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Indian Journal of Fibre & Textile Research

Vol. 38, March 2013, pp. 109-113

Characterization of Egyptian cotton fibres measurements and the results of AFIS and HVI
spectrum apparatus. Despite of these differences, it is
Magdi El Messirya & Samar Ahmed Mohsen Abd-Ellatif possible to specify basic cotton fibre properties
Textile Engineering Department, Faculty of Engineering, having potential influence on the cotton yarn
Alexandria University, Egypt strength3. There are also differences between
Received 27 November 2011; revised received and accepted measurements of fibre strengths based on bundle
29 March 2012 concept and single fibre concept as described by
Militky and Kremenakova4. Equations relating single
In this work, the quality of Egyptian cotton varieties has been cotton fibre strength to bundle strength are presented
studied in terms of a morphological investigation, single fibres but proved to be of limited success5. Many
tensile properties and other tuft properties determined by HVI.
Finally, a new ‘modified fibre quality index (MFQI)’ for the research3,6,7 studies have been conducted to observe
characterization of the quality is presented and compared with the the phenomenon of spun yarn failure which is found
spinning consistency index. This index in most cases gives the real to be strongly dependent on yarn structure, fibre
potential of the cotton variety according to its physical properties. packing in the yarn cross section5,8 as well as the
cellulose accumulation inside the cotton fibres6.
Keywords: Equptian cotton Fibre quality index, Spinning
consistency index, Tensile properties Several studies have been published and different
formulas are suggested to define the cotton fibre
Cotton species (Gossypium hirsutum) is native to quality1,3,4,9,7. One of the first attempts to create
Mexico and Central America and has been developed aggregated criterion of cotton fibre quality is fibre
for extensive use in Egypt, accounting for more than quality index (FQI), as shown below:
80% of Egyptian Production. This group is known as
FQI = (Fibre strength × Length)/Fineness
long staple (LS) cotton. It varies in length from about
7/8 inch to 15/16 inch. Another group (Gossypium This is further modified by considering more fibre
barbadense), which makes up the most valuable and properties, as shown below:
the balance of the Egyptian production, is of early
South American origin, varying in length from 11/4 FQI = (Fibre strength × Length × Uniformity × Maturity
inch to 19/16 inch. It is commonly referred to as coefficient)/Fineness
extra-long staple (ELS)1. Egyptian cotton fibres are For HVI results, FQI is expressed in the form of
composed mostly of α-cellulose (88-96.5% w/w). The FQI = UHM × UI × STR/MIC
rest is non-cellulosic that are located on the outer Militky and Kremenakova4 described that the
layers and inside the fibre lumen. The non-cellulosic procedure for the evaluation of cotton quality index
include proteins (1-1.9% w/w), waxes (0.4-1.2% (U) can be simply modified for other selected
w/w), pectin (0.4-1.2% w/w), inorganic (0.7-1.6% properties or other set of weights. Considering
w/w), and other substances (0.5 to 8% w/w). The different fibre properties and assuming linear
specific chemical composition of cotton fibres varies geometric properties, some criteria based on the
according to their varieties and growth conditions2. regression models connecting fibre properties with
The cotton classification is a system of standardized parameters are used to characterize spinning ability or
procedures for measuring raw cotton properties quality of yarn (characterized by yarn strength)10. The
(physical attributes) that affect quality of processing spinning consistency index (SCI) is connected with
(spinning mainly) and quality of products (yarns). cotton HVI properties through regression model3, as
Several standards as well as testing techniques are given below:
available for the characterization of cotton fibres,
such as HVI and AFIS techniques. It is known that SCI =-414.67 + 2.9 STR + 49.1 UHM + 4.74 UI - 9.32
there are some differences in the principles of MIC + 0.95 Rd + 0.36 b
___________
a
Corresponding author. However, for Egyptian cotton the value of SCI does
E-mail mmessiry@yahoo.com not accurately reflect the spinnability of the different
110 INDIAN J. FIBRE TEXT. RES., MARCH 2013

