Analysis of Raw Water ( Part Analysis)

Date Description pH Chloride Hardness Analysed by

Analyst: Approved Chemist

Calculation :

1. Oxidisable substance:
Sample: 100 ml of sample + 10 ml of sulphuric acid + 0.1 ml of 0.02 M potassium permanganate; boil.
Observation: _________________________________________________.
Complies/ Does not Comply
 2. Sulphate:
Sample: 10 ml sample + 0.1 ml of 2M HCl + 0.1 ml of barium chloride solution.
Observation: The appearance of the solution change/ does not change within 1 hour.
Complies/ Does not Comply

3. Chloride
Take 100ml sample water in conical flask, add 5ml of 5% potassium chromate
solution as indicator and titrate Vs 0.1M silver nitrate, to change the colour from
yellow to brown.
Eeach ml of 0.1M silver nitrate contain 0.00355gm of chloride.

B.R. X Factor X 1000000X N = ________PPM of chloride

Water in ml X 0.1

4. Hardness
Take 100 ml of sample water in conocal flask + 20 ml Dil. Ammonia , add 1-2 ml Erichrome Black T, Titrate
against 0.02M EDTA

Calculation : T.R x 20 = ppm

5. Residue on Evaporation: (Lt. NMT 0.05% w/v)

100 ml of Sample taken for test
i) Weight of evaporating dish + residue =----------------------- gm
ii) Weight of evaporating dish =----------------------- gm
iii) Weight of residue =----------------------- gm
% Residue = _________________ x 100
100

= ----------------------- %

Analyst: Approved Chemist

Date :-
To,
Q.C. DEPARTMENT
Subject : Requisition for Raw water
Sir,
Please collect the sample of Raw Water for analysis purpose and give testing report as early as
posible.

Regards
Department

Date :-
To,
Q.C. DEPARTMENT
Subject : Requisition for Raw water
Sir,
Please collect the sample of Raw Water for analysis purpose and give testing report as early as
posible.

Regards
Department
To,
Q.C. DEPARTMENT

Subject : Requisition for DM water

Sir,
Please collect the sample of D.M. Water for analysis purpose and give testing report as
early as posible.

Regards
Production Department
 MICROBIOLOGICAL ANALYSIS OF RAW WATER

Department : Quality Control (Microbiology) Sampled By :

Point No. : Report No. :

Qty. sampled: Date of Analysis :
Date of Sampling: Date of Report :

REPORT OF ANALYSIS

Tests Result of Analysis Limits

MICROBIAL LIMIT TEST
1. Total Viable Count
a) Total Bacterial Count TBC) Action Limit-500 cfu/ml
Alert Limit-200 cfu/ml
c) Total Fungal Count (TFC)
Action Limit-10 cfu/ml
Alert Limit- 5cfu/ml
2. Pathogen Testing
a)Eschericha coli Absent
b) salmonella Absent
c) Pseudomans aeruginosa Absent
d) Staphylocococcus aureus Absent

]
REMARK: In the opinion of undersigned the above sample complies / does not complies with the specification
prescribed unde IP/BP/USP/ In House specification.

Tested By: Checked by : Approved By: