इंटरनेट मानक

Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.

“जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न' 5 तरफ”

Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru
“The Right to Information, The Right to Live” “Step Out From the Old to the New”

IS 1115 (1986): cutting oil, soluble [PCD 3: Petroleum,

Lubricants and their Related Products]

“!ान $ एक न' भारत का +नम-ण”

Satyanarayan Gangaram Pitroda
“Invent a New India Using Knowledge”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह”

है”
ह
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
 ISrlll5-4986
((Itdfhedl~)
Reaffirmed 2002 )
tndian Standard
SPECIFICATION FOR
GENERAL PURPOSE CUTTING OIL, SOLUBLE
( Second Revision)
Second Reprint JANUARY 1998

UDC 621.892.6

@ Copyrikht 1986

BUFAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI ~K100i

Cr 3 Ninwmbm1986
 IS t 1115 - 1996
( Reaairmd 1996 )

Indian Standard
SPECIFICATION FOR
GENERAL PURPOSE CU’ITING OIL, SOLUBLE
( Second Revision)
Lubricants and Related Products Sectional Committee, PCDC 4
Chaimuzn JZ+r#Wt&llg
SEW P. K. GOEL Petroleum Conservation Raearcb AIIociation, New
Delhi
Mmbm
SEBI A. K. ARORA Rourkela Steel Plant, Rourkela
Da N. T. BADDI Asaocitic;f Manufacturers Petroleum Specialities,

SERI R. CHAK~AVAWY( Al&net8 )

SERI N. P. BAKHSEI Indian Oil Corporation Ltd ( Marketing Division ),
Bombav.
SEW K. K. RAX ( Alkmolr )
Saaz M. BH~DRA Inter-Plant Standardization in Steel Industry, Sub-
committee on Oils and Lubricants, IPSS 1 : 9
Sasr M. K. BHAR~AVA Petroleum Rorefinerr Aaociation of I&a, Madras
SEW SHALITIIAI,DANA ( Altmol~ )
SESI S. R. BEATNAOAR Indrol Lubricants & Specialities Ltd, Bombay
SH~I N. SETEURAMAN( &m& )
DRK.S. BHATTMIE~ARAYA Ministry of Defence ( DGI )
SHRI A. K. SINKA ( A&ma& )
Ssim B. K. CEAPESA Central Institute of Road Tramport
_ (_Training &
Research ), Pune
Ds D. K. DAS National Teat House, Calcutta
SERI N. C. CHATTEKTEE ( Alfema& )
DEP;;; ;~xR;‘,“,” ( CHEH ), Railway Board ( Ministry of Railways )

A&TMT RESEARCE O~OICB

( CElEM-I) ( Ahmdr )
LT GOPAL BHARTI
SERI G. C. GOSWAMI
SHRI I. CHANDBA( Altmutr )
SERI P. K. GUPTA
SHRI J. D. HANDAS
SFIRI B. GOSWAMI ( AI&m& )
Naval Headquarters, New Delhi
Assam Oil Dlviaion, Bombay
Hindustan Fertilizers Cqporation Ltd, New Delhi
Tata Engineering dt Locomotive Co Ltd.
Jamsbedpur

Q Ce@ghr 1966
BUREAU OF, INDIAN STANDARDS
Thii publication b protected under tbe IndEw CopJrilirt Act ( XIV of 1957 ) *ad
teprohtion in whole or in part by any means except witb written pertnirion of tbs
Dublirber &all be deemed to be an infringement of copyright under the rid Act.
18 t 1115 1986 l

( Gmtindffem pug0 1 )

