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Research Article
Sandwich Structured Composites for Aeronautics: Methods of
Manufacturing Affecting Some Mechanical Properties
Copyright © 2016 Aneta Krzyżak et al. This is an open access article distributed under the Creative Commons Attribution License,
which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Sandwich panels are composites which consist of two thin laminate outer skins and lightweight (e.g., honeycomb) thick core
structure. Owing to the core structure, such composites are distinguished by stiffness. Despite the thickness of the core, sandwich
composites are light and have a relatively high flexural strength. These composites have a spatial structure, which affects good
thermal insulator properties. Sandwich panels are used in aeronautics, road vehicles, ships, and civil engineering. The mechanical
properties of these composites are directly dependent on the properties of sandwich components and method of manufacturing. The
paper presents some aspects of technology and its influence on mechanical properties of sandwich structure polymer composites.
The sandwiches described in the paper were made by three different methods: hand lay-up, press method, and autoclave use. The
samples of sandwiches were tested for failure caused by impact load. Sandwiches prepared in the same way were used for structural
analysis of adhesive layer between panels and core. The results of research showed that the method of manufacturing, more precisely
the pressure while forming sandwich panels, influences some mechanical properties of sandwich structured polymer composites
such as flexural strength, impact strength, and compressive strength.
Table 1: Relative characteristics of sandwich structures in relation and unambiguously determining the usefulness of a given
to solid material [9] (see Figure 10). material. It must be remembered that the material’s properties
determined in the course of mechanical tests are dependent
Property Laminate Sandwich Thicker sandwich
(skin) structure structure on conditions, in which they have been determined. The
Stiffness
obtained results are considerably influenced by the following
1.0 7.0 37.0
factors: the applied samples (their shape and dimensions),
Flexural strength 1.0 3.5 9.2
the strength machine used (fixtures for samples mounted
Weight 1.0 1.04 1.06 on it and also the stiffness of the measurement system),
and the speed of changing load. The mentioned reasons
allow for a conclusion that values determined as a result
panel described macroscopically can be rightly compared to of mechanical tests are not of the characteristic material
tasks performed by I-beam [9–11].
constants (coefficients), such as the density [26]. The mechan-
Sandwich composite materials belong to the group of
ical properties of a sandwich composite depend on partial
anisotropic materials. It means that their strength properties
properties of components from which this composite has
change depending on the applied load. Using the knowledge
concerning this anisotropy makes it possible to produce been constructed. Mechanical properties of foam and wood
composite materials, which display specific properties in depend to a large extent on the density of these materials,
desired directions, depending on needs. They are developed speed of deformation, temperature, and humidity [27, 28].
depending on requirements posed in relation to a given Increased temperature of use and presence of steam have an
composite. Moreover, these requirements are directly con- adverse effect on mechanical properties of sandwich polymer
nected with the application of a given structure. The most composites. In the case of humidity, water absorption occurs
significant requirements are as follows: stiffness, strength, in the material. If the composite has fiber reinforcement,
specific volume, thermoinsulating power, acoustic resistance, absorption occurs as diffusion on the separation boundary
ability to absorb energy, and hydrostatic weighing [1, 12–15]. between the fiber and matrix (in the interface). Long time of
The effects of innovative research performed on sandwich the material’s exposure to humidity can cause its degradation,
composite structures can be illustrated by the development of including cracking of the matrix and separation of fibers from
materials used in aeronautics. Initially, fillers in the form of it [29].
balsa were used (military aircraft “de Havilland Mosquito”). The flexural test of sandwich panels can be conducted
Next, cellulose acetate foams and later honeycomb fillers on the basis of ASTM C 393-00 or PN-EN ISO 14125:2001
[11, 16] were used. They are used for military purposes standards. These documents specify the following factors:
due to their nonmagnetic properties [11, 16, 17]. Skins are shape and dimensions of samples, the way of conducting
commonly made of standard materials used for structural measurement, and methodology of analysing results. The
laminates based on thermosetting resins and glass or carbon flexural test can be performed by means of either the three-
reinforcement. Skins can also be produced from thin plates or four-point method. Four-point bending test is more rarely
made of thermoplastic materials of high resistance to impact used despite its advantage—lack of destructive influence of
but of low temperature of use [18] or metallic materials [19]. the pressure stamp on the top part of the tested composite.
