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FRACTURE TOUGHNESS

TESTING AND ITS


APPLICATIONS

A symposium presented at the

SIXTY-SEVENTH ANNUAL MEETING

AMERICAN SOCIETY FOR TESTING AND MATERIAL~

Chicago, Ill., J u n e 21-26, 1964

A S T M Special Technical Publication No. 381

Published by the
AMERICAN SOCIETY FOR TESTING AND MATERIALS
1916 Race St., Philadelphia 3, Pa.
in cooperation with the
NATIONAL AERONAUTICS AND SPACE ADMINISTRATION
9 by American Society for Testing and Materials 1965
Library of Congress Catalog Card Number: 65-16811

Printed in Baltimore, Md.


April, 1965
Second Printing, May 1970
Third Printing, J a n u a r y 1975
Fourth Printing, October 1981
FOREWORD

The development of various new high-strength alloys and the broadening


range of their applications, particularly in aerospace and in cryogenics, has
brought about increased emphasis on the study of fracture characteristics.
As a result, the technology of testing for fracture toughness and crack propa-
gation has grown rapidly in recent years. So, too, has understanding of how
to apply this testing technology to design problems such as selection of
materials, heat treatment, welding procedures, structural shape and size,
and effects of environment.
This collection of papers constitutes an authoritative and reasonably
complete statement of the current procedure and concepts in the field of
fracture mechanics. It should thus be of primary value to those concerned
with fracture testing and with applications of test data.
This publication is a cooperative effort of the American Society for Test-
ing and Materials and the National Aeronautics and Space Administra-
tion. It helps to fulfill the obligation of the ASTM to provide the technical
community with test methods, and with a sound understanding of their
usefulness and their limitations. Through its Special Committee on Fracture
Testing of High-Strength Materials (now ASTM Committee E-24 on Frac-
ture Testing of Metallic Materials), ASTM has provided important tech-
nical leadership. This volume is the latest in a series of valuable publications
on fracture testing and its application sponsored by this committee.
By cooperation with the ASTM, NASA is helping to fulfill its obligation
to provide for the widest practicable and appropriate dissemination of re-
sults from its activities. Not only have aerospace problems directly furthered
activity on fracture mechanics, but NASA scientists and engineers have
directly contributed much to this new technology. It is the purpose of this
publication to make the information in this important field as widely avail-
able as possible.
The Symposium on Fracture Toughness Testing and Its Applications was
held at the Sixty-seventh ASTM Annual Meeting, in Chicago, Ill., June
21-26, 1964. It was sponsored by the ASTM Special Committee on Fracture
Testing of High-Strength Materials. Chairman of the committee is J. R.
Low, General Electric Co. Symposium chairman was W. F. Brown, Jr.,
National Aeronautics and Space Administration.
The symposium comprised three papers sessions and a panel discussion.
Co-chairmen of the first session, on basic aspects of fracture mechanics,
were T. J. Dolan, University of Illinois, and Harold Liebowitz, Office of
Naval Research. Co-chairmen of the second session, on test methods, were
Edward Steigerwald, Thompson Ramo Wooldridge, and Z. P. Saperstein,
Douglas Aircraft Co. Co-chairmen of the third session, on practical applica-
tions, were B. M. Wundt, General Electric Co., and C. M. Carman, U. S.
Army Ordnance. Mr. Brown was chairman of the panel discussion, and the
other panelists were V. Weiss, S. Yukawa, P. Paris, J. E. Srawley, C. F.
Tiffany, G. R. Irwin, T. J. Dolan, J. A. Kies, and W. F. Payne.
ill
NO'rE--The Society is not responsible, as a body, for the statements
and opinions advanced in this publication.
CONTENTS
PAGE
Basic Aspects of Fracture Mechanics
Critical Appraisal of Fracture Mechanics--V. Weiss and S. Yukawa . . . . . . . . . . . . . . . 1
Historical Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
The Surface-Energy-Plastic Work Analogy . . . . . . . . . . . . . . . . . . . . . . . . . .......... 4
Interpretation of Fracture Toughness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Plasticity Analysis and Effects . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Inhomogeneities, Scatter, and Size Effects . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Outlook . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Stress Analysis of Cracks--Paul C. Paris and George C. M. Sih . . . . . . . . . . . . . . . . . . 30
Crack-Tip Stress Fields for Isotropic Elastic Bodies . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Elementary Dimensional Considerations for Determination of Stress-Intensity
Factors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Stress-Intensity Factors from Westergaard Stress Functions . . . . . . . . . . . . . . . . . . . . 34
Stress-Intensity Factors from General Complex Stress Functions . . . . . . . . . . . . . . . . 36
Stress-Intensity Factors for Some Three-Dimensional Cases . . . . . . . . . . . . . . . . . . . . 38
Edge Cracks in Semi-infinite Bodies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Two-Dimensional Problems of Plate Strips with Transverse Cracks . . . . . . . . . . . . . . 40
Reinforced Plane Sheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
Thermal Stresses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Stress-Intensity Factors for the Bending of Plates and Shells . . . . . . . . . . . . . . . . . . . 45
Couple-Stress Problems with Cracks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
Estimation of Stress-Intensity Factors for Some Cases of Practical Interest . . . . . . . 48
Stress Fields and Intensity Factors for Homogeneous Anisotropic Media . . . . . . . . . . 52
Cracks in Linear Viscoehstic Media . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
Some Special Cases of Nonhomogeneous Media with Cracks . . . . . . . . . . . . . . . . . . . 57
Inertial Effects on the Stress Field of a Moving Crack . . . . . . . . . . . . . . . . . . . . . . . . . 58
Energy-Rate Analysis of Crack Extension . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
The E q u ; , , a l e ~ qf ~nergy-Rate and Stress-Intensity Factor Approaches . . . . . . . . 59
Other Equivalent Methods of Stress Analysis of Cracks and Notches . . . . . . . . . . . . 61
Limitations of the Crack-Tip Stress Field Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
Appendix I - - T h e Westergaard Method of Stress Analysis of Cracks . . . . . . . . . . . . . 63
Appendix I I - - A Handbook of Basic Sdutions for Stress-Intensity Factors and
Other Formulas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Appendix I I I - - N o t a t i o n . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
Plasticity Aspects of Fracture Mechanics--F. A. McCfintock and G. R. Irwin . . . . . . 84
Kinds of Elastic and Plastic Stress and Strain Fields . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Longitudinal (or Parallel) Shear, Mode I I I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91
Initial Strain Distribution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92
General Aspects e,f Stable and Unstable Crack Extension . . . . . . . . . . . . . . . . . . . . 93
Loading Without Crack Growth . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93
Fracture Criteria . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94
Initiation of Crack Extension . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
Crack Growth and Instability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98
Empirical Trend of High-Stress Level Kc Results . . . . . . . . . . . . . . . . . . . . . . . . . . . 102
Crack-Opening Considerations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103
Empirical Representation of Crack-Extension Observations . . . . . . . . . . . . . . . . . . . . 106
Vi CONTENTS

PAGE
Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 109
Appendix--Summary of Relationships Between Linear-Elastic and Plasticity View-
points . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . II
Crack-Velocity Considerations--J. M. Krafft and G. R. Irwin . . . . . . . . . . . . . . . . . . . . II 0
Running Cracks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 114
Crack Border Instability in Kr Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11,~
Instability at a Plane-Strain Crack Border . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117
General Strain-Rate Influences . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118
Influence of Temperature and Loading Rate upon KI, Values . . . . . . . . . . . . . . . . . . 118
Initiation Kx9 in a Mild Steel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 129
Model for Brittle Fracture by Tensile Instability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120
Adiabatic Heating . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 121
Initiation K],(r) in 6A1-4V Titanium Alloy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 122
Comparison with Precracked Charpy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123
Influence of Flow Strength Speed Versus Temperature Sensitivity . . . . . . . . . . . . . . 123
Equivalence of Loading Rate to Crack Speed . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128
Velocity Prior to Crack Arrest . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123
Crack-Arrest Measurements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 126
Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 126
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 126
8
Test Methods
Fracture Toughness Testing--W, F. Brown, Jr., and J. E. Srawley . . . . . . . . . . . . . . . . 133
General Considerations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 137
Quasi-Two-Dimensional Prototype Specimen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 137
Criterion of Fracture Instability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 138
Crack Extension Resistance and Occurrence of Instability . . . . . . . . . . . . . . . . . . 138
Actual Cracks in Specimens of Finite Thickness . . . . . . . . . . . . . . . . . . . . . . . . . . . . 143
Dependence of 9, and Fracture Appearance on Thickness . . . . . . . . . . . . . . . . . . 144
~t, Measurement at Meta-instability or "Pop-in". . . . . . . . . . . . . . . . . . . . . . . . . 147
Practical Specimen Types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 150
Symmetrical Plate Specimens for General 9~ Measurement . . . . . . . . . . . . . . . . . . . 151
Effective Crack Length and Plastic Zone Correction Term . . . . . . . . . . . . . . . . . 152
~ Measurement Capacity in Relation to Specimen Size . . . . . . . . . . . . . . . . . . . 153
Variation of 9~ with Crack Length and Specimen Width . . . . . . . . . . . . . . . . . . . 155
Thickness of Symmetrical Plate Specimens. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 158
Plastic Zone Correction Term; fix, and Kie Calculations . . . . . . . . . . . . . . . . . . . . 160
Specimens Suitable for 9Ir Measurement Only . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 160
Single-Edge-Notched Tension Specimens. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . I60
Notched Bend Specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 164
Cracked Charpy Specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 166
Surface-Cracked Plate Specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 167
CircumferentiaUy Notched Round Bars . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 168
Summary Comparison of Specimens for ~rr Measurement . . . . . . . . . . . . . . . . . . 171
Instrumentation and Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 173
Cinematography . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174
Electrical Potential Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 175
Testing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17S
Reduction of Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 177
Advantages and Limitations of Potential Method . . . . . . . . . . . . . . . . . . . . . . . . . 180
Displacement Gages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 180
Gage Types and Testing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181
Reduction of Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 184
Advantages and Limitations of Displacement Gages . . . . . . . . . . . . . . . . . . . . . . . 185
Sensitivity of Displacement Gages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 185
CONTENTS vii

PAGE
Acoustic Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 186
Examples of D a t a . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187
A d v a n t a g e s a n d Limitations of Acoustic M e t h o d . . . . . . . . . . . . . . . . . . . . . . . . . 187
Continuity Gages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 188
Appendix--Practical Fracture Toughness Specimens; Details of Preparation, T e s t -
ing, and Reporting D a t a . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 188
Specimen Machining . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189
Fatigue Cracking a n d H e a t T r e a t m e n t . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 191
Testing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 192
D a t a Reporting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 193
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 196
Evaluation of Proposed Recommended Practice for Sharp-Notch Tension T e s t i n g - - R .
H. H e y e r . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 199
T e s t Specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202
Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202
Evaluation T e s t s . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 206
Summary ................................................................ 207
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 208
Electron F r a c t o g r a p h y - - A Tool for the Study of Micromechanisms of Fracturing
Processes--C. D. Beachem a n d R. M. N. Pelloux . . . . . . . . . . . . . . . . . . . . . . . . . 210
Uses of Electron Fractography . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 211
Fracture M e c h a n i s m s Studied by Electron Fractography . . . . . . . . . . . . . . . . . . . . . . 215
Cleavage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 217
Quasi-cleavage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 220
Coalescence of Micro-voids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 223
Intergranular Separation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 228
Fatigue . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 230
FailureAnalysis .......................................................... 241
Summary ................................................................ 242
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 245

Practical Applications
Applied Fracture M e c h a n i c s - - C . F. Tiffany a n d J. N. Masters . . . . . . . . . . . . . . . . . . . 249
T h e Selection of a Fracture-Toughness Specimen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 252
T h e Application of Fracture Mechanics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 255
T h e Prediction of Critical Flaw Sizes a n d Their Role in Material Sdection . . . . . 259
T h e Estimation of t h e Life of Pressure Vessels Subjected to Cyclic and Sustained
Stresses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 264
T h e Determination of Nondestructive Inspection Acceptance Limits . . . . . . . . . . 275
Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ............................. 276
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 278
Fracture Toughness Testing in Alloy D e v e l o p m e n t - - R . P. Wei . . . . . . . . . . . . . . . . . . . 279
Selection of Fracture T o u g h n e s s P a r a m e t e r and Test M e t h o d s . . . . . . . . . . . . . . . . . 280
Fracture Testing in Alloy Development . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 282
Relationships Between Microstructure and Toughness in Quenched and T e m -
pered Low-Alloy Ultrahigh-Strength Steels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 282
Effect of Sulfur on Fracture T o u g h n e s s of AISI 4345 Steels . . . . . . . . . . . . . . . . . . 285
Fracture T o u g h n e s s Anisotropy in a Maraging Steal . . . . . . . . . . . . . . . . . . . . . . . . . 287
Summary ................................................................ 288
Fracture Toughness Testing at Alcoa Research Laboratories--J. G. K a u f m a n and H.
Y. Hunsicker . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 290
Tear T e s t s . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 290
Sharp-Notch Tension Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 294
Fracture Toughness Tests . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 294
Correlation Between Tear Tests a n d Fracture T o u g h n e s s Tests . . . . . . . . . . . . . . . . . 299
viii CONTENTS

PAGE
Alloy Development ....................................................... 299
Strain-Hardening Alloys ................................................. 300
Precipitation-Hardening Alloys ........................................... 302
High-Strength Aluminum-Zinc-Magnesium-CopperAlloys . . . . . . . . . . . . . . . . . . . . 303
Alloys for Cryogenic Applications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 307
Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 307
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 309
The Application of Fracture Toughness Testing to the Development of a Family of
Alioy Steels--J. S. Pascover, M. Hill, and S. J. Matas . . . . . . . . . . . . . . . . . . . . . 310
Test Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311
Anticipated Use of Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311
Selection Criteria . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311
Application of Selection Criteria . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311
Testing of Sheet Materials at Ultrahigh-Strength Levels . . . . . . . . . . . . . . . . . . . . . 311
Testing of Tough Materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 314
Specific Examples of the Use of Fracture Mechanics in Alloy and Process Devel-
opment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315
Study of Thermal Treatments on Strength and Toughness o[ HP 94-45 Steel . . . . 316
The Effects of Anisotropy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 318
Welding Studies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 321
Summary and Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 322
Appendix--Cost of Various Types of Specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 324
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 326
Fracture Testing of Weldments--J. A. Kies, H. L. Smith, H. E. Romine, and H.
Bemstein . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 328
The Bend Specimen and Testing Fixtures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 330
Formulas and Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332
Demonstration of Linearity Between KI~ and Nominal Fiber Stress . . . . . . . . . . . . . . . 336
Limitations on Specimen Size and Notch Depth . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336
Comparison of Plane-Strain Fracture Toughness by the Slow Bend Test and by the
Single-Edge-Notch Test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 337
Material and Ku Test Results for i-in- Thick Plate of 18 Per Cent Marag-
ing Steel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 341
Tungsten Inert Gas Welds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 341
Metal Inert Gas Welds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 350
Summary of the Test Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 350
Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 350
Appendix--Failure Anal~ sis Example--Weld Flaw . . . . . . . . . . . . . . . . . . . . . . . . . . . . 351
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 353
Incorporation of Fracture Information in Specifications--W. F. Payne . . . . . . . . . . . . . . 357
Specimen Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 357
The Use of Subsize Specimens. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 359
Toughness Variations in Commercial Mill Products . . . . . . . . . . . . . . . . . . . . . . . . . . . 360
Effect of Flaw Geometry and Multiple Flaw Interactions . . . . . . . . . . . . . . . . . . . . . . . . 365
Quantitative Inspection Limits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 366
Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 367
Appendix I--Comparison of Critical Crack-Size Determination with Gross- and
Net-Stress Criteria for Surface-Cracked Specimen . . . . . . . . . . . . . . . . . . . . . . . . . . 368
Appendix II--Calculation of Equivalent Crack Size for Various Crack Geometries
and Interaction of Multiple Cracks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 370
Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 372
Panel Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 373

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FRACTURE TOUGHNESS TESTING AND ITS APPLICATION

INTRODUCTION
BY W. F. BROWN, j~.l

The phenomenon of structural failure strength of metals in the presence of


by catastrophic crack propagation at cracks or crack-like defects. The goal
average stresses well below the yield has been to provide laboratory tests and
strength has been known for many analytical techniques which will permit
years. Rashes of such brittle failures a quantitative measure of crack toler-
have occurred with increasing frequency ance useful not only in evaluating mate-
as the strength and size of our engineer- rials for a given application but also in
ing structures have increased. In the past, development of rational procedure for
each series of failures has given rise to a design against fracture. To achieve this
set of empirical tests and procedures goal requires the development of an
that sometimes provided a solution to essentially new branch of engineering
the specific problem at hand but did not science, and this, of course, is an evolu-
result in a generally useful approach tionary process which will take con-
that would permit avoiding future fail- siderable time to complete. However,
ures. with the Irwin linear elastic fracture
Recent military and aerospace re- mechanics as a basis, considerable prog-
quirements for very-high-strength, Iight- ess has been made in the desired direc-
weight hardware have given added im- tion, and today there are available re-
portance to the problem of brittle frac- liable if somewhat overconservative
ture and greatly emphasized the need procedures for avoiding failure by frac-
for a quantitative approach to the gen- ture in a new structure.
eral problem of crack tolerance in struc- The primary purpose of this sym-
tures. This need was dramatically high- posium was to review the methods for
lighted several years ago by the repeated fracture toughness testing as proposed
failures of early Polaris rocket motor by the ASTM Special Committee on
cases at stresses well below the design Fracture Testing of High Strength
value. The ASTM Special Committee Materials, with a view toward defining
on Fracture Testing of High Strength their limitations and the extent to which
Materials was formed at the request of they can be applied in structural design
the Office of the Secretary of Defense to and alloy development. With this in
assist in providing a solution to this and mind the authors were asked to direct
related problems. attention more toward clarification of
Over a period of the last five years concepts and procedures rather than
this committee has been concerned with toward presentation of new information.
the question of how to evaluate the In order to further assist in this review
1 Chairman of the symposium committee,
function, the last session of the sym-
NASA-Lewi~ Research Center, Cleveland, Ohio. posium consisted of a panel discussion
ix

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x FRACTURE TOUGHNESS TESTING

which gave those concerned with frac- to demonstrate a correlation between the
ture testing an opportunity to put results of pre-cracked Charpy tests and
questions to a group of persons who fracture toughness tests on larger speci-
have been active in the work of the mens. A paper by G. M. 0rner and C.
ASTM Fracture Testing Committee. E. Hartbower on this topic was pre-
There are, of course, many fracture
sented at the symposium meeting, but
test methods other than those discussed
because of space limitations does not
in this volume. Some of these often pro-
vide useful information regarding the appear in this volume. However, the
fracture behavior of metallic materials. reader should note that the panel dis-
The pre-cracked Charpy impact test is cussion contains a considerable amount
a recent example of such a test which is of information regarding the use of the
easy to perform and uses only small pre-cracked Charpy test and references
specimens. Some efforts have been made to investigations in this area.

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Basic Aspects of
Fracture Mechanics

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C R I T I C A L APPRAISAL OF F R A C T U R E M E C H A N I C S

BY V. Wrlss 1 AND S. YUI(AWA2

SYNOPSIS
A critical review of the basic premises of fracture mechanics is presented.
The applicability of the theoretical concepts developed by Griffith and con-
siderably expanded by Irwin and co-workers to materials testing and the de-
termination of a unique and characteristic value of "fracture toughness" is
examined. Finally, the usefulness and limitations of sharp crack fracture me-
chanics to the solution of engineering design problems are discussed.

The present symposium is devoted to reaction to this concept has ranged from
an evaluation of fracture testing and complete acceptance to total rejection
its applications. I t is devoted to a dis- over the past 44 years. The proponents
cussion of the question concerning the of the concept have endorsed it primarily
condition under which a sharp crack because: (1) it yields the correct func-
propagates to failure in a cataclysmic tional relationship between stress at
fashion, in terms of what is now referred fracture and flaw size as evidenced b y
to as sharp crack fracture mechanics or many results on brittle-behaving ma-
fracture mechanics. I t is not a sympo- terials including those obtained originally
sium devoted to a discussion of fracture by Griffith (2,3); and (2) because it
per se, ductile or brittle, but a sympo- predicts a theoretical cohesive strength
sium on the engineering aspects of of the defect-free material of the right
fracture, fracture testing, and utilization order of magnitude (0.1 E) which has
of results from fracture testing in design also been verified approximately on
applications for avoiding fracture. single-crystal whiskers (4).
Sharp crack fracture mechanics origi- The principal argument against ac-
nated from a crack-propagation concept cepting the Griffith concept is the elu-
proposed some 44 years ago by A. A. siveness of the value for surface tension
Griffith (1)3 which states that an existing which figures so dominantly in the
crack will propagate in a cataclysmic concept (5,5). Others object to it on
fashion if the available elastic strain experimental grounds, mostly on the
energy release rate exceeds the increase basis of data obtained with ductile
in surface energy of the crack. The materials where no appreciable crack-
1Associate professor of metallurgy, Syracuse length effect, as predicted by the Griffith
University, Syracuse, N. Y. concept, was observed (7); or on the
2Manager, Metallurgy, Materials and Proc- grounds that in addition to sur;ace
eases Laboratory, Large Steam Turbine-Gen-
erator Department, General Electric Co., energy and elastic strain energy, the
Schenectady, N. Y. possibility of an energy barrier to crack
3The boldface numbers in parentheses refer
to the list of references appended to this paper. initiation must be admitted. One last

Copyright9 1965 by ASTM International www.astm.org


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2 FRACTURE Totlom~ss TESTII~G

and perhaps most serious objection to mechanics for the solution of actual
the application of the Griffith concept design problems. In this fashion, the
to structural materials may be that it symposium hopes to show that the
represents an oversimplification (8) of a engineering approach to the solution of
series of much more complicated phe- problems--the theoretical (mathemati-
nomena in an age where there is no need cal) model -~ testing ~ design-applica-
to resort to such gross oversimplifica- tion sequence--is also applicable toward
tion, because of the development of a solution of the problem of designing
science and the availability of computers, against fracture. The final section is a
etc. Yet, the very simplicity of the panel discussion. In addition to provid-
fracture-mechanics approach, a one- ing an over-all summary, the panel
parameter design concept of great poten- discussion provides for further clarifica-
tial, is to a large extent responsible for tion of the various problem areas, for
the recent progress in design against the establishment of various inter-
brittle fracture. disciplinary connections that have not
To adopt either of these two extreme already been clearly established during
positions would be unrealistic; to ignore the first three sections, and for extended
the arguments would be folly. As en- discussion of the current status and
gineers we must attempt to solve the urgent research requirements.
problems put before us. The wealth of This introductory paper has the same,
experimental data on sharp crack frac- if somewhat more mixed, organization
ture mechanics in itself attests to serious and is, therefore, a broad preview of what
consideration or acceptance of the pro- is to follow. After a brief historical
posed analysis by a good portion of the review of the developments of fracture
engineering community. The present mechanics since Gritfith, the surface-
appraisal should, therefore, be aimed at energy-plastic-work analogy and its
inspiring the necessary caution in ap- consequences will be discussed. This will
plying the recommended concepts by be followed by comments on the aspects
delineating the limitations of sharp of initiation, propagation, and reinitia-
crack fracture mechanics on the basis fion of cracks which are intimately re-
of the applicability of the fundamental lated to plasticity and the various
premises utilized. The emphasis has to plasticity-correction procedures. An at-
be placed on the engineering usefulness tempt will also be made to relate the
of the approach rather than on its observed section-size effects to the
scientific and philosophical accuracy. stress-concentration effects as predicted
The symposium reflects this orienta- by fracture mechanics, taking into
tion towards the use of sharp crack consideration the influence of in-
fracture mechanics for the solution of homogeneities on the mechanical be-
engineering problems. The basic mathe- havior of the material. Finally, an out-
matical model, its physical implications, look is given on the potential of the
and limitations are discussed in the first fracture-mechanics analysis to fatigue,
~ection; in the second section, test stress-corrosion cracking, liquid-metal
methods to obtain the "design numbers" embrittlement, and fracture of non-
suggested by the mathematical model metals.
are discussed; the third section is de-
voted to a discussion of tile use of the HISTOa~ICAL REW~W
results of these tests and the mathe- Our present view of fracture certainly
matical analysis of sharp crack fracture started with the Griffith concept of