MOlllbWS R@wnting
SERI Ii. JAFFBEY Pttrodl Oil Co Ltd. Bombay
S-I M. A. Pans ( .4lternato )
JIB G. JAYARAXARAO Ministry of Petroleum
KU~ARI RAJIALAPSHYI( Al&rxatr )
Saar 0. K. JIJN~~A Bharat Petroleum Corporation Ltd, Bombay
SEBI I. M. MEWEAXT ( Ahmatr )
SHRI S. K. KALB Bhilai Steel Plant, Bhilai
Soar J. L. G~ovaa ( Alterme.)
SEW R. KU~A~IIXABA~P Ministry of Defence ( R & D )
SERI R. N. PADEY ( Atfmatr )
SRRIV. LOB0 Oil Co-ordination Committee, New Delhi
SBR~S. N. MATEUX ( Afkrnorr )
Smtx R. MUxIiERJ1PE Indian Oil Blending Ltd, Bombay
SHEI M. J. SHAE ( Allrmofr)
DR P. K. MUKHOP.+DEYAY Indian Oil Corporation Ltd ( Research & Develop-
ment Centre ) , Paridabad
SEW K. C. MEHTA ( Altmatr )
SHRIJ. P. NI~AM Development Commissioner, Small Scale Induatriet,
New Delhi
SHRIJ. C. PAS~IJA( Altamut~)
Snnr RAJSXD- Surua Indian Oil Corporation Ltd ( Refinery & Pipeline
Division ), New Delhi
Sasr D. K. DA~QUPTA( Ahmatu )
SHRIT. R. RAMAKR~~HNAN Tata Iron & Steel Co Ltd, Jamahedpur
SRRI C. MIEHRA( Akrnek )
SHSI R. A. RAO Lubrixol India Ltd, Bombay
SERI K. L. MALLIK ( Ahudr )
SaranS. V. SASTRY The Automotive Research Association of India, Pune
SERI B. Grtoan ( Aftumet#)
SRRI v. R. SESHU Hindustan Petroleum Corporation Ltd, Bombay
SHRIP. M. RAO ( Altmutr )
SERI D; K. SJNQR Bharat Heavy Electricals Ltd, Bhopal
SHRI R. K. GUF-TA( Aknutr I )
SERI T. v. SUnDEnnAJan ( AkmetU II )
SERI SIJDEIRSINWAL Indian Institute of Petroleum, Debra Dun
DR A. SETEURAYIAA( Alfmmtr )
SHRI T. V. VARCWESE Madras Refine&r Ltd, Madras
SHRI V. K. GOPINATE( Aflnnotr )
DR P. S. VEX~ITARAMANI Ministry of Defence ( DM & SR & DE )
DR R. D. SRIVA~TA~A( Al&m& )
SHRIM. S. SAXENA, Director General, IS1 ( Ex-o&cioMm&n )
Director ( P & C )
SIcrrkr~
SERI M. A. U..KHAN
Joint Director ( P & C ), IS1

(conlhwdonp8g8 11)

2
 IS : 1115 - 1986

Indian Standard
SPECIFICATION FOR
GENERAL PURPOSE CUTTING OIL, SOLUBLE

( Second Revision)

0. FOREWORD
0.1 This Indian Standard ( Second Revision ) was adopted by the Indian
Standards Institution on 3 March 1986,‘after the draft finalized by the
Lubricants and Related Products Sectional Committee had been appro-
ved by the Petroleum, Coal and Related Products Division Council.
0.2 This Indian Standard was first published in 1957. It was subsequently
revised in 1973. In the first revision the requirements for emulsion and
frothing test copper strip corrosion test and low temperature stability
test were modified. The standard was also amended twice in 1975
and 1977.
0.3 The present revision has been prepared as a result of a review of
the standard by the Ad-hoc study group especially set up for this purpose
as we11 as by the concerned technical committee in the.light of the current
requirements of cutting oils and advancement in the field of lubrication
technology in the country. In this revision the title of the standard has
been changed and the requirements for emulsion, frothing and high
temperature stability tests have been modified as per the latest test
methods being followed by the industry.
0.4 In the preparation of this standard considerable assistance has been
derived from the following publications:
i) 3-GP-334 4 Oil, cutting, soluble. Canadian Government
Specification Board; and
ii) INDjSL 3626 ( a )-1951 Oil, 2x-l. Ministry of Defence,
Government of India.
0.5 For the purpose of deciding whether a particular requirement of this
standard is complied with, the final value, observed or calculated,
expressing the result of a test or analysis, shall be rounded off in accord-
ance with IS : 2-1960’. The number of significant places retained in
the rounded off value should be the same as that of the specified value in
this standard.