The so-called low density spacer materials, whose density This adverse influence occurs during a test conducted by
is far lower than water density, are chosen to manufacture means of the most commonly used method of three-point
the core. These are most frequently polymer and ceramic bending [21]. Consequently, samples subject to four-point
foams, wood, and “honeycombs” which are materials made bending test show increased flexural strength of the sandwich
of elongated cells of a hexagonal or another shape. panel [30]. Failure of sandwich panels in the flexural test
The sandwich structure is most widely used in applica- occurs mainly in the core of the material. It is a sliding crack
tions, in which stiffness of an element is particularly signif- in the core caused by shearing forces. Ultimate shear strength
icant. Redoubling the core thickness (Table 1 and Figure 10) increases proportionally to the density of the used foam core
influences the stiffness of the sandwich panel more than and at decreasing the level of porosity. The increase in foam
seven times at barely 4% increase in the weight of the thickness does not improve this characteristic.
product. Increasing the core thickness of a panel by four The increase in flexural strength of a sandwich panel can
times increases its stiffness more than 37 times at a barely be obtained by using a skin of a material which has a greater
6% increase in the weight. Additionally, flexural strength stiffness or increasing its thickness [27]. If the foam core has
improves. However, its change is smaller than in the case of low shear strength or is fragile, its failure can be immediate
comparing the changes in the element’s stiffness [9]. and unpredictable. When a material of high shear strength is
The most frequently tested mechanical properties of used for the core, decohesion causing delamination between
sandwich composites are measurements of compressive the core and outer structural layers of the panel can appear
strength [11, 20], three-point bending test [5, 21–23], and [31]. Destroying the core during a flexural test usually occurs
impact tests of a panel [7, 24]. In the case of materials directly under the load point, that is, a place where shearing
used in military technology, additionally ballistic tests are forces and bending moment reach maximum values [32]. For
conducted [25]. Discovering values of these properties mea- the mentioned reasons, initiation, propagation, and stopping
sured in simulated conditions of the element’s work gives the development of cracking which leads to delamination are
the possibility of relating them to real operation conditions an essential aspect while testing sandwich structures [17].
International Journal of Aerospace Engineering 3
One of the faults in layered materials, including sandwich STR 010-300-125 which had surface weight, respectively, 200
type composites, is low resistance to delamination as a result and 300 g/m2 . The weave of both fabrics was the same type
of impact caused by small objects of low energy. Such an “one to one.” It means that linear density of warp’s roving
impact can lead to the separation of the outer structural layer and weft’s roving was 200 or 300 depending on whether it
from the core, which can facilitate the absorption of humidity was the first or second fabric. In all cases, glass fibers of 12 𝜇m
by the material. Consequently, strength properties of a com- diameter from E type glass produced by Krosglass S.A. were
posite can significantly decrease. In the sandwich material, used as reinforcement.
the laminate plays the most significant role in absorbing The matrix of outer skins was made of low viscosity
impact energy. On the other hand, the thickness of the epoxy resin with a CES R70 symbol based on Bisphenol A/F
core has influence on the decisive failure mechanism of the (modified by means of an active two-function diluter) and
material [10]. The quality of the connection between the core CES H71 hardener. Such a composition is used to produce
and outer skin of the composite has a considerable influence laminates from glass fibers, creating glue connection and
on the impact strength of the layered material. It depends to impregnation of porous materials. Dosing CES R70 + CES
a large extent on the used method of producing a panel [17]. H71 composition is 100 : 54 of weight parts (or 100 : 56 of vol-
Evaluation of the composite resistance to impact can ume parts). The estimated time of gelling 100 g of the mixture
be performed with the use of a hammer drill according to at a temperature of 293 K was approximately 30 min. During
Charpy’s method. There is a test with recording total energy the work with a mixture of resin and hardener, the minimum
and a test with a separate recording of initiation and crack temperature of application was 281 K (optimal 291–293 K) at
development energy [33–35]. In the case of fiber composites, relative humidity not higher than 75%. The lifetime of 100 g of
the latter recording provides a lot of information concerning CES R70 + CES H72 mixture was approximately 45 minutes
the crack mechanism and gives a possibility of isolating the at a temperature of 293 K. The density of hardened resin was
influence of components of a tested composite and structure determined as 1.17 g/cm3 .
of fibers on impact strength test [5].
