ah terial peificaton and party the test metho ‘he specication inthe text method myst be ven Prony and stegandod only ater careel teckel oncievation. Ac mumber of these requ irc hot ge shove Th thal ane a ofthe heat ieanstar procestes involved Ter mal éondgction, radiation and tonveston ave he Primary mechanisms. Of thes, only conducon Inca depen ob At occ a Prove uikineat effects tht se del fo ans ‘Nag, and cven more eifcut to measure, XU: 2" Dependence on Specinen Thviness —Of Ine pues volved only conduction places & callow that fs hell proportional tthe thick, sess of 8 specimen The others acl i's mone ‘mplex relationship. The thinner and Iss dense the atetal the move likely that the resbtanes ‘epands on proxessos other than sonduction ths ‘out is condition that dose not say the fe= Iuiterteats of the detition for thea Cote {yan thccmal resist, both ting ntsc Mupties, ince the apparent respecte tales tna a dependence on the splat thiknes: or ih onatctals it may be dese to determine the inemalreistance a conditions sppliesle to helt ne Tete & belived to bert lower hating tech °S3 forall mera below which such a depend fice cuts Below thie thickness the speeamen "ay tare igo thermal tranmnsion’ properties, “aot the materi real, tse to esta Sth minimom thickaes by measurements NU43.Depentent on Tennperms Direce— he magnitude ofl the terial transfer proces hens om the temperature diferenes aetas tt since he dopedcaces more compet than "rect proportionality for all process except one ot many atria te comp depend fase Insuch semet wae Wo eave ot ‘est that i yplal wf use, and to determine st soulmate Felalonship for ange ol tempers ‘erences. The dependence cat be tinder for a ‘e tange in temperature diferiee Xtidst Muha! of Determining Dependence ow cnr ference He iapcuren ‘en fr amtr a nano dittes mews nts is necessary. These ace made ith wide iting temperature iifrencen A socondansey pdgnee tan be revealed by these meavsre: is When simple linear eelationshp known Feromy geen the omen sclhe'mades This estabishes the inca depend for that particular ssmple " Nias Delormiuation of iiimumy Thickness Which Thermal Propertes of the htarial May Defined It the minis thickness for whe thermal conducuiy and restiiy can be de ssn Enown, itis necessary to etiate ti ves. There fo esabinhed procedure foe “rimiiag this sickness (Note Xd). The some, A crude! procedure cuted below may be used cur for determining the thickness and whether i ose inthe range of thicket which a materi sa tobe wed (Mote 3) Nore, X1~ifimproved methods fr doterms the thskness In question ate developed ore Dose ASTM Suommitce C1650 sould nee Sate ceiving information about em Coma Seman ofthe subcomenteenbugh ASI ‘feeders, X1A6 Procedure X14.6.1 Select a uniform sample of materi thickness equal te the great hthass fo Be sas skietaed, OF to the nixamom allowable tices forthe test apporatan Thi tess eemed Not X2—This pasticlar text moy be ce lutein the Guard Hot Box, Mond C236, X1.4.6.2 Cut five sets of specimens fom be samples ihese shoul range in highness fom he Eis eicknasy Tey to he “uc prac, termed 9140 5 in Sooronnaly cl re ments The ets ofspecimensare then esate $5 according to fa tckyes, XLT Measure the thchnas and thermal sistances of 183, and 33 186.4 Cieuate UR NADLDI, (RS. (28.055, and SIDS. The are teed ai ALG thee ha 29%, then the material can be churatehcl Oy ¢ aetna natty and esi i IA.606 Ihe tee values uikr by more thar 2.4, ien measure the hcknetsand tesa et anceio San $4 Calulnte te ven (REIN, (Eby, MRS RaMDs.b 3) RERIDEDS (aSnanios-ba) and RDS Note X3=11 is important to differentia be: ten a thermal eaance in measures tated y the paceaeh of the ierncpies he ibethe ara athe plac, ald rene ined by pur specimen func, aod adel he ‘Mal ressance