*Rules for rounding off numerical values ( reuisud ).

3
 IS:1115-1986

1. SCOPE

1.1 This standard prescribes the requirements and the methods of

sampling and
__ test for general purpose cutting oil, soluble intended for
use in machines where the use of a suitable cutting oil giving a non-
transparent aqueous emulsion.is permissible as coolant and lubricant for
cutting tools.

2. REQUIREMENTS

2.1 General Requirements

2.1.1 The material shall be prepared from mineral lubricating oil

having a flash point of 15O”C, Min when tested by IS : 1448 ( P : 69 )*,
together with emulsifiers, bactericides, stabilizers and other additives, if
necessary.

2.1.2 The oil shall be clear, homogeneous and free from foreign
matter, sediment and visible impurities. It shall not contain any
ingredients injurious to persons using or handling it either in the original
state or in the form of an emulsion. The oil should be free from any
pungent or unpleasant odour.

2.2 Specific Requirements - The material shall comply with the.

requirements prescribed in Table 1 when tested according to the methods
prescribed in the relevant appendix to this standard and ‘P :’ series of
IS : 1448t. Reference to the relevant methods of test is given in
Table 1.

3. PACKING AND MARKING

3.1 Packing - The material shall be packed in securely closed metal

drums or any other suitable containers of appropriate size and strength
as agreed to between the purchaser and the supplier.

3.2 Marking - Each container shall be marked with the following

information:

a) Name of the material;

b) Manufacturer’s name, initials or his trade-mark, if any;
c) Quantity of the content; and
d) Batch number and year of manufacture.

*Determination of flash and iire point by Cleveland ( open) cup.

tMethods of test for petroleum and itsproducts.

L
 iS:lllS-‘1986

TABLE 1 REQUIREMENTS FOR GENERAL PURPOSE CUTTING

OIL, SOLUBLE
( Clauses 2.2, 4.1 anu 5.2 )

RLQUIREMENXS METHOD OF TEST,

REFTO
~__-_*----~
Appendix P:ofIS:’
1448+

(1) (2) (3) (4) (5)

Aah, percent by mass, Max 3.5 - P:4
i)
ii) Water, percent by mass, Max 10’0 - P:ul
iii) Emulsion test, 5 : 1 and 20 : I 0-l ml oil and - P : 98
ratio in water of 400 ppm 0.2 ml cream
hardness ( as CaCO, ) permitted
iv) Frothing test, 5 : 1 and 20 : 1 No froth after - P : 99
~$;t$)~ ppm hardness 15 minutes

v) Cast iron corrosion test,20 : 1 Oil-1 A -

ratio emulsion with 400 ppm
hard water ( as CaCO, ),
Max
vi) Copper strip corrosion teat at Not worse than - P: 15
100% for 3 hours No. 1
vii) Thermal stability teat Shall pass the test - P: 100
viii) Flash point, COC, “C, Min 150 P : 69
( sac Note )
ix) +%scodty at 40°C, CSt, Mitt 20 - P : 25
x) *Volatile matter at 100°C for 20 IB
16 h, percent by mass, Max
NOTE -- Take 200 g of soluble oil teat sample. Add 25 to 30 g of anhydrous sodium
sulphate. Stir thoroughly for 5 minutes, keep it in the oven at 40% for one hour.
Decant tile oil and subject it to,flaah point determination by Cleveland ( open ) cup
method.
*Methods of teat for petroleum and ita products.
tl’hese tests are applicable only for defence requirements.

