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Int J Adv Manuf Technol

DOI 10.1007/s00170-017-0306-1

ORIGINAL ARTICLE

Effects of friction stir spot welding parameters on morphology


and mechanical property of modified cast nylon 6 joints produced
by double-pin tool
Yinfei Yan 1 & Yifu Shen 1 & Wei Zhang 1 & Wei Guan 1

Received: 24 December 2016 / Accepted: 13 March 2017


# Springer-Verlag London 2017

Abstract A newly designed tool with double pins was uti- performed by a tool with a conventional cylindrical pin. The
lized in the underwater friction stir spot welding (UFSSW) of maximum shear strength of 30.2 MPa was obtained, which
modified cast nylon 6 sheets. A circular gasket was added was about 58.4% of the base material.
between two sheets, acting as additional filler material to the
nugget zone. The effect of welding parameters (rotational Keywords Double pins . Friction stir spot welding . Modified
speed, plunge rate, plunge depth, dwell time, and waiting cast nylon 6 . Morphology . Shear strength
time) on weld formation and joint shear strength was investi-
gated. Crown appearance and cross-sectional morphology of
joints produced at different welding parameters were observed 1 Introduction
and compared. Lap-shear tensile tests were carried out to eval-
uate the joint strength. The results showed that joints per- Modified polymeric materials with lightweight as well as im-
formed at excessive rotational speed, large or low plunge rate, proved mechanical properties are increasingly replacing metal
high plunge depth, and extreme dwell time displayed extru- alloys in the automotive industry [1]. This tendency aims at
sion rings accompanied with cavities throughout or near the reducing the weight of vehicles to improve their performance
bonded areas. Cracks were formed at small rotational speed and decrease the energy consumption. It is well known that
and short dwell time. With the increase of welding parameters spot joining is a common and critical joining technology in the
except waiting time, the joint strength increased first and then manufacturing of vehicles [2]. The increased application of
decreased. Increased waiting time exerted a positive effect on polymeric materials in automotive industry undoubtedly
the weld formation and strength. Two fracture modes, namely makes a new request for the spot joining method [3].
cross nugget mode and pull nugget mode, were observed in Generally, polymeric components can be spot joined by me-
the lap-shear tests. Joints failed with cross nugget mode gen- chanical fastening (riveting, bolting, etc.), bonding (adhesive
erally showed larger fracture loads and displacement than bonding and solvent bonding), or spot welding (friction spot
joints fractured with pull nugget mode. The maximum joint joining, laser transmission spot welding). However, mechan-
fracture load was 2825.2 N, which was larger than the joint ical fastening requires external parts and substantial labor in-
put. Also, stress concentration usually happens near the fas-
tened joint [4]. The evaporation of adhesive or solvent used in
Electronic supplementary material The online version of this article
(doi:10.1007/s00170-017-0306-1) contains supplementary material,
the bonding process is harmful to the environment and the
which is available to authorized users. workers’ health [4]. What is more, surface preparation in ad-
hesive bonding and slow reaction in solvent bonding are both
* Yifu Shen time-consuming. Friction spot joining [5] relays on the con-
yfshen_nuaa@hotmail.com duction of the frictional heat generated between the upper
sheet and rotational tool to soften the material near the lapped
1
College of Materials Science and Technology, Nanjing University of
surface. However, due to the low thermal conductivity of ther-
Aeronautics and Astronautics (NUAA), Yudao Street 29, moplastic, it is hard to be applied to join two plastic work-
Nanjing 210016, People’s Republic of China pieces. Laser transmission spot welding works by the laser
Int J Adv Manuf Technol