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WEISS AND YUKAWA ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 3

crack propagation which was presented Griffith-type energy balance must be


on February 26, 1920 (1). The now well- between the strain energy stored in the
known concept essentially states that specimen and the surface energy plus
an existing crack will propagate if the work done in plastic deformation.
thereby the total energy of the system is He also recognized that for relatively
lowered. The stress analysis used to ductile materials the work done against
calculate the stored elastic energy was surface tension is generally not signifi-
taken from Inglis's work (9) published cant in comparison with the work done
in 1913 and was also based on the work of against plastic deformation. The same
Taylor and Griffith (10) dated 1917. In arguments were also stated independ-
his paper Griffith states that "the ently at that time by Orowan (22) who
general conclusion may be drawn that in 1955 demonstrated that the modified
the weakness of isotropic solids, as Griffith condition for brittle fracture is
ordinarily met with, is due to the pres- not only a necessary but also a sufficient
ence of discontinuities, or flaws, as they condition for crack propagation. In
may be more correctly called, whose 1955, Irwin indicated (23) and in 1957,
ruling dimensions are large compared showed (24) that the energy approach is
with molectflar distances. The effective equivalent to a stress-intensity approach
strength of technical materials might according to which fracture occurs when
increase ten or twenty times at least if a critical stress distribution, charac-
these flaws can be eliminated." His teristic of the material, is reached. In
theory provides a means of estimating 1959, the ASTM Special Committee on
the theoretical strength of solids. It Fracture Testing of High-Strength Me-
also gives, for brittle materials, the tallic Materials was formed to launch a
correct relationship between fracture broad assault on fracture, based on the
strength and defect size. There is no by-then called Griffith-Irwin concept or
evidence that the advent of dislocation sharp crack fracture mechanics. The
theory in 1934 has influenced fracture need to design specimens with a most
research along the lines proposed by severe artificial flaw and to test these
Griffith or stimulated the application of specimens under the most severe con-
Griffith's concept to solids other than dition was recognized and advocated by
glasses. Smekal has published a number 1959 (2s,26). Subsequently, the demand
of papers (11-17) on the brittle fracture of for plane-strain fracture toughness values
glasses in which he recognizes the need was voiced and pop-in reactions were
to consider other material inhomoge- observed (27). Recent work at the Lewis
neities in addition to the starting cracks. Research Center of NASA with highly
This concern was shared by Weibull sensitive acoustical devices (28) indicates
who in 1939 published his statistical the need to study plane-strain crack
theory of fracture (18). In 1944, Zener extension instability in greater detail.
and Hollomon (19) connected the Grifl~th Plasticity treatments of the stress and
crack-propagation concept with the strain fields of notches were given by Hill
brittle fracture of metallic materials (29), Allen and SouthweU (3o), Lee (31),
for the first time. Orowan referred to and Neuber (32,33). In 1956, Hult and
X ray work in 1945 (20) which showed McClintock (34) presented, for the first
extensive plastic deformation on the time, a plasticity analysis of the stress
fracture surfaces of materials which and strain fields of sharp cracks in shear;
had failed in a "brittle" fashion. In McClintock subsequently applied this
1948, Irwin (21) pointed out that the analysis to ductile fracture (35). A non-

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4 FRACTURE TOUGHNESS TESTING

linear solution for loading without first symposium devoted solely to sharp
growth was presented by Neuber in crack fracture mechanics in relation to
1961 (33). The conditions for the dy- engineering and design applications.
namics of a propagating crack were
THE SURYACE-ENERGY -- PLASTIC-
first formulated by Mott (36) in 1948
WORK A N A L O G Y
and a specific aspect of it was treated
later by Yoffe (37). A good review is According to Griffith (1) crack growth
given by Schardin (38). Dynamic loading under plane-stress conditions will occur
problems are now being studied by if
Krafft et al (39) in relation to strain
rate sensitive materials. d (\ - - - o~Ta
- ~ - ' + 4aT) = 0 . . . . . . . (1)

where the first term inside parentheses


represents the elastic energy loss of a
plate of unit thickness under a stress,
a, measured far away from the crack, if
ergy -"4oT a crack of length 2a were suddenly cut
into the plate at right angles to the
direction of #. The second term repre-
~..,.~slot ~ Crock Length sents the energy gain of the plate due
\ to the creation of the new surface having
a surface tension, T. This is illustrated
in Fig. 1 which is a schematic representa-
tion of the two energy terms and their
sum as a function of crack length. When
Elostic Stroin the elastic energy release due to an
EnergyReleose \ increment of crack growth, da, outweighs
"r
the demand for surface energy for the
same crack growth, the crack will become
unstable. One can define a gross frac-
FIG. 1--Energy Balance of Crack in Infinite ture stress from this instability condition
Plate. as
9 = (2ET/fa) 11.. . . . . . . . . . . (2)
There have been a number of im-
portant symposia which devoted major which has, in the form ~v/a = con-
attention to this approach starting with stant, been shown to hold quite well for
an ASM symposium in 1947 (4o), an brittle and semibrittle metals. However,
MIT symposium on fatigue and fracture application of this analysis to such brittle
of metals (41), the First (42) and Second and semibrittle metals has also shown
(43) Symposium (1958 and 1960) on that the data extrapolate, for 2a values
Naval Structural Mechanics, the 1959 of atomic dimensions, to T values con-
International Conference on the Atomic siderably above most realistic estimates.
Mechanism of Fracture held in Swamp- This, together with experimental X ray
scott (44) and, most recently, the 1962 evidence of cleavage facets, etc. (zo,46),
AIME conference held at Maple Valley, led to the conclusion (2,3) that in the
Washington (4s). The present symposium fracture of metals the energy balance is
is perhaps unique in its relation to the primarily between the elastic energy
symposia mentioned, in that it is the release and the plastic work in crack

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WEISS AND YUKAWAON CRITICAL APPRAISAL OF FRACTURE MECHANICS 5

propagation, which overshadows the might expect it to depend on the plastic


energy reqtfirements for the creation of volume per trait thickness which is
new surfaces. Since the predicted func- proportional to a2.4 The calculations of
tional relationship between the stress Goodier and Field (47), which are based
and the crack length was in good agree- on Dugdale's hypothesis (48), confirm
ment with experimental evidence, it was this. Other calculations show at least
suggested (2,2o) simply to add a plastic- terms of the type, log a, to be present
work factor, P, to the surface tension, T, after differentiation.
in Eq 2. The inadequacy of the energy, and
The implications of this assumption in particular surface-energy, approach
together with the fact that av/-a = is further illuminated by a consideration
constant holds for a great variety of of fracture results obtained under con-
ditions of liquid-metal embrittlement
(49), or other environmental effects which
P'IOS"T affect the crack-fracture strength. At
io' - \ = ~ T
first glance these effects would tend to
confirm the predicted influence of surface
-" -.. I energy on fracture strength. As a matter
!
of fact, the Griffith-type fracture analysis
is unique in this respect as it is the only
-V=o ~"- 'l crack- or notch-fracture analysis of the
Liquid ~'- I many proposed which seems to provide
,o' Metal ~" -~ an understanding of environmental ef-
Embriltled I ~'...
I fects. However, Fig. 2 and Eq 2 clearly
I show the inapplicability of the type of
t t i I r
I 0 "e I 0 "6 I 0 "4 I 0 "z I l0 z reasoning whereby the loss in fracture
Crack Lenglh, 2a - in strength in the presence of liquid metals
is due to a reduced surface energy. If
FiG. 2--Schematic Illustration of Observed surface energy alone were responsible
and Predicted Strength-Crack Length Relation-
ship, the Plastic Work Term, and the Effect of for fracture, the fracture toughness, Kc,
Liquid Metal Embrittlement. would be somewhere around 10-5 E psi X
inY 2, where E is Young's modulus.
test conditions (plane strain, plane Even quite brittle materials have K,
stress, circumferential cracks, etc.) are values near 10- 3 to 10- 2 E psi X in. 1/*.
quite astonishing. If the elastic energy Thus, the plastic-work factor, P, is 10'
release due to the crack has the form, to 10e times the surface energy and any
Aa"a", then the plastic-work term must change in T due to environmental effects,
have the form, Ba'~-~a"-I. Since theory even if T is reduced to zero, would have
of elasticity dictates m -- 2, the plastic- negligible effect on the fracture strength.
work term must be independent of The experimental results in this area
stress. The elastic strain energy of a must, therefore, lead to the conclusion
cracked plate per unit thickness is that the influence of the environment, if
proportional to a s (that is, n = 2) and, it affects the fracture strength and the
therefore, the plastic-work term should fracture toughness, is on the material's
be proportional to a. However, one ability to deform plastically rather than
on a change in surface energy. This may
4See also: H. W. Liu, "Fracture Criterion indeed be accomplished by such phe-
of a Cracked Plate," GALCIT SM68-29, July,
1963. nomena as slow crack growth (So) or

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6 FRACTURE TOUOH~SS TESTING

other microscopic diffusion phenomena, the energy-balance dilemma, it can


which lock dislocations and thus impede serve to assert the reasonableness of
plastic flow. Allen (51), however, points fracture mechanics by not requiring a
out that the surface-energy term may be statement concerning the use of the
important during the early stages of released elastic energy. The statement
crack formation, when it is large com- that "fracture occurs when the stress
pared to the elastic-energy term. condition in a sufficiently large volume
The plasticity question raised above is exceeds a critical value" (52-54) may
not yet resolved. It obviously bears on readily be converted into a mathematical
the generality of iracture mechanics and, model with the help of Westergaard's
therefore, merits urgent experimental stress field equations for cracks

K o( o
~r~ = (27rr)V~cos ~ 1 -- sin ~ sin

Stress o 30\ !
gv = (2rr)'/' c~ ? 1+sin?sin7 ... (3)

K o o 30
= cos si , cos 7

which indicate that identical stress fields


are obtained for identical K values. The
17"
coordinate system is shown in Fig. 3.
The stress-intensity factor, K, is a
or== K cos 0 / 2 (I-sin 0 / 2 sin 3 0 / 2 )
2~/-~-~" function of applied stress and crack
geometry and, for a crack of length 2a
cos 8 / 2 in an infinite plate, is given by K =
o"v : K ~ ( l + s i n 0 / 2 sin 3 8 / 2 )
'l~r n" a(lra) ll2. If the critical stress system
under which failure occurs is charac-
cos 8 / 2 terized by a stress-intensity factor, K c ,
rxy=K 2---~--~w s i n e / Z cos 3012
which in itself is a material characteristic
FzO. 3--Schematic Illustration of the Elastic (fracture toughness), then a Griffith-type
Stress Distribution near the Tip of a Crack. relationship results without consideration
of any energy-dissipation processes in-
and theoretical attention. The paper by volved. Primarily because of the straight-
Irwin and McClintock in this symposium forwardness of the fracture assumption
will show another attack on the same and the ability to ignore the little-under-
question. stood surface-energy and plastic-work
Linear theory of elasticity provides phenomena accompanying fracture de-
unique and single-valued relationships velopment, the stress-intensity approach
among stress, strain, and energy. There- is now preferred to the energy approach.
fore, a fracture criterion expressed in The dilemma is, however, not resolved
terms of an energy concept has its by choosing the stress-intensity factor
equivalent stress and strain criteria, all approach. Our ignorance concerning the
of which are mathematically indistin- plasticity problem is just as detrimental
guishable. here as it was in the energy-balance
While a stress rather than an energy model. An elastic stress distribution,
criterion for fracture may not resolve with a singularity at the crack tip, is

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WEISS AND YUKAWA ON CRITICALAPPRAISAL OF FRACTURE MECKANICS 7

assumed to describe the stress field chanics represents a good mathematical


ahead of the crack, where plastic yielding model as long as the gross fracture stress
has certainly taken place during loading. is small compared to the yield strength
In either case, the mathematical model of the material. As a refinement to this
chosen to describe the event of fracture statement, one must consider that the
fails to describe this event realistically error will not only depend on the ratio of
enough and causes some error in the plastic-zone size to crack length or of
prediction of the event in ctuestion. This fracture strength to yield strength, but
error is due solely to plasticity phe- also on the load-carrying capacity, that
nomena. Thus, if these plasticity phe- is, the stresses and strains inside the
nomena are negligible in relation to the plastic zone (Ss) which in turn depend on
phenomena occurring in the elastically the strain-hardening characteristics of
stressed region of the structure, the error the material (SS-S8).
will be negligible. As circumstances A fracture mode change, from plane
develop which increase the ratio of stress to plane strain, on the other hand,
volume subjected to plastic flow versus may be accompanied by a more drastic
volume under elastic conditions, the change in plastic-zone size (sS,Sg-61) and
error will increase. When it will reach an a fracture-mechanics analysis may well
intolerable level depends on the design apply to the severe plane-strain condi-
or analysis problem; however, because of tion but not to the plane-stress condi-
the nature of the error, it may be safe to tion. Such a mode change can be caused
assume that it will increase gradually by a change in the test-section geometry.
rather than abruptly. The problem is particularly bothersome
As fracture mechanics provides a because: (1) it is connected with a
method to measure the "brittle" strength rather abrupt change in fracture be-
of a material, it is necessary to insure havior; and (2) there exists no method
that the errors introduced by plastic to predict whether the fracture-mode
flow are minor or adequately corrected. will be plane-stress or plane-strain.
This demand is readily met if plasticity An answer to the second problem may
effects are negligible, that is, if the plas- be attempted, based on our knowledge
tic-zone size is small in comparison with of the stress state of mild notches. There
the crack length as well as the net Weiss and Sessler (62--64) have shown
remaining cross section. In this case, the that plane-strain conditions prevail at
stress field will be adequately described mid-thickness of the notch root if
by linear elasticity theory. A plastic- B / p > 10, where B is the specimen
zone correction factor, r r , can be esti- thickness and p the notch-root radius.
mated from Eq 3 by setting % = a t 8 , Since the plastic-zone size of a sharp
the yield strength of the material, which crack may be related to the root radius
results in of a mild notch, the ratio of specimen
thickness to plastic-zone size may be
r r = 2-'~ . . . . . . . . . . . (4) assumed to determine the fracture state
(6o). Thus, a condition of plane strain
At the onset of fracture, where K = would obtain if ( 2 B / a ) / ( ~ / ~ r ~ ) ~ > 10,
K . , one may estimate the error intro- which again shows the need for small
duced by plastic flow from the ratio ~r~/ars values, since there normally
(r,s/a) = (1/27ra)(K/ars) 2 which is exists a limit on specimen thickness.
equal to 89(a,/~rs) ~, where ~, is the gross The problem is further complicated
fracture strength. Thus, fracture me- by the difference in response of different

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8 FRACTURE TOUGHNESS TESIINO

materials to a change in stress state. In methods proposed for the determination


most cases, the yield strength increases of plane-strain fracture toughness, K I,,
and the fracture ductility decreases on with specimens which do not necessarily
changing from plane-stress to plane- lead to plane-strain fracture. Reference
strain conditions; however, the relative is made to the various pop-in determina-
changes vary from material to material. tions by compliance gauge or acoustical
This is illustrated in Fig. 4, where the methods (2~,28,6s) of the first onset of
fracture-toughness value, Ko, is plotted crack growth. In order to retain the
technical usefulness of sharp crack
220 fracture mechanics, K zo must be defined
in terms of load and crack length for
200
which the first significant crack growth
occurs. Individual microscopic fractures
A, 2024-T4]
may and do occur at some lower stress,
180
iL
-~
9 AI 2024-T31 (60)
o AI 7075-T6J
D H-II Steel "
but little would be gained by ascribing
an individual Kzc value to each "ping"
1550~ 30 min. representative of the fracture of a
.•160 1850~ 15 min.
Air Cool .(90) microscopic region. Actually, since the
Temper 1075"F
~ 140 9
o 2 hrs. 4- 2 hrs,
engineering materials of concern are com-
0
v T i BI20 VCA " "1 plex aggregates of grains, grain bound-
o ST + Age 900~ "(91)
72 hrs.
/

J
aries, inclusions, defects, etc., each of
- E]
which may be highly anisotropic, one
=. must not expect a fracture behavior
~ 100
which was predicted for continuous
homogeneous isotropic solids. While the
_~ 80 weakest link fracture analogy may hold,
a weakest spot analogy certainly does
not. For engineering purposes, a Kz,
60
/ value based on the first "ping" would
40
certainly provide a careful and safe
design value. However, since the damage
to the structure from the fracture of a
20 20 40 60 80 I00 120 low load-bearing inclusion may be
Reciprocol Thickness, I/B, in-t
negligible, a somewhat higher Kzo value
FIG. 4--Variation of Fracture Toughness with may be more realistic and economical.
Thickness for Various Materials. Long time tests at these low load levels
may provide the necessary clues to
as a function of specimen thickness. As assess the damage of these early
the plane-strain case is obviously the localized fractures.
most severe, one is tempted to rate ma- Although it has been tentatively con-
terials in accordance with their plane- cluded that plasticity effects Will cause
strain fracture toughness, Kic. This is gradually developing errors in the sharp
readily justifiable for rather similar crack fracture mechanics analysis, quite
materials. It may, however, penalize abrupt changes in behavior, with per-
rather ductile materials, where the haps catastrophic consequences in service,
section sizes required to determine K ~ are not altogether precluded. The change
are much larger than those considered from plane-stress to plane-strain condi-
for service. tions is a case in point. Temperature,
A comment is in order on the various shape, metallurgical effects, and crack-
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WEISS AND YUY..AWA ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 9

orientation effects may precipitate such value ( K , , KIo or ff~, gi,) useful for
a n abrupt change. describing the fracture behavior of a
Thus, the applicability of sharp crack material, it is useful to consider some
fracture mechanics is basically limited factors bearing on the interpretation of
by plasticity phenomena. In a given this quantity.
technical material, fracture mechanics A pertinent starting point concerns
will not be applicable below a certain the elastic strain energy input term in
minimum size (23,~6) where the material the energy-balance picture of the frac-
is essentially "notch- or crack-insensi- ture process and particularly, the rela-
tive." K~ values calculated from tests tionship between the strain energy
in this region would be too low. With an release rate, 9, and the notch- or crack-
increasing ratio of specimen width to tip geometry. Experimental measure-
plastic-zone size, the fracture-mechanics ments of ~ have been determined for
analysis becomes more and more ac- several specimen geometries via the
curate. For thicker specimens, this may compliance measurement technique (59,
occur earlier due to the smaller plastic- 65,66). These are made using specimens
with relatively mild root radii, such as
200 0.005 or 0.010 in. In nearly all cases
where this technique has been used,
.~ I oo the functional relationship between
.- 80
i
60
and crack dimensions obtained agrees
very closely with that calculated from
a sharp-crack model assuming linear
~c elastic behavior. Thus, experimental
20'
evidence indicates that the elastic strain
energy release rate is relatively insensi-
10
0.1 I I0 tive to tip-root radius in the range from
Crack Length, 2a-in a mathematical "sharp" crack to macro-
FtG. 5--SchematicIllustrationof a Transition scopic finite root radii.
from Plane-Stressto Plane-Strain Failure. This is also to be expected on theoreti-
cal or analytical grounds. For example,
tone size in plane strain. By the same from Griffith's original work on a center-
token, a gradual increase in specimen slotted infinite plate model, it can be
size (including thickness) may also shown that the release rate decreases
cause an abrupt change from the K, to by only about two per cent in going
the K~, portion of the curve (see Fig. 5). from a sharp crack to a root radius
Once the plane-strain fracture toughness, equal to one tenth of the crack length
Kx,, has been suitably established, it (67). The same thing can be seen by
should provide an accurate fracture examining the stress-intensity factor
analysis for specimens beyond a limit- formulation for fracture mechanics. As
ing size, save for certain material condi- noted by Irwin and others, the stress-
tions which will be discussed later under intensity factor, K, is directly related
"Inhomogeneities, Scatter, and Size to the energy-release rate in the fully
Effects." linear elastic situation:
INTERPRETATION OF FRACTURE K = (Ecd)In(for plane stress). . . . . (5)
TOUGHNESS Irwin (68) has further noted a relation
Since the aim of sharp crack fracture between K and elastic stress concentra-
testing is to obtain a fracture-toughness tion analysis:
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10 FRACZVRE T O U G ~ S S TESTZNG

K = lim 89,r,,,(~'p) 1/~ . . . . . . . . . (6) be significantly lower for a fatigue-


p~0
cracked specimen than for a small but
where: finite root-radius specimen (69). Other
data show that above a certain minimum
a~, = maximum stress at notch root
root radius, the apparent Kc increases
p = notch-root radius.
in proportion to the square root of the
In this relationship, K will become in- radius. This minimum radius is evi-
sensitive to root radius whenever ~ is dently dependent either on material or
inversely proportional to p~/2. This is strength, or both. Values ranging from
the case when the root radii are small 0.00025 in. for H-11 steels at high-

4001.

2 0 0~ ' ~ _ _ ~ p ="zero"
100~
-= 0.000~,,,~
=., 8 c -

,o- .....

