Caliculation of Measurment Uncertainity

Details of UUC
Instrument Name Electronic Weighing Balane
Make SHIMMADZU
Range 220 g
Readability 0.00001 g
SL.No D450041248
Model.No BC/EWM/01
ID.No

Details of Master Used

Instrument Name Weight Box
Make WI
Range 1 mg to 200 g
SL.No
Model.No F1 Class
ID.No
Uncertainity of The Master 0.000099 g

Environmental Condition
Initial Final Mean Variation
Temperature 21.7 21.5 21.6 0.2
Relative Humidity 48 52 50

Drift (taken from Manual) 1 ppm 0.000001

Sensitivity Drift due to Temperature Variation(t*drift*Max Load)= 0.00004400
Pan Radius d2 = 10 d1= d2*1/2 = 5

Observation Data

test pointReferance Used

Referance mass UUC Reading in g
SL.No in g in g values in g Set 1 Set 2
1 0.100 0.100 0.1000100 0.10008 0.10008
2 0.500 0.500 0.5000400 0.50006 0.50006
3 1.000 1.000 1.0000300 1.00004 1.00004
4 2.000 2.000 2.0000400 2.00007 2.00007
5 5.000 5.000 5.0000800 5.00004 5.00004
6 10.000 10.000 10.0001000 10.00011 10.00011
7 20.000 20.000 20.000140 20.00018 20.00018
8 50.000 50.000 50.000000 50.00022 50.00022
9 100.000 100.000 100.0001 100.0002 100.0002
10 200.000 200.000 200.000200 199.9995 199.9995
Max error due to linearity =
Eccentric Load Test
Weighing LocationUUC Indication(g)
Mean of each point
Mean Diff from centre to Others
 1 CENTER 50.00005 50.00005 1
2 BR 50.00004 50.00004 2 -0.00001
3 FR 50.00004 50.00004 3 -0.00001
4 FL 50.00005 50.00005 4 0.00000
5 BL 50.00006 50.00006 5 0.00001
1 CENTER 50.00005 Eccentric error (Max mean diff from center to other points)
5 BL 50.00005 Eccentric error(D) 0.00001 g
4 FL 50.00005
3 FR 50.00004 d1/d2*D = 0.0000025
2 BR 50.00004
1 CENTER 50.00005
Standard Deviation(half load)0.00004830 g
Standard Deviation of Mean 0.00001528 g

ua Uncertainity Due to Reapetability = 0.00004830

u1 Uncertainity due to Standard(taken from cal.certificate)= 0.000099
u2 Uncertainity due to Resolution(50% of Balance Resolution) 0.000005
u3 Uncertainity due to drift sensitivity due to temp(t*drift*Max
0.00004400
Load)=
u4 Uncertainity due to Eccentic Loading(d1/d2*D)/2√3 0.0000025
u5 Uncertainity due to Linearity Test(Max Error)= 0.000160

Uncertainty Budget
Source of Limits
Probability distribution
Standard UncertaintySensitivity Uncertainty
Uncert Xi ± Xi mg Type A or Type B U(Xi) Coefficient Ci
Contribution Ui(y)
ua 0.00004830A N /sqrt(10) 0.0000153 1 0.0000153
u1 0.000099 B N/2 0.0000495 1 0.0000495
u2 0.000005 B R/sqrt( 3) 0.000003 1 0.0000029
u3 0.00004 B R/sqrt( 3) 0.0000127 1 0.0000127
u4 0.0000025 B R/sqrt( 3) 0.0000007 1 0.0000007
u5 0.00016 B R/sqrt( 3) 0.00004619 1 0.0000462

Combined Uncertainity
Uc = √ *(ua)² + (u1)² + (u2)²
Uc 0.00007062 g
Degree of Freedom=Veff=(Uc/U5)^4*n-1
4111.362951
n is Number of Readings
Coverage Factor(K)= 2
(95% of Confidence Level)
Expanded Uncertainity Ue=Uc*k 0.0001412 g

After Rounding Ue=

0.00014 g

After Rounding Ue= 0.14 mg