caused bythe cupling of the te ‘Weaon and ation meen of at tne i Specimens. Al tie ean affect tae miemmnemen ihesane ay, and oen the tice may Besdaee ales eifer by X1.4.6.7 Thickoesics above wich al the a AAD values agree with the vac of RSID o within 2 % may be charateize by thermal contacter and thermal sitivity. Allowance nn be ma ierpcition fhe ele or eperimena A plovof te ait) ADs and RS/D4 ver thse ‘ay ad in redoing the uncertainty: estates Senn ot erate Bway ah eee ‘umber of specimens may be unc wire greet Aetinion requteedTikeknea sxpenende ay bea fonction of mean iemperatare a temperate aliforeceacros the specanens Tor pfs {hs method. this snge choc. pertrmned ty fal operating temperate and enced sna be {rr Tein ind Mtr hem psn paige df aye seen een "ar moments and hse i ane wi ond emake rsoment saga eee Fy arabe deca es a a F 1 Seope eee imal PAER La DerER LUA CLO gs LA ‘ Tearcenporecloles Rs 106 | He Ee RO UCT AAS DE CUSTES DE VIDAL eee UcGnden DEStAbES aA Benuieto ‘ Standard Practice for DETERMINING CHEMICAL RESISTANCE OF R THERMOSETTING RESINS USED IN eae REINFORCED STRUCTURES INTENDED FO! SERVICE’ sch cet dan ee a i et ew Te sanadis es i ecommende Prats Casing Pa Dees fn Gnsenred Pete Laminate Parts 1p 2583 Test Method for Indentation Hardness ‘of Rigid Plastics by Means of Barcol Impress? 7 238s Test Method for Ignition Loss of Cured Reinforced Resins? to evaluate nan 11 This practice i designed an nsiessed sate, the chemical resistance of the tnostting resins used ia the fabrication of cin fend themosting plsie (RTP) laminae ‘This practice provides for the determination 0 hanes in the proper, described a ews, and test reagent after ox ff the test specimens 7 Tens to the reagent: harUNeSS 3, Sigufcance and Use Sirsa pao ie st by this practice shall specimens, appearance of specimens, aPP acai br : seortamecan ea nd url oreh 20 gra ne | Ee ware shen of thermeseting sn wie nan RTP 12" ation isa rg Na fen oe tobe regarded asthe standart nate, Nee : ‘neta ig weet change andthe ye structure when subjected to chemical oviron, bet 2SRayenas mayabotewedioennage scucture when Si el sehtaas othe ra 13 This tendered may oe acres teat peas. and emp. Tt std fc nt pron oars of the safely fers essere hisses the esponsi I her tes hs andr to con ad aback apropat eet a heath practices seatcrne tapi fregulatry ti tatin prior to we 4. Apparatus 4.1 Hardness Testing Insirament—This sal teas described in Test Method D2S83. 42 Flecral Properes Testing Apparat “This shall be in accordance with Test Metho D100. Bans on Remtored asic Fiping Systems and Chem aype ation approve Nov. 2%, 198, Rushed sary ws Dagan gascoaec Hi 48 1-8 ea Canoe an aot od of ASTM Sad, Vd Aca ck 74 Stand, VD cesT Commitee 2, Apc Dscomets 2st Sndant et 1 Ta tots fox Pes Proper " Unreinforced and Reinforced Plastics and eile tra 35 <43 THekues Messen micrometer suaie for mexsrement 40 OGDE in (4025 Le Conuines—Consien of ule ize cape and neste aw tl immesion rnd hermretng past scuimens in AhcSpuciceorenves the fret Tesco tats when scary, eenpeble trai rattle oll slusons tat {ves Ts canbe acomplia byte we ot ‘en conden, SS TlemingApartis—A cvs kempe- avr oven tng ano gi ba ape Be'sCwetinngtemperstre within range of Sear bay, reper precaosshould te iSite coroaes sete te laminae tas % 6 Analytical Balunce—The balance shall be suai oracuae wen 100.001 B 5, Reagents 5.1 The tes media shall consist of the reagents cor solutions to which the RTP laminates are to be exposed, 6. Test Specimens 6.1 Standard Laminates—Prepare standard Siber-ccinforced Jaminates using ientical rein forcement in all ofthe laminates, The laminates shall be constructed ofthe folowing materials: Gill Suufecing Mor (Veil —Type C glass fiber ‘with binder compatible with the resin, Synthetic Drganie fiber surfacing mats may be used, but Should be considered as variables for evaluation gains the standard laminate. Nominal thickness 0.010 in. (0.25 mm). 