=~ l0 - l i l t
3
.o

I I I II I I ~ LI
2 4 68 2 4 68 2 4
0.00001 0.0001 0.001
Distonceoheodof NotchTip- in
FIG. 6--Comparison of Local Stresses in the Vicinity of the Notch Tip.

compared to the notch depth or the slit strength levels to 0.010 in. for 7075-T6
length. aluminum have been observed 0'o,71).
If the viewpoint is adopted that un- These observations show that, in a
stable fracturing is solely dependent on finite radius specimen, it is possible to
attaining a critical value of the strain reach and exceed a value of strain
energy release rate, the preceding would energy release rate that is sufficient to
indicate that fracture strength and satisfy the condition for unstable fracture
fracture toughness should be relatively and yet not have fracture ensue.
insensitive to root radius in the small I t is evident that more than just the
radius range. However, experimental attainment of a critical value of ~ (or
fracture data show that this is not always its equivalent as K) is involved in un-
the case, Fracture-toughness values can stable fracture. This forces attention on

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WEISS AND YUKAWA ON CRITICAL APPRAISAL OF FRAc~u~ MECHANICS 11

the small region immediately surround- unstable fracturing of metallic materials.


ing the crack or notch tip and it is One of these pertains to the conditions in
pertinent to examine how small this a very small localized region near the
region actually is. For example, Fig. 6 crack tip which are necessary to initiate
shows the distribution under elastic unstable fracturing. The other involves
conditions of the longitudinal stress conditions more remote from the crack
ahead of a crack or elliptical slots of tip which are necessary to sustain un-
various radii for the classical slotted stable crack motion once the initiation
infinite plate geometry. The distribution condition has been fulfilled. The material,
for a crack is derived from the stress- in turn, offers resistance to each of these
intensity factor formulation; the finite conditions. The problem in fracture
radius cases are from Neuber's analysis testing is to determine which of these
as recently calculated by Jackson (72). resistances is controlling and being
The curves for a finite radius differ from measured in any particular test. For
that for a crack only in the region ahead example, if the notch tip is not
of the tip over a distance approximately extremely sharp, it is the initiation
equal to one fourth the respective root resistance which is controlling and
radius. Beyond this region, the elastic consequently being measured.
stress distributions for an infinitely Ideally, then, in sharp crack fracture
sharp crack and a small but finite root testing, it is desirable to perform the
radius are virtually identical. The one- test under conditions where the ma-
fourth factor shown by the curves agrees terial's resistance to the initiation stage
with Weiss's analytical treatment of this has been reduced as low as possible. From
subject (73). For the specimen geometry a practical testing and application view-
considered, this means that for a root point, indications are that this is easier
radius of 0.005 in., the difference in to achieve in relatively higher-strength
stress distribution compared with a materials. This may explain the greater
sharp crack occurs only in about the first success of sharp crack fracture mechanics
0.001 in. of the distance ahead of the tip. in higher-strength steels than in lower-
Therefore, one must conclude that strength steels.
whatever happens in this small region With regard to sustaining unstable
ahead of the crack is crucial to the frac- fracture, it appears that fracture me-
ture process, especially the plastic de- chanics provides an adequate tool for
formation which occurs in this nearly describing the necessary conditions. It
microvolume. Furthermore, it may be is reasonable to presume that an energy-
that the magnitude of the plastic de- balance condition must be fulfilled and
formation within this region is more this is equivalent to having a unique
important than its spatial extent. It distribution of elastic stresses in regions
would seem that the spatial extent of remote from, but surrounding, the crack
plastic deformation should not differ tip. Fracture mechanics provides a
appreciably between a crack and some description of these elastic stresses.
small but finite radius, such as 0.005 in. In contrast, the conditions important
However, the magnitude of the strains to the initiation stage are not well
close to the notch tip would be expected understood. Possibly, some limiting
to be quite different. state of plastic strain needs to be at-
These considerations indicate that tained to initiate the process of unstable
apparently two conditions have to be fracture. With some differences in the
prescribed to characterize fully the assumptions regarding the limiting

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12 FRACTURE TOUGHNESS TESTmO

strain, this is essentially the viewpoint be less under plane-strain conditions.


followed by McClintock (35), Krafft The presently unanswered question is
(74), and others who have attacked this which of these predominates in lowering
problem. Whatever the specific details, the fracture toughness as plane-strain
if the conditions for initiating unstable conditions are approached.
fracture are to be handled within the An interpretation of the pop-in phe-
present framework of fracture mechanics, nomenon can be made in relation to the
an implicit assumption is necessary. The difference in initiating and sustaining
strains within the plastic zone must de- the fracture under plane-strain and
pend only on the stress-intensity factor plane-stress conditions. In the mid-thick-
and be independent of crack and speci- ness region along the crack front, plane-
men geometries and loading conditions. strain conditions occur and resistance to
This is identical to assuming that the fracture initiation is relatively low.
elastic stresses surrounding the plastic When this region fractures, the load
zone fully specify the strains within the carried there shifts to regions closer to
zone. the side surfaces. These regions, however,
The above considerations indicate are in a state of plane stress and have
that fracture toughness as derived from higher resistance to fracture initiation.
fracture-mechanics tests combines the Therefore, sustained fracture is arrested
two aspects of the fracture process into after.only a small region has fractured
a single value. The successful application and further loading is needed for reinitia-
of fracture mechanics, then, depends on tion under the changed conditions. It
how closely these two aspects of initiation would seem, on this basis, that pop-in is
and sustained propagation are related to most likely to occur in crack-notched,
each other. sheet-type specimens within some re-
The complexities involved in this stricted range of thickness. On the
distinction between these two aspects of thicker side of this range, pop-in and
fracture can be seen by considering the unstable fracture propagation tend to
effect of plane-stress and plane-strain become simultaneous events. On the
conditions. As noted in the next section, thinner side, it becomes more difficult to
the plastic zone is smaller under plane- develop plane-strain conditions to induce
strain conditions than under plane-stress pop-in.
conditions. Presumably, this means that Recognition of the need to determine
the magnitude of plastic strain is smaller plane-strain fracture toughness values
within the plastic zone. However, there and to determine the earliest event in the
is a region ahead of the crack which is over-all unstable fracturing process has
outside of the plane-strain zone but led to several evolutionary modifications
which would be within the plastic zone in sharp-crack testing. The round
if plane-stress conditions existed. Within notched tension and the embedded
this region, the stress normal to the surface crack specimens provide two
crack (and the actual stress intensity) means of attaining plane-strain condi-
is higher in the plane-strain situation tions at the crack-notch front. As dis-
because it has not been relaxed by plastic cussed above, the pop-in determination
flow as in the plane-stress situation. is an attempt to measure the fracture
These higher elastic stresses would event that occurs under plane-strain
presumably enhance the initiation of conditions in a specimen that otherwise
fracture. At the same time, the limiting is generally under plane stress.
plastic strain for fracture initiation could Sharply notched specimens tested in a

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WEISS AND Y U K A W A ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 13

Charpy impact machine have been sug- Some reasons for this have already been
gested as another procedure for obtaining discussed. In addition, procedures for
fracture toughness values by calculating adjusting for plasticity effects are a part
the energy absorbed per unit area. It of the current treatment of sharp crack
should be recognized that all the diffi- fracture testing and the suitability of
culties associated with resistance-to- the procedures needs to be examined.
fracture initiation, with pop-in, and Calculation and experimental verifica-
with the transition from plane strain to tion of localized plastic deformations are
plane stress are also present in this exceedingly difficult problems, but it is

Shaded Area- Crack Surface


Heovy Solid Line -Crock Front

Iostio Zone

FIG. 7--Three-Dimensional Schematic Diagram of the Crack Surface, the Crack Front and the
Plastic Zone.

method. Furthermore, the absorbed useful to consider some aspects of the


energy per unit area will be an integrated present knowledge.
value across the fracture area. Thus, it Most analytical calculations of the
would seem more difficult to distinguish early stages of tensile deformation from
between the separate events, and inter- a sharp notch predict that the deforma.
pretation of the values obtained requires tion should occur in a double lobe-
careful analysis. shaped region extending outward from
the notch tip. The lobe tends to be con-
PLASTICITY ANALYSIS AND ~EF~ECTS stricted in a direction directly ahead of
A full understanding of the localized the crack. Observations (for example,
plastic deformations around the crack Knott and CottreU O'S) and Gerberich
or notch tip is essential if all aspects of (74)) indicate that the deformation zone
the fracture process are to be understood. roughly has this shape. However,

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14 FP~ACrmU~ TOUOHNESS T~STm6

Gerberich has also shown that material chanics can be considered. Based on
properties and the extent of deformation suggestions originally made by Irwin,
strongly influence the shape and orienta- the current procedure corrects for crack-
tion of the plastic zone, as well as its tip plasticity by adding an extra incre-
size and the strain distribution within it. ment to the initial crack length. The
The zone is more pinched and distended adjustment is made as follows:
in low strain-hardening materials. These
a = ao + r r ............. (7)
observations indicate one challenging
area in which further refinements of where a0 and a are the initial and the
plasticity analyses are needed. adjusted crack half-lengths and rr is
It should be noted that other shapes as defined by Eq 4.
have been postulated for the shape of the The net effect of this adjustment pro-
plastic zone. Dugdale's model (~) for cedure is to increase the calculated
example, assumes a thin zone extending fracture-toughness value for a given
directly ahead of the notch. He notes test. Although empirical in nature, the
that this occurs when the slit length is procedure does adjust the fracture-
small in relation to the width in a center- toughness values in the direction of
slotted plate specimen. This suggests trends observed experimentally. When a
that the plastic deformation behavior series of increasingly larger specimens is
near a crack can be influenced by speci- tested, the uncorrected fracture-tough-
men dimensions and boundary condition, ness values tend to be low for small
and that analysis only in terms of local specimen sizes and to increase toward an
conditions (as in elasticity analysis) may asymptotic value for larger sizes. Based
be inadequate. on present concepts of fracture me-
A very important question concerns chanics, the toughness values for large
the effect of plane-stress versus plane- specimen sizes are more truly representa-
strain conditions on the shape and extent tive of actual material behavior. For
of the plastic zone. The details of this the larger sizes, the plastic-zone size
question will be covered by others in this tends to become smaller, both absolutely
symposium. Qualitatively, there is good and relatively, with respect to over-all
basis for expecting that the deformation specimen dimensions. Thus, a procedure
zone will be smaller and more constricted which has the effect of increasing the
directly ahead of the notch in plane fracture-toughness values to adjust or
strain than in plane stress. Nearly all correct for plasticity effects seems
experimental studies have been limited intuitively and empirically proper.
to specimen-surface observations where In using this present form of the
plane-stress conditions exist. Ingenious plasticity-correction procedure, one must
experimental techniques are needed to recognize its approximate nature and
provide more information on plane-strain limitations. For example, the procedure
deformation behavior. A related ques- isnot intended to handle situations where
tion concerns the abruptness of change general yielding precedes the fracture.
in plastic behavior between plane stress For this reason, the recommended pro-
and plane strain. Figure 7 shows Liu's cedurcs for sharp crack fracture testing
(W) schematic visualization of this include definite limitations on the ratios
change across the specimen thickness, of fracture stress to yield strength
but virtually nothing is known about necessary to obtain meaningful values of
the specific details of this problem. Kc and K~c in various specimen con-
With this background, current usage figurations (78).
of plasticity analysis in fracture me- It should also be recognized that the
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W E I S S A N D Y U K A W A ON CRrrzcAL APPRAISAL OF FRAcTuP~ MECHAmCS 15

present plasticity correction was not sions, the present procedures of fracture
intended to account for the notch- mechanics are adequately applicable
blunting effect which can become a currently, the future extensions of
factor with extensive plastic deformation. fracture mechanics will be largely de-
This refers to the change in the geometri- termined by the progress made in charac-
cal shape of the crack tip. Based on the terizing the plasticity effects as affected
earlier discussion of the notch-radius by plane-stress and plane-strain con-
effect, such blunting could have the ditions, by the material deformation

I$1LE DATA D,TA


200
SERIES A SERIES A

R
0
0 %r-"-g---o "~ -'] r-------- t
oi tOO
-.r
BO
to
Z SERIES B SERIES g

~100 ~"g-~-~'-'g.- ~-.-- .--u..


80
SERIES C SERIES C

I O0 c~'n'-'~
-~ e0
0
o 60
o
~: o ULTIMATETENSILE STRENGTH 0.1 0.2 0.4 0.6 0.8 1.0 2.0
b- NET THICKNESS, IN.
to ~TRUE FRACTURE STRESS
z ._~___~
~loo~ ~ o -A
~80 "g---" ~ g --g--

Ol 0.2 0.4 0.6 08 1.0


NOTGHDIAMETER,IN.

Series A: Constant stress-concentration factor, Kt = 6, constant stress gradient, p = 0.004 in.


Series B: Constant stress-concentration factor, K t = 6, constant percentage of notch depth (50
per cent for tensile data, 30 per cent for bend data)
Series C: Constant root radius, p ~ 0.001, constant notch depth (50 per cent, 30 per cent)
FIG. 8--Effect of Section Size on the Tensile, Notch-Tensile, Bend, and Notch-Bend Strength
of 7075-T6 Aluminum.

effect of increasing the resistance to behavior, and by changes in specimen


initiation if it were the sole factor con- geometry and loading conditions.
sidered. However, at this point, signifi-
INHOMOGENEITIES, SCATTER, AND
cant redistribution of the stresses and
strains has occurred and must be taken SIZE EFFECTS
into account. One of the most important and useful
In the strictest sense, localized plastic features of fracture mechanics is the
deformation cannot be eliminated in prediction of a geometric section-size
fracture tests of structural alloys of effect on strength. This prediction "al-
engineering interest. However, there is lows" the designer to estimate the frac-
ample evidence that if plastic deforma- ture strength of a large part on the basis
tion is restricted to a region small in of laboratory tests obtained on small
comparison with test-specimen dimen- specimens. Such a design concept takes
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16 Fl~Cr~ TOUGH~mSS TESTING

TENSILE DATA BEND DATA


"1000
SE.,ES s SER,ES s o
800

~ 600
o

1-

2OO
40O

R
0
0
_o
~zoo
(.9

m I00

2 ~, , . . . . . 0~ .4 0. . 9 , , . I . .

NOTCH DIAMETER,IN~ NET THICKNESS, IN.

Series S: Smooth specimens


Series A: Kt = 6, percentage notch depth = 50 per cent for tensile, 30 per cent for bend
Series C: Constant root radius, p ~ 0.001, constant percentage of notch depth, 50 per cent and
30 per cent
F I O . 9---Effcct of Section Size on the Tensile, Bend, Notch-Tensile, and Notch-Bend Strength
of H-11 Steel.

the form, K~ = constant, or, for the K~ = r tan ( ~ a / W ) l l t 2 = c o n s t a n t .... (8)


specific case of a finite specimen If the crack length increases in propor-
(width = W) with a center crack (length, tion to W, then a/W = constant, and
2a): the relationship, #o (W)" s = constant, is

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WEiss AND YUKAWAON CP~TtCALAPPRAISALOY FP.ACTUP~MECHAmCS 17

obtained. Since these considerations are of a superposition of the statistical size


entirely elastic and, therefore, represent effect, expressed in Eq 9, and the geo-
the most severe case (namely, totally metrical size effect, predicted by fracture
brittle fracture), one may consider the mechanics as Kc = constant, for the case
relationship, K c - - constant, a safe of relatively brittle inhomogeneous ma-
design criterion--as is, indeed, the case terials. This has, indeed, been observed
for the 7075-T6 aluminum alloy data in sharp notch tension and bend tests on
shown in Fig. 8 (79). In this case, of H-11 steel, as shown in Fig. 9 for both
course, the material is not truly brittle tension and bend tests on specimens
and any in_homogeneities present will be having a notch-root radius, r =< 0.001
homogenized by plastic flow. In such a in. The slope of the log an versus log
material, the tensile strength will be in- size curve exceeds --3. The existence
dependent of section size, provided that of these inhomogeneities is further
very small samples (wire, etc.) and manifested by the unusual scatter of the
metallurgical variations are excluded. test results which is in agreement with
Weibull Os) has shown, however, that Weibull's predictions. However, tension
tests on smooth specimens over the same
section-size ranges did not show a notice-
C) C) C) able size effect.
In order to resolve this question and
get a better insight into the physical
meaning of Weibull's m value, Weiss
and Schaeffer ('/9) have proposed a
simplified model of an inhomogeneous
j (2) (2) C)
material containing an elliptical hole, as
shown in Fig. 10. The inhomogeneities
Fro. lO--"Model" of an InhomogeneousMa-
terial ContainingFlaws in UniformSpacing. are spaced a distance b apart and are
characterized by a stress-concentration
a section-size effect exists in inhomo- factor, Kb. The average net-section
geneous smooth specimens which may be strength of such a model is given by:
expressed as (1 + 4 b / p ) 8/2 - - 1
~N = X q~, ~ i o . . (10)
~2/~, ffi (V,/VO -11m. . . . . . . . . . (9) 6b/p

where a is the fracture strength of a where p is the root radius of the elliptical
specimen having a test volume, V , and hole, and oN. mi, is the minimum net-
m is Weibull's statistical exponent. Thus, section strength which is obtained from
a large size effect is predicted for low m a model where the stress-intensifying
values (inhomogeneous materials), while inhomogeneity is located at the root of
none is predicted for m -- oo (homo- the /taw. Accordingly, a size effect is
geneous materials). Unfortunately, the predicted for such a material if the test
physical meaning of m is not clearly specimens are geometrically similar, that
established, other than that a high m is, having a constant geometrical stress-
value indicates many small inhomoge- concentration factor; none is expected in
neities and a low m value indicates few sharp crack specimens since, in them,
larger ones. p = constant. Thus, the sharp crack
From these considerations (which fracture mechanics approach takes care
have also been verified for ceramics of two dimensions with regard to the
(73,so)), one may suspect the possibility volumetric size effect, x and y in Fig. 3
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18 F ~ c ~ m ~ TouGm~ss TESTn~o

but not of the third, that is, the crack- lem of inhomogeneity effects, especially
front length. As the size increases, this with respect to the applicability of
length and, therefore, the volume sub- fracture mechanics to ceramics, a knowl-
jected to a critical stress also increase; edge of the experimental scatter may
hence, the chance of finding an in- indicate whether such a problem may
homogeneity closer to the crack tip or of develop.
finding a more severe inhomogeneity
OUTLOOK
(increased Kb or decreased aN. rain) in-
creases, and thus the strength decreases. There are many aspects of the failure
The experimental scatter reflects the of solids to which the sharp crack frac-
degree of inhomogeneity and it is evident ture mechanics analysis has been success-
that it should depend on the volume fully applied. Among these are the
subjected to a high stress, as is indeed already mentioned embrittlement by
observed on comparing the notch and liquid metals (49) and delayed failures
smooth H-11 data of Fig. 9. such as hydrogen embrittlement and
From the model of Fig. 10, one obtains stress-corrosion cracking (81,82). Such
an expression for the net-section strength analysis has also served to explain
as a function of the root radius and the failures in nonmetals such as glass,
distance ~ between notch root and Plexiglas, and ceramics (1,79,83), and
nearest inhomogeneity in the strength of adhesive joints (84).
A particularly interesting application
O'N ~ ~N, min[~j0 ~- 4 ~ ) / p ] ll'j . . . . . . (11)
concerns an analysis of crack propagation
which reduces to eN, rain as p --* oo, that under alternating loads. As the stress
is, for smooth specimens. It can be distribution in the vicinity of a sharp
shown that the scatter likewise depends crack is uniquely defined by the stress-
only on b/p and either vanishes for intensity factor, K, and the stress at a
smooth specimens or reduces to the finite distance from the crack tip is
scatter of ~N, mi, 9 proportional to K, one may expect the
A direct application of the Weibull crack-growth rate in fatigue to be
analysis as above leads to the following related to the stress-intensity factor.
results. If there exists a relationship From dimensional analysis considera-
between m and the standard deviation tions, Liu (~) postulates
as Weibull indicates, then the "ap-
da
parent" value of m is not a material --
4N ~ K ~ ............. (12)
constant but depends on the "critically
stressed volume." It will decrease with while Paris (86) finds better agreement
increasing notch sharpness. Conse- with experimental results for
quently, the statistical size effect ac-
cording to Eq 9 will also increase with da
~ K' ............. (13)
increasing notch sharpness. The im- dN
portance of these considerations lies in
the fact that because of the possibility of Other researchers (~/,ss) obtain different
superposition of statistical and geo- values of the exponent.
metric size effect, the use of the relation- While a good fit of a great variety of
ship, K~ = constant, may not be con- experimental data is indeed observed
servative for very large cracks in large with Eq 13 (proposed by Paris), no
components. While more research is satisfactory physical model can be postu-
required in this area to clarify the prob- lated for this case. The dimensional

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WEiss AND YIIKAWA ON CRITICAL APPRAISAL O1~ FRACTURE MECHANICS i9

model for E q 12 is quite satisfying and alternating stresses or strains. The


Liu (89) has pointed out that thickness above analysis is in agreement with
effects m a y be expected to influence Liu's (88) formulation of the fatigue-
the crack-growth rate and change the crack growth problem insofar as crack
exponent. length is concerned; however, it disagrees
An estimate of fatigue-crack growth with the theoretical results of both
in technical materials following a stress- Paris and Liu insofar as whether the
strain relationship of the type a = stress or strain amplitude dependence
Ke" has been proposed by Weiss and should enter the fatigue-crack growth
Sessler (92). With the help of Neuber's law under some exponent which is
plasticity analysis for cracks (33) they related to the strain-hardening exponent.
obtain Insufficient experimental evidence is
available to check the validity of these
da = a f\ :~/ , + l / , . . . . . . . . . (14)
d--N relationships. A more exhaustive plas-
ticity treatment was given by Mc-
for stress-controlled fracture or Clintock (93) in 1962. In view of the fact
that an incremental fatigue-crack growth
-- cc a . . . . . . . . . . (15) is of the order of magnitude of the plastic-
dN zone size, a strict elastic fracture me-
for strain-controlled fracture. Here a* chanics analysis of the problem m a y
and e* are the stress or straifi values not be as applicable as an analysis
causing fracture, and a and e are the which incorporates plasticity effects.

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20 Fr.AcTtrRE T o u o m q x s s TESTINO

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WEISS AND YUKAWA ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 21

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22 FRACTURE TOUOHN~SS TESTING

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(79) V. Weiss and G. Sehaeffer, "Effect of Titanium Alloy at Room and Low Tem-
Section Size on Notch Strength," MET.E. peratures," ASTM STP No. 302, Am.
1078-1064-FR, Syracuse University, Octo- Soc. Testing Mats., 1962, p. 213.
ber, 1964. (92) V. Weiss and J. G. Sessler, "Strain Con-
(80) L M. Daniel and N. A. Well, "The In- trolled Fatigue in Pressure Vessel Ma-
fluence of Stress Gradient upon Fracture terials," Paper No. 63-WA-226, Am. Soc.
of Brittle Materials," Paper No. 63-WA. Mechanical Engrs., 1963.
228, Am. Soc. Mechanical Engrs., 1963. (93) F. A. McClintock, "On the Plasticity of
(81) E. A. Steigerwals, "Delayed Failure of the Growth of Fatigue Cracks," in Fracture
High-Strength Steels in Aqueous Environ- in Solids, Proceedings of AIME Metal-
ments," Proceedings, Am. Soc. Testing lurgical Society Conferences, Maple Val-
Mats., Vol. 60, 1960, p. 750. ley, Washington, Interseience Publishers,
(82) E. A. Steigerwals and C. J. Guarnieri, New York and London, Vol. 20, 1962, pp.
"Influence of Surface Oxidation en the 66-102.

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STP381-EB/Apr. 1965

DISCUSSION
H. W. Live--Fracture mechanics en- zone exists near the crack tip. It is not
compasses an enormous body of knowl- the elastic stresses and the elastic strains
edge, which includes fundamental theo- outside the plastic region that cause
ies as well as practical experiments. It fracture. Rather, fracture results from
includes both the macroscopic phenom- the stresses and strains within the plastic
enological work as well as the micro- zone. The elastic stresses are only a
scopic mechanistic investigations. For measure or an indicator of the stresses
their excellent appraisal, the authors and strains within the plastic zone. The
should be complimented. elastic stresses given by Eq 3 are ap-
In this discussion, it is not intended proximate solutions, which are valid
to provide any new solution to fracture only in a region near the crack tip. The
mechanics. It is rather intended to offer solid lines in Fig. l l show the exact
additional insight into the theoretical e, and e~ in a cracked infinite plate
bases and the accepted practices in along x-axis given by Inglis.3 The dashed
experimental investigations. With this line is the approximate solution given
understanding the direction of future by Eq 3. As the distance from the crack
research is clearly indicated. tip approaches zero, the approximate
The concept of fracture toughness, solution approaches the exact solution.
~c, can be derived from energy balance~ If the applied stresses in two specimens
as well as from the concept of stress and are 01 and 02 and the crack lengths are
strain environments at the crack tip. bl and b2, respectively, and furthermore,
The energy approach is well known and for these two specimens, K1 = K s ,
further elaboration is not necessary. according to Eq 3, the elastic stresses in
An attempt will be made to bring for- these two specimens are identical. Figure
ward the understanding of fracture 12 shows the ratio of ~1 to e~ along the
mechanics from the concept of stress x-axis for different ratios of b~/b2. These
and strain environments. As noted in curves were calculated from Inglis's
the appraisal, the stress-intensity factor, exact solution. The figure indicates that
K, completely specifies the elastic stresses near the crack tip the stresses are nearly
and strains in a region adjacent to the equal to each other for various crack
crack tip. It is well known that a plastic lengths. However, away from the crack
1 Associate professor of metallurgy, Syracuse
tip, the stresses differ considerably even
University, Syracuse. N. Y. if K's are all the same. Therefore, it can
2 A. A. Griffith, "The Phenomena of Rupture be concluded that regions exist within
and Flow in Solids," Philosophical Transactions,
Royal Society (London), Series A, Vol. 221, which the stresses are approximately
1921. the same, if K's are the same. Let this
G. R. Irwin, "Fracture Mechanics, Struc- region be prescribed by r' as shown in
tural Mechanics," Proceedinos, First Sym-
posium on Naval Structural Mechanics, Perga Fig. 13. If the plastic zone, r~, is very
mon Press, 1960.
If. W. Liu, "Fracture Criterion of Cracked s E. E. Inglis, "Stresses in a Plate Due to
Metallic Plate," GALCIT S M 63~9, Graduate the Presence of Cracks and Sharp Corners,"
Aeronautical Labs, California Institute of Transactions, Institution of Naval Architects
Technology. July, 1963. (London), Vol. 60, 19!3, p. 219.
23
Copyright9 1965by ASTM International www.astm.org
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24 FRACTtrRE Touom,mss TESTING

J small, that is, r, ~ r', the relaxation of


stresses within the plastic region from
that given by elastic solution will not
change the stresses on r' significantly.
Look at two regions bounded by rl' and
r2' in two specimens. For these two
specimens, r l ' = r2' and K1 = K2.
Therefore, if the plastic zones are very

2.o\ 1 small, the stresses on rl' and r2' are


approximately the same. These two re-
gions, bounded by n ' and r2', are geo-
metrically identical and the applied
b"llb~ X ~ "~(Y:0)Inglis Solulion stresses on the boundary are the same.
b'ib" i .
\\\ ~ ~ 1 Therefore, the stresses and strains at
geometrically similar points, even within
the plastic zone, are identical. Conse-
,.c --'~Z."~ g e~T

i Lly=O) Ingli$Solution

0.2 Q4 r 0.6 0.8 1.0


b
Fig. 11

1.24 bz=IObv-~
Fig. 13
brsb, ///
1'20i bz=6bl- - " 7 ~ quently, if one specimen fails at a stress
and strain environment, so will the o t h e r
at the same stress and strain environ-
ment. Therefore, it can be concluded
that K , for fracture is a constant; and
r~ << r' is a sufficient condition for a
constant K , . Small r~ implies low frac-
ture stress and brittle mode of fracture.
If rp is not small in comparison with

1.04
,y r', the relaxation of the stresses in the
plastic zone will change the stresses on
r' significantly, so that the stress field
of one crack tip interacts with the stress
field of the other crack tip. For different
crack lengths, the interaction is different.
I'OOF ~l O.'Z
r
05 0,~'=1 Therefore, the stresses o a r ' are no longer
characterized by K. Hence Kc is no
Fig. 12 longer constant.