radiation. Upper sheets are usually transparent to transmit the PMMA and PMMA-SiO2 nanocomposite. Sharp weld lines
laser, and the lower sheets should effectively absorb the laser were generated at low rotational speed, and excessive plastic
radiation [6]. In this case, the weld materials are limited and deformation, volumetric defects, and a lack of material mixing
the additional work, such as adding absorbing particles be- were observed when rotational speed was excessive. They
tween lapped surfaces [7] to reinforce the absorbing efficien- [12] also found that the existence of SiO2 was able to improve
cy, is required before welding operation in some cases. the material conductivity, which, in turn, enhanced the soften-
Friction stir spot welding (FSSW) is another spot welding ing and the flow of weld material. The weld was better refilled,
technology to thermoplastics, which depends on the frictional and the defect of weld line became smoother. Gonçalves et al.
heat and deformation heat to soften the materials. It possesses a [14] also friction spot welded carbon fiber-reinforced polyam-
number of advantages compared with above methods, such as ide 66 laminates. They concluded that the strength of the joint
small or no preparation work, low energy consumption, no was comparable to that produced by ultrasonic welding.
emission of harmful gas, and small thermal effect on the work- Paoletti et al. [22] monitored the evolution of plunge force
pieces. Also, it is easy to be automotive and has been demon- and torque in the FSSW of PC plate. The maximum plunge
strated to be feasible to joining almost all thermoplastics, in- force was generated just after the pin touched the sheet surface,
cluding high-density polyethylene (HDPE) [8–10], and the torque underwent a steep increase when the shoulder
poly(methyl methacrylate) (PMMA) [11–13], polyamide (PA) touched the upper sheet. The tool temperature increased with
[14], polypropylene (PP) [15–20], acrylonitrile butadiene sty- the plunging of the tool. In another paper, they [23] showed that
rene (ABS) [21], and polycarbonate (PC) [22–26]. Until now, the plunge force and torque simultaneously increased with the
researchers have done excellent work in the FSSW of thermo- increase of plunge rate or the decrease of rotational speed; the
plastics, including the investigation of tool geometry and fea- material temperature was lowered when plunge rate increased
tures, the investigation and the optimization of process param- and rotational speed and dwell time decreased. Lambiase et al.
eters, the modification of FSSW tool, and the measurement and [24, 25] investigated the influence of tool geometry on plunge
the control of material temperature and tool force. load, torque, and mechanical behavior in FSSW of PC and
The effect of pin profiles on joint formation has been studied concluded that the taper angle of the pin had a negligible effect
by Bilici and Yükler [8] in the FSSW of HDPE. The tool with on plunge load and torque and it affected the joint shear strength
tapered pin and concave shoulder bottom was found to be the only when the diameters of shoulder and pin were small. The
best in producing a joint with excellent performance. Tool fea- load and torque increased with the increase of shoulder diame-
tures were found to be an important factor to the joint quality by ter and pin diameter. Increased shoulder diameter had a positive
Bilici [16] in the FSSW of 4-mm PP sheets. The tapered pin tool influence on shear strength while large pin diameter was not
with 7.5 mm pin diameter, 15° pin angle, 5.5 mm pin length, beneficial to joint strength. Based on their previous work, they
30 mm shoulder diameter, and 6° shoulder angle was determined investigated the effect of plunge force on the joint strength.
to be the optimal geometry. Using such optimal tool, Bilici and They found that the proper control of the plunge force in the
Yükler [9, 10] determine the influence and importance of process FSSW process can promote joint strength up to 37% [26].
parameters on HDPE joints. Increased rotational speed, dwell Optimizing the welding parameters, selecting an appropriate
time, and plunge depth led to an obvious increase of joint strength FSSW tool, developing an advanced tool, adding additives, and
initially, but a slight strength decrease happened when parameters so on are some feasible ways to promote joint strength. An
became larger than the critical values. Plunge rate had a negligible FSpW tool [14] is an advanced tool that can successfully pro-
effect on joint quality. Dwell time was determined to have a duce joints without keyholes, but it makes a high request for the
dominant effect on joint strength while plunge depth was found
to be insignificant. The optimization of process parameters to
produce optimal joints was done by Bilici [15] in another paper.
The Taguchi approach was utilized to arrange the experiment,
and the optimal welding parameter was determined. Compared
with welds produced with initial parameters, the joint strength
was promoted about 47.7% at the optimal parameter conditions.
Dashatan et al. [21] successfully friction stir spot weld
PMMA and ABS sheets by an improved tool with a stationary
shoulder. All the parameters, especially the plunge rate, had
dramatic effects on joint strength. Increased dwell time or
decreased plunge rate had a positive effect on joint quality.
To remove the undesired keyhole usually produced by a con-
ventional tool, Junior et al. [11] adopted a tool whose sleeve Fig. 1 a The dimension (in mm) and b the photograph of the double-pin
and pin can move independently to friction spot weld (FSpW) tool
Int J Adv Manuf Technol