3.2.1 The container may also be marked with Standard mark.

3.2.2 The use of the Standard Mark is govered by the provisions of the
Bureau of Indian Standards Act, 1986 and the Rules and Regulations made
thereunder. The details of conditions under which the Iicence for the use of
StandardMark may be granted to manufrcturenror producc~ may be obtained
from the Bureau of Indian Standards.

5
D

IS I 1115 - 1986

4. KEEPING PROPERTIES
4.1 The material when stored in original sealed containers under
ambient temperature conditions in shade shall retain the properties
described in Table 1 for a period of not less than 6 months after the
date of delivery.
5. SAMPLING
5.1 Representative samples of the material shall be drawn as prescribed
in IS : 1447-1966*.
5.2 Number of Tests and Criteria for Conformity - Tests for
emulsion, frothing, cast iron corrosion and thermal stability shall be
conducted on three of the individual samples each, and there shall be
no failure if the lot is to be accepted as satisfactory in respect of the
above characteristics. For the remaining characteristics prescribed in
Table 1 the tests shall be conducted on the composite sample prepared
according to IS : 1447-1966’ and no failure shall be reported for the
acceptance of the lot.

APPENDIX A
[ Tublc 1, Item (v) ]
CAST IRON CORROSION TEST
( Adapted with permission from the Institute of Petroleum, Standard
No. IP 125/77 Aqueous cutting fluid, corrosion of cast iron )
A-l. SCOPE
A-l.1 Cutting oils which are used in the form of aqueous dispersions or
solutions should not readily permit corrosion of equipment with which
they come into contact. This method is accordingly designed to assess
the behaviour of such fluids in contact with a typical metal, such as cast
iron; and is applicable to samples submitted either in the form of an
aqueous fluid as used in practice or as a concentrate requiring dilution
with water.
A-2. OUTLINE OF THE METHOD
A-2.1 Steel millings are placed on the cleaned surface of a cast-iron plate
and emulsion of the cutting oil under test is poured on to them. After
24 hours the millings are removed and the surface of the plate ia
examined for corrosion.

*Methodr of sampling of petroleum and its products.

6
 A-3. APPARATUS

Ab3.1 Teat Plate - Conforming to Grade 15 of IS’: 210-1978+; 10 cm x

10 cm: x 6 mm ( originally ) of grey cast iron, the surface being ground
to a smooth finish free from chatter marks and burniahings ( CLA 025
to 0.38 pm ).
A-3.2 Steel Millinga - Approximately 6 mm long and 1’5 to 3 mm
width prepared by dry-milling the steel conforming to IS : 226-1975t.
A-3.3 Test Chamber - No dimensional limits are prescribed 6~ the
chamber. The temperature shall be maintained at 27 & 2°C. and the
humidity at 52 f 5 per&m’. The required le.vel of humidity can be
obtained by placing at the bottom of the cabinet at least one open dish,
not Iess than 15 mm diameter, containing a-saturated solution of sodium
bisulphate in contact with an excess of solid bisulphate which give a
humidity of 52 percent at 20°C. Lumps ‘of solid bisulphate should stand
out of the liquid. If a large chamber is used with several platea under
test, several dishes may be desirable. Alternatively, separate chambers,
each with a dish of bisulphate, can be used one for each test plate.
A-3.4 Pipette - Calibrated to deliver 2 ml of the fluid.

A-4. PRErARATION OF SAMPLE

A-4.1 For carrying out this test the 2O:l ratio emulsion shall be prepared
with 400 ppm hard water in accordance with the method given for
emulsion and frothing tests.