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DISCUSSION ON CRITICAL APPRAISAL 0~" FRACTURE MECHANICS 25

For a large plastic zone, in order to calculate K,I, is the sum of the actual
keep the condition of rp << r', the size crack length plus the plastic-zone size,
of r ~has to be enlarged. If r' is enlarged, r~. The correction factor, r~, is more or
Eq 3 will no longer give the correct less a constant. Therefore, for long
stresses on r'. Figure 12 indicates that, cracks, that is, 2b >> rp, the effect of the
in this case, *vl along the x-axis within correction factor, rp, is insignificant.
the region rl ~ is higher than ,v~ within On the other hand, for short cracks, the
the region r2~. In order to give the same size of rp relative to b increases; there-

Frocture Yield
Stress .Stress
ksi ksi
/
0 52.7 230 /
V 53.3 230 /
A 50.8 250
1.4 - 9 534 230 - - - /2x
[] 53. I 230
9 74.5 205
9 65.4 205
9 62.9 210
O 65.1 210
,c
c~
c
=,L:
u
o
oA /
| A oID~ /
0 [[]
1.2 9 " .0,~0 0
| 6rn
| V V
~x 9 /I
AA /
/
/ /
I-ill 4 1.5 1.6 1.7 1.8 L9 2.0
Onet
%

Fig. 14

stress environment within rl ~ and r, ~, fore, it increases the value of K~ con-


the applied stress on Specimen 2 has to siderably.
be raised, or vice versa. Consequently, The crack length is usually determined
K~I < K,2, that is, K 9 decreases with by either ink stain or visual observation
crack length. In this case, in order to of the "last unstable crack." This
maintain a constant K , , an empirical peculiar way of determining the crack
correction factor is needed. This cor- length is another empirical correction
rection factor must be characterized by factor. Figure 14 shows slow crack growth
a small K , increase for a long crack, and of centrally cracked 3-in. wide plates.
a considerable Kc increase for a short The original fatigue cracks in the plate
crack. Irwin's plastic-zone correction are 1 in. long. al is the gross sectional
factor satisfies these requirements. The fracture stress. As the load increases,
effective crack length, which is used to the crack grows slowly. The solid line

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26 FRACTURZ Touomc~ss TEsTr~O

is the crack-growth line under the con- length" serves as another correction
stant fracture load. The dashed line is factor, with the similar characteristics
the crack-growth line at 98 per cent of of r r , in order to give constant K~.
the fracture load. It is obvious that the These corrective measures are needed
crack growth at late stage is very un- if the size of the plastic zone is large,
stable. The cracks grow with very little that is, for ductile fractures. They are
increase in load. For all practical pur- needed because of our meager knowledge
poses, the crack becomes very unstable with respect to stresses and strains within
at the length of 1.3 in., but the values the plastic zone. It has been noted that
used in calculating K~ are often 1.5 in the stresses and strains within plastic

jJ
zones depend upon the plastic behaviors
of the materials such as strain-hardening
6 R8
exponent, etc) Therefore it is uncertain
that these two corrective measures can
ic

4--
take care of both the plastic-zone size
ILfZ" effect and the material effect. Conse-
quently, this leads to the conclusion that
2
'I ,I
) ,o,,9o
an understanding of stresses and strains
-~ 49,500 psi within plastic zones is the next logical
psl
step for further advances in fracture
mechanics.
RIO This discussion is a portion of Ref
06
;> (3) and (7), which were written while the
1.67" author was at the Graduate Aeronautical
F I.~4 Laboratories of the California Institute
1.41" of Technology. The experimental work
J 1-
was conducted at the H. F. Moore
52,500 psi "] I 5~,,TbOpsi" Fracture Research Laboratory at the
I 2o.o ] University of Illinois. The assistance
extended to the author by these two
Time-sec.
institutions is gratefully acknowledged.
Fig. 15 A. KENT SHo]~ArJm?--One of the
questions frequently raised in this paper
or longer, if the last unstable crack was the effect of the notch-root radius
length is used. on the crack toughness of a laboratory
Figure 15 shows the slow crack growth specimen. Although some work has
of the same type of specimens of Fig. been reported for high-strength steels
14, as measured by voltage output. ~
Figure 15 also indicates the instability of 5 William W. Gerberich, "Plastic Strains and
the crack growth at late stage. The Energy Density in Cracked Plates. I. Experi-
"last unstable crack" is 1.64 and 1.67 mental Techniques and Results," G A L C I T
Shf 65-~$, Graduate Aeronautical Labs., Cali-
in. long in comparison with the original fornia Institute of Technology, June, 1963.
1-in. fatigue crack. The extra "added H. W . Liu, "Qualitative Discussion on the
Ei~ects of Strains Within Plastic Enclave on
H. W. Liu, "Effect of Water on the Fracture Fracture Criterion," G A L C I T ,SM 6~-3~,
Strength of Specimens with a Central Notch," Graduate Aeronautical Labs., California Insti-
NRL Project 62R19-05, ~l'echn~cal Memorandum tute ol Technology, September, 1963.
No. I~3, U. S. Naval Research Labs., August, s Department of Theoretical and Applied
1960, Mechanics, University of Illinois,Urbana, Ill.

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DISCUSSION ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 27

by the ASTM committee reports/there ture for ~-in. thick A-201 mild steel g
are very few data available for mild or using a single-edge-notched specimev.
"low-strength" steels which are tempera- shown in Fig. 16. It was thought that
ture- and rate-sensitive. 8 The purpose of the notch radius may have been too
this discussion is to present some of these large to obtain minimum values of K*~,.
data for mild steel. Subsequent experiments were made on
specimens with notch radii varying
from 0.0005 to 0.010 in. with essentially
72 constant initial crack lengths and speci-
M
men geometry. Since no slow crack
growth was observed in mild steel, the
maximum load coincided with fracture
initiation. These results for three differ-
ent combinations of temperature and
loading rate are shown in Fig. 17 in
i terms of the fracture load and the square
root of the notch radii.
The notch radii of 0.0005, 0.001,
0.002, and 0.003 in. were fabricated by
the use of a "string saw." A diamond
abrasive compound was spread along
U the notch base and tungsten wires of
the dimensions mentioned above were
.
pulled back and forth across the notch

[
-
base to make the desired radius. This
sawing increased the crack length by an
amount equivalent to three to four notch
radii. The notch radii are quoted ac-
cording to the radius of the wire used

5.00" ~lq" to cut them. The 0.005 and 0.010-in.

_[
radii were machined with a preshaped
lathe tool mounted in a horizontal mill-
ing machine used in a fly-cutting manner.
The results, as shown in Fig. 17,
indicated that at the low temperature,
- 2 7 0 F, the fracture load was approxi-
Fig. 16
mately independent of the notch radius,
while at - 1 7 5 F the fracture load in-
In previous work, initial crack-ex- creased with increasing notch radius.
tension (K'I,) values were measured as There is enough scatter in the data,
a function of straining rate and tempera- however, particularly at the lowest
7 Fifth Report of the Special A S T M Com- temperature and smallest notch radii,
mittee, "Progress in Measuring Fracture Tough-
ness and Using Fracture Mechanics," Materials
Research dc Standards, Vol. 4, No. 3, March, 0 A. K. Shoemaker, "The Influence of T e m -
1964, pp. 107-119. perature and Strain Rate on Crack Toughness
8 M. J. Manjoine, "Biaxial Brittle Fracture of Mild Steel," TdcAM Report No. 235, Uni-
Tests," A S M E Paper No. 8S-Met-3, Am. Soc. versity of Illinois, Urbana, Ill., November,
Mechanical Engrs., 1964. 1962.

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28 FRACTURE TOUGHNESS TESTING

to suggest a possible deviation from a pendent upon a constant plastic-zone


straight-line relationship. size necessary to form a microcrack.
The trends can perhaps be explained This very low-temperature cleavage
by previous workI~ where it was found fracture which initiated from the first
that for temperatures just below the formed microcracks would also indicate
transition range, equivalent to the the possibility of greater data scatter at
- 1 7 5 F data, fracture occurred after these temperatures; since the plastically
large numbers of microcracks had formed deformed zone of material is very small,
in the yielded zone at the crack tip. there is less probability of a random

70
6
Load Rate Temp.
60 -- 0 . . . . 6,020 Ibs./see. -270 ~
I-I . . . . 6,020 Ibs./sec. -175eF I ""El
f
&---12,200 Ibs./sec. -270 ~ f

50-t Indicates Na Fracture


I

"o
- 40-
"0
0
0
Two Points Each
.,J
50- A

1
0---- o 0
20--

IO I I I I I I I I
0.01 0.02 0.0:5 0.04 0.05 0.06 0.07 0.08 0.09 0.10
I
-/Notch Radius, in. z
Fig. 17

However, at still lower temperatures, microcrack starting and growing in this


equivalent to t h e - 2 7 0 F data, few smaller zone compared with a larger zone
microcracks were found near the frac- which occurs at a higher temperature.
ture initiation, thus indicating that This is further exemplified by the two
cleavage fracture occurred from the specimens which did not fracture at the
first microcracks formed. Thus the very low temperature.
independence of the fracture load with The specimen which did not fracture
notch radius at --270 F is perhaps de- at --175 F had not been cut by the
z0 G. T. Hahn, W. S. Owen, B. L. Averbaeh, String saw in the central section of the
and M. Cohen, "Mieromechanism of Brittle notch base. Thus the notch radius at
Fracture in a Low-Carbon Steel," Welding the center section was somewhat in
Journal (Research Supplement), Vol XXIV,
No. 9, September, 1959, p. 367-s. excess of 0.020 in.

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DISCUSSION ON CRITICAL APPRAISAL OF FRACTURE MECHANICS 29

The data presented above are offered of a better understanding of plasticity


only as a preliminary study of the notch- phenomena in the immediate vicinity of a
sharpness effect on initial crack exten- stress raiser such as a notch or a crack.
sion values for mild steel. The specimen The data of Fig. 14, which show stable
configuration used did not lend itself slow crack growth with increasing gross-
to the fabrication of a natural crack so section stress (load) clearly indicate the
these data do not appear in Fig. 17. At importance of a better understanding of
the very low temperature, the possibility the crack length-plastic zone size rela-
of a slight increase in fracture load as a tionship for finite thickness and finite
natural crack tip is approached could width specimens, and the complexity of
be construed from the data. However, the onset of crack instability in semi-
these data as well as the mechanism of brittle materials.
fracture which cause them are far from The microcrack explanation of the
conclusive and warrant further attention. data in Fig. 17, as well as stress-state
It does appear that even though crack considerations, are probably applicable.
blunting occurs at the higher test tem- The latter would suggest a varying stress
perature, a notch radius of not more than biaxiality with varying root radius cor-
0.0005 to 0.001 in. is necessary to ap- responding to the ratio of thickness to
proach minimum initial crack extension root radius. The plastic-zone size ahead
values for mild steel. of the notch is then determined not
V. WEISS AND S. YVKAWA (authors).-- only by the value of the root radius but
The authors are grateful for the contri- also by the corresponding stress state,
butions of Prof. Liu and Mr. Shoemaker that is, it would decrease on going from
which serve to emphasize the importance plane stress to plane strain.

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STRESS ANALYSIS OF CRACKS
BY PAUL C. PARIS I A N D GEORGE C. Sra I

SYNOPSIS

A general survey of the results of elastic stress analyses of cracked bodie


is the basic objective of this work. The stress-intensity-factor method ors
representing results is stressed and compared with other similar methods. All
three modes of crack-surface displacements are considered, as well as special-
ized results applicable to plate and shell bending. Results for various media
(for example, anisotropic, viscoelastic, or nonhomogeneous) are contrasted
with the analysis of homogeneous isotropic media. The accuracy of the repre-
sentation of the crack-tip stress fields by stress-intensity factor methods is
discussed, pointing out some limitations of applicability. Methods of estimat-
ing and approximate analysis /or stress-intensity factors in complicated
practical circumstances are also discussed.

The redistribution of stresses in within them and other requirements of


bodies caused by the introduction of a formulation of a complete theory o[
crack is one of the essential features fracture behavior.
which should be incorporated into an In his now famous paper, Griflith (1)2
analysis of strength of structures with made use of the stress solution provided
flaws. Moreover, the high elevation of by Inglis (2) for a flat plate under uniform
stresses near the tip of a crack should tension with an elliptical hole which
receive the utmost attention, since it is could be degenerated into a crack. How-
at that point that additional growth of ever, neither Griffith nor his predecessors
the crack takes place. As a consequence, had the knowledge of stress fields near
it is the purpose of this paper to present cracks which is now available, so as a
a summary of current knowledge of consequence, he devised an energy-rate
crack-tip stress fields and of the means analysis of equilibrium of cracks in
of determination of the intensity of those brittle materials. Sneddon (3) was the
fields. first to give stress-field expansions for
Small amounts of plasticity and other crack tips for two individual examples;
nonlinear effects may be viewed as however, it was only later that Irwin
taking place well within the crack-tip (4,5) and Williams (5) recognized the
stress field and hence may be neglected general applicability of these field
in this presentation of the gross features equations and extended them to the
of those fields. It is the subject of other most general case for an isotropic elastic
discussions to assess the effects caused body (5). It is this analysis to which
by the fields, for example, the plasticity initial attention shall be given.
I Aasociate professor of mechanics, Lehigh s The boldface numbers in parentheses refer
University, Bethlehem, Pa. to the listof references al~imnded to this paper.
30
Copyright9 1965 by ASTM International www.astm.org
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PARIS AND SIH ON STESS ANALYSIS OF CRACKS 31

Y Y
Y

FIG. 1--The Basic Modes of Crack Surface Displacements.

~z

/
f
J

leoding edge
of lhe crock

FIG. 2--Coordinates Measured from the Leading Edge of a Crack and the Stress Components
in the Crack Tip Stress Field.

CRACK-TIP STRESS FIELDS FOR ISOTROPIC associated with a local mode of deforma-
ELASTIC BODIES tion as illustrated in Fig. I. The opening
mode, I, is associated with local dis-
The surfaces of a crack, since they are
placement in which the crack surfaces
stress-free boundaries of the body near
move directly apart (symmetric with
the crack tip, are the dominating in- respect to the z-y and x-z planes). The
fluence on the distributions of stresses edge-sliding mode, If, is characterized
in that vicinity. Other remote bound- by displacements in which the crack
aries and loading forces affect only the surfaces slide over one another perpen-
intensity of the local stress field. dicular to the leading edge of the crack
The stress fields near crack tips can (symmetric with respect to the x-y plane
be divided into three basic types, each and skew-symmetric with respect to the

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32 FRACZ~rR~ TOUGHNESS TESTING

x-z plane). Mode III, tearing, finds the Mode II:


crack surfaces sliding with respect to
Kxl 0 [" 0 30-]
one another parallel to the leading ~r= = ~ s i n - 1 2 + c o s ~ cos - - /
edge (skew-symmetric with respect to (z,~,)',* 2L 2 2J
the x - y and x - z planes)9 The superposi- Kn 0 0 30
sin cos cos
tion of these three modes is sufficient to =

describe the most general case of crack-


tip deformation and stress fields. r=, (2rr)V2cos ~ 1 -- sin sin
The most direct approach to deter-
mination of the stress and displacement ~, = v(~= + ~.), * , , = *~, = 0
fields associated with each mode follows
in the manner of Irwin (4,7), based on KII [r/(2r)]ln sin O 9 .(2
the method of Westergaard (8). Modes I
and II can be analyzed as plane-exten-
sional problems of the theory of elas-
ticity which are subdivided as symmetric
and skew-symmetric, respectively, with KII {
v = ~ - 1,/(2=)1~' cos
respect to the crack plane. Mode III
can be regarded as the pure shear (or
torsion) problem. Referring to Fig. 2
for notation, the resulting stress and
displacement fields are given below (a w=0
full derivation is found in Appendix I). Mode III:
Mode I :a Km . 8
"= = (2,,-,')'~ s m

~r x ~
KI 0 [-
(21rr)a/* cos 2L' -- sin
0
,,n;]' Km
~" --- (2~),n cos
#

KI cos~ [ l + s i n }o .... (3)

KI 0 0
cos
30 w K~x [(2r)/~l,/2 sin
Txl t ~ - -

u v----0
~(~= + ,r~), ,-., = *~, = 0
Equations 1 and 2 have been written
U----- K_.~[r/(2r)l,n cos _0 ..0) for the case of plane strain (that is,
G 2
w = 0) but can be changed to plane
stress easily by taking #, = 0 and re-
placing Poisson's ratio, ~, in the dis-
Kt 0
placement~ with an appropriate value.
= ~ [r/(2r)]l/~ sin - Equations 1, 2, and 3 have been obtained
G 2
by neglecting higher-order terms in r.
Hence, they can be regarded as a good
approximation in the region where r is
small compared to other planar (x-y
w=0
plane) dimensions of a body such as
a See Appendix III for explanation of mathe- crack length and exact in the limit as r
matical symbols. approaches zero.

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PARIS AND SIH ON STRESS ANALYSIS OF CRACKS 33

The parameters, Kx, K~I, and Kin force transmission through the crack tip
in the equations are stress-intensity region.
factors 4 for the corresponding three types
]~LEMENTARY DIMENSIONAL CONSIDERA-
of stress and displacement fields. It is
TIONS :FOR DETERMINATION OF
important to notice that the stress-
STRESS-INTENSITY FACTORS
intensity factors are not dependent on
the coordinates, r and 0; hence they An infinite plate subjected to uniform
control the intensity of the stress fields tensile stress, ~, into which a transverse
but not the distribution for each mode. crack of length, 2a, has been introduced,
From dimensional considerations of is shown in Fig. 3. As a two-dimensional
Eqs 1, 2, and 3, it can be observed that problem of theory of elasticity, only
two characteristic dimensions are pres-
O" ent, ~ and a. Moreover, this configura-

l 2"

2"

T
FIo. 4--An Infinite Cracked Sheet with Uni-
form In-Plane Shear at Infinity.

FIG. 3--An Infinite Cracked Sheet with Uni- tion is symmetric with respect to the
form Normal Stress at Infinity. crack plane; therefore, only the first-
mode fields are present. Then, simply
the stress-intensity factors must contain from dimensional consideration (9) with
the magnitude of loading forces linearly Eqs 1, the only possibility is:
for linear elastic bodies and must also
depend upon the configuration of the K~ = C,~a 112 }
(4)
body including the crack size. Conse- Ku Km= 0
quently, stress-intensity factors may be
physically interpreted as parameters Hence, observations of symmetry and
which reflect the redistribution of stress dimensional analysis can aid in the
in a body due to the introduction of a determination of stress-intensity factors.
crack, and in particular they indicate Though C1 is undetermined by such
the type (mode) and magnitude of considerations, later results will show it
4These stress-intensity factors differ by a
to be ~a[~, (see Eq 17). However, even
(actor of ~1/2 with earlier definitions of them. if C1 is left undetermined, the fracture-

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34 FRACTURE TOUGHNESS TESTING

size effect can be predicted for this Stress-intensity factors can be de-
configuration, since 5 as Kx ~ K~r then termined from the limiting values of
elastic stress-concentration factors (7)
~ral/2 = constant . . . . . . . . . . . (5)
as the root radius, p, of the notch ap-
By similar considerations of the plane- proaches zero. Consider a symmetrically
extensional problem of a plate under loaded notch whereupon the tip will be
shear, as shown in Fig. 4, the stress- embedded within a mode I stress field.
intensity factors are The maximum stress, go will occur
directly ahead of the notch. Again,
(6) dimensional considerations of Eqs 1
KI ~ K m ffi 0 J lead to

| | | | K, = C~o(p)~n. . . . . . . . . . . . (8)
In the limiting case, the notch approaches
a crack, as p --~ 0, or
7r
K I ffi lira -~- eop 1/~ . . . . . . . . . (9)
R-~0

The constant has been evaluated from


Eq 4 and the stress-concentration solu-
tion for an elliptical hole in the con-
figuration shown in Fig. 3, which is:
~o = ~[1 + 2 ( ~ / p ) , / , ] . . . . . . . . (10)

A multitude of stress-concentration
solutions available in the works of
Neuber (1o), Peterson (n), Savin (12),
@ @ Q @ Isida (13) and others can be used to
T determine stress-intensity factors for
Fro. S - - A n Infinite Body w i t h a " T u n n e l many configurations. Formulas cor-
Crack" Subjected to Out-of-Plane Shear at responding to Eq 9 can be as easily
Infinity. derived for modes II and III. They
appear in Appendix II.
Moreover, analogous results may be From the above dimensional considera-
obtained for the problem shown in Fig. tions, it is evident that the appearance
5, that is, an infinity body with shear of the 1/r in type of singularity in the
applied parallel to a tunnel crack of stress-field equations (Eqs 1, 2 and 3) is
width, 2a. They are: a controlling feature in fracture-size
K m -- r(,ra) In ] effects, the relationship of stress con-
centrations to stress intensity factors,
K1 ~:I, = oJ~. . . . . . . . . . . (7)
and, as will be noted later, extension of
Though these are relatively interesting fracture mechanics concepts to other
examples, more complicated configura- than isotropic, elastic media.
tions are of practical importance; con-
STRESS-INTENSITY FACTORS FROM
sequently, more powerful methods of
analysis will be cited. WESTERGAARD STRESS F~mCTIONS
5 K[--~ K I , , as a fracture criterion, is dis-
Several sources (4,5,'/,8) give Wester-
~ussed in m a n y other papers in this symposium. gaard stress functions, Z, for crack
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PARIS AND SIH ON STRESS ANALYSIS OF CRACKS 35

problems. A discussion of the analysis As an example, consider a plate with


of plane problems with this type of an infinite periodic array of cracks along
stress function is given in Appendix I. a line with uniform tension, a; the half
For each of the three modes of crack- period is b and the half-crack length, a,
tip stress fields the Westergaard stress as shown in Fig. 6. The stress function
function in the neighborhood of the for this configuration is (4):
crack tip takes the form
~rZ
cr sin - -
f(~) 2b
Z ~-1/~ ' i"-- re ~s .(11)
Z,--[(sin 7zz~'_2b](sin z'a~'l'/'
.J ' "
(16)2b,
where f(~') must be well behaved in that
vicinity in order to ensure stress-free In order to move the crack tip to the
crack surfaces. 6 Hence in the region close origin, substitute z = x + iy = a -4- ~"
to the crack tip, that is, I~" [ --* 0, it is and trigonometric identities. Eliminating

[J
T
4
b L
-]- "7-"
7-
O"

i--
Fro. 5 - - A Periodic Array of Cracks Along a Line in a Sheet with Uniform Stress at Infinity.