clamped by a properly designed clamping system, and the


overlapped area was set as 50 × 50 mm2. A modified comput-
er numerical control (CNC) milling machine and a self-
designed double-pin tool were used to friction stir spot weld
MC901 sheets. The diameter and the length of double pins are
Fig. 2 The schematic of the water tank
3 and 7.8 mm, respectively, and the distance between the
double pins is 4 mm, as illustrated in Fig. 1. The pin and the
equipment and consequently increases the cost. A conventional
shoulder were machined from bearing steel GCr15 and struc-
single-pin tool always produces joints with large keyholes in
tural steel 1045, respectively.
the center of the weld, which occupy large volumes of the
Material extrusion was the common phenomenon in the
nuggets. To reduce the equipment cost as well as increase the
FSSW of polymeric materials in air condition in the previous
nugget size, a tool with double pins was designed and applied
researches. Simões and Rodrigues [28] reported that the loss
in the FSSW of modified cast nylon 6 in the present paper. It
of filler material usually happened in the material squeezing
aimed at increasing the nugget size by softening the material
process, which, in turn, resulted in the formation of weld dis-
around and between the rotating pins simultaneously. In this
continuities. Therefore, in order to avoid the formation of
experiment, the FSSW process was designed to be operated
defects resulted from the extrusion of filler material in the
underwater [27]. The feasibility of FSSW modified cast nylon
FSSW of modified cast nylon 6, the experiments were de-
6 sheets by a double-pin tool in water was demonstrated first.
signed to be carried out underwater. In this case, an under-
Soon afterwards, the effect of welding parameters (plunge rate,
shoulder material was hard to be softened and material extru-
plunge depth, rotational speed, dwell time, and waiting time)
sion can be restricted. To carry out experiments underwater,
on the weld formation and joint shear strength was studied.
water tank is installed on the surface of the upper sheet, as the
schematic shown in Fig. 2.
Figure 3 shows the steps of underwater friction stir spot
2 Materials and methods
welding (UFSSW) of MC901 sheets. At the beginning of
the plunging phase, the tool rotates at a predetermined speed
In the present investigation, the modified cast nylon 6
(rotational speed) and then moves to the workpiece in the
(Nylatron MC901) with the size of 120 × 50 × 6 mm3 was
vertical direction at a certain rate (plunge rate). The initial
friction stir spot welded. It is a kind of heat-stabilized cast
axial displacement (DA) of the tool is 0 mm, and it starts to
nylon with high toughness and fatigue resistance. The mea-
increase when the pins touch the upper sheet. When the shoul-
sured result shows that the tensile strength of MC901 is
der touches the upper sheet, the rotating tool continues to
89.6 MPa and the break elongation is about 28%. Then, the
plunge for a certain depth (plunge depth). The stirring phase
corresponding shear strength of 51.7 MPa can be calculated
starts after the finish of the plunge of the tool. In the stirring
according to the von Mises criterion [26]
phase, the tool only rotates at the preset speed. The material is
pffiffiffi
τ s ¼ σs = 3 ð1Þ gradually softened by the frictional heat and is mixed by the
rotating tool simultaneously. The duration of the stirring phase
where τs is the shear strength of the base material and σs is the is called dwell time. At the end of the stirring phase, the tool
tensile strength of the base material. The specimens were stops rotating immediately and keeps immobile for a proper

Fig. 3 Steps of UFSSW of


MC901 sheets by the double-pin
tool. a Plunging. b Stirring. c
Waiting. d Retracting. A-A
geometry of the bonded area [8]
(X is the diameter of the bonded
area)
Int J Adv Manuf Technol

Table 2 The experimental arrangement of welding conditions

Constant parameters Variables Specific values

PR15PD0.4DT25WT15 R 400 600 800 1000 –


R600PD0.4DT25WT15 PR 5 15 25 35 –
R600PR15DT25WT15 PD 0.2 0.4 0.6 0.8 –
R600PR15PD0.4WT15 DT 5 15 25 35 45
Fig. 4 The morphology of the spot welds a without a gasket and b with a R600PR15PD0.4DT25 WT 0 5 10 15 –
gasket performed at the same welding parameters

time (waiting time). The proper waiting time was demonstrat- is the plunge rate (mm/min), PD is the plunge depth (mm), DT
ed to be necessary by Bilici and Yükler [9], who reported that is the dwell time (s), and WT is the waiting time (s). Therefore,
the joints produced with no waiting time had the fracture load R 6 0 0 m e a ns a r o t a t i o n a l sp e e d o f 6 0 0 r p m a n d
much lower than that performed with 30 s waiting time. PR15PD0.4DT25WT15 means a plunge rate of 15 mm/min,
Finally, the tool retracts from the weld zone and a spot weld plunge depth of 0.4 mm, dwell time of 25 s, and waiting time
joint is formed. It should be noted in Fig. 3a that a cylindrical of 15 s.
gasket (MC901) is placed between two workpieces and a cir- In the preliminary trial and error phase, it was found that
cular groove with the depth of 0.5 mm is processed on the R600PR15PD0.4DT25WT15 was a proper welding condition
surface of the lower sheet to locate the gasket. The addition of because the weld produced with such combination was excel-
gasket aims at removing the cavities that resulted from mate- lent. Then, based on the parameter combination, each single
rial shortage. The diameter and thickness of the gasket are 9.6 parameter was allowed to change among the ranges shown in
and 2 mm, respectively, which are determined after the trial Table 1 according to the control variable method. The detailed
and error method. Figure 4 shows the morphology of two arrangement of welding parameters is listed in Table 2. The
joints performed with and without a gasket at the same crown appearance and cross section of spot welds performed
welding conditions. The weld produced without a gasket with the arranged parameter combinations were observed and
shows a concave crown appearance and a cavity while the compared. The characteristic morphology was analyzed by an
weld performed with a gasket is defect-free, as shown in optical microscope. In this way, the influence of parameters on
Fig. 4a, b. Figure 3(A-A) shows the geometry of the bonded the joint formation can be investigated. The lap-shear tensile
area, which is produced by cutting along the lapped interface. loads (LT) of the specimens (as the configuration shown in
The area of the bonded area can be calculated by putting the Fig. 5) were tested via the CMT 5105 SANS microcomputer
diameter of the bonded area (X) into the following equation: control electronic universal tensile testing machine. Tests were
  carried out at room temperature (20 °C), and the cross-head
AB ¼ π X 2 −18 =4 ð2Þ speed was set as 50 mm/min according to ASTM D638-10.
The joint shear strength (SS), which was influenced by the
material mechanical properties, the weld morphology, and
The crude ranges of welding parameters were obtained by
the joint geometry, was calculated by the equation
referring to the research studies conducted by previous re-
 
searchers. Then, the proper ranges of parameters that can pro- S S ¼ LT =AB ¼ 4LT =π X 2 −18 ð3Þ
duce joints with characteristic morphology were determined
by trial and error. Table 1 reveals the corresponding symbols
and ranges of the welding parameters. The utilization of sym- where SS was the shear strength, LT was the lap-shear tensile
bols aims at simplifying the expression. The specific designa- load, and AB was the area of the bonded area. The shear
tion is depicted as follows: R is the rotational speed (rpm), PR strength of the joints was obtained by averaging five