2.2. Methods of Producing Material for Tests. Every produced
2. Materials and Methods of composite panel had a structure built of two glass-epoxy skins
and core made of polyurethane foam. Every skin included
Experimental Tests one layer of reinforcement in the polymer matrix. In order
2.1. The Objective of Research and Used Materials. Tests were to mark samples, symbols including one letter and one
aimed at determining the influence exerted by the production number were used. The letter referred to the method of
technology of sandwich laminates on chosen mechanical contact laminating (T—composites reinforced with fabrics,
properties including structural characteristics occurring at M—composites reinforced with mats), press method (P),
the boundary of core stages and sandwich panel skins. and producing with the use of autoclave (A). The number
Moreover, the objective of the tests was to analyse the process concerned the reinforcement used in panel skins. The fabric
of developing cracks occurring after impact. The knowledge called STR 015-200-110 was replaced with number 2, whereas
of such a process is indispensable for evaluating the degree STR 010-300-125 fabric is referred to by means of number 3.
of damage in sandwich laminates and the usefulness of EM 1002/300/125 and EM 1004/300/125 mats were marked
laminates, especially used in aeronautics. with numbers 2 and 4, respectively.
Sandwich panels of dimensions 500 × 210 × 10 mm, from The most common methods of manufacturing sandwich
which samples for strength tests were cut, were produced structured composites were chosen. This allowed for focusing
by means of three methods: hand lay-up, press method, and on the practical aspect of applying these methods. However,
autoclave use. These methods were chosen due to their wide in order for such a comparison of methods to be possible,
application for producing composites used in road transport such types of resin and hardener were chosen to ensure the
and aeronautics. Panels were built of a core in the form hardening of resin both at room temperature (hand lay-up
of polyurethane foam surrounded by a composite made of and press methods) and at increased temperature (autoclave).
epoxy resin. Two types of materials were used for reinforcing The extent of resin crosslinking was not analysed.
the resin. Namely, foam sheet S63 (Connector) used for the
core was characterized by the apparent density of 67.3 kg/m3 2.2.1. Hand Lay-Up. For hand lay-up, a mixture of epoxy
and compressive strength which equaled 0.594 MPa for resin and hardener in a ratio 100 : 54 of weight parts (a digital
measurements in the direction of cell increase during its scale with the accuracy of 0.01 g was used for measuring
production and 0.309 MPa for perpendicular directed mea- out) was prepared. The liquid was mixed for approximately
surements. According to the manufacturer’s data, the foam 2 minutes until a clear consistency without visible streaks
S63 with 93% cells of closed type showed water absorption was obtained. After applying a small quantity of liquid, it
at 1.6%. Water absorption test was described by means of the was spread by means of a wide brush and hard roller, which
PN-EN ISO 1609 test standard. facilitated squeezing air bubbles and even impregnation of the
fabric.
The following reinforcements were used in panel covers:
Producing one structure required the following actions:
two types of mats, EM 1002/300/125 and EM 1004/300/125,
which differed in the type of silane preparation (resp., emul- (1) simultaneous parallel impregnation of two fragments
sion and powder) and two types of fabric STR 015-200-110 and of the fabric,
4 International Journal of Aerospace Engineering
(2) impregnating the first element of reinforcement, Table 2: Measurement results of sandwich panel samples used for
tests.
(3) placing and pressing the core to the first impregnated
fabric, Average Standard
Production Type of Weight ratio of
thickness, deviation,
(4) turning over the crosslinked fabric with the core and method panel reinforcement, %
mm mm
placing the second fragment of the fabric on the core
and precise pressing. T2 10.96 0.20 16.26
Hand lay-up T3 11.00 0.14 22.56
2.2.2. Forming with the Use of the Press Method. Panels M2 12.42 0.13 10.03
prepared by means of the contact method were subject M4 12.47 0.18 9.84
to pressing. Next, plates were placed one on another and P2 10.64 0.06 23.39
Press
separated by means of stiff covers. Pressure of approximately P3 10.84 0.05 26.26
0.05 MPa was used for pressing. It was close to but not
A2 10.54 0.04 27.09
higher that the foam’s compressive strength. The pressure Autoclave
was maintained until the resin was hardened, that is, for A3 10.66 0.04 32.19
approximately 24 hours.
(a) (b)
Length = 100,31 𝜇m
Length = 246,26 𝜇m
100 𝜇m 100 𝜇m
Figure 2: A comparison of thickness of outer structural skins in composites produced by means of contact reinforcement method with (a)
STR 015-200-110 fabric and (b) EM 1004/300/125 mat.