6.12 Chopped Strand Mat—Type E glass fe ber with sizing and binder compatile with the resin, Other las fer compositions may be used but should be considered as variables for come parison to the standard 6.1.3 Resin-—Catalyzed and promoted ac cording to the resin manufacturer’ recomme dation. Nore, Firs, such antimony tioxie fr ime proved five etardancy or thiotepes or viscosity eon ‘edrenay be add, bat nay detract fom He corrosion restange ofthe tt mint, 62 Dimensions ane General Properties—The laminates shall conform to the equired dimen. sions and general properties of 6.2 and be fabri- cated in accordance with 6.3. G21 Laminate Size—A, suitable laminate Gh cso ( size has been found to be 26 by 33 in. (660 by 838 mm) afer trimming, This laminate size is not restrictive and other dimensions may be se 16222 Thicknesy—The thickness of the cured standard laminate shall be between 0.120 and 0.130 i, 3.03 and 3.30 mm). 6.23 Reinforcement Content-—The gas fiber snd binder content shall be 0.635 + 0.064 gin, {two layers of TY» o2/M? chopped strand mat— 1.551 glin? having & nominal binder content of 3/2% and two layers of 10 mil surfacing mat (0.044 g/in? having « nominal binder content of 17 Yey-—etermined by preweighing the materials prior 10 construction of the laminate. This is feauivalent 10 23.6 eight % (12.5 volume) fase fiber when using a cesin having a cured ‘specific gravity of 1,15, Such 2 laminate will have 8 thickness of 0.125 in. (18 mm), The use of resins having diferent specific ravities wil result in different weight percentages of glas ier, but the volume percentage of glass fiber will remain the same. When using synthetic organic fiber surfacing mat, the glass content shall be 0.591 10.059 in? (wa Tayers of 114 07/? chopped ftcand mat having & nominal binder content of 34%). 624 Hardness—The hardness shall be at east 90 9 of that ofa fuly-cured clear casting ct the resin, or of a similarly constructed laminate fs defined by the resin manufacturer. Hardness Shall be determined in accordance with 4.1 I Should be noted that the use of synthetic vei wil Fesult in significantly lower hardness values. The hardness value will vary with the type of resin and number of plies of synthetic vel, The resin manufacturer should be contacted fo the allo able Bareol hardness value ofa laminate contr ing synthetic veils with the specific resin ‘625 Latninate Condition-—The laminae shali meet Acceptance Level 1 of Table 1 of Recommended Practice D2563, (63 Fabrication of Standard Larinate—Ue sequence of lay-up shall be as follows 631 Apply catalyzed resin end a (Oil (0.25-min) surfacing mat on a fat surface cor tered with plastic release flm™ or treated witha Suitabie release agent and rell fo distribute resi Nors 4—The following forma ay be us 2 ule to deermine te tol weight of resin tobe ed “gt nd apr nb i MYLAR ae C22 Fotow witht pes of 1% ou? coe al nl ea seth lot ie Sond we Feu hlng nis ra wire tele teomintcedoce wine Thema poet fatewitan 25 %of en ec ert sery ssn cn toty say eee Grater deen ceo get gana Ae 5 mat Mat ween saaton ll mex eopey Sia Poms cainrisaes 53 alm wha toni 025m) st 54 Renee th lig es acc oon an ae Rea ot Senin en 6100 al 3 Seti 3 hs Ar harap compe coe he inmate ee a a sufi, roth, Cael sooth down fe. Seka ee ges eee poorer fet cs iene B renoved by rutting 2 tonaue depron sroat the Fas fn surface Cary pall he fn tt and P fisen atthe dacs to prevent rihlng te sng srs mre and oe eth) runt the ees the lnminate and passing 9 hea tl br over the lari lp ose nit ond Pk x” CC ane 9 Sc ee Cone 3 hose Ral es + tt 11 Mecarnient