Table 1 The welding parameters and the employed value ranges

Symbols Welding parameters Units Range

R Rotational speed rpm 400–1000


PR Plunge rate mm/min 5–35
PD Plunge depth mm 0.2–0.8
DT Dwell time s 5–45
WT Waiting time s 0–15
Fig. 5 Configuration of lap-shear tensile test specimens (in mm)
Int J Adv Manuf Technol

Fig. 6 The schematic of the


formation process of weld
R600PR15PD0.4DT25WT15

replicates. Then, the influence of welding parameters on joint rotates following the rotational pins at high rotational speed.
strength can be investigated. What is more, the relationship Subsequently, with the further plunge of the tool, the column
between the joint morphology and joint strength can be touches the shoulder bottom and is compressed to tilt towards
studied. the center. Under the shoulder compression, the heat generated
between the rotating column and the base material increases
and then more material is softened inside the weld zone, as can
be seen in DA = 8.0 mm. At DA = 9.3 mm, the shoulder bottom
3 Results and discussion touches the upper sheet surface and the fragmented material is
compressed to be compact. The plunge depth of 0.4 mm is
3.1 The effect of gasket addition on weld formation carried out subsequently, and the weld material is sufficiently
softened and mixed after proper dwell time, as can be seen at
As shown in Fig. 4, the welds produced with and without a DA = 9.7 mm. Finally, a weld joint is formed after the retrac-
gasket show different weld morphologies. Apparently, gasket tion of the tool.
addition can effectively solve the problem of cavity formation
inside the weld. To reveal the effect of gasket addition on weld 3.2 Effects of welding parameters on spot weld
formation, the morphology of the welds produced at different morphology
DA values was observed, as schematized in Fig. 6. At the
beginning of the tool plunge phase, the center column that Figure 7 shows the morphology of the spot weld
consists of unsoftened region and thin-outer softened region R600PR15PD0.4DT25WT15. The indentation the shoulder
is formed, as the figures of DA = 2.0 mm and DA = 4.0 mm are produced and two keyholes the pins left can be clearly observed
shown. The surrounded annular groove is fractionally filled from the joint crown appearance. In addition, the shoulder-
with fragments fabricated by rotating pins. Extrusion ring is affected zone and the pin-affected zone can be clearly distin-
formed due to the upper flow of softened material caused by guished due to different colors. Figure 7a, b presents the cross
the extrusion of rotating pins. At DA close to 6.0 mm, the sections of the joint, which are obtained by cutting along lines
upper sheet is forced downward by a clamping force, making a-a and b-b through thickness. Different from the joint produced
the groove more filled with fragments and the column higher by the conventional single-pin tool [8], the joint performed by
than the upper sheet surface due to the gasket. The center the double-pin tool is characterized by two small keyholes
column is separated from the upper sheet at the same time (Fig. 7a). The profile of the joint is almost axisymmetrical.
and is forced to offset away from the center region. Then, it The weld interface (marked by the black dotted line in

Fig. 7 The macromorphology of


the joint produced by the double-
pin tool
Int J Adv Manuf Technol

Fig. 8 a–c The


macromorphology of the joint
performed by tool with a
conventional cylindrical pin

