(ERA AWaters Company Product: Catalog Number: 502 Lot No. 278-502 Certificate Issue Date: May 15, 2018 Expiration Dat January 31, 2021 Revision Number: Original CERTIFICATION Certified Parameter Value! mgit Phenol 0.709 Cyanide, total 0.529 ‘Amenable Cyanide 0.306 ANALYTICAL VERIFICATION Certified Value! mgi. Phenol 0.709 Cyanide, total 0.529 ‘Amenable Cyanide 0.306 Reference Materials icate of Analysis = = Certi WatR™ Pollution Total Cyanide ‘Product use Instuctons are incuded as part of the certiiation packet and ae paginated ‘Separately rom tis Certiate of Analyse. Please ‘eronce the product usa instructions lor caliog £502 revision 030512, Qc Performance PT Performance Uncertainty? “Acceptance Limits? Acceptance Limits* * gi git 0.827 0.592 - 0.886 - 27 0.405 - 0.645 0.344-0.714 251 0.173-0.471 0.198-0.413 Proficiency Testing Study NIST Traceability Mean Recoverys nn © SRMNumber Recovery git * * 0.513 97.0 70 : : 0.286 93.5 15 - Page 1 of 2 Lot: P278-502 16341 Table Mountain Pkwy - Golden, CO 80403 + T: 800.372.0122 + 303.431.8454 - www.eragc.comReference Materials « Certificate of Analysis « 1. The Certified Values ar the actual ‘made-to" concentrations conirmed by ERA analytical vorieation, The ceried values are monitored and purchasers willbe rotted of any signitcant changes resulting in recertication or withdrawal ots ceilied relerence materal during the period of vay of fis ceca 2. The Uncertainty is he total propagated uncertainty atthe 95% confidence Interval, The uncertainty ie based on the preperation and internal analytical ‘etffeation ofthe product by ERA, mulpied by a coverage factor. The uncertainty apples tothe product as supplied and does not ake Into account any Tequred or opional dion and’ preparaions the laboratory may perform while Using tis product {The QC Performance Accoptance Limits (QC PALs™)are based: PPALS™ reflect any inherent biases inthe methods used to establish the nits a imale a 85% confidence iiaval of the parformance that xoerienced laboratories should achive using accopted environmental methods. Use the QC PALs™ to ralslcaly evaluate yout perfomance against your peers. 4. The PT Performance Acceptance Limits (PT PALS™) ae calculated using the regression equations and fixed acceptance erteria spect’ in the [NELAC proficiency testing requirements. Use the PT PALs™ when analyzing his QC standard alongside USEPA and NELAC compliant PT standard Please note hat many PT study accepiance limits ae concentration dependent (some nomineaty) and, therelore, the accoptance lis ofthis QC standard and any PT standard may der relative to thir ference In concent 8. The PT Data/Traceabilty cata include tho mean value, porcont recovery and ruber of data points raported by the aboratries in our Proficiency Testing study compared tothe Certed Values. In addition, where NIST Standard Reference Malerils (SAMS) are avalabe, each analy has boon analylealy vaced fo the NIST SAM Isted. Ths product's raceae (othe ft rumbers oe startng materi. Al gravimetric and volumetric measurements Felatod o te manufacture ar traceable to NIST through an unbroken chain of compargons. ‘Tracesbilty Recovery (%) = (recovery certified standard)(% recovery NIST SPA] 100, “The raceabity data shown were complied by aralyzing the ERA standarss or thot associated steck sluione against the applicable NIST SAME. 6. For addtional ntomaton on thie product such a intended use, instructions fr use, level of homgenely, and safety information, please refer to the Provided instruction Sheet If you have any questions or need technical assistance, please call ERA technical assistance at 1-800-372-0122 or send an email to info@eraqc.com. Certifying Officer Quality Officer Brian Miller ‘Matthew Seebeck Bian Molen Jude hie ea a 16341 Table Mountain Pkwy « Golden, CO 80403 T: 800.372.0122 + 303.431.8454 + www.eragc.com Page 2 of 2 Lot: P278-502@ERA ‘AWaters Company Instructions for Catalog'# 502 Cyanide & Phenol Revision 030812 Description ‘+ This standard is packaged in a 15 mL serew-top vial containing approximately 14 mL of standard concentrate. ‘+ This concentrate is preserved with approximately 0.2% (\w'v) sodium hydroxide. ‘The concentrate can be stored at room temperature. ‘This product is intended to be used as a quality control check of the entire analytical process for the analytes/matrix included inthe standard, * The dilution instructions below represent the minimum suggested sample size for this product. Using a smaller sample size may invalidate the assigned value and/or uncertainty shown on the certificate of analysis, Helpful Hints: ‘+ This standard has been prepared as a concentrate and mustbe diluted prior to analysis. * As the USEPA Criteria Document requires that cyanide be present in a complex form, the diluted standard must be analyzed for total cyanide * This standard should be analyzed as soon as possible after the concentrate is diluted, Instructions: 1, Add 100-200 mL of deionized water and approximately 1 to 2 mL. of 50% sodium hydroxide to a clean 1000 tal class A volumetric flask. Shake the Cyanide & Phenol vial prior to opening. Using a clean, dry, class A pipet, volumettically pipet 5.0 mL. of the concentrate into the 1000 mL volumetric flask. Dilute the flask to final volume with deionized water. Cap the flask and mix well. Immediately analyze the diluted sample by your normal procedures. Report your results as mg/L forthe diluted sample. Bane Safet ERA products may be hazardous and are intended for use by professional laboratory personnel trained in the competent handling of such materials. Responsibility for the safe use ofthese products rests entirely with the ‘buyer and/or user. Material Safety Data Sheets (MSDS) for all ERA products are available by calling 1-800-372- 0122,