ratio, and 0.7 to 1.8 percent for the
where τ0 is the shear yield stress of the concrete, and μ its superplasticizer/cement ratio, giving slumps ranging from
plastic viscosity. 80 to 260 mm. The following findings are then made:
However, reality does not exactly match the diagram of • the measured shear yield stress ranges from 500 to
Fig. 2. It is known that in a viscous fluid, the velocity field is 2000 Pa; the differences between concretes are there-
continuous in the vicinity of the wall. It is then technologi- fore large with respect to the repeatability error;
cally impossible to impose a speed that increases linearly • the plastic viscosity ranges from 70 to 500 Pa.s (same
with height at the outside wall of the sample. The friction of remark);
the concrete on this wall therefore perturbs the flow of the • there is no correlation between the two Bingham char-
concrete with respect to the ideal configuration of Fig. 2. acteristics, which demonstrates the inadequacy of tests
Finite-elements calculations have been performed, in order delivering only one parameter. In particular, for the
to evaluate the effect of wall friction on the measured rheo- same cone slump, the viscosity of the concrete can vary
logical characteristics. These investigations, reported else- in a ratio of 1 to 4.
where,5,10,11 show that a decrease of about 10 percent should As for the behavior under vibration, the few preliminary
be applied to the apparent plastic viscosity. On the other tests performed suggest the following general trends:
hand, the wall friction does not influence the value of shear • the behavior remains Binghamian;
yield stress. • the viscosity is not much affected by the vibration;
Three series of repeatability tests have been carried • on the other hand, the shear yield stress is considerably
out.5,10 The standard deviations of the measured Bingham’s reduced, and sometimes even practically disappears.12
characteristics are about 10 percent. The diversity of vibration responses obtained already
shows that it is advantageous not to apply only tests
Obtaining the rest yield stress without vibration.
In this case, the only quantity measured is the torque Γr 0,
corresponding to a very low speed of rotation (less than 2 Tracking of losses of workability with
rpm). Neglecting the effect of viscosity: only one sample
When a mix design is developed, especially for an HPC, it
is necessary not only to meet specifications for the initial
3Γ r0 rheological behavior, but also to ensure that this behavior
τ r0 = -----------------------------
- (7)
3 3
2π ( R 2 – R 1 ) remains stable as long as necessary for placement. This
leads, in the laboratory, to very cumbersome tests: a batch
where τr0 is the rest yield stress of the concrete. having a large volume must be kept in the mixer, and
samples taken at regular intervals for rheological tests.
With the rheometer, this operation is greatly simplified.
EXAMPLES OF LABORATORY USES
Initial rheological characteristics of different Only one sample need be taken and kept in the container to
concretes undergo the successive shear sequences. However, the possi-
Figure 7 gives experimental results for a series of bility that this repeated shear modifies the evolution of the
concretes, most of them high-performance, with and without microstructure of the material, and so its rheological
Retarder
(dry extract) kg/m3 0.25
Processing of measurements—correlation
between rheological behavior and pumpability
Consider first a simplified theory of pumping.15 A
Binghamian fluid having the characteristics τ0 and μ travels
in a pipe in laminar flow. The pump flow rate is then related
to the characteristics of the pumping pipe and of the material
according to the following equation:
4
πΔPR
Q = ----------------- ⎛ 1 – --- D + 1
--- D ⎞
4 4
(8)
8μL ⎝ 3 3 ⎠
2Lτ
D = -----------0- (9)
ΔPR