of. Spcinent—tnmedi acy flowing te rng pos nese Be | thle of th spcines fo the neat 0.01 in (0025 nm) atthe poe cet enh OF the nent nS TOL. mm) spscimens tha il ct or Rea ess afer the competed expres These chess ee. Surements‘may Neo fe wed or comparon Seas ticknes measurement a te sm Ded eine 72 Expnre—Following te can pro 2s specif in 63. rr to nro, ced 2 tet eocspton ofthe color and suc ae penance ofthe coupons and te cio and the> 1 Geet lait of the tet solution, The total number of coupons per container is not limited except by the ability ofthe container to hold the coupons without touching each other or the container. ‘The coupons must aways be completely im- mersee, Coupons should be vertical, parallel and Spaced # minimam of Win. (635 mm) apar. “There shoule bea minimum of fin. (12.7 mm) ‘beween coupon edges and the container ofthe Tiguid surfuce. Plage the closed container in a tonsa temperature oven adjusted 10 the re ‘ured vemperature or ina suitably adjusted Ki tid bath. Examine the coupons after 30,90, 180 faye and one year of immersion of other time intervals as required to determine the rate of attack 521 The test solution should be discarded and replaced with esh solution as offen as ne- {ssiry to mania orginal eompostion and con- Centration, As & miinimen, solutions Known 10 be siable should be replaced at the end of each test petod. 78 Cleaning and Exarnination Afier Expo- sinte—Ciean the coupon and dry by blotting with a paper towel. Cold tap water is normally used for specimen cleaning. If ther cleaning agents fare used, verify that they do not attack the resin bring tested 75 Note any indication of surface atack on fa coupon, any discoloration of the test solution, land the formation of any sediment. "13.2. After Final blotting, immediately mea- sure the coupon thickness fo the nearest 0.001 jn, (0025 mm) in the gecmeitic center of each intended 1 by 4 in, (25 by 100 ma) specimen. ‘Te Barco! hardness can then be checked, taking an averaze of ten eeadings on each coupon, & ranimum of Yin, (12.7 mam) from the edge "73.3 Alter washing and measuring thickness and Bareol hardness, place the coupons in en. air Tight polyethylene ag for conditioning or ship ping as described in 7.4.1 "Fe. Flexural Testing —Determine the flexural strength and modulus for: (1) two sets of three Specimens immediatly following the curing De od, and (2) one set of three specimens after tach inspection, for each solution, and each tet ‘emperature, Calculation of flexural strength and rmedulus after exposure should use the coupon {hikness determined at se time of flexural tes ing as measured in 7.3.2, The two pretested sets ‘hall be taken from tho center ofthe laminate as escibed in 6.2.1. The Mexoral strengths for these two sets shall be 2. saged together for use in taleulating the retained flexural strength in 8.2 ‘The flexural modulus values shall also be aver aged for use in 82. ‘741. Flexural tests shall be conducted in ac. cordance with Procedure A of Test Methods 15790, except for the conditioning parameters specified in this document. Coupons being ested tthe exposure location shall he placed in the Conditioning environment for 8 minimum of 2 immediately following the "cleaning. and ex- mination” described in 7.3, The coupon shal be tested during the same day after removing he coupon from the test environment, For testing ft a different location, the clean, dry courors houl be placed in a vapor tight bag for Ship- Nore &tn eases of volatile chemical expose spec maths peste barangay be regu 7142 Treee | by 4 in. 25 by 100 mm) (see Fig, I) are cut from each 4 by Sin. coupon, After tealligy the specimen edges shall be routed oF fanded to provide a nickel edge. Test speci tnene shall be the full thickness of the exposure ‘coupon. 