(a) (b)
250 𝜇m 250 𝜇m
Figure 3: A comparison of structural skins in composites produced by means of (a) press method and (b) in the autoclave.
were used for the test with the following parameters: length of
160 mm, width ranging from 13.32 to 13.95 mm, and thickness
ranging from 10.72 to 12.78 depending on the type of material.
Flexural strength tests were performed with the use of Zwick
Roell Z100 device. The test was conducted with a support
spacing of 100 mm. Velocity of the movement of the lifting
beam was 10 mm/min, whereas velocity while determining
the flexural modulus was 2 mm/min. The ray of used supports
and stamp forcing deformation was 5 mm. During the test,
the stamp always exerted influence on the smooth side of the
panel.
Flexural strength 𝜎𝑓 was calculated on the basis of the
Figure 4: Way of mounting the sample while performing three- following formula:
point bending test.
3𝐹𝐿
𝜎𝑓 = , (1)
2𝑏ℎ2
2.3. Methods of Determining Chosen Mechanical Properties where 𝜎𝑓 is flexural strength (MPa); F is load (N); L is support
span (mm); h is sample thickness measured in the direction
2.3.1. Compressive Strength Tests. For the purpose of com- of force impact (mm); and b is sample width (mm).
pressive strength tests, samples with the following parameters For calculating the flexural modulus of elasticity, flexural
were used: length of 100 mm, width ranging from 38.2 maximum deflections 𝑠 and 𝑠 were calculated. Equations
to 40.6 mm, and thickness ranging from 10.9 to 12.8 mm used were
depending on the type of material. Samples were cut with a 𝜀𝑓 𝐿2
DEDRA DED7731 cut-off machine with a diamond circular 𝑠 = ,
saw. Zwick Roell Z100 device was used for the test. Deflection 6ℎ
(2)
velocity was 0.5 mm/min. 𝜀𝑓 𝐿2
𝑠 = ,
2.3.2. Flexural Strength Test. Samples for the three-point 6ℎ
bending test (Figure 4) were prepared according to the where 𝑠 and 𝑠 are flexural maximum deflections in the half
PN-EN ISO 14125:2001 standard. Cuboid-shaped samples length of the beam (mm) and 𝜀f and 𝜀f are strain.
6 International Journal of Aerospace Engineering
The maximum deflections 𝑠 and 𝑠 (2) correspond to the where 𝐴 𝑛 is impact energy used for breaking the sample, kJ;
following adopted strain values: 𝜀𝑓 = 0.0005 and 𝜀𝑓 = 0.0025 b is sample width, mm; and t is sample thickness, mm.
[23].
Flexural modulus of elasticity was calculated by means of 2.4. Macroscopic Analysis of Structure. Observations of the
the following equation: structure were performed after tests of mechanical properties
were conducted. For this purpose, Nikon SMZ 1500 stereo-
𝐿3 Δ𝐹 scopic microscope with a magnification range from 0.75x to
𝐸𝑓 = ( ), (3)
4𝑏ℎ3 Δ𝑠 11.25x was used. By means of a Kodak Easyshare v803 digital
camera mounted on a tripod stand, photos visible in the
where 𝐸𝑓 is flexural modulus of elasticity (MPa); Δs is microscope lens were taken in the macro mode. Tests made
difference of flexural maximum deflections between 𝑠 and it possible to evaluate the quality of produced materials and
𝑠 ; and ΔF is difference between 𝐹 load and 𝐹 load, at identification of technological structural faults.
flexural deflection which equaled, respectively, 𝑠 and 𝑠 .
3. Test Results and Their Analysis
2.3.3. Impact Strength Test. Impact test by means of Charpy’s
method was conducted in accordance with the PN-EN ISO 3.1. Compressive Strength Test. Table 3 presents average test
179:2001 standard by using samples of the same dimen- results obtained as a result of the compression trial. The
sions as in the flexural test. Samples used for measuring obtained value of compressive strength for all panels was
impact test did not have a notch. For the test, a VEB in accordance with the one estimated by the foam pro-
Werkstoffprüfmaschinen Leipzig type 400/12 hammer with ducer and was approximately 0.59 MPa (Table 3). A similar
a support spacing of 70 mm and a pendulum of 0.4 kJ energy deformation, independent of the composite type reached
impact was used. The blade of the used hammer was wedge- approximately a 2% level. Nevertheless, the influence of
shaped, with an internal angle of 30 ± 1∘ and a rounding of reinforcement and method of producing a composite on the
an 𝑟 = 2 ± 0.5 mm ray. The test was performed at room E modulus value at compression was proved. The lowest E
temperature. During the test, energy used for the sample modulus value at compression was recorded for composites
failure was recorded. Energy measurements during the test reinforced with fabrics, which were produced by means of
made it possible to determine impact strength of the material, hand lay-up.
