Sheet1

FMR-01 FMR-02 FMS-01 FMS-02

Intial Vacuum 340 360 330 240

350 to 500 mmhg Vacuum time 25 min 15 min 10 hrs 15 min

Upto 550 mmhg 11 hrs 30 min 11.5 hrs 30 min
Upto 600mmhg 25 hrs 7.25 hrs -
Upto 700 mmhg 36 hrs 57 hrs ** 19 hrs
Final Vacuum 730 mmhg 730 730 750

Max Temp 125.4 °C 124.6 °C 125.4

Starting Temp. 57.9 @ 545 mmhg 60.3 @ 560 mmhg 69.7 @ 330 mmhg

Final %HCM 0.24 0.36 0.05

** = Cahrge Hold up for 33 hrs @ 60 to 65 °C

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 Sheet2

HCM Distillation Data

FMR-01 FMR-02 FMR-03 FMS-01 FMS-02 FMS-03

Max temp 125.4 °C 124.6 °C 126.3 °C 125.4 °C 120.9 123
Max Vacuum 730 730 730 730 750 730
Time of Above 115 °C 6.45 hrs 12.3 hrs 12.15 hrs 7.15 hrs 7.15 hrs 11.15 hrs
Total Time 79 hrs 65 hrs 37.5 hrs 35 hrs 90.5 hrs 40 Hrs
Final % HCM 0.24 0.36 0.2 0.05 0.17 0.25

Hold up time 30 hrs 28 hrs - - 43 Hrs -

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