permissible to represent the stress func- terms of the order of i" compared to
tion as (5): terms of the order of a, the limiting
process in Eq 13 leads to:
f(o)
z [ m - 0 = -~-1/$
- . . . . . . . . . . (12)
KI ~ ~(ra) 11' ~a t a n ~ ] ..(17)
for mode I stress fields (see Appendix I). KxI = Km -- 0
Comparing ~u along the x-axis as com-
puted from Eq 12 and as given in Eq 1 Referring to Fig. 6, the indicated axes
leads to: of symmetry are lines devoid of shear
stress. Subtracting a uniform normal
Kz = lira (2ri')~nZi. . . . . . . . (13) stress, a, in the horizontal direction
I~'l-,0
leads to no change in Kx and leaves
In a similar fashion for the other modes: only small serf-equilibrating normal
KII = lim (2~r~)InZii ....... (14) stresses, a , , along these lines provided a
H'I~0 is small compared to b. Consequently,
K m = lim ( 2 7 r ~ ) l n Z m ....... (15) it is regarded as permissible to cut the
tl'l~0 sheet along these lines and to use Eq 17
s Simple poles away from the crack tip will as an approximate solution for finite
a p p e a r a t locations of concentrated forces. width strips with central cracks pro-
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36 FRACTURE TOUGHNESS TESTING

vided a is less than b/2. Results com- amples of stress-intensity factors from
puted for strips by Isida (13) and Ko- Westergaard stress functions, Eqs 17, 19
bayashi (14,15), which are accurate to and 20, lead to the results in earlier
much larger relative values of a, indicate examples, Eqs 4, 6, and 7, if b becomes
that this practice is sound (within 7 very large compared to a.
per cent) (see Table 1). Westergaard stress functions are avail-
Similarly, cutting the problem in able for many problems, and with some
Fig. 6 along the y-axis and similar lines experience it is easy to add solutions,
leads to an approximate solution, Eq 17, but there are limitations to the scope of
for double-edge-notched strips which is the method. The most serious drawback
acceptably accurate if a is greater than is that the method is normally restricted
b/2 (within 2 per cent) (see Table 3). to infinite plane (two-dimensional) bodies
Bowie (16) has calculated results for with cracks along a single straight line.
edge-notched strips which verify this Another more versatile approach to
accuracy. plane problems is available.
The configuration shown in Fig. 6
STRESS-INTENSITY FACTORS t'ROM
with the applied stress, ~, replaced by
G E N E R A L COMPLEX STRESS
in plane-shear stress, r, leads to:
FUNCTIONS
zcz
r sin -- A complex stress-function approach
2b
developed by Muskhelishvili (17) and
others has some advantages over the
Westergaard method by treating a
broader class of plane extensional
Making use of Eq 14 results in: problems.
An Airy stress function, ~, must
KII = r(ra) In ~-a tan 2b] ~ ..(19) satisfy the boundary conditions of a
problem and the biharmonic equation,
(KI = Km -- 0) J that is (see Appendix I),
In a like fashion, all results such as
Eqs 16 and 17 for symmetric problems, v,~ --- 0 . . . . . . . . . . . . . . (21)
mode I, are analogous to the correspond- The general solution to Eq 21 may be
ing mode II problem Eqs 18 and 19, expressed as (17)
obtained by rotation of boundary
= Re [~r -[- x(z)] . . . . . . . . (22)
forces or stresses through 90 deg in plane,
or both, when treating extension of From this form /or q,, the sum of the
infinite plates and certain other cases. normal stresses becomes
Moreover, for the corresponding mode
~ q- ~u --- 4 R e [~'(z)] . . . . . . . . (23)
III problem, with the stress, ~, replaced
by out-of-plane shear, r, for a body of Defining a complex stress-intensity
infinite extent in all directions, the stress factor (18) by
function is identical to Eq 18 and the K --- KI -- ~Kll . . . . . . . . . . (24)
stress-intensity factor is:

Km = r(,:a) v2 2__b tan


\~a
,)T(tij12}
~ .. (20)
Eqs 1, 2, and 24 may be combined to
give the same stress combination in the
vicinity of a crack tip. The result is
(KI = K u = 0)

It can be noted that the above ex- ~ . + ~. = ReL(T~.)., K 1 . . . . . (25)

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PARIS AND SIH ON STRESS ANALYSIS OF CRACKS 37

for a crack tip at z~ and for correspond- KI -- - -P (a+b]'/'


ing coordinate directions, that is, 2(,~a)'/' \U'L--- b l

~" = z - z~ . . . . . . . . . . . . . (26)

Substitution of Eq 26 into Eq 25 and


+ 2-Ci
9(32)
comparison of the result with Eq 23 --P ~-- 1
lead to KIt ----- - -

K = Kt - iKu = 2(2r)v2 lim


z~ z 1 + Q (o+q,,,
9(z - zl) v2 r (27)
The concentrated force results, Eqs
The function, ~(z), has been determined
32, provide the Green's functions to
for a large number of crack problems
(12,17-2o), since with this technique
conformal mapping of holes into cracks Y[ P F 4~ F
is permitted.
For a mapping function, z = w(~/), Eq
27 becomes l.o =!: o ,4

r ( z - prone) ('r/- plone)


K = 2 x/~= lim (w(~/) - w(~n))'f' w--~)'" (28)
~'~1
Fro. 7--A Concentrated Force (Per Unit
The mapping of a crack of length, 2a, Thickness) on the Surface of a Crack in an In-
finite Sheet.
into a circular hole of unit radius is
given by

z = w(n) = ~ ~/+
o(;) . . . . . . (29)

For this mapping, Eq 28 simplifies to


K = 20r/a)'/=!~'(1) . . . . . . . . . (30)

The example of a single concentrated


force, F (per unit thickness), on a crack
surface with arbitrary inclination, as
shown in Fig. 7, is solved by (17,18):
FIG. 8--A Curved Crack in an Infinite Sheet
Subjected to Uniform Biaxial Tension9
4,(7) = ~ ( a ~ ~ b~)~n ~

solve any single straight-crack problem


in an infinite plane from a knowledge of
the stresses on the prospective crack
surface with the crack absent, that is,
a~(x,O) and rxu(x,0). The solution is

where ~/o corresponds to z = b, F = 1 fa ./a+x\'n )


P - - i Q , and K is an elastic constant, Kx = ! ~,(x,0)/--/ ax/
(ra) ~/2 a-a \a - x/ ! .
which for plane strain is K = 3.4v.
1 ;a . . [a+x\] n |..(33)
~
Using Eq 30 with Eq 31, the stress- K. = -- / ,z,(x,o) 1 ~ ] dx/J
intensity factors are: (ra) 1/= a_= \a - - x~

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38 FRACTURE TOUOIINESS TESTING

In order further to illustrate the intensity factors in prismatic bars (with


versatility of the complex stress-func- prismatic cracks) subjected to torsion
tion method, the problem of a crack of and flexure (24-26). This type of con-
radius R, subtending an arc of angle, 2a, figuration leads to mode III stress-
symmetrically with respect to the x-axis
in an infinite sheet subjected to uniform O"
biaxial tension may be treated, see Fig. 8.
For this case, Muskhelishvili (17) gives
~,(R)1/2
r ffi

9 ~ - - COS

! - 2 ~ cos +

Relocation of a crack tip on the x-axis,


as required by Eq 27, may be accom- FIo. 9--A "Penny-Shaped" (Circular Disk)
plished by the substitution: Crack in an Infinite Body Subjected to Uniform
Tension.
ieia ( ~ - i - sin ~ cos a) (35)
R O"

whereupon Eqs 27, 34, and 35 give


~(TR) I/~ I
KI
(I-4-sin' ~)

. (sin a (1~- c~ a)) m

.(36)
~(TR)In
g l I -----

(1if-cos (~))I'~
FIG. 10---An Elliptical Crack in an Infinite
Other notable examples of stress-in- Body Subjected to Uniform Tension.
tensity factors for rather complicated
cases of plane extension have been intensity factors, some of which will
provided (18,21-23), using this and also be tabulated in Appendix II.
similar methods. The power of this
STRESS-INTENSITY FACTORS ~OR SOME
method for plane extension has been
sufficiently illustrated, consequently, ad- TroUPE-DImENSIONAL CASES
ditional examples will be removed to Using a method employing Fourier
Appendix II, transforms, Sneddon (3) treated the
A similar complex-variable approach case of a circular disk crack of radius, a,
has been developed to determine stress- in an infinite solid subjected to uniform

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PARIS AND Sm ON STRESS ANALYSIS OF CRACKS 39

tension, g, normal to the crack plane, see theless, the results which are presented
Fig. 9. His results for crack-tip stress form the basis for sensible judgments
field expansions lead to: from which three-dimensional effects
may be assessed.
2
K~ = ~ ~(~)~, . . . . . . . . . (37) Moreover, as a prime example of the
fact that three-dimensional effects are
(by symmetry Kit --- K I n = 0) always present and yet may most often
be justifiably neglected, consider sheet
The analysis of stresses near eUipsoidal of finite thickness with a through-crack.
cavities in infinite bodies subjected to If the sheet were infinitely thick, plane
tension has been discussed by Sadowsky strain would apply; or, if infinitely thin,
(2~) and Green (28). However, difficulties then plane stress would apply. But with
arise in the stresses computed from their finite thickness, a mixed situation of
results near the crack edge when the plane stress near the surfaces of the
ellipsoid is degenerated into a crack, plate and plane strain in the interior
see Fig. 10. Subsequently, Irwin (2~) cal- occurs in the crack-tip stress field.
culated the stress-intensity factor at Consequently, the stress-intensity fac-
any location on the crack border, de- tors computed for plane problems repre-
scribed by the angle, /~, by comparing sent only their values averaged through
Green's results for displacements with the thickness. Therefore, considering
Eq 1. The formulas obtained are: that plane-stress versus plane-strain
( 4' ),/, displacement fields differ by a factor of
KI = ~(~ra)l/-----~ sin ~ j8 -t- cos2 ~ . (38) (1 - r~), the actual values of stress-
9o ~ "
intensity factors for a straight-through-
(by symmetry KH = K m = 0) crack can vary by (1 -- v~)I/~ (or less)
from the surface to the interior. The
where ~o is the elliptic integraF
values at the surface are a maximum of
5 per cent less than computed values
9o ~ 1 -- \ - - - ~ ] sin ~ 0 dO.. (39)
and, correspondingly, a maximum of 3
per cent more in the interior (for v =
Notice that for b = ~ , B = lr/2, Eqs 38 0.3). Though crack-tip plasticity further
and 39 reduce to Eq 4 or, for b = a, to complicates the situation, it is partially
Eq 37, with corresponding changes for this reason that the crack often
from Fig. 10 to Fig. 3 or Fig. 9. begins to grow in the interior of a plate
Though the above results for three- rather than at the surface to form a
dimensional problems are of extreme "tongue." Even though this effect is
practical interest, the mathematical frequently observed, ignoring it leads
difficulty in attempting other such solu- to a desirable level of accuracy of com-
tions is so great that a discussion of the puted values of stress-intensity factors
possible methods would be of little in developing fracture criteria?
interest. However, in practical applica-
tion of results it must be kept in mind EDGE CRACKS IN SEMI-IN~'INITE BODIES
that all bodies are really three-dimen- The plane-extensional problem of an
sional and often the cracks which must edge notch, a, into a semi-infinite plane
be analyzed do not suit the idealized subjected to tension, ~, has been dis-
results exactly as presented here. Never- cussed by several authors (30-32,16)
Values of elliptic integrals are to be found s So-called pop-in tests actually make direct
in many mathematical tables. use of this effect.

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40 FRACTURE TOUGHNESS TESTING

(see Fig. 11). With dimensional analysis line of the crack, no correction is re-
leading again to Eqs 4, with Ct left quired (25).9 Therefore, corresponding to
unknown, the task is merely to evaluate Fig. 12, the stress-intensity factor is:
that constant. However, formidable
methods must be employed to obtain Km = r(~ra) ~/2 1
(KI KII = 0)J . . . . . . . . . . . (41)
the effect of the free surface of the half-
plane. These methods use series-type There is no directly analogous mode II
mapping functions with the complex case corresponding to Figs. 11 and 12.
variable stress-function method (15,30) With these examples and their re-
and dual integral equations resulting suits, the methods of determination of
from a Green's function approach "closed form" stress-intensity factors
(31,32) or both. The results may be for some basic configurations have been

O"

L
o"
FIG. 12--An Edge Crack in a Semi-Infinite
FIo. ll--An Edge Crack in a Semi-Infinite Body Subjected to Shear.
Sheet Subjected to Tension.

illustrated. Subsequently, some other


computed to any desired degree of types of problems which have not lent
accuracy and (within 1 per cent of each themselves to closed form solutions
other) they are: bear discussion.
KI = 1.12~(xa)t/2~ (40~
T W 0 - D Y M E N S I O N A L P R O B L E M S OF P L A T E
(Kxx K i n = 0 ) J . . . . . . . . . . .
STRIPS WITH TRANSVERSE CRACKS
Comparison of this result with either The class of two-dimensionM problems
Eq 4 or Eq 17 leads to the conclusion of plate strips with transverse internal,
that the free surface correction factor edge, and dual colinear edge cracks
is 1.12 for edge notches perpendicular subjected to tension and in plane bend-
to uniform tension. ing is of great practical interest for frac-
On the other hand, for the analogous ture testing procedures. However, closed-
mode III case, Eq 7 and Fig. 5 with the form solutions for such problems are not
introduction of a free surface perpendicu-
lar to the crack plane along the center- o Unpublished resultsof G. Sih.

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PARIS A N D S i n . ON STRESS ANALYSIS OF CRACKS 41

available and many of the approximate strip width. The functionf(X) is obtained
solutions in the literature are of doubtful as a power series as a result of using
accuracy. Therefore, it is important not power-series mapping and stress func-
only to cite these results but to give tions. The form of Eq 42 lends itself to
estimates of their accuracy. direct substitution into Eq 9 or alter-
The limitations on use of the so called nately, to techniques developed by
"tangent" formula, Eq 17, for centrally Kobayashi (14). The resulting stress-
cracked strips and double-edge-notched intensity factors can be computed to
strips subjected to tension were already any degree of accuracy by Isida's
discussed. The work cited (13-16) which methods, provided the power series
employed in the analysis converge,
which they do for relatively large varia-

l O"
tions in X. Within this minor limitation,

TABLE 1--CORRECTION FACTORS


FOR A C E N T R A L L Y C R A C K E D F I N I T E -
W I D T H STRIP.
ffi a/b [2b/fa t~n .a/2b] zg a f(~)

0.074 1.00 1.00


0.207 1.02 1.03
0.275 1.03 1.05
0.337 1.05 1.09
0.410 1.08 1.13
0.466 1.11 1.18
0.535 1.15 1.25
0.592 1.20 1.33

Eq 17.
Isida (18).
Isida's values agree within 1 per cent of an
approximation by Greenspan (100).

Isida's results lead to accuracies of


within 1 or 2 per cent.
Fro. 13--A Central Crack in a Strip Sub- Isida has computed results in the form
jected to Tension. of Eq 42 for a variety of problems (13)
of special interest in fracture testing
evaluated those limitations was from such as the case of the centrally notched
direct attacks on the strip problems. strip in tension, as shown in Fig. 13.
One of the most formidable approaches Upon substitution of Eq 42 into Eq 9, it
to this class of problems is found in the can be noted by comparing the result
work of Isida (13,34-36). Isida has with Eq 17 that f(~) corresponds to the
extensively developed mapping func- exact correction factor for the stress-
tions for strip problems for determina- intensity factor of a finite width strip
tion of stress concentrations at the tips whose approximate form is [(2bfira) tan
of round-ended cracks of end radius, p. (ra/2b)] 11~. Table 1 compares the two
His results are presented in the form (13) to illustrate the accuracy of Eq 17.
Buecknefl~ (36) has developed integral
2~ al/~
0"o = O'msx ~---~ f(~) ...... (42) equation procedures and solved many
l0 H. F. Bueekner in internal reports of the
where X is the ratio of crack length to General Electric Co., Schenectady, N. Y.

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42 FRACTURE TOUGHNESS TESTINO

( ) M

Fro. 14---An Edge Crack in a Strip Subjected to In-Plane Bending.

TABLE 2---STRESS-INTENSITY FACTOR COEFFICIENTS FOR NOTCHED BEAMS.


a/h ....... O. 05 0.1 0.2 0.3 0.4 0.5 0.6 (and larger)
g(a/h) . . . . . O. 36 0.49 0,60 0.66 0.69 0.72 0.73

with Eq 40, which is a 12 per cent error.

l O"
However, as noted following Eq 17, the
effect of the crack's emanation from a free
edge disappears with deepening cracks;
consequently, the error should diminish.
The results are expressed as follows:

r, = ch6M_~, gCa/h) l ..... (43>

21.
(KIt = K m -- 0) J
where g(a/h) is given in Table 2.
The values in Table 2 suit the limiting
case of deep notches as determined from
2b Neuber's results (1o). Therefore, it might
be presumed that Table 2 reports values
with errors of far less than 12 per cent
for a/h greater than 0.2. Several recent
papers on notch-bending analysis agree
with the values in Table 2 and these
recent results also claim agreement with
o" "compliance calibrations" for a/h in
FIG. 15--Double-Symmetric Edge Cracks in the normal testing range.
Strip of Finite Length Subjected to Tension. Bowie developed polynomial mapping
functions for use with the complex stress
crack problems. He obtained (37) the function technique to solve plane prob-
solution to a strip with a single edge lems, such as cracks emanating from
notch subjected to bending, see Fig. 14. circular holes (38) and the double-edge-
The results so reported obviously lack the notched strip in tension (15). The latter
correction factor for a free surface, for example, as illustrated in Fig. 15, pro-
small crack sizes discussed in conjunction rides an indication of the validity of

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PARXS AND S m ON SZRESS ANALYSIS O]r CRACKS 43

TABLE 3--CORRECTION FACTORS FOR A DOUBLE EDGE-NOTCHED STRIP. ~

a/b h(a/b), b(a/b),-, [(2b/a'a) tan Ora/2b)]llSk(a/b)


(L/b = 1.00) (L/b ffi 3.0oj (L/b -* ~o)

0.1 . . . . . . . . . . . . . . . . . . 1.13 1.12 1.12


0.2 .................. 1.13 1.11 1.12
0.3 .................. 1.14 1.09 1.13
0.4 .................. 1.16 1.06 1.14
0.5 .................. 1.14 1.02 1. l b
0.6 .................. 1.10 1.01 1.22
0. 7 . . . . . . . . . . . . . . . . . . 1.02 1.00 1.34
0. 8 . . . . . . . . . . . . . . . . . . 1.01 1.00 1.57
0. 9 . . . . . . . . . . . . . . . . . . 1.00 1.00 2.09

a T h e last column agrees within 1 per cent with a similar formula proposed by G. R. Irw i n on
the basis of e s t i m a t i n g the various effects. I t is

__ + o.1

employing Eq 17 for this configuration.

l
O"
Comparing Bowie's results with Eq 17
is most lucidly accomplished using a
correction factor, h(a/b), on Eq 17, or

K I •ffi r ll' ~a tan 2b / h(a/b) . .(44)

(KII ffi K i l l ---- 0)

for which his computed values are given


in Table 3.
From Table 3 it can be immediately
observed that for low a/b values, the -i

correction factor of 1.12 for a crack from


a free surface, as illustrated by Eq 40, is
present. As a/b increases, its effect 2b
disappears and Eq 17 applies as noted
previously. The last column of Table 3
combines the two effects, that is, the
free surface and the finite width strip,
to give the complete correction factor
(within 1 per cent) for all values of a/b.
From this study it can be noticed that
using Eq 40 for a/b < 0.5 and Eq 17 FIG. 16--A Single Edge-Cracked Strip Sub-
for a/b > 0.5 results in errors of less jected to Tension.
than 3 per cent for the configuration
shown in Fig. 15, provided that L/b > 3. Collocation procedures for strips of
As a consequence, it has been illustrated finite length have been developed by
that basic solutions such as Eqs 17 and Kobayashi (iS) and Gross.n As an el-
40 can often be used with proper judg- l1 B. Gross, J. E. Srawley, and W. F. Brown,
ment to provide approximate analyses Jr., "Stress I n t e n s i t y Factors for a Single Edge
Notched Tension Specimen by Boundary Collo-
of more difficult situations such as are cation of a Stress F unc t i on," unpublished report
shown in Fig. 15. from NASA, Lewis Research Center.

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44 FRACTURE TOUGHNESS TESTING

ample of the method, Kobayashi treated shown in column 4 of Table 4 assures the
the strip configuration in Fig. 13 using accuracy for this configuration.
the general complex stress functions of Following the procedures of Kobayashi
M u s k h e l i s h v i l i (17), collocating equally and Gross, it is a straightforward mat-
space points on the sides and ends of ter to solve additional problems. More-
the strip. He observed agreement within over, similar numerical procedures based
about 5 per cent of Isida's results as on collocation of boundary conditions
given in Table 1. in the mean, using other representations
Gross treated the single-edge-notched of the Airy stress function, or energy
strip using Williams' (5) eigenfunction methods, or both, are available for
representation of the Airy stress func- development.