8. Caleuations Bt Barco! Hardness Change—Tebulate or construct a griph showing the actual hardness readings of the specimens exposed at a given temperature, and the test period in days 32 Revained Flexural Strengdh and Mod Jus -Caleulate to the nearest 1.0%, the percent fage retention of flexural strength and flexural frodulus of the specimen during immersion for tech examination period, taking the flexural Srenath and flexural modulus afer curing 3s 100 %: Retained Menu song, f= (SSi] x 100 where ‘Sre Aekural strength of specimen after curing period, and Sy = Mlewural strength of specimen after test ied Retain lexural soda, = (1/6) x 100 ‘where Er = flesural modulus of specimen after curing period, and By = flexural modulus of specimen afer ts pe riod. 82.1 Calculate flexural strength and mods properties in accordance with Section 11 of Tet Methods D790. 38 w 822 Construct grophs showing the ave percentage of retained Rearing an !verage fexural mols of the specimens ro- ken at a tien examination period afer immer sion in a Farol est ston at gen tome perature oting the percentage of eine lex tra srength ng Nexral module asthe etal axis and the test period, in days, asthe horizontal 9. Imerpretaion of Results 9.1 Mechanical Properties ofthe Speimen— Because ofthe chemi atte of certain (pes ofl mater the rte of change wth me S of more ncince than the aca vale at any one time A pot ofthe tt res ll ine ht pce ni each constant Netra engin, Neural mos th or hardness wih time owl contnge fo Change asthe tes prowess 9.2 dppeerance of Specie Visa inspec Son ofthe expned specimen fr uri ere Bbsofeloe cing tstenpptingsotenng lures thickness. te Ie ey important, ft thee condone inst some degradation te laminate by a chemical environment 3.3 ppt of Inert din —Dis exon ofthe ft ston andthe formation etsdiment maybe sini ts, A al Scecoration may indat exactions components th st mont on te iste when ene 10, Report 10.1 The seport shall include the folowing: 11.1 Company. and individual standard laminates. 10.1.2 Complete identification of material ‘sted including resin, nonvolatile content, accel= ior, catalyst, reinforcement, surfacing mat, Tedmercon Sm sak Mew andthe nef inine Thastandnd i (arc » (C581 and flr, such a fire-etardant sitive oF thine tropes, 10.13 Corecyeleincluding room temperature 2 time, time at room temperature before testing ‘or before postcure if required, pot-cure time, and femperature. Any special post-curing tech niques suchas boiling water or steam for FDA type applications shal also be reported 10.14 Gls content of sancor laminate, it run in accndance it Note 1015 Hardes, Nera strength of contol ooo TS Color and sufice appearance of pc imens before testing. ses fa 10.7 Tea conditions; immersion medium, temperature, etc. = TDs.8 Toil om of in day, and ex anit res ye. Fora amie ton pid the da ied In TO 8 to 10.1.8.6 ate required, eee TOUR! Pretring samples conditioning sitet an standard enn TOU? Appetrance of spciens a in mmeion re cca Tow , ech Pitting, softening, etc.). : . 1083 Apesance of immeion mesiym (checoration semen TO_LAA arco tana ofthe specimens be- foreand ater enpcsue TOIPAS Thicker bef and ater eps IDL Fen stength and enol med uit coupons and pera etenion fxr ‘eng on fea models T0t9Graph showing percent renton of Asal seat and ral mol pated daa ext pei M1, Precision and Dias 11.1 No precision statement can be made for this prac, since contol oun tt Preparing programs fave nt Seen rn, Th tet esis of this pace are ota to sgn bay ste tents tothe sete esl sn thre ae no Sundaes Teas of he quate rests ae covered by Tet Netas B70. wo in ch he en ade one ed fend re iceman oa ned We ae pm elon uh mata eat cha eee aman he event xed bea a “ST4/ Conmieron Sanda 18 Rare Pi Po 08