Fig. 7b) is straight and nearly perpendicular to the workpiece effect of rotational speed independently, the other welding
surface. The bottom profile of the weld (marked by white dotted parameters are set as PR15PD0.4DT25WT15. The spot welds
line in Fig. 7b) is wavy with a concave-up profile below the produced with a rotational speed of no more than 600 rpm
rotating pins and a concave-down profile between the rotating present a smooth crown surface, as illustrated in Fig. 9a, b,
pins. A region which is different from stirring zone (SZ) in color respectively. The extrusion ring, however, is formed at R800
can be observed in the upper paracentral region of the spot weld and becomes severer at R1000, as shown in Fig. 9c, d. This
in Fig. 7b. From the weld formation process schematized in variance is closely related to the friction between the shoulder
Fig. 6, it is reasonable to infer that the region is the rest of the and workpiece surface at different rotational speeds. Low ro-
unsoftened region of the column. Three factors can explain its tational speed results in small heat input to the material under
generation. On the one hand, the friction between the shoulder the shoulder. In this case, elastic deformation occurs to the
and the workpiece surface is small in the paracentral region. On sheets and little surface material is abrased by the shoulder
the other hand, the heat in the upper region is lowered due to bottom. The thickness reduction of the upper sheet is small
thermal transmission from the tool to water. Moreover, the sur- in this welding condition. At rotational speed larger than
rounding heat is hard to transmit to such region due to the poor 600 rpm, the heat produced by the shoulder is sufficient to
thermal conductivity of MC901. Thus, the material in the upper soften the under-shoulder material. Rings are generated due to
paracentral region undergoes insufficient heat and is defined as the extrusion of the softened material at the shoulder compres-
the heat-affected zone (HAZ). Figure 7c displays the image of sion and the centrifugal force [29]. In addition, it is well
the circular bonded area. The diameter of the bonded area is known that the increased heat input and shear force at higher
11.7 mm, which is a little larger than the revolve diameter of the rotational speed reduce the viscosity of the polymers [30] and
pins. Through Eq. 2, the corresponding AB of 93.4 mm2 can be centrifugal force becomes larger with the increase of rotational
calculated. Figure 8 presents the crown appearance (Fig. 8a), speed. Therefore, the material extrusion becomes heavier at
cross section (Fig. 8b), and bonded area (Fig. 8c) of the weld R1000, which results in bigger rings, as shown in Fig. 9d.
produced by a conventional cylindrical pin tool at Cavity and cracks are observed in the interior of the joint
R600PR15PD0.4DT25WT15. The diameter of the cylindrical produced at R400. This phenomenon is mainly attributed to
pin is equal to the revolve diameter of the double pins. By the insufficient heat generation and material flow at low rota-
measuring and calculating, the effective diameter of the bonded tional speed. The spot weld made at R600 presents an excel-
area (X) is 11.9 mm and the corresponding joint AB is lent weld formation without defects, according to Fig. 10,
32.7 mm2, which is much smaller than AB of the joint made where the magnification of the SZ is shown. However, cavi-
by the double-pin tool. Also, compared with the images in ties emerge again when rotational speed becomes larger than
Fig. 7, it is easy to find that the joint produced by the double- 600 rpm, as displayed in Fig. 9c, d. As mentioned above, the
pin tool presents smooth surface formation and a small volume occurrence of the extrusion of under-shoulder material at high
of keyhole. rotational speed makes the touch between the shoulder bottom
Figure 9 shows the crown appearance and cross section of and the workpiece incompact. Also, it results in the generation
joints made with different rotational speeds. To analyze the of ejection channel under the shoulder, as is schematized in

Fig. 9 Macrographs of spot


welds performed at
PR15PD0.4DT25WT15 and
different rotational speeds (a
400 rpm, b 600 rpm, c 800 rpm,
and d 1000 rpm)
Int J Adv Manuf Technol

Fig. 12 Macrographs of spot weld performed at the same R600PD0.


4DT25WT15 and different plunge rates (a 5 mm/min, b 15 mm/min, c
Fig. 10 The micromorphology of the nugget of weld R600PR15PD0. 25 mm/min, and d 35 mm/min)
4DT25WT15
parameters are kept as R600PD0.4DT25WT15. The joints
Fig. 11. In this case, a nugget material is easy to be squeezed performed at low or high plunge rates show extrusion rings
out from the nugget zone due to high shoulder compression together with cavity defects, as shown in Fig. 12a, d. A small
and strong stirring, which, in turn, leads to the generation of plunge rate indicates a longer frictional time, which results in
cavity. What is more, material extrusion often results in the more heat generation. A high plunge rate usually leads to
decrease of shoulder compression, which makes the weld increased shoulder compression. Then, frictional heat genera-
shrinkage obvious at the cooling phase. Based on the expla- tion between the shoulder bottom and upper sheet surface is
nation above, the porous nugget morphology that originated highly enhanced. Therefore, in both cases, the under-shoulder
from an excessive shear action at R1000 can be easily under- material can be softened and then be expelled out of the shoul-
stood. The morphological variance suggests that rotational der bottom to form rings. The nugget material is squeezed out
speed has an important effect on the joint formation. By ob- through the ejection channel produced by material extrusion,
serving Fig. 9, it is also reasonable to conclude that high ro- which causes the formation of cavities. At PR15 and PR25,
tational speed results in the enlargement of the shoulder- well-formed joints with a smooth crown surface and a defect-
affected zone and the reduction of the upper sheet thickness. free nugget are produced, as shown in Fig. 12b, c. Through the
By measuring, the X values of the joints produced at R400, X marked at plunge rates of 5, 15, 25, and 35 mm in Fig. 12,
R600, R800, and R1000 are 11.6, 11.7, 11.8, and 11.8 mm, the corresponding A B values of 95.2, 93.4, 93.4, and
respectively. According to Eq. 2, the corresponding AB values 95.2 mm2, respectively, are calculated using Eq. 2. Low and
of 91.5, 93.4, 95.2, and 95.2 mm2 are calculated. More heat high plunge rates lead to more heat input, so that the corre-
generation at increased rotational speed leads to the increase sponding AB values are relatively larger and that a moderate
of AB. But, the decrease of frictional coefficient and that of plunge rate is produced. However, the small variation of AB
shoulder compression lead to decreased heat input. So, AB towards the plunge rates infers that the dimension of the nug-
cannot keep a consistent increase with rotational speed. In get is slightly affected by the plunge rate.
other words, the variation of AB towards rotational speed is Four joints performed at the same R600PR15DT25WT15
small, which means that rotational speed has a small effect on but different plunge depths are chosen to investigate the influ-
the nugget size. ence of plunge depth on joint formation. As illustrated in
The morphology of the spot welds performed in different Fig. 13, the voids are clearly observed at PD0.2 but disap-
plunge rates is shown in Fig. 12. In this investigation, only peared at PD0.4 and PD0.6. The morphological variance
plunge rate is allowed to change and the other welding