T A B L E 4 - - C O R R E C T I O N F A C T O R S F O R A S I N G L E E D G E - N O T C H E D STRIP.
a/b k(a/b) a [(2b/Ta) tan (xa/2b)] h(a/b) b k(a/b) r

0.10 1.14 1.12 1.15


0.20 1.19 1.12 1.20
0.30 1.29 1.13 1.29
0.40 1.37 1.14 1.37
0.50 1.50 1.15 1.51
0.60 1.66 1.22 1.68
0.70 1.87 1.34 1.89
0,80 2.12 1.57 2.14
0,90 2.44 2.09 2.46
1.00 2.82 ... 2.86
a Grossu
b Table 3 and Eq 44
c Bowie (16)

tion. The configuration is shown in Fig. REINFORCED PLANE SHEETS


16. He found that collocation at 20 or
Many conventional structures are
more boundary points was required to
fabricated from plane sheets (plates)
obtain convergence. His results can be
with reinforcing stiffeners or doubler
stated in the form:
plates attached by riveting, welding,
K I = a(a~r)'t~k(a/b) ) . . . . . . . (45) and other means. Often the attachments
(KII = K m ~ 0) f are designed as crack-arrestors in order
to provide so called "fail-safe" struc-
where k(a/b) is given as a correction
tures.
factor for this strip problem in Table 4.
In order to analyze some of these
By comparison of Gross's results
configurations, it is appropriate to
(Fig. 16) with Bowie's double-edge-
notched specimen results (Fig. 15) determine stress-intensity factors for
cracks in sheets with stiffeners perpendic-
(columns 2 and 3 of Table 4), the ap-
parently large influence of bending due ular to the cracks. Romualdi (39,40) and
to the lack of symmetry in the single- Paris (41,42) provided some early at-
edge-notch case is observed. Gross's tempts to estimate the effect of rivet
results reportedly agree with experi- forces tending to hold a crack dosed.
mentally measured values (that is, Sanders (43) discussed the problem of
compliance measurements) within a few action of an integral stiffener crossing
percentage points for 0.40 < a/b < 1.00. the center of a crack. Isida (13,44)
Moreover, new results by Bowie (16) extended his methods to give results for

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PARIS AND SIII ON STRESS ANALYSIS OF CRACKS 45

centrally cracked strips with integrally tensity factors is in general applicable to


reinforced edges and to infinite sheets thermal stress problems.
with a periodic array of cracks along a As an example, consider the case of
line with interspersed integral stiffeners. uniform heat flow in a sheet, with an
Greif (45) has solved the problem of a undisturbed temperature gradient, VT,
single crack and an integral stiffener at an angle, fl, with respect to a crack
(passing outside the crack) in an infinite of length, 2a, acting as an insulator, as
sheet, and in a continuation of that work shown in Fig. 17. Florence and Goodier
the riveted stiffener has been treated. 12 (48) have provided the complex stress
Moreover, Terry (46) has analyzed some function for this configuration. It is:
similar riveted and welded stiffener
problems, as an extension of work by r ---- i E ~ a ~ T sin fl log ~ . . . . . . (46)
8
Erdogan (21). Cracks within one sheet of
a riveted doubler-plated area of a struc- as a consequence of similarity of the re-
ture were treated by Paris (41). Since
z

Fro. 17--An Insulated Crack Disturbing FIo. 18--Coordinates Used in a Cracked


Uniform Heat Flow in a Sheet. Plate Which Will Be Subjected to Transverse
Bending.
this class of problems is difficult to
formulate, the methods employed are suiting crack-tip stress field equation
rather obtuse and specialized. Conse- with ordinary (isothermal) plane ex-
quently, they will not be described here tension, Eqs 29 and 30 may be applied
other than to remark that the most to Eq 46 which results in:
general approaches available are those of Eaa3nV T
I s i d a (13), Greif (4S) and Terry (46).
Ku = - - ~ - sinfl~
(47)
t
Tm~R~AL STRESSES (KI = K n l = 0) )
It has been shown that the crack-tip where a is the coefficient of thermal
stress field equations for isotropic bodies, expansion and E is Young's modulus.
Eqs 1, 2, and 3, also provide the proper Other examples (47), will be cited in
field equations for thermal stress states Appendix II.
(47) (with the unlikely exception of the
crack tip as a point source of heat). STRESS-INTENSITY FACTORS FOR THE
Therefore, the concept of stress-in- BENDING OF PLATES AND SHELLS

1~Private communication from J. L. Sanders,


The field equations for the stresses
Jr. near a sharp notch in a plate subjected

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46 FRACTURE TOUGHm~SS TESTING

to bending were first considered by pactness in Eqs 48, the similarity of these
Williams (49,50) who later applied like results with Eqs 1 and 2 is immediately
methods to a more detailed discussion of apparent. This similarity ~_s further
cracks (51). Using the classical Kirchhoff clarified upon computing K s and Ks
theory of plate bending, he obtained for some configurations and loadings of
the following stress-field equations (see interest.
Fig. 18) : The governing equation for free
bending of plates (no transverse loads)
(7+v) Ks z by the Kirchhoff theory is:
~" -- 2(3 + v) (2*rr)1/2 h
V4w = 0 . . . . . . . . . . . . . . (49)
F(3 + 5v) o
"I_ cos - COS
where w is the transverse displacement.
Consequently, an analysis (18) ensues of
+ (5
- -+ 3v) K s z
2(3 + v) (2=r)u2 h

9[ ((53g+ 5~~ ) .sm ~0 + sin 301


~-

(7+v) Ks z
=0 = 2(3 + ~) (2rr) 'n

V(5
"k (7 ++ 3v)
v) cos ~O + cos ~ 1
. . (48)
(5 + 3~) Ks z M~- ~ , ~ ~ J M~
- 2(3 + ~) (2~r)~n

FIO. 19--A Through Crack in an Infinite


Plate Subjected to Uniform Biaxial Bending.
(7 + v) Ks z
r,o 2(3 + v) (2rr) in h an identical nature to Eqs 21-27 which
gives:
9 (7 T ,,) sin ~ + sin (2f)lnEh(3 + ~)
KB - - iKa =
(1 -- ,~)
+ (5
- +- 3v) K s z
2(3 + y) (2rr) In h 9lim (,. - z0"*s'(~)..(S0)
z'~l 1

(1 -- v) O cos ~- where ~bB(z) is the plate bending stress


9 - (5 + 3,) cos ~ +
function discussed extensively by Savin
where the constants in Williams' analysis 0z).
(Sl) have been modified in order to define Furthermore, mapping is again per-
(re,s2) the plate bending and plate mitted; or, as Eq 30 followed from Eq
shearing stress-intensity factors, KB and 27, for the mapping function given by
K s , in a manner consistent with (but Eq 29, Eq 50 becomes
not quite corresponding to) the first- Eh(3 + v)
and second-mode types, KI and K s , K s -- i K s = -- (w/a)in - - 4~n'(1).. (51)
(t - ,~)
respectively, as defined by Eqs 1 and 2.
Though polar instead of rectangular For the example of an infinite plate
stress components are given for corn- subjected to uniform moment, M o , all

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PARIS AND SIH ON STRESS ANALYSIS O1~ CRACKS 47

around the boundary, and with a crack and crack-surface boundaries are loca-
of length, 2a, as in Fig. 19, Savin (lz) tions where details are not clear.
gives the stress function, Subsequently, Knowles (s4) pointed
out that using Reissner's (55) more
3Moa(1 -- J,) accurate plate theory leads to a correc-
~a(,7) =
Eh 3 tion of Eqs 48 which on the surface of the

[
9 "+ C'-+-~ ...(52)
plate makes them identical to Eqs 1
and 2, except for a constant factor.
Moreover, the character and role of KB
Using Eqs 51 and 52, the result is: and Ks are preserved through this cor-
rection. Hence, it is concluded that they
6Mo ) are directly proportional to (completely
analogous to) their counterparts, KI
(Ks = 0) and KH, where elastic action is con-
cerned. Williams (55) pointed this out
Since the stress in the surface layer of in reference to the experiments by
the plate, ~o, away from the crack is Erdogan (St). This correspondence has
also been observed for fatigue crack
6Mo
h2 growth. ~s
Therefore, both theoretical and experi-
the analogy between Eqs 53 and 4 is mental results for fracture tests have
evident. led to:
Moreover, Erdogan (52) has shown ( 3 + v)
experimentally that in brittle materials Ks = ~ K1 . . . . . . . . . (5S)
(i +~)
(like Plexiglas) the fracture mechanics
concept of Ks reaching a critical value, on the surface of the plate. The sensi-
K~e, is appropriate and analogous to bility of using the Kirchhoff theory to
the extensional first-mode case, that is, compute K s values is also clear when it
K ~ . Incidentally, Erdogan (52) also is reasoned that the values of stress-
shows that the critical value of stress- intensity factors reflect the intensity of
intensity factors applies to the extension general transmission of applied loads
second mode, that is, Ku~, which again into the crack-tip region. The general
is shown to be analogous to the shear properties ot gross-load transmission
case of bending, that is, Ks,. Conse- are unaffected by the boundary layer
quently, the plate bending and shearing of about one plate thickness, h, in which
stress-intensity factors as defined in the Reissner theory applies. Conse-
Eqs 48 are of some immediate practical quently, Eq 55 is always correct for
interest. converting Kirchhoff theory stress-
However, Eqs 1, 2, and 3 were pur- intensity factors, K s , to the Reissner
ported to give all tip-stress fields for theory result, Kz, for a given configura-
elastic bodies; yet the field for plate tion.
bending as predicted by Eqs 48 is not Several solutions for Ka and Ks are
identical to them. This is because the now available (is) and others can be
classical Kirchhoff theory of bending is obtained in a direct fashion using Eqs
an approximate theory which does not 50 or their equivalents for other types
take into account the details of the stress
distribution near boundaries nor dis- 'aR. Roberts, Ph.D. dissertation, Lehigh
continuities in the plate. The crack-tip University,1964.
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48 FRACTUP.E TOUGmCESS TESTING

of stress functions. Some of the available difficult. Nevertheless, since this problem
results are tabulated in Appendix II. is of prime interest in tear-resistant
The case of general bending and ex- design, efforts are being made toward
tension of thin shells with cracks has empirical methods of design (64,66).
been shown by Sih (57) to give crack-tip The complete analytical solution to such
stress fields equivalent to combining a problem is as yet improbable.
modes I and II with the bending fields,
COUPLE-STRESS PROBLEMS WITH CRACKS
that is, Eqs 1 and 2, and Eq 48. Modes
I and II result from extension of the Another area analogous to shell
middle surface of the shell, and the problems through having similar govern-
bending fields result from changes in the ing equations is that of couple stresses
curvature of the middle surface. Conse- (67,~). The formulation of couple-stress
quently, the stress-intensity factor con- problems takes into account the gradients
cept is also of general applicability to of stresses in terms of couples on infin-
shells. itesimal elements in order to account
However, computing the values of the for the effects of lattice curvature in
stress-intensity factors for particular crystals, and so forth. Setzer (69) has
configurations in shells is very difficult. shown that for extension of cracked
Moreover, it may be observed (57) that plates due to uniform applied stress away
the extension and bending effects in from the crack, no modification in the
shells will be coupled, so that the stress- field equations (Eqs 1), nor the stress-
intensity factors resulting from solutions intensity factors (for example, Eq 4),
must reflect this coupling. As a conse- is required. However, where the applied
quence of the coupling, formulas for stresses away from the crack possess
stress-intensity factors will involve many gradients, the values of stress-intensity
parameters (coupling terms) so that factors will be modified by factors of the
they will, to say the least, be compli- form
cated.
Folias (~,59) and Ang (6o), noting
the similarity of equations for plates on
elastic foundations and shallow spherical
shells (61), have attempted some problems
-I-A, (~)' -.t--..... (56)]
in these areas. However, no other at- where l is a couple-stress (lattice)
tempts at the complete solutions to shell parameter or characteristic length of the
problems are known. material. The A~ are of the order of
On the other hand, some parametric unity or smaller, and l is of the order of
studies of possible shell effects on cracks lattice dimensions; consequently, these
in cylinders have been attempted in results would be of a greatest interest
several articles (62--65). The results in analyzing fine cracks in crystals,
indicate that the experimental data on except for the fact that the methods
failure of cracked shells can in fact be involved are similar to and may be car-
correlated in terms of elastic shell ried over to the analysis of shells.
parameters. Hence, it is hopeful that
further progress can be made soon toward ESTIMATION OF STRESS-INTENSITY
quantitative prediction of shell effects FACTORS FOR SOME CASES OF
on an analytical basis. PRACTICAL INTEREST
The problem of crack-arrestor rings Armed with the principles of linear
on shells is at least another degree more elastic theorv, such as "the principle of

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PARIS AND SItt ON STRESS ANALYSIS OF CRACKS 49

superposition," and with an intuitive Consider the configuration of a


grasp of a strength-of-materials ap- notched round bar with an outside
proach, it is possible to form estimates diameter, D, and notched-section diam-
of stress-intensity factors. This was made eter, d, and subjected to extension caus-
partially evident in the case of an em- ing a net-section stress, #,or (see Fig. 20).
bedded elliptical crack in the discussion From dimensional considerations and
symmetry, it is noted that the stress-
intensity factor may be stated in the
form,

KI -- #net(rD)l/~F(d/D)l
K:tz K m = 0 J . . . . . . (57)

where F(d/D) is an unknown dimension-


less function of the diameter ratio. The
end values (that is, d i d ~ 0 or 1.0) of
the function can be established by
examining limiting cases.
As D ~ oo, dimensional analysis leads

~ j d' _]< to

K1 = Cs#~t(~'d)'n. . . . . . . . . . (58)

thus, for small values of d/D,

F~,(d/D) = Cs(d/D)tl*. . . . . . . . (59)

the value of C8 is found to be [1/(2V~)]


using Eq 9 and the stress-concentration
! solution for the problem given by Neuber
I rio) and Peterson (IlL Since the free
surface introduced by the finite diam-
eter of the bar lowers the stress-intensity
factor, F,,(d/D) is an upper bound on
F(d/D) for all values of diD.
FzG. 20--A CircumferentiallyCracked Round On the other hand, for dID ~ 1,
Bar Subjected to Tension.
Bowie's solution for the double-edge-
notched sheet, Eq 44, simulates the
of limiting cases following Eqs 38 and
39. Other situations where limiting cases problem upon substituting
of different problems are comparable
were illustrated in Tables 1, 3, and 4
and examples in the text. Notice es-
pecially, as in these tables, that one a d
problem solution often forms an upper . . . . . . . (6o)
b D
or lower bound on the solution of others.
These concepts will be employed in
examples of estimating to follow.

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S0 FRACTURE TOUOHI~SS TESTINO

The result conforms with Eq. 57, that is, Consequently,

(!= (, - ;); (, - ;)3


TABLE 5---STRESS-INTENSITY FACTOR
where h( ) is as tabulated in Table 3.
COEFFICIENTS FOR NOTCHED ROUND This function, FL(d/D) is a lower bound
BARS. on F(d/D) for all values of d/D, since
diD Fr~(d/D) Fu(d/D) F(d/D) the curvature of the bar causes increased
crack-tip stress over the flat plate solu-
o 0 o 0
0.1 .-- 0.111 0.111
tion as d/D recedes from the value 1.
0.2 0.046 0.158 0.155 Finally, from Peterson's (n) stress-
0.3 .__ 0.194 0.185 concentration values and Eq 9, and
0.4 0.118 o.223 0.200
0.5 ... 0.250 0.227 other considerations, the maximum value
0.6 0.185 0.274 0.238 of F(d/D) is estimated to be 0.240.
0.65 0.203 .__ 0.240 Interpolating between these solutions
0.70 0.217 0.296 0.240
0.75 0.226 ._. 0.237 results in the estimated values in Table 5.
0.80 0.230 0.317 0.233 By making use of careful judgment of
085 0.224 __ 0.225
0.90 0.205 o.336 0.205
the limits of applicability of the limiting
0.95 O.lO2 ... o.162 cases, Eqs 59 and 62 and the analysis of
007 0.130 __ 0.130 stress concentration (11), the accuracy
1.00 0 0.353 0
of F(d/D) in Table 5 can be stated with

Or

FIo. 21--A Serai-Eliiptical Surface Crack in a Plate Subjected to General Extension.

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PARIS AND Srrr ON STRESS ANALYSIS OF CRACKS 51

confidence. With a diD of 0 to 0.4, it is intensity factor, but less so in this case
4-3 per cent; with a d/D of 0.4 to 0.85, since the uncracked portion of the plate
it is 4-5 per cent; and with a diD of would inhibit bending. Finally, Table 1
0.85 to 1.0, it is -I-2 per cent. Therefore, shows the underestimation of the tangent
a solution with sufficient precision for correction as a/t becomes larger. Taking
practical applications has been con- all these factors into account, Eqs 17.
structed. 20, 38--42, 44, and 45, and their con-
This configuration is often used for siderations lead to the approximations:
fracture testing and a simplified formula
is employed, that is (70),
KI -- 0.233 ~net(rD) 1/*. . . . . . . . (63)
0"(~'~)1/2 'lra~ 112
This formula seems most reasonable
since 0.233 agrees with the values of " r 5/ ..(64)
F(d/D) in Table 5 within 5 per cent over Kn = 0
the range of did from 0.48 to 0.86.
Further improvements in the accuracy
Km (2t~a
.~ tanrra~]
= r(a'a)112q~__.
of the values given would require a full
analysis of the problem, such as sug- for the stress-intensity factors at the end
gested by Sneddon (71) or Bueckner. 14 of the semi-minor axis, a. For the ranges
Another configuration, which has been of b/a from 1 to 10 or more, and of a/t
discussed by Irwin (29), is that of a semi- from zero to one half the accuracy is
elliptical surface crack in a plate (see within about -4-5 per cent. Moreover,
Fig. 21). This configuration is both for b/a up to about 5 and a/t up to three
typical of flaws and is used in fracture fourths the accuracy is still probably
testing (simulating this type of flaw). better than 4-10 per cent, considering all
If the plate is subjected to general the compensating errors. This case has
uniform extension by stresses, g, gt and at least provided a classic example of
r, the stress, a ~, parallel to the crack estimating methods using many other
causes no singularity or no contribution solutions for stress-intensity factors to
to stress-intensity factors. Consequently treat an important problem which is all
a' will be ignored. but impossible to solve directly.
If b/a is large and a/t small compared A word of warning with complicated
to 1, the stress-intensity factors at the cases such as Eqs 64 is in order. If the
end of the semi-minor axis, a, can be crack-tip plasticity subtends a major
estimated from Eqs 17 and 20, making portion (say one half) of the distance
use of free-edge corrections as in Eqs 40 between the crack front and the back
and 41. Then, the correction, ~o, in side of the plate, use of these equations
Eqs 38 and 39 should be applied as b/a would become indeed doubtful. More-
values are reduced toward 1. However, over, estimation of the amount of plas-
the free-edge correction probably dimin- ticity is clearly more complicated here
ishes as b/a approaches 1, and the tangent than in other situations, but surely
correction in Eqs 17 and 20 is also an possible. Such estimates are beyond the
overcorrection in that limit. On the scope of this discussion and the reader
other hand, Eqs 44 and 45 and Table 4 is referred to Ref (72). Moreover, in
show that single-edge notches induce passing, it is noteworthy that restric-
bending which increases the stress- tions on crack-tip plastic-zone sizes
l~ Private communication from H. Bueckner. are always present in making direct

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52 FRACTtrRE TOUGHNESS TESTING

applications of the elastic analyses (7o). contour marked, K1, in Fig. 22. Now,
For certain situations estimated cor- Ks is closer to the tunnel-crack case or,
rections to the analysis for crack tip a guess is
plasticity effects have been proposed /q ~ 0.85 ~(~al)1/'. . . . . . . . . (68)
',41,70,72).
Estimates can be made for stress- The neck of width, 2a3, makes K~
intensity factors for quite arbitrary slightly higher than the comparable
crack-front contours in three-dimensional tunnel crack, or
bodies subjected to uniform tension, ~, K3 ~ 1.05 a(ra3) z/' . . . . . . . . . (69)
perpendicular to the crack plane in the
region including the whole crack. Con- Similar to K1, the guess for K4 is
sider the embedded crack whose plan K4 ~- 0.75 ~(~a0~n. . . . . . . . . (70)
view is shown in Fig. 22. Using the
previous results for circular disk cracks, These estimates are surely all correct
Eq 37, and for tunnel cracks, Eq 4, within -4-10 per cent (and probably -4-5
bounds on the values of stress-intensity per cent). Moreover, additional refine-
factors can be established on the crack ments are possible, such as noting that
K3 on the upper part of the contour is
K~ K3 likely to be about 5 per cent less than on
the lower contour in Fig. 22, due to the
II , , ,
curvature of the centerline of the neck,
20 KI K4 2a3.
j.___~ K3 Corrections can also be added for the
proximity to a free surface, such as the
Kz tangent correction in Eq 17, or for the
FIG. 22--The Plan View of an Irregular Crack emanation of the crack from a free sur-
in an Infinite Body. face, such as Eq 40. The method of
estimating has now been sufficiently
front for various portions of the contour, illustrated to allow direct application to
where a multitude of examples. In order to
KI -~ Kx or K~ or Kz or K4 I develop confidence in estimating pro-
cedures, it is suggested that one may,
Ku 0 l ..... (65) for example, estimate the stress-in-
Km = 0 tensity factor values for an elliptical
crack using the above procedure, Eqs
the value of K1 will be slightly greater 66-70, and compare the results with
than that for a disk crack of radius, the exact values, Eq 38.
al, but far less than a tunnel crack of
width, 2al. Therefore, from Eqs 4 and STRESS FIELDS AND INTENSITY FACTORS
37, FOR HOMOGENEOUS ANISOTROPIC
M~DIA
2r < KI << ~,(ral) an . . . . . (66)
An interest in stress analysis of cracks
for various media, such as anisotropic,
Since 2 / r is about 0.64, if K~ is guessed viscoelastic, or non-homogeneous ma-
to be terials, stems from two motivations.
Ka ~'~ 0.75 a(ral) 1/2. . . . . . . . . (67) First, the effects of slight amounts of
directionality, creep, and inhomogeneity
the result is surely within 4-10 per on the stress distribution and intensity
cent along the whole portion of the are useful in assessing the limits of

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PARIS AND SIH ON STRESS ANALYSIS OF CRACKS 53

applicability of the conceptual model The superposition of results from these


of fracture mechanics based on linear plane problems will allow treatment of
elastic theory. In addition, studies of the general case of crack-tip stress fields
the stress analysis of these various types similar to Eqs 1, 2, and 3.
of media will provide the basis of ex-
Plane Strain:
tension of fracture mechanics to such
materials. For this case, Hooke's law m a y be
Several authors have treated special reduced, using the restrictions on strain
cases of crack problems in anisotropic to eliminate the appearance of z-com-
media, such as orthotropy (32,73,74) or ponents of stress, to give:
particular configurations (75,76). How- ~ = An ~ + Al~y + A1Brxu/
ever, the general anisotropic case can /
be treated in order to determine crack- ~v A21 a, + A22 au + A2o rzu?... (72)
tip stress fields and to define intensity I
V~u A 61 ~ + A 12 au + A 66 r . u J
factors in a manner completely analogous
to Eqs 1, 2, and 3. The methods dis- where again, A~y = As.i and the A O. can
cussed extensively by Lekhnitzki (77) be expressed in terms of a~i directly if
will be employed here. la desired. Using an Airy stress function,
Hooke's law for a homogeneous U, with stress components defined as
(rectilinearly) anisotropic material is: the usual second derivatives, equilib-
rium is automatically satisfied and the
compatability equations lead to:
+ at~ ru, + a u r~, + a ~ r.u /)1 D2 D3 D4 U = 0 . . . . . . . . . (73)
ell ---~ a21 o'z "~ " " " where Dk = (0/0u) -- tze(O/O~) and #~
es ~ all ~rz "~" """ are the roots of
...(Tt) Autt 4 -- 2 A l l t t 3 + (2A12 + A l l ) # ~
"Yym ~--"all O'z "~- " " "
-- 2A21# -~-A~2 ~ 0..(74)
7zz = gill ffz all- " ' "

These elastic constants, # , , are complex


"/~u ~ aez a,: -I- ai2 au -I- al~ of
or pure imaginary and occur in conjugate
+ ai4 ru~ + a66 r,, + air ~,u pairs (77), that is, m = Ca and m = #2.
cohere, from reciprocity Defining the complex variables, Zl and
z2, b y
aii : aii
zl = x + m Y \
Referring to Fig. 2 for the coordinates ( (7S)
z2 x + u2 y )
and notation with respect to a crack
front, the crack-tip stress fields m a y be the general solution to Eq 73 can be
resolved from two cases of plane prob- written, if m = u2,
lems which are defined as: U = U~(z~) + ~U~(z~) + U~(~) + z,U~(~)
(1) Plane strain, that is, (Ou/Oz) =
(Ov/OZ) = w -- 0 or r = 7u. = or, if m r m ,
~,** = 0 U = Uffz) + U2(z2) + us(~) + u,(~2).. (76)
(2) Pure shear, that is, u = v =
(Ow/Oz) = 0 or ~, = e~ = ~ = and with the further restriction that U
Ta'l/ ~ 0 must be real, they become
11 T h e m a t h e m a t i c a l d e r i v a t i o n of s t r e s s fields U = 2 Re[Ul(zl) + ~lU2(zl)]1
l e a d i n g t o E q s 8 1 - 8 5 a r e n o t a r e q u i r e m e n t of
useful i n t e r p r e t a t i o n of t h o 0 e results.
U 2 Re[U~(z~) + U2(z2)] / .... (77)

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54 FRACTURE TOUGHNESS TESTING

The similarity of the first case of Eq 77 posing these conditions, as well as those
with Eq 22 is appropriate since for mentioned earlier and then substituting
isotropic media, ~1 = #2 = i. Therefore, the variable,
the orthotropic case with the crack on a
z - - x + r = r # e. . . . . . . . . (80)
principal plane which leads to ~1 = ~2
has been reduced to the same case as the crack-tip stress fields are found from
isotropic elasticity with the simple Eqs 78 - 80 and can be stated in the form
change of variable zl = x + /~zy. The
more general case of anisotropy, the
gla [ #1#3
ax -- (2rr)112Re L.m - p2
second of Eq 77, or ~1 ~ p2, will follow
in the remaining discussion. 9{ /z2
The stress and displacement compo- (cos 0 + #3 sin 0)tn
nents are found from the Airy stress
function, U, by the usual combination
of derivatives which give: (cos 0 + m sin O)tn
r : 2 Re[p, 2 UI" (zl) q- #22 U2" (z~)] Kn, [ 1
+ ~ Re., - #3
a~ = 2 Re[&" (Zl) + Us" (z2)]
r~ = - 2 Re~ Ut~ (z~) + us U2~ (z2)] 9{" #32
(cos O + m sin O)~n
and
u ffi 2 Re[p~ U~' (z~) + p2 U2' (z2)] ~.. (78) /a12 }
v = 2 Re[q1 U/(zl) q- q2 U2' (z2)] -- (cos 0+ pl sin 0)=/~

where: Kx~ [ 1
o"v = (2~rr)ll 2 Re pl -- /~
p~ = A n / ~ z + Az2 -- Alo p,
qi = An #, + (A2~/p,) - - A ~ o . 9{ #1
(cos 0 + u2 sin 0)In "..(8D
Therefore, solution to any specific prob-
lem is reduced to finding the UI and U2
which satisfy the boundary conditions. (cos 0 + m sin O)U2
Referring again to Fig. 2 and Eq 75,
Kzx~ [" 1
in the neighborhood of a crack tip, I zll
+ (2~ReLpl-- m
and I z2[ are small compared to other
planar dimension of problems. Conse-
quently, the stress functions for cracks
.{ 1
(cos 0 + m sin O)U2
given by Lekhnitzki (77) m a y be reduced
to the form,
(cos o + m sin O)~n
/, (#1, #2, a) ]
ul~(zt) ZII/3 !
. . . . . . (79) Kta
r~ = (2rr)xl------
~ Re 9 - -
V #t~3
/2(#*, #2, ~2) "| Lm - u~
UV(z2) z-~

where fl and f2 are well-behaved in that


)
.{ 1
(cos 0 -I- m sin O)1/~
neighborhood and some restrictions on
their form are imposed by the stress-free
crack surface boundary conditions. Im- (co.~0 + m sin O)u2

