LIGA PROCESS: SENSOR CONSTRUCTION TECHNIQUES VIA X-RAY LITHOGRAPHY
W. Ehrfeld 1), F, Gotz 2), . MUnchmeyer 1), W. Schelb 1,. Schmidt 1)
1) Kernforschungszentrum Karlsruhe GmbH,
Institut fur Kernverfahrenstechnik, P.O, Box 3640,
15:7500 Karlsruhe 1, Federal Republicof Germany
2) Steag AG, P.O. Box 10 37 62, 0-4300 Essen 1
Federal Republicof Germany
Abstract
A large variety of microsensors and components for
microactustors can be fabricated by the so-called UGA
method which s based on deep-etch Xray ithography,
croforming and molding processes (im German Leh
‘raphie, Galvanoformung, Rbformung), This microfabn.
Ebtion technique allows to generate devices wth minimal
tateral dimensions inthe micrometer range and structural
heights of several hundred micrometers rom metalic and
plate materia, In contrast to rventation dependent
Etching of monocrysaine silicon there are no retrtions
inthe crow-sectional shape of the microstructures Various
Concepts of sensors for measuring vibration, acceleration,
postion, spectral distribution, radiation, composition of
mixtures etc are presented
{Introduction
Technological advances in lithography continue to drive
the level of integration and the reduction in minimum
feature size of semiconductor products. In the laboratory
scale, optical lithography which 1s by far the most im.
portant technique in present production lines has reached
the 0.5 um range required for the fabrication of 16 Mbit
memory chips. For mass production of 64 Mbit and even
more advanced devices, X-ray lithography is expected to
Became the preferred technique [if itis capable to gen
erate minimum dimensionsin the 0.2 um range.
Besides semiconductor devices, a large number of other
‘microstructure products may be fabricated by means of X
Fay lithography. The so-called LIGA process which i based
on deepsetch X-ray lithography with high quantum ener
‘ay synchrotron radiation, electroforming and molding
Brocesses {in German’ Lithographie, Galvanoformung,
Abformung) allows to produce microstructures with lat
feral dimensions in the micrometer range and structural
heights of several hundred micrometers from a variety of
materials (2, 3). ts application potential covers microelec
tronics, sensors, microoptis, micromechanics and biotech
nology (4
This paper gives a short overview of the LIGA process and
its application patential for fabricating microsensors
Microfabrication Process
The principle of the LIGA method 1s evident from the pro-
cess sequence shown in Figure 1. A polymeric material
{resist} which changes its dissolution rate in a liquid
folvent (developer) under higheneray irradiation, is ex
posed through an X-ray mask to highly intensive parallel
Kcrays. The radiation source ss an electton synchrotron oF
an electron Storage ring which, at present, = the only pos
Sibiiny to_generate the highly collimated photon flux in
the spectral range required for precise deep.etch X-ray
lithography in thick resist layers. f one considers a thick.
ness between 10 and 1000 um for the resist layers to be
Structured, the optimum critical wavelength of the syn-
chrotron radiation source ranges from some 0.1 to 1 nm
for typical resist materials.
Fesist structure rp Ty evelopment
Mott ciuclre STEER cabancterming
tool ot ESTEE eo ae
Moving mess STE — mou ting
Fig. 1: Schematic representation of a process sequence of
{heTIGA metho for mors fabrication of micro-sevices
In the next step, the resist structure is used as a template in
an electroforming process where metal is deposited onto
the electrically conductive substrate, In this way, 9 com.
plementary metallic structure is obtained which can oe
either the final microstructure produet or can be used as 3
‘microtool {mold insert) for multiple reproduction by
means of a molding process.
The micromolding process has been optimized usin
methacrylate based casting resins with avspecial interna
mold release agent In the process sequence shown v0 Fig,
The mold matensal is introduced ino the mold cavities
through the holes of gate plate. Ths plate which has a
formlocking connection with the polymeric microstruc
tures alter Rardering of he reanwrvet ava letras n
8 Second electroforming process for generating secondary
imetallic merostructures, has been demonstrated by
many experiments that inspite of on ospect rato of about
{00 and minimum lateral dimensions of only some micro:
meters, ayeld of approximately 100 % can be obtained in
the micromolding process
The secondary structures are perfect copies of the primary
structures Consequently, mass production of plastic and
metallic merostructures should be feasible without 3
Continuous utilization of a synchroteon radiation source
‘hich only necessary for fabricating mold inser
Sensors
The development of modern sensors aims at miniaturiza:
tion, more complex or array structures and integration
with electronic signal conditioning. Furthermore, the
expenditure for adjustment, trimming and replacement
Should be minimized and, accordingly, the manufacturing
tolerances should be as small as oossible. In this respect
‘THO215~4/88/0000-0001$1-00@ 1988 TEREthe LIGA method has a number of advantages which will
be ilustrated by a description of several sensor devices in
the following.