Fig. 13 Macrographs of joints produced in R600PR15DT25WT15 and


Fig. 11 Schematic of the material ejection channel different plunge depths (a 0.2 mm, b 0.4 mm, c 0.6 mm, and d 0.8 mm)
Int J Adv Manuf Technol

suggests that plunge depth has an important effect on the joint


morphology. Increased plunge depth leads to higher shoulder
compression, which is beneficial to the increase of heat intro-
duction and the reduction of weld shrinkage after material
solidification [31]. The joints performed at PD0.2, PD0.4,
and PD0.6 show smooth crown surface. However, an extru-
sion ring is formed around the shoulder when plunge depth
increases to 0.8 mm (see Fig. 13d). This can be explained by
two factors. On the one hand, heat input increases due to
higher pressure. On the other hand, higher pressure makes
material flow easier. Therefore, the softened material is easier
to be expelled at higher shoulder pressure, resulting in the Fig. 15 The magnification of the interface between the HAZ and SZ
production of extrusion ring and also the leakage of nugget (marked by square in Fig. 14a)
material. Inevitably, a cavity defect is formed inside the nug-
get, as shown in Fig. 13d. The variation of nugget size towards input. Under-shoulder material is softened and expelled out-
the plunge depth can be investigated by putting X of joints side the weld zone to form a ring. Meanwhile, the contact
made at PD0.2, PD0.4, PD0.6, and PD0.8 into Eq. 2. Then, between shoulder and workpiece becomes untight and then
the corresponding AB values of 91.5, 93.4, 95.2, and 95.2 mm2 the leakage of nugget material happens. A lack of enough
are obtained. AB increases from PD0.2 to PD0.6 and keeps filler material results in the generation of cavity defect. Bilici
constant regardless of the further increase of plunge depth. and Yükler [9] showed that the thickness of the bonded area
The increased AB can be explained by more heat generation obviously increased with the extension of dwell time due to
at larger compression. However, material extrusion at exces- more heat input. Similarly, the AB values of the joints pro-
sive plunge depth causes the pressure to decrease and then duced at DT5, DT15, DT25, DT35, and DT45 are 91.5,
heat input reduces. So, AB keeps constant at higher plunge 91.5, 93.4, 95.2, and 95.2 mm2, respectively, which shows
depth. Similar to the results mentioned above, AB also varies the increased tendency. However, the increase of AB towards
slightly towards the plunge depth, which indicates that plunge the dwell time is slight, which means dwell time has a negli-
depth has a negligible effect on nugget size. gible effect on nugget size. Also, extreme dwell time cannot
The morphology of the spot weld is largely influenced by lead to the consistent increase of AB owing to the decreased
dwell time, as can be confirmed by the morphological vari- shoulder pressure resulted from material extrusion and the
ance shown in Fig. 14. DT5 means a short frictional time decreased material friction coefficient resulted from stronger
between the tool and material. Therefore, the heat input is shear action.
low and material flow is insufficient, which, in turn, causes The effect of waiting time on the weld formation can be
the formation of cavities inside the nugget, as shown in investigated by comparing the joint generated at different
Fig. 14a. Furthermore, a long crack is formed between HAZ waiting times, as shown in Fig. 16. Unlike the phenomenon
and SZ, as can be seen in Fig. 15, where the magnification of found by Bilici and Yükler [9], the welds produced with no or
the interface is revealed. With the extension of dwell time, short waiting time show convex crown appearances and big
more frictional heat is introduced into the spot weld and the cavities, as shown in Fig. 15a, b, respectively. When the tool
flow of material is promoted. Then, the mixture of weld ma- retracts immediately after stirring phase or retracts after a short
terial is enhanced and the cavity dimension is reduced, as waiting time, the internal nugget material is still in colloidal
shown in Fig. 14b. Defect-free spot welds are produced at state with small Young’s modulus and is unable to resist the
DT25 and DT35, but extrusion ring and cavity defect are retracting force the tool applied. So, the spot weld material is
observed at DT45, as illustrated in Fig. 14c–e. Long-time easy to be pulled out and then the cavities are formed. As
friction between the tool and material means extreme heat waiting time increased, the weld material solidifies under the

Fig. 14 Macrographs of joints


produced in
R600PR15PD0.4WT15 and
different dwell times (a 5 s, b 15 s,
c 25 s, d 35 s, and e 45 s)
Int J Adv Manuf Technol

Fig. 16 The cross section of the spot welds produced in R600PR15PD0.