cotton varieties. The present study is therefore Moreover, these frictional properties affect the
undertaken to investigate the Egyptian cotton varieties values and the variability of the drafting forces
and to develop a modified fibres quality index (MFQI). applied on the fibres during their processing and are
Cotton samples representing the different Egyptian considered to be one of the main factors determining
cotton varieties are prepared in order to perform the unevenness of the products at different spinning
different fibre tests determining their physical stages12. Furthermore, surface characteristics are
properties. Fibres from different ELS and LS expected to have a considerable effect on the yarn
Egyptian cotton under investigation Giza 45, Giza 70, strength. Therefore, the analysis of the SEM for the
Giza 87, Giza 88, Giza 80, Giza 85, Giza 86, Giza 89 different varieties of Egyptian cotton considers the
and Giza 90. The single fibre properties are tested in relative number of convolutions, surface smoothness
Department of Textile Materials, Textile Faculty, and and surface irregularity, which, in turn, should largely
Technical University of Liberec Cz. Fibre bundle affect fibres and yarn strength properties. Table 1
measurements are performed on the HVI (high shows a comparative classification of the surface
volume instrument)at the laboratories of the Modern characteristics of the different varieties of the
Nile Cotton Co. Egyptian cotton. The properties presented in Fig. 1
could be of a great significance regarding the single
Structure and Morphology of Egyptian cotton fibre strength properties. It is expected that highly
An analysis of the potential relationship between convoluted fibres would give a less fibre strength.
the microstructure and the surface properties of
different cotton fibres has previously been performed Although the testing of single fibres is considered
and proved to be of high importance11. to be exhaustive, demanding and difficult, it proves
It is necessary to carefully analyse the structure and sometimes to be of great use especially to breeders
the surface properties of cotton fibres in order to and researchers with limited testing material available
enhance the performance of cotton based materials and or in the areas where the detailed data is able to justify
fabrics. In this context, the relationships between the the investment in time and effort. In this research
microstructure and the surface properties of different work, a study on the single cotton fibres tensile
cotton fibres should be thoroughly considered. Figure 1 properties is conducted. Samples from five different
shows the SEM images of grey cotton samples at varieties of Egyptian cotton are drawn (Giza 86, Giza
magnifications of ×1000 and ×10000 for different 87, Giza 88, Giza 90 and Giza 45), and 50
cotton varieties. The samples were used without measurements are applied for each variety. The
treatment. The convolutions on the cotton fibres Vibroscope, a device for the measurement of strength
surfaces are clearly shown and the fibre surface is characteristics of single fibres, is utilized. For each
found to be different for each type tested. This certainly sample, numerical values for fibre count, breaking
reflects on their performance in the spinning process force, breaking elongation, tenacity and young
and the quality of the yarns produced from the different modulus are recorded. Table 2 shows the mean
types of cotton. Efforts have been made to observe the values, CV%, minimum values and maximum values
convolutions present on the surface of cotton fibres, of the single fibres strengths for the five cotton
representing different cotton types and relating them to varieties under investigation. The variation in
their surface characteristics. Sinoimeri12 attempted to properties is related to genetic of the cotton verities10.
group different types of cottons according to their inter-
fibre-friction properties. It is apparent that these Fibres Tuft strength
properties are mainly due to the surface properties of Cotton fibres are usually tested in bulk form
the fibres including micro- or nano-scopic surface of utilizing a mass or beard of fibres to a test instrument
fibres. Fibre surface characteristics have a significant for measurement. There are many reasons for this, not
influence on their frictional characteristics11. the least of which is that handling single cotton fibres

Table 1—Comparative classification of the different varieties of Egyptian cotton


Cotton type G45 G70 G87 G88 G80 G85 G86 G89 G90
Convolutions Low Low Low Low Medium Medium Medium Medium High
Surface smoothness Smooth Smooth Smooth Smooth Smooth Rough Rough Rough Rough
Surface irregularity Low Low Low Low Low Medium Medium High High
SHORT COMMUNICATIONS 111

Fig. 1—SEM images of single raw cotton fibres [(a) G.45, (b) G.70, (c) G.87, (d) G.88, (e) G.80, (f) G.85, (g), G.86, (h) G. 89, and
(i) G.90] [(i) ×1000 and (ii) ×10000]

is tedious and time consuming. Another argument for variations for all the measured single fibre properties,
the application of the tuft strength testing technique is which is much higher than the tuft values.
that cotton fibres are seldom used in the single fibre Comparison between Single Fibre and Tuft Testing Techniques
form and the properties which are of interest are the In a further step, a comparison between the single
properties of a tuft of these fibres3,5. Several fibre tensile characteristics obtained from the
investigators5,6,8,13 correlate the yarn tenacity by the Vibroscope and the tuft fibre strength obtained by the
value of the bundle strength. However, the tuft testing HVI is conducted. The summary of the results is
has many drawbacks especially while testing the shown in Table 3.
strength characteristics of the fibres. It is expected A statistical analysis is then performed as a
that the strength of a yarn is not predicted accurately comparison between the fibre strength values
by averaging the strength of the individual fibres. The obtained from the Vibroscope and those obtained
above results indicate high value of the coefficient of from the HVI. The value of R2 = 0.807 is found
112 INDIAN J. FIBRE TEXT. RES., MARCH 2013