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PARIS AND SIR ON STRESS ANALYSIS OF CRACKS 55

+~Re
9t~lla [ 1 force problem, as shown in Fig. 23, the
pl -- p~ stress functions are:
,{ /.~1 u:(a) =
,.. (81)
(cos S + m sin o)m

(cos 0 + p= sin O)'/2 9log [ fl + (fi2 _ a~)i/2 _ ia


~i + (~i~ a~)]12 "4- ia ]
-ip~,~ .(84)
where higher-order terms in r have been U~'(r =
2~(~ - ~)
neglected. Reiterating, /~1 and m are
dimensionless elastic constants. Notice
the striking similarity of Eqs 81 with + (h" a,),:,
(~'k = + a + zk)

Using Eqs 78 - 80 with Eqs 84 and com-


paring results with Eqs 81, it is found
that

X
KI. = (,~a)'~ . (85)
KIIa = o

Equations 85 can also be obtained from


the isotropic case, Eqs 32 or 33, directly.
It is therefore easy to add a multitude
of examples by simply constructing
I stress-intensity factors from symmetric
and skew-symmetric isotropic counter-
Fro, 23--A Crack in an Infinite Sheet Sub- parts. Attention shall now be turned to
jected to CentrallyApplied WedgeForces. the condition of pure shear.
Eqs 1 and 2. The definitions of KI. and Pure Shear:
K n , have been chosen to be identical to
For this case the generalized Hooke's
K~ and K n for the cases of symmetrical
law, Eqs 71, may be reduced by the
configurations with symmetric or skew-
definition of pure shear to:
symmetric loadings, respectively.
Consequently, it can he shown that aw
A.r~, + A~:=]
for the general anisotropic problem of
the configuration illustrated in Fig. 1: "~" ay ~.... (86)
Ow A~4r~,+ A~'r..
KI. = r (,~a)'n~ 7z: OX
/ (82) '

KIIe -- 0
where An4 = A46. Substituting these
and for the problem in Fig. 2, expressions into the equilibrium equa-
tions, the result is
K~. = .......... (83)
0ho 0~w O~x
a• ~-~ -- 2Aa ~ -{- As, - - -- 0.. (87)
Moreover, for the symmetrical wedge-

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56 FRACTm~.E TOUGHI~SS TESTING

which can be written for all boundary-value problems of pure


shear. For example, for the configuration
D5 D6 w = 0 . . . . . . . . . . . . (88)
in Fig. 5 the result is
where, as previously defined, KIn~ =Km -- r (~-a) 1/~. . . . . . . (96)
0 0
D~= ~ - . ~ upon constructing the solution and
comparing the result with Eq 7.
Comparing Eqs 87 and 88, it5 and g6 Consequently, it has been shown that,
for the general homogeneous anisotropic
are the roots of
case, the crack-tip stress fields and their
Ass~ 2 - 2A45tt + A . = 0 ..... (89) intensity factors, the complete analogy
It is observed that these roots are a with the isotropic case .is preserved. By
conjugate pair, that is, it6 = ~5. Defining judicious definition of the afiisotropic
a complex variable, zs, by stress-intensity factors, they are identical
to those for the isotropic case. The re-
z5 = x + ~5 Y . . . . . . . . . . . (90) suiting stress field equations (Eqs 81
the general solution to Eq 88 may be and 94), when superimposed 16 give the
expressed as most general state of stress in the neigh-
borhood of a crack tip in an anisotropic
w = W~(zs) + W~(~5) . . . . . . . . (91) body with any configuration or loading.
Since w must be real, for convenience Perhaps most important of all is the
W~ can be taken _~ ~'.v negative of W~ or fact that like the isotropic case, the
1/r 1/~ singularity appears in the stress
w = 2 I m [Wx(z6)] . . . . . . . . . . (92) field equations (Eqs ~ 81 and 94). This
Referring to Fig. 2 for a description of fact implies that fracture size effects for
the coordinates, in order to satisfy the homogeneous anisotropic media will be
stress-free crack surface conditions, W identical to the isotropic case.
takes the form, However, for nonhomogeneous aniso-
tropy, such as polar orthotropy; discussed
W l = A (zs) In . . . . . . . . . . . (93) by Williams ~3), singularities 'other than
where A is a real constant in the vicinity the 1/rm type may appear, causing
of the crack tip. Making use of Eqs 80, different size effects than the isotropic
case.
86, 90, 92, and 93, the stress may be
written in the form: CRACKS IN LINEAR VISCOELASTIC
MEDIA

rv, = Re cos 0 + ~6 sin O)~I~ The deformation of cracks in plane


. . (94) viscous extension has been studied by
Berg (78,79). He has shown that in a
r., = Re (cos 0 + gs sin O)112
linear viscous sheet, elliptical holes
where it is necessarily implied that near (including the limiting cases of cracks
the crack tip and circles) always deform into other
ellipses for the cases where additional
K t I I a ( A ~ A ~ -- A~2) ll~
a . . . . . (95) separation is not taking place. The exclu-
(2~r)m sion of separation means that adjacent
The anisotropic stress-intensity factor, is C o m p o n e n t s of ~ r e s s e l i m i n a t e d f r o m t h e
K i n , , is defined so that it is also identi- ~ress-~rain l a w s a h o u l d be r e - i n t r o d u c e d . T h e y
a r e d e r i v a b l e d i r e c t l y f r o m t h e listed ~ o m p o n e n t s
cal to its isotropic counterpart, K i n , in Eqs 81, 94, a n d 71.

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PARIS AND Sm ON STRESS ANALYSISOF CRACKS 57

points on the contour of the hole are re- been attacked. However, some special
maining adjacent. This assumption may cases of practical interest have been
be somewhat restrictive, but it permits treated.
the important conclusion of ellipses The problem of two semi-infinite
deforming into ellipses, which in turn half-planes of different material bonded
aUows the use of increments of infinitesi- (or welded) together along a line (or
mal deformation analysis to provide a plane) containing a crack has received
stress analysis of this class of problems. the most attention (84--87). The applica-
Therefore, for stationary cracks Berg tions of these analyses include faults in
has shown that the treatment by Sih laminations in rock or other materials,
(80) of stress fields near sharp crack tips cracks formed at steps in the thickness
for arbitrary linear viscoelasticity is in of plates in extension or bending, or
fact pertinent even though "blunting" both; stresses in glued joints and bond
of the crack tip takes place. Sih has cracks in composite materials.
shown that the crack-tip stress fields are The stress fields (84,85) for crack tips
as given in Eqs 1, 2, and 3, where the along such bond lines take the form:
stress-intensity factors are functions of
K
time, that is, u~i = (2wr)lnf~i(~,8, log r) . . . . . . (98)
Kr = KI(t) )
glI gil (t) ~. . . . . . . . . . . (97) where the terms of the type "log r" are
Km Km(t)J shown (85) to be of little influence on
These stress-intensity factors may be the stress fields. Consequently, the
regarded as representing the time history 1/r 112 type of singularity is the con-
of intensity of a crack-tip stress field of trolling factor in the stress field. There-
constant spatial distribution. fore, again the dimensional character
Treatment of problems of moving of K is essentially preserved and fracture
(extending) cracks in viscoelastic media size effects will' be identical to the
is currently unknown. However, they homogeneous case.
are obviously pertinent to formulating However, Zak (88) observed that for
the condition instability of cracks in a crack perpendicular to and reaching
viscoelastic media where slow growth an interface between two materials, the
precedes sudden failure. coefficient, n, of the stress singularity,
On the other hand, the fact that Eqs 1, r-", will be other than 89 If the new
2, and 3 have been shown to apply to material being entered by the crack
any crack in a linear viscoelastic body, has a lower modulus of elasticity, then
leads to the conclusion that slight n will be greater than 89and vice versa.
amounts of viscous action may cause This seems to indicate a tendency to
time effects but size effect will be iden- promote the entering of cracks in hard
tical to the elastic Case. Consequently materials into softer ones due to the
viscous "strain-rate effects" in studies increased severity of the type of singu-
of fracture, see for example Refs (81-s3), larity.
may be based on the usual elastic stress Another implication here is that size
analysig, that is, Eqs 1, 2, and 3. effects in transmitting fracture from the
harder phases of composite materials
SOME SPECIAL CASES ON NONI-IOMOGENE- to a softer matrix will be different than
OUS MEDIA WITH CRACKS the case of cracks in homogeneous ma-
The general problem of nonhomogene- terials. (More specifically, the stress
ous media with cracks has as yet not required for failure should depend in-

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58 FRACTURE TOUGENESS TESTING

versely upon the size of the hard phase of crack branching at velocities near
grains to the nth power.) 0.5 C2 add further evidence.
In addition, Mort (96) and Roberts
INERTIAL EFFECTSON THE STRESS (97) studied the acceleration of a crack
FIELD OF A MOVING CRACK through dimensional considerations and
Long before many solutions to elasto- obtained results tentatively in agree-
static crack problems were available, ment with those above.
Yoffe (89) presented the steady-state Most important in this discussion of
solution to a crack of constant length, dynamic effects is that the stress fields,
2a, movingthrough plate subjected to Eq 99, are preserved in a form nearly
uniform tension, ~. Moreover, she noted identical to the elastic stress up to very
that the extending crack tip possessed high velocities, that is, C --~ 0.5 C,.
a stress field of the form, Moreover, the 1 I t ~1~ singularity appears

ao -- (2~)tlI g~(o,C,E,v,.y) . . . . . (99)

where a(~-a)t can be recognized as the


stress-intensity factor, C is the crack
velocity, and 7 is the mass density of the
material. Notice that for all values of
the crack velocity the 1/r 112 singularity
is preserved. McClintock 00) obtained
similar results for steady-state problems
of the mode III variety, pure shear.
Both note that g~; is virtually the same
as the static case, Eq 1, up to crack
speeds, C, of over 0.4 of the shear wave
velocity, C2, where Fro. 24--A Crack in a Body of Arbitrary
Shape Subjected to a Load.
c, = 2(~ + ~ / . . . . . . (x00)
for all velocities so that fracture size
However, at some velocity, C, in the effects are virtually unchanged,
neighborhood of 0.5 C2, the location of
the maximum in the 0-direction stresses ENERGY-RATE ANALYSIS OF
changes from 0 = 0 deg to an angle of CRACK EXTENSION
about 0 = 60 deg to the crack tip and Griffith (l) in his original analysis of
the distribution of stresses, g~j in general fracture and later Irwin 0s) and Oro-
becomes quite different from the static wan (99) discussed the equilibrium and
case. The highest triaxiality of stresses stability of cracks from an energy-rate
near the crack tip shifts from directly viewpoint. Subsequently, Irwin 000,4,5)
ahead of the crack to about 0 = 60 deg provided a more detailed study of the
which is most easily observed from the energy-rate analysis and its relationship
calculations of Baker (Ol). Other authors to the crack-tip stress field approach.
(02--94) have re-emphasized these ob- The details were further generalized and
servations, including the transient states clarified by other authors (2o,41,1Ol). The
(m). results of these works prove the equiv-
Experimental photoelastic studies (os) alence of the energy-rate and stress-
confirm these results and observations intensity factor approaches. Application

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PARIS AND SIH ON STRESS ANALYSIS OF CRACKS 59

to "compliance calibration" (that is, forces, or intermediate cases. This result


experimental determination of energy applies for an unlimited number of forces
rates) of test configurations is an addi- on the body (41) and for mixed types of
tional benefit. This discussion will load application (101).
proceed to cover the essential features Equation 105 is useful for the experi-
of energy considerations. mental determination of energy rates of
An elastic body subjected to loads and test configurations. This is accomplished
containing an extending crack provides through measurement of the compliance,
an energy rate (that i% energy per unit X, as a function of crack size, A, in order
of new crack area generated), ~, avail- to compute the derivative in Eq 105.
able for the crack-extension process. Though this so-called "compliance cali-
Referring to Fig. 24, the uvailable energy bration" method is straightforward in
for an increment of crack extension, principal, the derivative depends on
dA, is provided from work done by small changes in X, which in practice
the force, PdA, and the release, --dV,
in the total strain energy, V, stored
in the body (lO0). Consequently,
(o)
dn dV
9 == P ~ " ~ - - d-A . . . . . . . . (101)
a
the displacements of a linear elastic body
are related to the load by
a = xP . . . . . . . . . . . . . (102)
where X is the compliance (that is,
inverse spring constant), which depends
upon the configuration, including the Fro. 25--The Tip of a Crack (a) Which Has
crack size, A. Been Pulled Closed (b) Along a Segment Ad-
The strain energy in the body is work jacent to the Tip.
done in loading, that is,
require very accurate measurement
pn x~ techniques.
v . . . . . . . . . . . . . (103)
2 2
THE EQUIVALENCE OF ENERGY-RATE
From Eqs 102 and 103 and, using the AND STRESS-INTENSITYFACTOR
rule of differentiation, APPROACHES
d a dP O In the previous section it was noticed
a-A = o~ + -d-2"~P ....... (lo4)
that the energy rate, 9, is independent
of the type of load application. Hence,
Eq 101 becomes for convenience in the discussion to fol-
/~ 0x low, the fixed-grip situation may be
9 = 2 a-A- . - - .......... (los) employed with no loss in generality of
results.
Terms involving dP cancel in Eq 105. If an elastic body is loaded and the
Therefore, the available energy rate, 9, grips (load-point displacements) are
for infinitesimal crack extension is then fixed, the strain-energy change,
independent of the type of load applica- dV/dA, is the only contribution to
tion, for example, fixed grips, constant (see Eq 101). Under this condition, the

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60 FRACTImE TOUGHm~SSTESTING

work required to close a small segment For the isotropic case, the result of
of the crack, a, as shown in Fig. 25, these substitutions and performance of
from the opened position, (a), to the the integration in Eq 106 leads to (for
closed position, (b), is identical to the plane strain) :
change in the strain energy. The work 1 -- P 1 -- P
can be computed as the crack-surface = - T 6 - ~e + -Yd- ~'"
tractions required to close the crack
times their closing displacements times
one half (since the displacements will be + ~1 K m ~..(lo7)
proportional to the tractions). The trac-
tions required are the stresses on the The terms on the right-hand side of
prospective crack surface with the tip at Eq 107 indicate that the energy-rate
x = 0 as in Fig. 25(b). The displacements contribution of each mode of crack-tip

T A B L E 6 ~ E L A S T I C C O E F F I C I E N T S R E L A T I N G E N E R G Y R A T E S TO
S T R E S S - I N T E N S I T Y FACTORS.
(cJ~ = eKd)
(Values of c given below for the ease of plane strain)

Orthotropic ($2) Anisotropic


Mode Isotropic (w Atl = At6 = A** = 0

I ......
(,-.') {a,,A~,l,,,r~, 2a,, + A.],,, I rm [_A ~,,+__~,)l
\ 2 I Lau + 2-~u A 2 ~,z a

II . . . . . . (l
' E - v2) "2-An[A~n + 2Att~+A661t12A ]1 Im [An0~l +/,12) ]

(1 + v) i 1 (Av,A~ - A~') u'


III ......
E 2 (A~4~) t/2 2 Ai~A~

are the crack-surface displacements of stress field m a y be considered separately


corresponding points in Fig. 25(a). Since E -- 2(1 + ~)G, the separate con-
Therefore, as originally proposed by tributions are (for plane strain):
Irwin (4,s,7), the energy rate, g, can be
(1 - ~)/C~'
obtained from these considerations in
the form
-- ~u = (1 -p. ~') g ~ . . . . . . . (t08)
~ fixed gripa a-~O

l+v
~uI = - - ~ Km 2
9 + T + d x . . (106)

where
The stresses, *v, r~, and ru,, may be
obtained from the crack-tip stress field 9 = 9~ + 9H + 9m . . . . . . (109)
equations, such as Eqs 1, 2, and 3, with
r -- x and 0 = 0. The corresponding Equations 108 and 109 also may be
displacements are also those of the crack- adopted to the case of plane stress by
tip field equations, but with r -- a -- x appropriately discarding (1 -- v2) in
and 0 = ~r. the first two of Eqs 108.

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PARIS AND S m ON STRESS ANALYSIS 0~' CRACKS 6]

As a consequence of Eqs 108 and 109, tip which is regarded as that which
the direct relationship between energy precipitates failure.
rates and stress-intensity factors has More specifically, these phenomena
been illustrated. are: developing a plastic particle of
Equation 106 can also be used to critical size, developing the ultimate
determine the relationships between stress at a specific radius from the crack
energy rates and stress-intensity factors tip, and developing stresses approaching
for other elastic media. For example, the the cohesive bond forces ahead of a
relationships for anisotropic media can crack, respectively. Now, since each of
be obtained by using the appropriate these phenomena occurs imbedded within
stress fields, Eqs 81 and 94, and cor- the elastic crack-tip stress field, their
responding displacements in Eq 106. occurrence will always correspond to
Table 6 provides the modified elastic having that stress field reach a critical
coefficients for the equivalent of Eqs value. As a consequence, these and any
108 for orthotropic (a2) and general other methods which draw attention to
anisotropic 9 media. Equation 109 applies specific critical phenomena at a crack
to orthotropic media, but in its present tip, which proceed to use an essentially
form not to the general anisotropic case. elastic stress analysis, will lead to a
However, since cracks normally do failure theory equivalent to the current
not extend in a planar fashion (S3) with fracture mechanics concept of critical
K n and K m present, or even with KI values of stress-intensity factors.
present in generally anisotropic media, Even though these alternative meth-
these relationships are somewhat of ods may be regarded as just as true,
correct and, useful in a practical sense,
academic interest. It is sufficient to have
shown the equivalence of the energy- the attention that each draws to a
rate and stress-intensity factor ap- specific phenomenon within the crack-
proaches, in order that the direct rela- tip stress field embodies an assumption
tionship between the Griffith theory and which is unnecessarily restrictive in
current theories of fracture mechanics be formulating a failure criterion. The
fully understood. strength and generality of fracture
mechanics as based on the stress-field
O's EQUIVALENTMETHODS OF STRESS approach is in part due to the absence of
ANALYSIS OF CRACKS AND NOTC~IES such an assumption.
Several other methods of stress On the other hand, this does not mean
analysis of cracks and notches for that the phenomena which do in fact
incorporation into failure criteria have occur within the stress fields near crack
been proposed. The most notable in the tips should be disregarded. Attention
to the details of the processes by which
recent literature are those developed
materials resist cracking will undoubt-
by Neuber (10,102), Kuhn (66,1o3), and
edly lead to development of superior
Barenblatt (23). Identical to the elastic materials. Each of the alternative the-
field approach, each of these methods ories of fracture mentioned above (and
uses an elastic stress analysis to deter- others) does in fact draw attention to a
mine the general character of redistri- phenomenon which may be a key fea-
bution of force transmission around ture in the fracture process. Therefore,
cracks. In addition, it is important to their high worth in con'unction with
note that each of these analyses draws and complimentary to the methods of
attention to a phenomenon at the crack fracture mechanics is clear.

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62 FRACTURE TOUGHNESS TESTING

LIMITATIONS OF THE CRACK-TIP STRESS the approximate stress, %, ahead of the


FIELD ANALYSES crack, obtained by substituting Eq 4
into Eq 1 and setting 0 = 0, is:
In this paper results of linear elastic
stress analyses of cracked bodies have ~ul/2
~ p p ~ o x ffi (2r)1I, . . . . . . . . (109)
been presented for a typical variety of
problems which have already been
treated. The determination of stress- The exact stress can be most easily
intensity factors for any particular determined by the Westergaard stress
problem can with time be accomplished. function technique, see Appendix I, and
Therefore, the elastic stress analysis is:
is not in itself a real limitation on frac- 9 (a + r)
ture mechanics. ev . . . . t -- (2at "4- ~)tt2 . . . . . . (110)
However, the accomplishment of a
stress analysis does represent a delay in where, in Eqs 109 and 110, r is the dis-
the application of fracture mechanics to tance ahead of the crack tip along the
configurations with cracks which have crack fine.
not yet been treated. Moreover, the Now, taking the ratio of the exact
accuracy of known solutions for stress- to the approximate stresses gives:
intensity factors represents a temporary
limitation on the accuracy of immediate (
try sp.rox -- ~1 + 2"~a/
applications. Usually, this limitation is . . . . . (iii)
far less severe than others, such as varia-
bility of materials, in practical applica-
tions. Consequently, the elastic stress
In a similar fashion, this ratio may
analysis itself may be regarded as
also be computed for the configuration
"exact" and the real limitations of
shown in Fig. 23 and is:
fracture mechanics come only in its
application to situations where non-
linearity of material behavior at the
crack tip (or elsewhere) disrupts the
~,,pp,o.=,,.,o, = (:)(
1 -F 1 q-~a] " .(112)

gross features of the stress distribution. The types of loading in these two
A certain amount of nonlinear be- configurations, Figs. 3 and 23, are
havior such as plasticity can be tolerated opposite extremes, yet Eqs 111 and 112
within the crack-tip stress field without show similar deviations of the approxi-
grossly affecting the field outside the mate stresses from the exact, at like
nonlinear region. Moreover, the dis- values of fla. Therefore, if the relative
turbances, if embedded within identical tolerable size (compared to crack size,
fields, will themselves be identical and a) of zone of nonlinearity can be estab-
hence self-compensating in comparisons lished for one configuration it is bound
of fracture strengths. Therefore, it is to be applicable to others.
important to resolve the relative sizes Recent experimental evidence (To) in-
of zones of nonlinearity which can be dicates the validity of the elastic stress
tolerated within the crack-tip stress field approach up to stress levels, r of
fields. This size is of course related to 0.8 of the yield strength, eyp, for the
the relative size in which the field equa- configuration shown in Fig. 3. For this
tions, such as Eqs 1, apply. configuration, the width, o~, of the zone
For the configuration shown in Fig. 3, of plasticity is predicted to be (~):

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PARIS AND SIR" ON STRESS ANALYSIS OF CRACKS 63

well. At any rate, this conclusion should


ffi 2 a ......... (113)
give full confidence that slight amounts
of these effects do not invalidate the
Substituting the upper limit of stress, useful application of the concepts of
= 0.8 Cyp, mentioned above, the fracture mechanics.
relative size, w/a or r/a, for reasonable As a consequence of the above re-
accuracy is about 0.3 from Eq 113. marks, it is observed that the only real
For this value of r/a, Eq 111 predicts a limitation of elastic stress analysis
deviation of actual stresses from the commences with the advent of sizable
field equations of about 20 per cent. Thus zones of nonlinearity that is, plasticity,
it appears that the zone of nonlinearity at the crack tip. The current hope for
at a crack tip may be fairly sizable, that extension of the applicability of fracture
is, of the order of 0.3 of the crack length mechanics to such situations lies in
(and other planar dimensions such as developing a full analysis based on the
net-section width), without grossly theory of plasticity. This topic is a sub-
disturbing the usefulness of the elastic ject left for other discussions.
stress field approach. However, a more
extensive evaluation of this limitation A cknowledgment:
should be the subject of further research. The authors gratefully acknowledge
In addition to nonlinearity in the the support of this work under the NASA
region of the crack tip, consideration of Grant NsG 410 to the Lehigh University
other conditions (such as anisotropic and Institute of Research. Portions of the
viscous effects having cracks in the bond analysis were based on previous work
line between dissimilar materials, ther- supported under grants from the Na-
mal stresses, couple stresses, inertial tional Science Foundation, G24145,
effects of moving cracks) and of all and the Boeing Co.
three modes of crack-tip stress fields, The many suggestions and data pro-
has led to positive results. The conclu- vided by W. F. Brown, O. L. Bowie, and
sion is that the current techniques of G. R. Irwin were most helpful in prep-
fracture mechanics may be extended to aration of this paper. Appreciation is
all of these areas, since similar types of also expressed for aid in collecting infor-
crack-tip stress fields exist for them mation for Appendix II given by M.
and the stress-intensity factor methods Kassir of the Department of Mechanics
of assessing failure should apply equally of Lehigh Univerisity.
APPENDIX I