A-5. PREPARATION OF APPARATUS

A-5.1 If the surface of any plate is corroded or pitted, regrind the plate
to a smooth surface. Do not allow the plate to become burnished. I

A-5.2 If the thickness of. the plate is reduced to 3 mm, discard it.
A-5.3 Immediately prior to test, prepare the ground surface of the test
plate as follows and do not touch the surface subsequently, Carry out
this procedure irrespective of whether or not the plate has been used
before, and whether or not it is new or reground:
a) Wipe with cotton wool soaked in toluene;
b) Wash with acetone from a wash-bottle;
c) Wipe dry with cotton wool;
-.
*Specification fix grey iron castings. (Udrd rmi~bn ).
tSpecification for rtructural ateel ( standard quality ) (&IA mision j.

- .
IS t 1115 - 1986

4 Rub the plate on a new piece of No. 0 emery cloth placed on

flat surface ( plate glass for example ), rubbing heavily by bar
for 30 double-stokes without lifting in each of two directions
right angles. A hand magnet may be found convenient to ho
the plate for this operation. If .stain marks are still apparet
treat. the plate.as pitted and regrind it;
4 Wipe with clean filter Paper soaked in acetone; and
f) Rub with successive pieces of dry clean filter paper until I
marks are apparent on the paper.

A-6. PROCEDURE
Ad.1 Make the test in a room free from corrosive fumes.
A-6.2 Take the millings and sieve with a standard 710-micron IS siel
[ sss IS : 460 ( Part 1 )-1985* 3. Discard the dust and retain the m:
lings. Discard all the millings if any rust is present.
A-6.5 Wash the millings in acetone and allow to dry in air. Thereafts
the millings should remain untouched by hand.
A-6.4 With the aid of a spatula, place 4 portions each of approximate
2 g of steel millings in a single layer each centrally in a quarter of tl
prepared surface of the plate. Each portion shall be so disposed th
the edges are not in contact either with adjacent portions or the edges
the plate.
A-g.5 Pipette the fluid to be tested on the each portion of millings, ;
that the millings are thoroughly wetted. The fluids on adjacent portio!
shall not run together. About.2 ml of the fluid will be required PI
portion of millings. If testing several fluids at once, put the 4 portio;
on different plates as far as possible, so that each plate has several fluic
on it. This minimizes error due to possible variations in plates.
A-6.6 Transfer the plate to the test chamber, the temperature am
humidity of which is maintained as specified in A-3.3.
A-6.7 After 24 hours, remove the plate from the cabinet, remove tl
millings from the plate and discard them. Wash the surface of the pla
with acetone then with toluene and finally rub gently with a filter pap1
soaked in toluene.
A-6.8 Inspect the surface areas of the plate for corrosion, and recoi
pittings and staining results separately for each test area, for exampl
the areas previously covered by 2 g of steel millings as follows:
Pitting - Record the number of pits present.

lSpecificatiim for test sieves : Part 1 Wire cloth test sievea ( &rd reuitin ).

8
 IS t 1115- 1996

Staining - Record the extent and intensity of staining using the

following numbers.
ProQortioas of Test Arta Staintd Inttnsity of Staining
0 Nil 0 Nil
1 Less than 10 percent ! Hardly perceptible
2 Between 10 and 25 percent 2 Slight staining
3 Between 25 and 50 percent 3 Heavy staining
4 Between 50 and 75 percent 4 Surface damage ( not
including pits )
5 Over 75 percent
NOTE- If staining ia not uniform record the maximum intensity observed.

A-7. REPORTING
A-7.1 Report the results by three numbers, the first being the number of
pits, followed by an oblique stroke; the second, the area of staining
followed by a hyphen; and the third, the maximum intensity of staining
( for example: O/l-l, S/O-O, O/3-2, etc ).
A-7.1.1 Also report’relevant test details, as follows:
a) Nature of added water used; and
b) Dilutian if known and method of preparation, if relevant.

