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Borang Rags Sharin
Borang Rags Sharin
Kod Rujukan:
(Diisi oleh RMC)
Satu (1) salinan borang permohonan asal hendaklah dihantar kepada Bahagian Perancangan
Kecemerlangan IPT, Jabatan Pengajian Tinggi, Aras 7, No.2, Menara 2, Jalan P5/6, Presint 5, 62200
Putrajaya
Syarat-syarat permohonan:-
1. Terbuka kepada kakitangan akademik (pensyarah) di Institusi Pengajian Tinggi Awam bukan
Universiti Penyelidikan.
2. Mempunyai pengalaman sebagai ahli akademik tidak melebihi lima (5) tahun DAN gred 52
dan ke bawah.
3. Mestilah Warganegara Malaysia
4. Pensyarah tetap di IPTA.
5. Hanya satu (1) projek penyelidikan dibenarkan untuk dipohon dan diperaku.
6. Tidak pernah memegang mana-mana geran nasional atau antarabangsa.
7. Pensyarah sedang cuti belajar tidak dibenarkan untuk memohon dan menjalankan
penyelidikan.
Feasibility Study of Palm Oil as New Insulation Medium for Power Transformer
B MAKLUMAT PENYELIDIK
Tempoh Perkhidmatan
C MAKLUMAT PENYELIDIKAN
A. Sains Tulen
B. Sains Gunaan
Bahan dan Polimer Kejuruteraan Kimia dan Tenaga dan Teknologi Hijau
Proses
Kepelbagaian Biologi
Sains Komputer
Makmal Voltan Tinggi, Fakulti Kejuruteraan Elektrik, Universiti Teknikal Malaysia Melaka, 76100 Hang Tuah
Jaya, Durian Tunggal, Melaka
C(iii) Tempoh penyelidikan ini (Maksimum 24 bulan):
Tempoh : 2 Tahun
C(v) Sila sediakan maklumat termasuk termasuk tajuk, nama geran, peranan, tempoh, tahun mula dan
tahun tamat bagi penyelidikan yang sedang/telah dijalankan oleh ketua penyelidik dalam tempoh tiga
tahun terakhir.
Tajuk penyelidikan Nama Geran Jawatan / Tempoh Tarikh mula Tarikh tamat
Peranan
C(vi) Sila kemukakan maklumat berkaitan penerbitan akademik yang telah diterbitkan oleh ketua
penyelidik dalam tempoh lima (5) tahun terakhir. (Contoh: Jurnal, buku, bab dalam buku, dll)
The main requirements of oil in power transformers are to increase the dielectric strength between
conductors by replacing air with a high dielectric strength fluid, and filling the pores of the Kraft insulating
paper and pressboard, to prevent discharges. In fact, insulating oil is an important information carrier
whereas providing information about the degradation of Kraft insulating paper, by depolymerization, which is
very important in transformer diagnostics [1]. Figure 1 shown the typical insulation oil flow inside the
transformer. During the last century, power transformers have generally been filled with mineral oil, which has
good compatibility with the Kraft insulating paper; good physical and electrical properties, not only as a
cooling fluid but also as an electrical insulator; and suitable properties such as good electrical arc quenching
and mainly availability, low cost, and long history. However, in a situation where there is accidental leakage in
a transformer, the oil could constitute an environmental hazard because it is toxic and non-biodegradable
[2,3].
Thus, vegetable oil turn out to be an alternative insulating oil for transformers, mainly for accommodate the
safety and environmental issues arise from mineral oil. These vegetable oil products include Soy-bean oil,
Sunflower oil, Coconut oil, Olive oil and oil extracts from the seed of Moringa Oliefera. The sunflower oil,
which is 100% environmental friendly, is used as a transformer oil for special purposes. Two typical
commercial vegetable oil products are Envirotemp® FR3 TM, introduced by Cooper Power System in 1996 [4],
and BIOTEMP®, developed by ABB in 1999 [5]. These two vegetable oil variants are being used in small
power and distribution transformers across the United States [6,7]. For utilizing the local resources of
vegetable products, Palm oil is the solution according to previous research [8] point out that the Palm oil
properties are suitable to become transformer insulating oil in term of breakdown voltage, which is one of
paramount importance to dielectric fluids, has been found to be adequate and good biodegradability. Palm oil
usage can be expanding from this research besides its well established applications and it also a line to one
of 12 National Key Economic Areas (NKEA): Palm Oil (Chapter 9: Deepening Malaysia’s Palm Oil Advantage)
[9].