between the single fibre and bundle strength for the networks and fuzzy logic have been used for
different varieties (Fig. 2). Thus, the tenacity of single predicting textile products quality from fibre
fibre from the Egyptian cotton can be obtained using properties. However, Hunter14 concludes that, until
the following equation: now, there is no viable solution. Such and Sasser7
have reviewed the impact of HVI systems on both the
STRf = 5.705 TSt − 170.24 ... (1) domestic and world cotton textile industries. Several
formulas have been suggested for defining the cotton
where STRf is the single fibre tenacity in cN/tex; and fibre quality. Considering other fibre properties and
TSt, the tuft strength measured HVI in cN/tex. assuming linear geometric properties, a modified
However, no reasonable correlation is observed formula is presented as:
between the single fibre and the bundle elongations.
MFQI = [UHM × UI × STRf × (1+EL) × (1-SF)]/ MIC
Cotton Fibre Quality
14
Hunter study was to predict the most important … (2)
yarn quality characteristics derived from cotton fibre The fibre length is expressed by upper half mean
properties that were measured by means of an HVI UHM (mm), UI (%) stands for the fibre length
system. Linear multiple regression methods were used uniformity index, STRf (cN/tex) stands for the single
for the estimation of yarn quality characteristics. More strength, EL (%) stands for the fibre elongation at
recently, many approaches including artificial neural break, (MIC) stands for the micronaire value
Table 2—Characteristics of cotton varieties representing the fibre fineness and maturity and
SF(%) stands for the short fibre content. Taking into
Cotton Parameter Fibre count Tenacity Elongation Young
dtex cN/tex % modulus consideration the variability in the fibre length, the
g/den term FQI represents the specific work of rupture
which is defined as the amount of energy needed to
G.45 Mean 1.33 37.88 9.24 32.11
CV% 20.97 34.59 26.86 39.83
break a material and is represented by the area under
Min. 0.76 9.3 4.1 11.05 the stress strain curve. It measures the ability of a
Max. 1.7 65.3 13.6 71.83 material to withstand a given energy. In order to
compare different materials, work of rupture should
G.87 Mean 1.51 37.13 6.53 42.59 be normalized to take account of the various masses
CV% 17.52 41.17 33.43 41.46 of different materials. Hence, specific work of
Min. 1.06 9.47 1.9 17.91
rupture, which is the amount of energy needed to
Max. 2.14 74.09 10.9 115.29
break a material of unit mass, should be used. Thus,
G.88 Mean 1.62 35.55 6.32 43.55 MFQI is more consistent for the comparison between
CV% 21.04 41.89 26.92 34.9 different types of cotton. The MFQI given in the
Min. 1.07 7.66 3.1 16.81
Max. 2.4 72.66 10.7 88.85

G.86 Mean 1.76 39.01 8.69 42.09


CV% 17 29.73 27.17 43.2
Min. 1.05 12.65 4.2 20.08
Max. 2.38 68.11 14.2 87.31

G.90 Mean 1.64 32.75 8.51 34.3


CV% 21.39 29.99 30.17 32.62
Min. 1.1 13.19 3.9 14.58
Max. 2.33 59.36 14.2 63.95 Fig. 2—Correlation of single fibre and tuft tests
Table 3—Tuft fibre strengths measured by HVI
Parameter G.45 G.87 G.88 G.86 G90
Strength Elongation Strength Elongation Strength Elongation Strength Elongation Strength Elongation
g/tex % g/tex % g/tex % g/tex % g/tex %
Mean 42.3 6 45.2 6.5 45.1 5.1 43.1 5.8 33.5 7.7
CV% 3.3 3.2 3.6 3.1 3.91 3.05 4.9 3.5 4.02 3.89
SHORT COMMUNICATIONS 113

Table 4—Values of MFQI and SCI for different Egyptian cotton Table 5—Values of MFQI and SCI for different global cotton
varieties cultivars
Cotton MFQI SCI Cotton MFQI SCI
Giza 45 411.67 214 Barakat (Sudan) 261.1 162.79
Giza 87 352.56 217 US Pima (USA) 312.07 196.54
Giza 88 288.13 218 Sovin (India) 355.17 176.78
Giza 86 262.47 204 DCH32 (India) 257.45 145.04
Giza 90 193.21 146 132 (China) 302.41 173

formula is calculated for different Egyptian cotton behaviour and tuft fibre tensile behaviour has also been
varieties and the results are given in Table 4. The performed giving a correlation factor of 0.807 between
values obtained are compared with the values of the both values. No relationship is observed between single
spinning consistency index given by the HVI. In spite fibres and tuft fibres elongations. Finally, a term for the
of the relatively high degree of conformation between characterization of cotton quality (MFQI), as a function
the two indices, it is noticeable that the MFQI is more of fibre length, fineness and strength has been
relevant representing the differences between the introduced and compared with the SCI. The MFQI is
behaviour of the different varieties in spinning mills. proved to be better than SCI in describing the
The performance of Giza 87 is found to be better than performance of cotton fibres.
that of Giza 88 during the different stages of the
spinning process. This is shown clearly by the value References
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