Konsentrasi(ppm) Absorbansi 1 Absorbansi 2 Absorbansi 3 Absorbansi Rata-rata

0.5 0.012 0.003 0.002 0.0056666667

1 0.005 0.006 0.006 0.0056666667
2 0.017 0.017 0.017 0.017
3 0.019 0.02 0.02 0.0196666667
4 0.024 0.024 0.024 0.024
Sampel 0.006 0.007 0.006 0.0063333333

KURVA KALIBRASI
y=0.005x+0.002
Konsentrasi Sampel= 0.8666666667

Konsentrasi(ppm) Absorbansi 1 Absorbansi 2 Absorbansi 3 Absorbansi Rata-rata

0 0.002 0.002 0.002 0.002
0.5 0.005 0.006 0.006 0.0056666667
1 0.009 0.008 0.008 0.0083333333
2 0.014 0.016 0.018 0.016
3 0.019 0.02 0.019 0.0193333333
4 0.023 0.023 0.024 0.0233333333

KURVA ADISI STANDAR

y=0.005x+0.003
Konsentrasi Sampel= -0.6
0.6
 Kurva Kalibrasi
0.03

0.025
f(x) = 0.0056463415x + 0.0025426829
0.02 R² = 0.9363381438
Absorbansi

0.015

0.01

0.005

0
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5
Konsentrasi(ppm)

Kurva Adisi Standar

0.025
f(x) = 0.0053754386x + 0.0030374269
0.02 R² = 0.9787205178

0.015
Absorbansi

0.01

0.005

0
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5
Konsentrasi(ppm)
No. Panjang Gelombang (nm) Absorbansi
1 400 -0.001
Grafik panjang gelombang maks
2 399 -0.001
3 398 -0.001 120

4 397 -0.001 100

5 396 -0.001 80
6 395 -0.001

Absorbansi
60
7 394 -0.001
40
8 393 -0.001
9 392 -0.001 20
10 391 -0.001 0
150 200 250 300 3
11 390 -0.001 -20
12 389 -0.001
Panjang gelombang(nm
13 388 -0.001
14 387 -0.001
15 386 -0.001
16 385 -0.001
17 384 -0.001
18 383 -0.001
19 382 -0.001
20 381 -0.001
21 380 -0.001
22 379 -0.001
23 378 -0.001
24 377 -0.001
25 376 -0.001
26 375 -0.001
27 374 -0.002
28 373 -0.002
29 372 -0.001
30 371 -0.001
31 370 -0.002
32 369 -0.002
33 368 -0.001
34 367 -0.002
35 366 -0.002
36 365 -0.002
37 364 -0.002
38 363 -0.002
39 362 -0.002
40 361 -0.001
41 360 -0.001
42 359 -0.001
43 358 -0.001
44 357 -0.001
45 356 -0.001
46 355 -0.001
47 354 -0.001
48 353 -0.001
49 352 -0.001
50 351 -0.001
51 350 -0.001
52 349 -0.001
53 348 -0.001
54 347 -0.001
55 346 -0.001
56 345 -0.001
57 344 -0.001
59 343 -0.001
59 342 -0.001
60 341 -0.001
61 340 -0.001
62 339 -0.001
63 338 -0.001
64 337 -0.001
65 336 -0.001
66 335 -0.001
67 334 -0.001
68 333 -0.001
69 332 -0.001
70 331 -0.001
71 330 -0.001
72 329 -0.001
73 328 -0.001
74 327 -0.001
75 326 -0.001
76 325 -0.001
77 324 -0.001
78 323 -0.001
79 322 -0.001
80 321 -0.001
81 320 -0.001
82 319 -0.001
83 318 -0.001
84 317 -0.001
85 316 -0.001
 86 315 -0.001
87 314 -0.001
88 313 -0.001
89 312 -0.001
90 311 -0.001
91 310 -0.001
92 309 -0.001
93 308 -0.001
94 307 0
95 306 0
96 305 0
97 304 0
98 303 0.001
99 302 0.002
100 301 0.002
101 300 0.002
102 299 0.003
103 298 0.005
104 297 0.006
105 296 0.008
106 295 0.01
107 294 0.013
108 293 0.016
109 292 0.019
110 291 0.023
111 290 0.027
112 289 0.031
113 288 0.036
114 287 0.041
115 286 0.046
116 285 0.052
117 284 0.059
118 283 0.065
119 282 0.072
120 281 0.079
121 280 0.086
122 279 0.094
123 278 0.101
124 277 108
125 276 0.115
126 275 0.121
127 274 0.128
128 273 0.133
129 272 0.138
130 271 0.143
131 270 0.146
132 269 0.149
133 268 0.152
134 267 0.153
135 266 0.153
136 265 0.153
137 264 0.152
138 263 0.151
139 262 0.148
140 261 0.145
141 260 0.141
142 259 0.137
143 258 0.132
144 257 0.127
145 256 0.121
146 255 0.115
147 254 0.109
148 253 0.103
149 252 0.097
150 251 0.091
151 250 0.084
152 249 0.078
153 248 0.073
154 247 0.068
155 246 0.062
156 245 0.057
157 244 0.052
158 243 0.047
159 242 0.043
160 241 0.039
161 240 0.035
162 239 0.031
163 238 0.027
164 237 0.024
165 236 0.021
166 235 0.018
167 234 0.015
168 233 0.013
169 232 0.01
170 231 0.008
171 230 0.006
172 229 0.005
173 228 0.003
174 227 0.002
175 226 0.001
176 225 0
177 224 -0.001
178 223 -0.002
179 222 -0.002
180 221 -0.003
181 220 -0.004
182 219 -0.004
183 218 -0.005
184 217 -0.005
185 216 -0.006
186 215 -0.007
187 214 -0.008
188 213 -0.009
189 212 -0.011
190 211 -0.012
191 210 -0.014
192 209 -0.017
193 208 -0.02
194 207 -0.024
195 206 -0.027
196 205 -0.031
197 204 -0.035
198 203 -0.039
199 202 -0.042
200 201 -0.046
ng gelombang maksimum asam askorbat