Many previous research works have been carried out to compare the physicochemical and dielectric
properties of vegetable oil with the properties of mineral oil. However, only few reports on the property
change of vegetable oil especially Palm oil during the thermal aging process has been made. The influence
of Palm oil on aging rate of Kraft paper and related mechanisms have been hardly addressed. Many previous
studies gave early indications that the rate of paper aging is fluid-dependent [10]. Paper aged in mineral oil
degraded at a significantly faster rate than in vegetable dielectric fluid [11,12]. However, most published
studies only measured the Tensile Strength (TS) or the Degree of Polymerization (DP) to compare aging
rates of paper in mineral oil and vegetable oil; the mechanisms by which the aging rate of cellulose is slowed
down by impregnation with vegetable oil and variations of routine aging diagnostic parameters have been
rarely reported [13,14].
Hence, a feasibility study is needed on proving the Palm oil influence to the Kraft insulating paper for
developing chances in commercialize the Palm oil as insulation oil in power transformer. For this research,
Kraft paper is aged in mineral oil and palm oil in parallel to investigate the influence of oil type on the thermal
aging properties of oil paper. First, accelerated thermal aging tests will be performed at three different
temperatures using aging ovens. The Degree Polymerization (DP) of Kraft insulating paper will be used to
indicate the aging degree of insulation because of its efficiency and reliable test output compare to other
techniques such as Karl-Fischer titration and Frequency Dielectric Spectroscopy (FDS) [15]. Second, X-ray
Photoelectron Spectroscopy (XPS) technology is selected for analyzing the change of Kraft’s molecule
structures before and after aging. XPS is capable of detecting the difference in chemical state between
samples and also able to differentiate between oxidations states of molecules in Kraft’s paper [16]. Third, the
breakdown voltage level of the oil type samples will be tested according to the related standards [17,18].
Analysis of each results of the tested mechanism will be used to assess the performance between mineral oil
and palm oil.
Coils or winding is
wrapped with Kraft
insulating paper
(insulation between
winding)
1) To discover a new knowledge of Palm oil influence to the Kraft insulating paper on its chemical
structure behaviour in the thermal aging process.
2) To examine the Palm oil influence to the Kraft insulating paper aging degree and molecul structures
before and after thermal aging process using Degree Polymerization (DP) and X-ray Photoelectron
Spectroscopy (XPS). To investigate the electrical properties of Palm oil and established insulation oils
before and after thermal aging process from breakdown voltage testing.
The methodology of this research project is divided into two (2) major Work Packages (WP):
WP1: Review the theoretical aspects Kraft paper molecules structures and liquid dielectric mechanism.
Experimental setup for Kraft insulating paper through thermal aging process (temperature-controlled oven)
under Palm oil, mineral oil and established vegetable oil influence;
WP2: Condition assessment of Kraft paper using Degree of Polymerization (DP) according to ASTM D 4243-
99, IEC 61198 and IEC 60450 standards. Indicating Kraft’s molecule structures using X-ray Photoelectron
Spectroscopy (XPS) and breakdown voltage level for Palm oil, mineral oil and established vegetable oil.
In the context of WP1, Kraft insulating paper is usually made by the delignification of wood pulp by the
KRAFT process, in which wood is treated with a mixture of sodium hydroxide and sodium sulfide [14]. The
main chemical component of insulation paper is cellulose, which is a natural polymer of glucose. The
cellulose fibers consist of a bundle of molecules of different lengths, positioned side by side. They are held
together by hydrogen bonds involving the hydroxyl (OH) groups on the adjacent molecules, which are linked
together through the glycosidic bond as shown in Figure 2 [19].
The mechanism of cellulose degradation depends on the conditions to which the paper insulation is
subjected. There are four major factors that promote degradation, namely, exposure to elevated temperature,
oxygen, acid, and moisture. The degradation processes associated with these causes are thermal, oxidative,
and hydrolytic. Figure 3 shows the thermal effect to the cellulose paper degradation.
For this experiment according to [20], two sets of ampoules will be prepared: one set contained only the
insulating oil, and the other set contained the insulating oil with strips of Kraft paper (about 0.5 g) immersed in
the oil, as shown in Figure 4a. The ampoules are sealed using a torch and then uniformly heated in a
temperature-controlled oven (Figure 4b). The ampoules were maintained at 70°C for one week, and then the
temperature was raised to 110°C and maintained at this temperature for another week. The procedure
continued at 130, 150, and 190°C.
(a) (b)
Figure 4 a) Ampoules used for thermal aging: without paper (left) and with paper dipped in oil (right), b)
Thermal aging of oil and paper immersed in oil in a temperature-controlled oven [20].