which is work used for dynamic breaking of a sample without
a notch related to the initial cross-sectional area of the sample 3.2. Flexural Strength Test. Results of the flexural strength test
in the point of fracture. Impact was calculated by means of the are presented in Table 4. A greater stiffness is characteristic
equation given below: of materials, whose outer structural skins include fabric
reinforcement. The greatest flexural strength was observed
𝐴𝑛
𝑎𝑛 = ⋅ 103 kJ/m2 , (4) for composites with mat reinforcement. Probably it resulted
𝑏𝑡 from the occurrence of bigger amount of resin between
International Journal of Aerospace Engineering 7
5 4
4
3
Flexural strength (MPa)
1
1
0 0
0 1 2 3 4 0 1 2 3 4
Deflection (%) Deflection (%)
(a) (b)
Figure 5: Examples of flexural characteristics of composite bending (a) T3 and (b) M2.
loosely placed fibers (in fabrics, they were tightly placed). As (a)
shown by tests of the structure, the thickness of the outer
structural layer made of mat was twice bigger than in case
of the outer layer made of fabric. In mats, fibers are placed in (b)
many directions, which can also contribute to this effect.
Figure 5 presents examples of tension and deflection
characteristics obtained during a three-point bending trial for
some tested materials. The beginning of the deflection curve
was an increasing linear function, which then changed into a
slightly falling curve (Figure 5(a)). At reaching a maximum Figure 6: Examples of panels produced after conducting flexural
value of load, there was a failure of sample and change of the strength test of composites reinforced with (a) fabric and (b) mat.
function’s type into the nonlinear one was accompanied by
frequently quite rapid decrease in force value. In some cases
(Figure 5(b)), after lowering tension, there was a nonlinear
phase of its slight increase, yet it failed to reach a value close transverse cracking of the core at a 45∘ angle to the upper
to the previous maximum one. Then, the curve took the form structural layer and delamination between the core and the
of a decreasing function. Composites produced by means of bottom skin of laminate. Delamination occurred only in
the autoclave method showed the greatest flexural strength. certain places and stopped after reaching a certain length.
Additionally, they were distinguished by high repeatability of Figure 6(b) illustrates failure of a sample reinforced with a
results (low standard deviation). mat with a visible cracking of the core.
In most cases, tested panels did not show decohesive
failure. Nevertheless, a failure of core foam in the place 3.3. Impact Test. Values presented in Table 4 indicate that the
of contact of the load stamp directly under the structural greatest value of resistance to impact was observed among
layer (skin) and core deflection were observed. Figure 6(a) composites, whose outer structural layers were reinforced
presents an example of a sample reinforced with fabric after with fabric and produced by means of the autoclave method.
the flexural test. Obtained from results, higher standard deviation for impact
In several samples reinforced with a mat, failure caused by strength of materials made of fabric proves that there is a
cracking of the core was observed. Crack initiation occurred greater diversity in the quality of producing these samples
in the place where there was a connection core, the structural as compared to materials with mats. It can be caused by
layer directly under the stamp, which was a load on the the occurrence of faults in the structure of these materials.
sample. Propagation of crack in the layer of connecting com- Composites reinforced with a mat were distinguished by
posites occurred. It was further followed by delamination. grater thickness in relation to materials with fabric, yet their
After reaching a certain length of delamination, there was a impact strength was visibly lower (Table 5). It was probably
8 International Journal of Aerospace Engineering
Method of
Type of Average impact Standard
producing
panel strength, kJ/m2 deviation, kJ/m2
composite
M2 10.15 1.35
Hand lay-up M4 10.42 1.93
Figure 8: Impact failure observed for composites produced by the
T2 11.48 5.61 autoclave method (A2).
T3 12.87 4.47
P2 19.04 3.05
Press
P3 13.25 5.32 (a)
A2 20.30 2.37
Autoclave
A3 15.58 3.33
(b)
(a)
t 2t 4t
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