00 250 300 350 400 450

Panjang gelombang(nm)
 C asam askorbat(ppm) Absorbansi rata-rata

0.5 0.0483
Kurva Kalibrasi
1 0.092 0.35
2 0.152 0.3
f(x) = 0.074397561x + 0.011145122
3 0.231 0.25 R² = 0.9969347113

Absorbansi
4 0.3136 0.2
0.15
Sampel vitamin C Absorbansi 0.1
1 1.2167 0.05
2 1.2164 0
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5
3 1.2162
Konsentrasi(ppm)
Absorbansi rata-rata 1.2164333333

y=0.074x+0.011
Konsentrasi sampel= 16.2896396396
Konsentrasi sampel= 4072.4099099099
urva Kalibrasi

97561x + 0.011145122
47113
Kurva Kalibrasi
Linear (Kurva Kalibrasi)

2.5 3 3.5 4 4.5

si(ppm)
 Konsentrasi (mg/L) Absorbansi 1 Absorbansi 2 Absorbansi 3 Absorbansi rata-rata
0 0.0002 0 0.0001 0.0001
2.5 0.1016 0.1051 0.1079 0.1048666667
5 0.225 0.2275 0.2276 0.2267
7.5 0.3426 0.3443 0.3443 0.3437333333
10 0.4536 0.454 0.4533 0.4536333333

Sampel Absorbansi 1 Absorbansi 2 Absorbansi 3 Absorbansi rata-rata

Sampel 1 0.0023 0.0022 0.0021 0.0022
Sampel 2 0.0022 0.0023 0.0019 0.0021333333

y=0.045x-0.003
Konsentrasi Cu Sampel 1= 0.1155555556
Konsentrasi Cu Sampel 1XFP= 0.5777777778

Konsentrasi Cu Sampel 2= 0.1140740741

Konsentrasi Cu Sampel 2XFP= 0.5703703704

%RPD= 1.2903225806
 Kurva Kalibrasi
0.5
0.45
f(x) = 0.0458373333x - 0.00338
0.4 R² = 0.9994965132
0.35
ABSORBANSI

0.3
0.25
0.2
0.15
0.1
0.05
0
0 2 4 6 8 10 12
KONSENTRASI (mg/L)
std parac std kaffein 1:01 Asy/Asx Amix/Asx
0.3544 0.2139 0.2933 1.656849 1.371201
0.3373 0.2131 0.2879 1.582825 1.351009 Kurva Perbandingan
0.3347 0.2535 0.305 1.320316 1.203156
1.8
0.412 0.2397 0.3075 1.718815 1.282854
1.6
0.2932 0.2055 0.2725 1.426764 1.326034 1.4 f(x) = 0.2063889784x + 1.0737647164
0.336 0.2034 0.2556 1.651917 1.256637

Amix/Asx
1.2 R² = 0.0983789666
0.3714 0.1905 0.2792 1.949606 1.465617 1
0.339 0.2343 0.3252 1.446863 1.387964 0.8
0.6
0.358 0.2631 0.338 1.360699 1.284683
0.4
0.3325 0.2188 0.291 1.519653 1.329982
0.2
0.4137 0.2458 0.353 1.683076 1.436127 0
0.4231 0.2253 0.3757 1.877941 1.667554 1 1.1 1.2 1.3 1.4 1.5 1

0.4623 0.2913
0.325 0.2895
0.4942 1.587024 1.696533
0.4326 1.122625 1.494301
Asy/Asx