Meanwhile in WP2, the samples of the mineral oil and palm oil before and after aging process will be proceed
to the Degree Polymerization (DP) process by using the High Performance Liquid Chromatography (HPLC)
system shown in Figure 5. This process is used for analyzing the level of Kraft insulating paper
polymerization to the tested oils. To enhance the experimental process, X-ray Photoelectron Spectroscopy
(XPS) technology will be used as shown in Figure 6. The main purpose is to study the mechanisms by which
mineral oil and palm oil retards paper’s degradation rate by measuring the electron energy spectra of Kraft
sample before and after thermal aging process. Breakdown voltage test is used to determine in term of
electrical properties of mineral oil and palm oil before and after thermal aging process. AC High Voltage
Testing (Withstand and Breakdown Voltage) will be applied to the tested oil according to the transformer
insulation standards; IEC 156 and BS 148. Finally, the analysis of each tested samples of Palm oil and
mineral oil will be prepared by using statistical analysis.
2. Carta Alir (Flow Chart) Aktiviti Penyelidikan (Sila sertakan dalam Lampiran)
3. Carta Gantt (Gantt Chart) Aktiviti Penyelidikan (Sila sertakan dalam Lampiran)
4. Carta perbatuan dan tarikh (Milestones and Dates) (Sila sertakan dalam Lampiran)
The research outcome is to contribute to the understanding of Palm oil as a feasible insulation
medium for power transformers. In the same time, it is expected by using Palm oil it will
extend the remaining life of Kraft insulating paper compared by using mineral oil and other
established commercial vegetable oils.
2. Penerbitan Penyelidikan
One (1) publication in ISI journal: IEEE Transactions on Dielectrics and Electrical Insulation
(IF: 1.094) and one (1) publication in Scopus journal: Elsevier Electric Power Systems
Research (IF: 1.478) Q1.
The research findings can be used to inform the Malaysia utility companies and the relevant
parties for the usage of palm oil as an alternative to mineral oil insulating fluid for the
distribution power transformers in Malaysia.
Support one of the 12 National Key Economic Areas (NKEA) on Palm Oil. This research will
increase the market segment of palm oil applications especially in Power Transmission and
Distribution areas.
Peralatan Tempat
Workstation facilities equipped with MATLAB and Microsoft Research Laboratory, Faculty of Electrical
Office and Microsoft Visual Studio. Engineering, UTeM
Megger’s OTS80PB/60PB Oil Test Sets are portable liquid High Voltage Laboratory, Faculty of
dielectric breakdown testers. Electrical Engineering, UTeM
Sila nyatakan anggaran bajet bagi cadangan penyelidikan ini dan berikan butir – butir perbelanjaan
lengkap dengan berpandukan kepada garis panduan yang dilampirkan.
Untuk Pembantu
Penyelidik (RO/RA)
a) Journal and
proceedings fees for
international and 1,500 1,500 3,000
national level
1. Semua maklumat yang diisi adalah benar, KPT dan IPT berhak menolak permohonan atau
√ membatalkan tawaran pada bila-bila masa sekiranya keterangan yang dikemukakan adalah tidak
benar.
√ 2. Permohonan projek penyelidikan ini dikemukakan untuk memohon peruntukan di bawah Dana
Pembudayaan Penyelidikan, KPT.
3. Permohonan projek penyelidikan ini juga dikemukakan untuk memohon peruntukan geran
penyelidikan dari ________________________________________________ (nama geran) dan
_________________ (jumlah dana)
Sila tandakan ( √ )
Diperakukan:
A. Disokong
B. Tidak Disokong
Ulasan:
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Nama: Tandatangan:
Tarikh:
Nota: Semua permohonan dianggap sulit. Keputusan Jawatankuasa Geran Penyelidikan KPT adalah MUKTAMAD.
Appendix A - Flowchart of Research Methodology
Start
Result?
Reprocess
Data Collection
Analysis the results
and findings
End
Appendix B - Project Gantt chart
No Milestone Date
1 The reliability of Palm oil as insulation medium for power transformer is identified August 2013
Palm oil and established insulation oils influence to Kraft insulating paper under accelerated thermal aging
2 March 2014
process is completed
Completion of Palm oil and established insulation oils influence to Kraft insulating paper aging degree and
3 October 2014
molecule structures test
Completion of analyzing physical and chemical structure interaction of Palm Oil under thermal aging using
4 June 2015
Fourier Transform InfraRed Spectroscopy (FTIR)
Completion of correlating the Palm Oil chemical structure interaction and conductivity measurement under
6 December 2015
thermal aging influence. Final report of research project is completed.