4DT25 and different waiting times (a 0 s, b 5 s, c 10 s, and d 15 s)

shoulder compression. Therefore, the weld material is hard to


be pulled out and the convex crown surface is alleviated.
Cavities become small consequently, as shown in Fig. 16c.
A joint with smooth surface formation and defect-free nugget
is produced at WT15. Actually, solidifying under shoulder
compression can effectively restrict material shrinkage, which
avoids the generation of voids. Waiting time has a negligible
effect on the nominal AB because the X values of welds pro-
duced at WT0, WT5, WT10, and WT15 are all 11.7 mm.
Inappropriate welding conditions usually bring about cav-
ities throughout or near the bonded area or cracks between the
HAZ and SZ. Therefore, choosing appropriate parameters is
important in the welding process. Furthermore, AB is slightly
influenced by five welding parameters. However, it was re-
ported that the increase of nugget size can highly promote the
joint fracture load [8, 9]. Therefore, the following possible
actions can be taken to promote the joint strength: first, in-
creasing the revolve diameter of double pins properly; second,
reducing the volume of the keyholes; and third, adding exter-
nal additives to strengthen the joint, like Gao et al. [32, 33],
who added multiwalled carbon nanotubes into the weld and Fig. 17 a The cross sections. b The surface morphology. c The load
successfully increased the tensile strength and elongation of versus displacement curves of CNF mode and PNF mode (PNF pull
the joint. nugget failure, CNF cross nugget failure)

3.3 Effects of welding parameters on joint shear strength according to Fig. 17c, where the joint with PNF shows smaller
(SS) fracture displacement than the joint with CNF does. Also, the
curve of PNF reveals a steeper reduction of LT in the descend
Lap-shear tensile tests were carried out to assess the quality of stage than the curve of CNF does.
the spot welds. Two kinds of fracture modes, namely cross Table 3 lists the test results of the joints, including the
nugget failure (CNF) and pull nugget failure (PNF), were fracture modes, lap-shear tensile load (LT), the shear strength
observed in the test. Figure 17a, b reveals the cross section (SS), and the fracture displacement. Most joints fracture with
and fracture surface morphology of two fracture modes. To CNF mode, and only welds R400PR15PD0.4DT25WT15 and
CNF mode, fracture occurs along the lapped surface and the R600PR15PD0.4DT5WT15 fracture with PNF mode. By ob-
regions near the bonded area undergo plastic deformation. serving the morphology of two joints fractured with PNF
Therefore, the cavity distribution mentioned above undoubt- (Figs. 9a and 14a), it is reasonable to infer that the propagation
edly has a negative effect on the joint strength. To PNF, a of cracks between the HAZ and SZ results in the pulling out of
central part is pulled out from the upper sheet. Plastic defor- the center region from the upper sheet. This results in lower LT
mation occurs to both kinds of spot welds, but the joint failed of joint R400PR15PD0.4DT25WT15 and R600PR15PD0.
with CNF mode shows more obvious plastic deformation than 4DT5WT15 compared with joints with CNF mode in general.
joints failed with PNF modes. This can also be confirmed Furthermore, it is found that the spot welds with large LT
Int J Adv Manuf Technol

Table 3 The lap-shear tensile test


results and the corresponding Spot welds Fracture LT (N) SS Displacement
shear strength of welds performed morphology (MPa) (mm)
in various welding conditions
Tool with double pins
R400PR15PD0.4DT25WT15 PNF 1956.3 – 11.7
R600PR15PD0.4DT25WT15 CNF 2825.2 30.2 15.8
R800PR15PD0.4DT25WT15 CNF 2235.6 23.5 14.3
R1000PR15PD0.4DT25WT15 CNF 1106.8 11.6 11.9
R600PR5PD0.4DT25WT15 CNF 2364.4 24.8 15.1
R600PR25PD0.4DT25WT15 CNF 2732.1 29.3 16.6
R600PR35PD0.4DT25WT15 CNF 2530.4 26.6 15.1
R600PR15PD0.2DT25WT15 CNF 2483.9 27.1 15.0
R600PR15PD0.6DT25WT15 CNF 2674.5 28.1 15.6
R600PR15PD0.8DT25WT15 CNF 2156.2 22.6 14.0
R600PR15PD0.4DT5WT15 PNF 1870.8 – 11.1
R600PR15PD0.4DT15WT15 CNF 2439.7 26.6 15.4
R600PR15PD0.4DT35WT15 CNF 2684.7 28.2 15.2
R600PR15PD0.4DT45WT15 CNF 2128.6 22.3 14.5
R600PR15PD0.4DT25WT0 CNF 1094.2 11.7 10.5
R600PR15PD0.4DT25WT5 CNF 1470.4 15.7 13.6
R600PR15PD0.4DT25WT10 CNF 1890.1 20.2 15.3
Tool with cylindrical pin
R600PR15PD0.4DT25WT15 CNF 593.5 18.1 3.8