‘Measurement of vibration and acceleration:
A.LIGA configuration for measuring vibration or acceler
‘tion is shown schematically in Figure 2. By means of
deep-etch Xray ithography a template is generated
‘which allows to manufacture a spring plate and a rigid
Hationary electrode directly upon a microelectronic creurt
fr, correspondingly, a multitude of such arrangements
Spon a completely processed silicon water. The change in
capacity and the corresponding voltage change, respec-
tively, may change directly the electric potential of the
‘gate electrode of a MOSFET circuit
Spring
Stationary |_ sprins
oer. silicon
Z ‘water
MOSFET device
Fig. 2: Schematic representation of a LIGA sensor for
‘measuring vibration or acceleration
Compared to orientation dependent etching of mono:
Gytaline silicon whichis 9 wellknown and proven tech
nique for fabricating similar mntegrated sensors for vibra
{lon measurement. the LIGA. technique should have
‘eveal advantages In partula, he fabrication of the
tectonic circus can Be fully completed prior to the
fabrication of the sensor structure Therefore, no mixing
between micromechanical and microelectronic process
Slepe occurs and a separate optimizations possible forthe
‘ifferent fabriestion procedures Since the sensor element
miged vertcaly upon the electron eeu Une space
quirement is minmized. This should be 2 further ad
Vantage compared to siicon micromechanics where the
Spring plates are usually fabricated in a plane parallel to
ie'wface of the water, Nevertheless, the LIGA method
Silows also to produce cantilever structures which are
Sreanged parallel to the water surface. Moreover, «two
axis sensor arrangement can be simply realized
Measurement of position, displacement and magnetic
For measuring position, displacement, small distances or
changes of a magnetic field, sensor devices using inductive
‘ircuts are Used in alarge number of configurations. The
LIGA method allows to generate small coils or complex coll
arrays from matenais with high electrical conductivity 35
‘well'as microstructures with high aspect ratio from ferro
tlectne materials. Because of the large structural height
attainable by the LIGA process, 2 low electrical resistance
Gan De realized for small cals, which isan obvious advan.
tage compared to corresponding configurations. gener
ted by thin film techniques whereas, compared to thick
film techniques, much smaller dimensions and tolerances
can be obtained
Figure 2 shows a scanning electron micrograph of a helical
Structure generated by Xray lithography. It is used for
Fabricating two intermeshing coils by electrodeposition
which serve as the transmitting and receiving unit, re
spectively
fig. 2; Scanning electron micrograph of a resist template
ft Tabncating eno intermesting mitocols
Microoptical devices and spectrometry:
In the field of microoptics, the LIGA process could be used
for fabreating waveguides, gratings, small prisms and
Small cylindrical lenses. zone plates, polarizers and spectral
ters for the infrared range, spatial filters, modulators
and many other optical devices and structures. More or
less arbitrarily, one may discriminate between two basic
configurations. One Is represented by a perforated, set
Sepperting membrane of plate structure which is put into
the path of rays and where the optical effect vs de.
termined by the special pattern of perforation. The other
configuration may be characterized by the fact that opti
cal structures are generated on a stable substrate where
the path of rays is parallel to the surface of the substrate
land partially determined by a waveguide structure. In the
follawing, two special examples of these basic configura:
tions will be described.
Figure 4 illustrates the principle of a small simultaneous
spectrometer, It has @ Rowland configuration with 2
curved reflective grating and comprises a slab waveguide
Consisting of three layers of transparent X-ray resist with
matched refractive indices. In spite of the relatively low
Tesglution of this microspectrometer, it might be a cheap
‘nd reliable sensor for photometric analysis of mixtures,
chromatic testing, optical film thickness measurement,
fete in the field of communication technology, this device
‘Gan be applied 28.9 low-cost wavelength division mult:
lexeridemultipiexer.
Fig. 4: Schematic representation of a simultaneous micro-
spectrometerIn the field of infrared spectroscopy, bondpass oF cut-off
fiers can be realized as 9 So-called fesonant mesh, 6. By
B metalic membrane wth a multitude of rose shaped, Y
Shoped oF crcular openings whose cimensions and
tances correspond to the mavelength to be transmitted (5,
61 Such seltupparting membranes with the desired con
figuration of the openings can be fabricated by ray
thography and electrotorming a demonstrated by
Figures
Fig_S: Seanning electron microgeaph of 9 Y-shaped
‘pening with 2 sit width of 5 ym in'9 nekel membrane
‘with a thickness af 300.3,
further development work deals with the fabrication of
highly preese supporting and positioning elements fo
fiber optiesl sensors ana with ithographie generation of
tnaveguide elements from transparent Xray ress
Flusdic devices:
The first development work on the LIGA process aimed at
the fabrication of micron sized siit-shaped nozzles for
Uranium sotape separation a shown Wm Figure & Con
Sequently, other flow devices and, in particular, fluid
Sertsars Tor measuring positon, gas densty, composition
Gf mixtures ete. can be produced Because of the smal
dimensions, a favorably low response time should be ob.
tainabie and such devices would be applicable even unger
Conditions where mergelectrome dewces are difficult 0
operate, eat high fadiation level Further flow de:
kes might be columns for chramatograntiy, micra-coa
ing systems based on the Joule. Thompron effect. anemo:
mete sensors, sieves for determining the size distribution
Gh partcles, miro-vaives ete
Measurement of radiation
Concepts have been worked out for fabricating micro:
Shannel plates and arrays of secondary slectran mult
Dliersn Contrast to the standara processes far producing
Ehannel plates, the tolerances of the dimensions can be
feduced nd the positions canbe exactly determined. AS 3
fesult single channels or groups of channels can be
matched directly ta other dtcrete microstructures at the
Input or output af a miero-channel platen the case of
miniaturized electron multiplier arrays, the dynodes can
Be"arranged ina ringishaped or any other curved con.
figuration required nn experiment
Fig 6. Scanning electron micragraph of » double de
fiecting separation nozsie electioformed from miexel the
minimum sit width of the curved nozzle is 3 um, the sit
Fength is about 300 um
tical and Optical Micraconnectors
The continuous increase of logic functions in micro.
processor chips and the decrease in