Cx(kafein) 0.5365
Cy(parasetamol) 0.103
 Kurva Perbandingan 1:1

f(x) = 0.2063889784x + 1.0737647164

R² = 0.0983789666

1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2

Asy/Asx

recovery(kafein) 107.3
recovery(parasetamol) 20.6
std parac std kaffein 1:02 Asy/Asx Amix/Asx
0.3544 0.2139 0.4608 1.656849 2.154278
0.3373 0.2131 0.4562 1.582825 2.140779 Kur
0.3347 0.2535 0.5069 1.320316 1.999606
4
0.412 0.2397 0.5157 1.718815 2.151439
3.5
0.2932 0.2055 0.3881 1.426764 1.888564
3

Amix/Asx
0.336 0.2034 0.3987 1.651917 1.960177 2.5
0.3714 0.1905 0.4524 1.949606 2.374803 f(x) = 0.56
2 R² = 0.061
0.339 0.2343 0.7038 1.446863 3.003841 1.5
0.358 0.2631 0.6522 1.360699 2.478905 1
0.3325 0.2188 0.4833 1.519653 2.208867 0.5
0.4137 0.2458 0.6384 1.683076 2.597234 0
1 1.1 1.2
0.4231 0.2253 0.6721 1.877941 2.983134
0.4623 0.2913 1.0674 1.587024 3.664264
0.325 0.2895 0.5975 1.122625 2.063903

Cx(kafein) 0.7585
Cy(parasetamol) 0.881834
 Kurva Perbandingan 1:2
4
3.5
3
Amix/Asx

2.5
f(x) = 0.56721657x + 1.5174949944
2 R² = 0.0616337127
1.5
1
0.5
0
1 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2

Asy/Asx

recovery(kafein) 151.7
recovery(parasetamol) 88.18342
std parac std kaffein 2:01 Asy/Asx Amix/Asx
0.3544 0.2139 0.2019 1.656849 0.943899
0.3373 0.2131 0.205 1.582825 0.96199
Kurva P

Amix/Asx
0.3347 0.2535 0.2221 1.320316 0.876134
0.412 0.2397 0.224 1.718815 0.934501 1.6
0.2932 0.2055 0.2257 1.426764 1.098297 1.4
0.336 0.2034 0.2988 1.651917 1.469027 1.2
f(x) = 0.157669527
0.3714 0.1905 0.2427 1.949606 1.274016 1
R² = 0.0407043636
0.339 0.2343 0.2458 1.446863 1.049082 0.8
0.358 0.2631 0.2485 1.360699 0.944508 0.6
0.4
0.3325 0.2188 0.257 1.519653 1.174589
0.2
0.4137 0.2458 0.2718 1.683076 1.105777
0
0.4231 0.2253 0.281 1.877941 1.247226 1 1.1 1.2 1.3
0.4623 0.2913 0.3296 1.587024 1.13148
0.325 0.2895 0.3799 1.122625 1.312263

Cx(kafein) 0.8621
Cy(parasetamol) 0.07885
 Kurva Perbandingan 2:1

f(x) = 0.1576695271x + 0.8620743325

R² = 0.0407043636

1 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2

Asy/Asx

recovery(kafein) 86.21
recovery(parasetamol) 15.77
Asy Asx Amix Amix/Asx Asy/Asx
0.3544 0.2139 0.3582 1.674614 1.656849
0.3373 0.2131 0.3451 1.619427 1.582825
0.3347 0.2535 0.3485 1.374753 1.320316
Kurva sampel o
0.412 0.2397 0.3744 1.561952 1.718815 2.5
0.2932 0.2055 0.3033 1.475912 1.426764
0.336 0.2034 0.2847 1.399705 1.651917 2
0.3714 0.1905 0.306 1.606299 1.949606 f(x) = 0.5205053312x +
1.5

Amix/Asx
0.339 0.2343 0.4464 1.90525 1.446863 R² = 0.2792887077
0.358 0.2631 0.3872 1.471684 1.360699 1
0.3325 0.2188 0.3422 1.563985 1.519653
0.4137 0.2458 0.3797 1.544752 1.683076 0.5
0.4231 0.2253 0.3582 1.58988 1.877941
0
0.4623 0.2913 0.5139 1.764161 1.587024 1 1.1 1.2 1.3 1.4
0.325 0.2895 0.2765 0.955095 1.122625
 Kurva sampel obat sakit kepala
2.5

1.5 f(x) = 0.5205053312x + 0.7218439874

Amix/Asx

R² = 0.2792887077
1

0.5

0
1 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2
Asy/Asx

cx (kafein) 1.442 recovery(kafein) 72.1

cy(parasetamol) 0.52 recovery(parasetamol) 52

massa kafein/tablet = 36.05

massa Parasetamol/tablet= 130