PNF pull nugget failure, CNF cross nugget failure

usually show high fracture displacement and vice versa. The rotational speeds resulted in increased residual stress [35],
LT and fracture displacement of the spot weld produced by a thus leading to the further weakening of the joint strength.
cylindrical pin at R600PR15PD0.4DT25WT15 are 593.5 N Figure 18b presents the effect diagram of plunge rates on
and 3.8 mm, respectively, as listed in the last two rows of SS. Apparently, joints performed at PR5 and PR35 have low
Table 3, which are much smaller than the joint made by the SS due to the cavity formation at these two welding conditions
double-pin tool (2825.2 N and 15.8 mm, respectively) at the (Fig. 12a, d). SS values of the joints performed at PR15 and
same welding condition. According to Eq. 3, the shear strength PR25 are relatively high because they are well formed without
of joints fractured with CNF modes is calculated. The maximum defects (Fig. 12c, d). Joints performed in different plunge rates
SS of 30.2 MPa is produced at R600PR15PD0.4DT25WT15, show smaller strength compared with the base material due to
which is about 58.4% of the base material. The reduction of the defect formation, water absorption, molecular weight re-
molecular weight, the absorption of water, as well as the gener- duction, or residual stress generation. The variance of SS to-
ation of residual stress inside the joint are three possible factors to wards plunge rate is small compared with Fig. 18a, which
the reduction of the joint shear strength. indicates that plunge rate has a smaller effect on the joint
Figure 18 shows effect diagrams of five welding parame- strength than rotational speed.
ters on joint shear strength (SS). Figure 18a reveals the effect The effect of plunge depth on joint shear strength can be
of rotational speed on SS. All the joint strengths are smaller investigated through Fig. 18c. In order to study the effect of
than the strength of the base material. The maximum SS of plunge depth independently, all spot welds are produced with
30.2 MPa is obtained at R600, and SS decreases with the the same R600PR15DT25WT15. With the increase of plunge
increase of rotational speed. This variance can be explained depth, joint SS increases first and then decreases. Insufficient
as below. First, the dimension of the cavity that resulted from heat is generated due to small shoulder pressure at low plunge
the extrusion of nugget material (as explained above) in- depth [31]. Therefore, a weld material is poorly softened and
creases with the increase of rotational speed (Fig. 9c, d). mixed, resulting in the void generation (Fig. 13a). Defect-free
Meanwhile, residual stress concentration may exist around joints with similar AB are obtained at PD0.4 and PD0.6
the cavity [26], which results in the decrease of S S . (Fig. 13b, c), but the joint SS decreases from PD0.4 to
Furthermore, molecular weight may be further lowered due PD0.6. This phenomenon can be explained by the fact that
to stronger mechanical scission of molecular chains at higher high plunge depth results in excessive shoulder pressure and
rotational speed [34]. Also, it was reported that higher more heat input, which lead to the fragment of molecular
Int J Adv Manuf Technol

Fig. 18 Effects of a rotational


speed, b plunge rate, c plunge
depth, d dwell time, and e waiting
time on the joint shear strength

chains [34]. The further decrease of SS at PD0.8 can be easily a decrease from DT25 to DT35 although no defect is formed
explained by the presence of cavity (Fig. 13d) and the residual in both joints.
stress concentration around the cavity [26]. Figure 18e presents the plot about the influence of waiting
The influence of dwell time on the joint SS is illustrated in time on joint SS. The joint strength increases with the exten-
Fig. 18d. In this experiment, only dwell time is allowed to sion of waiting time. This can be explained by the modifica-
change. SS increases from DT15 to DT25 and then decreases tion of joint morphology with longer waiting time, as can be
with the prolongation of dwell time. The maximum SS is 30.2 observed in Fig. 16. Weld material has completely solidified at
MP, which is lower than the strength of the base material. WT15, and a further increase of waiting time is unnecessary
Voids, the main cause to the weakening of joint SS, are gener- and is not beneficial to the welding efficiency.
ated due to inadequate frictional heat generation as well as
insufficient material mixing at DT15 (as shown in Fig. 14b).
Long dwell time can promote the heat input and material 4 Conclusions
mixture, but extreme dwell time causes material extrusion
and the generation of cavity (as shown in Fig. 14d), which The feasibility of UFSSW of MC901 sheets by the double-pin
results in the reduction of joint strength. In addition, a molec- tool was demonstrated in the present research. A gasket with
ular weight decrease due to mechanical scission of molecular the diameter of 9.6 mm and the thickness of 2 mm were added
chains at excessive dwell time may be another factor to the between two sheets to improve weld formation. The effect of
strength reduction. It can also explain why joint SS undergoes rotational speed, plunge rate, plunge depth, dwell time, and
Int J Adv Manuf Technol

waiting time on joint formation and joint strength was inves- mechanical characterization, and bonds morphology. Opt Laser
Technol 88:205–214
tigated. The conclusions can be summarized as follows:
7. Aden M, Mamuschkin V, Olowinsky A (2015) Influence of carbon
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of cavities throughout or near the bonded area. polyethylene sheets. Mater Des 32:4074–4079
– The areas of the bonded areas were slightly affected by 11. Junior WS, Handge UA, Santos JFD, Abetz V, Amancio-Filho ST
the variation of welding parameters. (2014a) Feasibility study of friction spot welding of dissimilar
single-lap joint between poly(methyl methacrylate) and
– Two fracture modes, namely cross nugget failure and pull
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