A-8. PRECISION
A-8.1 The precision cannot be expressed in a useful form to cover all
cases. Extensive investigations have shown that it is very poor when the
corrosion probability is of the order of 50 percent, but that it is better
when either very little or considerable corrosion occurs. The use of
statistically designed programmes are recommended whenever compara-
tive tests are to be made.
PS:1115 - 1986

APPENDIX B
[ z-able 1, Item (x) ]
DETERMINATION OF VOLATILE MATTER

B-l. PROCEDURE
B-l.1 Place 10 f 0.1 g of the sample in a clean, dried and weighed
petri dish of 100 mm diameter and weigh to the nearest 0.01 g.
B-1.2 Place the sample in the petri dish in an oven maintained at
100 5 1°C for 16 h.
B-l.3 At the end of the heating period remove the petri dish from the
oven, cool to room temperature and weigh to nearest 0.01 g.
B-l.4 Calculate the volatile matter as percent by mass.

10
 IS : 1115- 1996
( Continfudfrom pub’ 2 )

Metal working Products Subcommittee, PCDC 4 : 13

c.hwma Rrpmmling
BERI K. C. MEHTA Indian Oil Corporation Ltd ( Research & Develop
ment Centre ), Faridabad

SHRI FAIURA Smoa ( Ahmatr to

Shri K. C. Mehta )
SHRI A. K. ARORA Rourkela Steel Plant, Rourkela
Da N. T. BADDI Association of Manufacturers of Petroleum Specia-
lities, Bombay
SARI R. CHAKRAVARTY ( Ahnatr )
SERI M. K. BHARQAVA Petroleum Re-Refiners Association of India, Madras
SH~I SHANTILAL DAYA ( A&em& )
SHRI S. R. BHATWAOAB Indrol Lubricants & Specialities Ltd, Bombay
SHRI N. SETHURUAN ( Altematc )
SHBI A. K. CAPRIHAN Indian Aluminium Co Ltd, Calcutta
SHRI A. K. HAJARA ( A&n& )
SARI C. V. CHANDEASEEHAB Balmer Lawire St Co Ltd, Bombay
SHRI R. R. SARAN ( AI&n& )
TEE CEEXIST & METALLURQIST Railway Board ( Ministry of Railways )
ASSTT RESEARCH OBBICER
( Came ), RDSO, LUCXNOW ( Altemats )
SHRI S. GHOSE National Test House, Calcutta
SHRI P. K. CEAKRABORTY ( Alternafe )
SHRI H. JA~EY Petrosil Oil Co Ltd, Bombay
SHRI M. A. PAES ( Alternate )
SHRI V. K. JAIN Indian Institute of Petroleum, Debra Dun
SHRI B. R. CHADHA ( Alternate )
SHRI 0. K. JUN~EJA Bharat Petroleum Corporation Ltd, Bombay
SERI P. P. NACURKAR ( Altcmak )
SHRI B. LAKSHMINARAYAN Indian Oil Corporation Ltd ( Marketing Division ),
Bombay
SHRI M. Q. KHAN ( Alt.matc )
SHRI A. K. MISRA Bokaro Steel Plant, Bokaro
SERI M. P. PATHAK ( Alternats )
SHRI M. RADHAERIBHNAN Central Machine Tool Institute, Bangalore
SBRI S. HANUMANTHA RAO ( Al&mats )
SERI B. SAN~HAVI Lubrizol India Ltd, Bombay
SHRI R. R. PARMAR ( Altarnate )
SHRI S. P. SARMA Hindustan Petroleum Corporation Ltd, Bombtiy
SERI’D. W. RAUT ( Alternate )
SH~I S. SATHPATHY Bharat Aluminium Co Ltd, Korba
SHRI S. C. VARBHNEY ( Altcrnatr )
SHRI M. J. SHAH Indian Oil Blending Ltd, Bombay
SHRI S. P. PERE~A ( Ahnate)
SHRI K. B. SHRIVASTAVA Tide Water Oil Co ( India ) Ltd, Calcutta
SHRI J. NAIK ( Altematr I )
SHRI N. C. MITTAL ( Altmats II )
SEEI R. V. SINQH Hindustan Aluminium Corporation, Renukoot
SERI 0. P. GUPTA ( Altmuztr )

11
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