THE WESTERGAARD METHOD OF STRESS ANALYSIS OF CRACKS


Any elementary text on the theory of The strain-displacement relationships and
elasticity gives a full development of the Hooke's law lead to the compatability
equations for plane extension. The equi- equation:
librium equations are:

ar ar,v ffi 0
ax + a-y
ffi + (~, + ,~) = 0..(115)
........ (114)
W+7 =o
The equilibrium equations (114) are auto-
9,~ = rv, matically satisfied by defining an Airy stress

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64 FRACTURE TOUGHNESS TESTING

function, 4,, in terms of its relationship to tI~I = Re ZI "4- y I m ZI . . . . . . (124)


the stresses, that is,
which as a consequence automatically satis-
fies equilibrium and compatability, Eqs 114
and 117.
Using Eqs 116 and 123, the stresses re-
~ = ~ ......... (116) suiting from ~, as defined in Eq 124, are
~.= ReZ x-yImZx')
--0~I~ r Re Z t + y Im ZI'~ . . . . . (125)
r.y -- --y Re Z I' J
Substituting Eq 116 into Eq 115 leads to: Now any function, Z1, which is analytic in
the region except for a particular branch
V ~ -- y ' ( v ~ ) = 0 ........ (117)
cut along a portion of the x-axis will have
In order to solve a problem, the stress func- the form
tion, r must satisfy Eq 117 and the bound- g(z)
ary conditions of that problem. Zl = [(z+b)(z_a)lU, ...... (126)
Choosing the stress function, q~, to be:
= ~kx + x ~ + ~ s . . . . . . . (118) This will solve crack problems for a crack
along the x-axis from x = - b to x = a,
it will automatically satisfy Eq 117 if the (y = 0), if g(z) is well behaved, since the
~ are each harmonic, that is, stresses, % and ~'zv, along that interval are
v ~ --- 0 . . . . . . . . . . . . . (119) zero, provided that

Define a complex variable, z, by Im g(x) - 0 (for --b < x < a)...(127)

z = x Jr iy . . . . . . . . . . . . (120) For example, if the function


q$
Functions of that complex variable, ~(z), ZI - (z2 _ a2)Xn . . . . . . . . (128)
and its derivatives,

d2 d2 z' dZ . . ( 1 2 1 ) is examined, it solves the problem of a stress-


free crack at - a < x < a, y = 0, and
leads to boundary conditions of uniform
have harmonic real and imaginary parts, if biaxial stress, a, at infinity (see Fig. 3).
the function is analytic, for example, if ~. = Now, reverting to the more general case,
Re ~ + i Im Z., then Eq 126, a substitution of variable
V'(Re Z) -- VS(Im Z) - 0 . . . . . (122) t" -- $ - a . . . . . . . . . . . . (129)
This is a result of the Cauchy-Riemann con- leads to
ditions, that is, ](r)
ORe ~g 0Im Z ] z, = ~ ............ (130)
Ox ~ y - - = Re Z . . . (123)
where, from Eqs 126 and 127, J(D is well
8ImZ 0ReZ ~ ImZ behaved for small [~'1 (that is, near the
Ox Oy crack tip at x = a). Moreover, in that re-
gion, as ] ~" [ ~ 0, f may be replaced b y a
Equations 123 may be used to differentiate
real constant, or Eq 130 may be written
t h e s e functions Z through Z.

First Mode: KI .. (131)


Z~ [ IrL'Q = (2r011s . . . . .
In conformit.x with Eqs 118-123, Wester-
gaard (8) defined an Airy stress function, q~, Other stress functions, Z I , for crack prob-
by lems, such as Eq 16, will also always lead

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PARIS AND S m oN STRESS AI~ALYSlS OF CRACKS 65

to this form9 Noting that Eq 13l may be Equations 133, 134, 136, and 139 are the re-
substituted into Eqs 125, and using polar sulting crack-tip stress and displacement
coordinates, that is, field, that is, Eqs I and 13, for the first mode.
.t = re;' . . . . . . . . . . . . (132) Second Mode:
the crack-tip stress field is: Instead of choosing the Airy stress func-
tion as in Eq 124, it is equally permissible
K'-"'-L-Icos ~ I - sin O_sin ~- to choose the form,
v~ = (2a.r)l/~ 2
~II = --y Re 2 1 1 ........ (140)
oF . o . 3;1
= Kt c o s ~ - L l + sm sm~-[~..(133) Repeating all of the operations from Eqs
124-139 andagain making useofEqs 114-123
K I 0 0 30 lead to:
r.y = (2,.r),/~ sin ~ cos ~- cos ~-
~z---- 2 I m Z u + y R e Z u ' ]
where, from Eq 131, av -- --y Re gli t ~ .... (141)
r~v = Re ZII --y Im ZII t J
KI = lira (21g')l/2Zi . . . . . . (134)
[tl-~0 and
The strain in the y-direction can be writ- l+p
ten in terms of displacements and stresses 1g' ~- - -

by Hooke's law, or E

OV ~ v 9 [2(1 - - p) Im Z,. + y R e ZH]


9v . . . . . . (a, + ~r,)...(135) ......... (142)
0y E E l+v
E
For plane strain, Hooke's law (~, = 0) also
leads to 9 [-- (1 -- 2v) R e ZIr - - y I m Zn]
*, = ,(a, + *,) . . . . . . . . . . (136) and in the neighborhood of a crack tip, that
is, I ~ ' l - ~ 0 ,
Substituting Eqs 125 and 136 into Eq 135
and integrating lead to ZIIII~I~ 0 m KIT . . . . . . . (143)
(2,'~)~t2
r -- 1 + v [ 2 ( 1 - v) Ira ZI - y Re Z~]..(137)
or
Similarly, consideration for e, gives Kn-- lim (2~r~')I/~Zu. . . . . . (144)
]~I-*0
1+ In addition, near the crack tip, substitution
u - WV[(l -- 2p) R e Z I -- y l m Z i ] . . ( 1 3 8 )
of Eq 143 into Eqs 141 and 142 leads to:
Substituting Eqs 131 and 132 into Eqs 137 -Ku 0
trz ~ - - sin -
and 138 and noting E = 2G(I + v) lead to (2~) ~/~ 2

u~
KI
G
(r/2,0 In cos ~-
a
r
9 2+ cos~cos--
L.
o o]
Ku 0 0 30
cu = (2wr),/s cos ~ sin ~ cos ~- . (145)
9 (139)
Kt (r/27r)lt2sin 0 Kn 0
r= G 2
*'~v = (2,rr)m cos 2

(for plane strain, w = 0)

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66 FRACTURE TOUGHNESS TESTING

and, for plane strain, Or,_._._.,+ Oru..__._,= 0 . . . . . . . . . (150)


dx Oy
Ku 0
u = - - (r/2r) 1/2 sin -
G 2 which, when combined with Eqs 149, gives
V2w =- 0............ (151)

9 .(146) Choosing
KII 0
= -G- ('/2'd~n cos 1
w = - I m Zm . . . . . . . . . (152)
G
leads to
%

9. = Im ZIIII L
These results are reflected in Eqs 2 and 14, f (153)
for the second mode. 9~, Re Z m ' )
The first and second modes may be super- The stress function, Zm, for a crack along
imposed, since the negative y-axis to the origin, takes the
-- @t + q,u . . . . . . . . . . (147) form near the crack tip

is a perfectly permissible Airy stress rune ZIII IIl'l-,'O = Kzlt


(2f~)vt . . . . . . . ( I ~ )
tion, in which case stress and displacement
components should simply be added to each
other. Consequently,

T h i r d Mode: Km= lira (2,q)lnZm . . . . . . (155)


I~l--0
The plane (two-dimensional) problem of
Moreover, substituting Eq 154 into Eqs 152
pure shear may be specified by:
and 153 and using Eq 132 lead to
u = O, ~ = O, w ffi w(x,y)..(148)

The strain-displacement equations and r,, = -- (2ft.)t/2 sin


Hooke's law give (105) K.I O . . . . . . (156)
~" = ( 2 ~ r ) " cos
O'gl "rztt
Ox G
. . . . . . . . (149) and
cqw ~.,
Oy G Km 0
= --d- ( 2 , / ~ ) " sin ~ . . . . . (157)
The stress components, az, au, a , , and
~'zu, all vanish so the equilibrium equations These results are reflected in Eqs 3 and 15 for
become the third mode.

APPENDIX II

A HANDBOOK OF BASIC SOLUTIONS FOR STRESS-INTENSITY


FACTORS AND OTHER FORMULAS
The results to be presented for stress- A selection of solutions for stress-intenmty
intensity factors will conform with their factors, in addition to those already listed,
definition as implied by Eqs 1-3, 48, 81, and will be chosen on the basis of their generality.
94. References which contain further re- Since superposition may be used, that is,
suits and details will be listed for the readers addition of the stress-intensity factors for
convenience. each mode. the results which lend themselves

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PARIS A N D S m ON STRESS ANALYSIS OF CRACKS 67

to generation of other solutions will be Infinite Sheets Subjected to in-Plane Loads:


emphasized. (See Fig. 26).

Formulas for Determination of Stress-In- Kx = cr sin2 O(xa)It2


tensity Factors from Stress Concentrations: KII = O" sin 0 cos #(~ra)xn
.... (161)
Mode I: ,,(1 -- :~#)a
,(,~) =
~.t/~
Kz -- lira r . (158)
~0 ~ ..... These cases may be found by the method of
Ref (18) or via Eqs 33 or by superimposing
provided KII = K m = 0, and where p is results of Eqs 4 and 6. (Note that all other
the tip radius of the notch and Cm~. is the cases of uniform loading at infinity or on the
crack surface may be derived from this case
by superposition.)

_ ko

Fxo. 26---A Crack in an Infinite Sheet Sub-


jected to Uniform Tension at an Arbitrary In-
clination.

Fie. 28--A Crack in an Infinite Sheet Sub-


jected to an Arbitrary Force and Couple at a
Remote Point.

For the right end of the crack in Fig. 27,


`,aII~ ( c b
Kx ffi 2 ~ I sin-1 - -- sin-1-
a a

Fzo. 27--A Crack in an Infinite Sheet with


Uniform Loads on Part of the Crack Surface.
+ ~ -- b) x- 1
maximum normal stress adjacent to the tip
(see Eq 9). .. (162)
` , ( c - b)(. -- 1~ ra'n
Mode II: K,, = + T.,,,

KII -- lira 'a'l/~`,mt,xpl/*. . . . . . . (159) 9 h-


p~0
a
provided Kz = K m = 0 etc.

Mode III:
Km= lira ~rl/*rm,,xpIt* ...... (160)
where
p~0
ffi 3 - 4u (plane strain)
provided Kt = K n = 0, and where r,,,~ is = (3 - v)/(1 + v) (plane stress)
the maximum shear stress adjacent to the
tip of the notch. See also Eqs 32.

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68 FRACTURE TOUGHNESS TESTING

For the right end of the crack in Fig. 28, E(k)


KI = ~r(Tr/a) 1/~ b~ K - ~ -- 0"~
1
K = Ki-iKlx = (b~ - a~)l/*
2(~a?/2(1 + K)' . 064)
{ [ a+z0
( P + i. ~ (zo~ - a~)' *
Kt~ = ~.(,da) '/~ b ~
E(k)
- a'

(b* - a*)"
0)
~(a +
J
]
At the far ends (see Fig. 29),

+ a(P -- iQ)(~o - Zo) + ai(l + ,t)U~


--Z(~ - ~ J(1~) ~
/1
.
E(k)
- F~i)/[

where KII = .r (.a.b),l, ( ~ E(k) '~I " "(165)


k-~31j
zo = xo + iyo
where k = [1 - (a2/b2)] 112is the modulus of the
complete elliptic integrals E(k) and K(k) of
~o = iyo
xo -
See Refs (21-23) or Eqs 33. the first and second kind, respectively. S~e
At the near ends of two equal colinear Refs (38,23); and for concentrated forces on
cracks (see Fig. 29), the crack surface, see Ref (21).
For an infinite array of cracks at the ends,
denoted by e in Fig. 30,

o (4b)1/2 sin ~r._c


2b

cos:re sin 2-b + s,n ]


.J i
_ -
_[_
b
L
2b/ '.. (166)
+ ( ~e _e
b sin ~ cos 2b
\

FIG. 29--Two Equal Colinear Cracks in an


(
9 sin ~ + sin 2b,I]

Infinite Sheet Subjected to Uniform Extension. Kn = 0

t o-

b b _L b l

C e r C e

Fro. 30--An Infinite Array of Colinear Cracks in an Infinite Sheet.

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PARIS AND SIH ON STRESS ANALYSIS OF CRACKt 69

For further information see Refs (4,5). At the right crack tip,
Note that this result may be used to evalu-
ate eccentrically located cracks in panels. P(c= - a2) '/~ )
For the semi-infinite crack in Fig. 31, KI = 2(~ra)t/= (c + a)
Q(c= _ a2)m ..(168)
P KIt = 2(~ra)l/2 (c + a)

.. (167)
Q For further information, see Ref (21).
KII .m Stress concentrations for deep hyperkolic
notches (see Fig. 33 and Ref (I0)) are as
follows.

P
0

V(•
FIG. 31--An Infinite Sheet with a Semi-in-
finite Crack.
FIO. 33--An Infinite Sheet with Load Trans-
mitted across a Neck Between Hyperbolic
Notches (Cracks).

For P= (force per unit thickness alone:

O'max

O'net
tan-kfl +L;) ,..(169)

.P~
Fxo. 32--An Infinite Sheet with Colinear 2a
Semi-infinite Cracks with a Concentrated Force.
For V~ alone:
For further information, see Eqs 32 or
Ref (21).
For the two semi-infinite cracks in Fig. 32:
A.t the left crack tip, --=( ..(17o)
P(c~ - a2) It= a~ \p/ \a/
KI
2 (,ra)~l= (c - a)
Vw
The t ~
Q(c2 - a~)lt=
2a
gII =
2 (~-a)1/= (c -- a) For M~ alone:

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7O FRACTURE TOUGHNESS TESTING

IO"
Fro. 34----A Crack (or Cracks) Emanating from a Circular Hole in a Sheet.

T A B L E 7--STRESS-INTENSITY F A C T O R
COEFFICIENTS F O R C R A C K S E M A N A T - /o\,,, l
ING F R O M A C I R C U L A R HOLE,

s
F(Mr), One Crack F(L/,), Two Cracks (Tm&x I
',uniaxial (biaxial (un~**ial (biaxial
strms) stress) stress) etr~)

0.00 3.39 2.26 3.39 2.26


0.10 2.73 1.98 2.73 1.98 3
O. 20 2.30 1.82 2.41 1.83 r "2a~'
0.30 2.04 1.67 2.15 1.70
0.40 1.86 1.58 1.96 1.61
0.50 1.73 1.49 1.83 1.67 Using Eqs 158 and 159, for the right crack
0.60 1.64 1.42 1.71 1.52
0.80 1,47 1.32 1.58 1.43 crack tip,
1.0 1.37 1.22 i .45 1.38
1.5 1.18 1.06 1.29 1.26 2,, 2M.
2.0 1.06 1.01 1.21 1.20
3.0 0.94 0.93 1.14 1.13
5.0 0.81 0.81 1.07 1.06 ,..(172)
Tvr** .
10.0 0.75 0.75 1.03 1.03
KII
oo 0.707 0.707 1.00 1.oo (,,'~)1"

For further information, see Refs (10,42).


For cracks emanating from a circular
hole (see Fig. 34 and Table 7),

o" o"

.. (173)

K n -- 0

For further information, see Ref (38).


FiG. 35--A Circular-Arc Crack in an Infinite For a d r c u l a r crack (see Fig. 35):
Sheet Subjected to Uniform Tension in an Ar-
bitrary Direction. for the crack tip a t 0,

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PARIS AND Sl'w ON STRESS ANALYSIS OF CRACKS 71

~(TR sin a)l/s { a


2
( 9
1 -t- sins
! h

FIG. 36---A Semi-infinite Crack Propped open


by a Wedge of Constant Thickness.

... (174)
~(~rR sin ~)l/s {
2
(1 + sins
9
-1- sin (2t~ "k" ~ a ) Isin' 2]

"[sin a sins 2] j FIo. 37--A Sheet Which is Loaded and


Clamped Prior to Introduction of a Crack.
For further information, see Ref (18).
P
Some Cases of Specified Displacements in
Infinite Planes:
I
For an infinite rigid wedge of constant
thickness (see Fig. 36), , 12c

KI (27ra)in (for plane stress) ..(177)


,- -~p
KII ffi 0
For further information, see Ref (23), FIG. 38---The Splitting of a Rod of Rectangu-
which also has a discussion of other examples lar Section.
of wedging.
When stress is applied first, then the K! -- ~hx/s/
boundaries are clamped, and then a crack
is introduced, this sequence (see Fig. 37~ Kxx ffi ~ I .......... (178)
results in constant energy release rate, ~z,
or For further information, see ReI (42).

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72 FRACTURE TOUGHNESS TESTII~G

Under forces:
Kx 2(3)U2Pal
{;sis ) (180)
Ku = 0 /
For further information, see either Ref

!o (23) or (105).

L l'
FIo. 39---Semi-finite Notch Approaching the
Free Edge of a Half-Plane.

Ip
FIg. 41--Concentrated Forces Applied to the
Axis of a Circular Disk Crack in an Infinite
Body.

A Semi-Infinite Notch Approaching the Free


Edge of a Half-Plane (see Fig. 39):
, /~-12XP. 1
/
+ cn/4.
k~-:--i] ~. /
- 8\ M (181)
KH ffi 0
For further information, see Refs (10,37).
FIG. 40"-Axisymmetrical Loading of a Body
with a Circular Disk Crack. Axisymmetrical Loading of a Body with a
Circular Disk Crack:
A Case of the Splitting of Rods, that is, For an axisymmetrical normal pressure
slender rectangular members (a >> 2c) (see distribution, p(r), on both crack surfaces
Fig. 38): (see Fig. 40),
Under wedging:
El ffi ~ 2 fe* (a2~-(~)s~ dr}" "(182)
x, 3_,,,=_~,, ]
Kxx ----0
KII:0 4a' / ........ (179)
For further information, see Ref. (23)

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PARIS AND S m ON STRESS ANALYSIS OF CRACKS 73

V
FIG. 42--Torison of a Cylindrical Bar with a FIG. 43--Torsion and Beam Shear of a
Partial Radial Crack. Cylindrical Bar with a Radial Crack.

| _| | | |

b b

--7
--|
| | G, |
Fro. 44--An Infinite Body with "Tunnel" Cracks Under Longitudinal (Pure) Shear.

Note that with superposition, this enables Torsion and Beam Shear of Prismatic Bars
treatment of all cases of axisymmetrical with Cracks:
loading." The K-values in prismatic bars under
For the type of circular disk crack shown torsion for the type of crack shown in Fig.
in Fig. 41, the K-values are: 42 are:

______f_e
[ *+ i --,
(1 + ~d~n (1 - ,~)~ [2(1 - ,~)|
KI (ra)3/2 1 --~ a2.J
s2]' . . . . . (183) + al/s(mjo + Jl)lxl/t r / . . (184)
Kill ~--~"~"~ ~'~ "~ " ~ ~ |
Ku = 0 (A + B)III a6nJ

Equations 182 may also be used. For where"


further information, see Ref (Z3). a = (b- a)/b

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74 FRACTURE TOVGaNESS TESTING

,n = 89 + 1/,~1 Cracks under Longitudinal (Pure) Shear:


Yo = 4 arctan (a)~ The K~ and Kn values for the three
cracks shown in Fig. 44 are all zero; the
J1 = [ - (1 -- a)/4a] [4(a)~ -- (1 -- a)Jol K m values vary with the location of the
A = 1/a [(1 + a) 2 (arctan crack tips as follows:
For the crack tips at a:
(~p)/(~)~- (1 - ~)1 { (0 - a')~an E(k)
B = [(1 - ~)/~1 [2 - l(t - ,~) A] K m = 4- \ ( b ' - a')/ K(k)

9~'(ra) ln

For the crack tips at b:


{(b' -- a')'~1'2
Km= • \(c' - bg]

[, ..(186)
For the crack tips at c:
FIr 45--A Plate Subjected to Uniform
Twisting Moments at Infinity
K,I, = + \ ~ - z - b S /

~ 9[ 1
(Ek) ]
L
where
((c~ -- a2)~*t2
k = k ~ /

Is the modulus of the complete elliptic in-


tegrals, E(k) and K(k) of the first and
second kind, respectively.
For further information, see Ref (106).
The Flexure of Infinite Plates:
A plate subjected to pure twisting moment
FIG. 46----APlate with Uniform Shear at In- (per unit length), H, at infinity (see Fig. 45)
finity. gives:
For further information, see Ref (26). ilia
Several other configurations are treated in 2D(3 -f- r),l
Refs (24,25).
For torsion and beam shear (Fig. 43) the or
K-values are:
KB = 0 ]
K1 = Kn ffi 0 ]
6H / . . . . . . . . . (187)
T (6.9~ + 6.47,m\ V t "' (185) K8 = h-V (~a)v,
,,, =0.969~-~-- -~-Z /a~J
For further information, see Ref (18).
For further information, see Refs (26,Z4). Uniform shear (per unit length), Q, at

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PARIS AND S m ON STRESS ANALYSIS OF CRACKS 75

Heat Flow

Fio. 49--A Sheet with Uniform Temperature


FIO. 47--A Plate with Uniform Bending Imposed on the Crack Surface.
Moments at Infinity.

FIG. 48--A Concentrated Couple of Ar-


bitrary Direction on a Crack Surface in an In- FIG. 50--A Clamped Plate with a Uniform
finite Plate. Thermal Gradient Through the Thickness.

infinity (moments required for equilibrium For further information, see Ref (18).
shown dotted in Fig. 46), gives: For a concentrated couple on the crack
surface (see Fig. 48),

3M* ~,, ( a + b~v,


tcB = h,C,~a----~ \ ~ - b/
or
31/*
+ ~ ( 1 + ,)

Ka 8,rmQaSn . . . . . . . . . (188) 3M* ~,.. (190)


Ka = 2hlOra)m (1 + v)
T' j
3//* (a + b~'"
The results are independent of Q~. kS(fa) tl~ ka -- b/
For further information, see Ref (18).
For uniform moments at infinity (see Fig. Thermal Sr Problems:
47),
A plate with uniform temperature sup-
plied on the crack surface (see Fig. 49) gives:

Ks KI -- ft/l(1 + . . . . . . . (191)
The results are independent of M'. KI[ = 0

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76 FRACTURE TOUOHNESS T E S T I N G

where

~z = thermal conductivity
q --rate of total heat per unit thickness
supplied to the plate

For further information, see Ref (47).


Note that this case has significance for high
pressure gas escaping through a crack.
A damped plate with a thermal gradient
through the thickness (see Fig. 50) gives:

~xEhVT(xa)tl2 }
K~ = 2(1 -- p) . . . . . . . (192)
Ks = 0

For further information, see Ref (47).

%
FIO. 51--An Infinite Body with a Uniform
An infinite body with a circular disk
crack perpendicular to a thermal gradient
(see Fig. 51) gives:

KH
EczVTa3n }
3*r(1-- v) . . . . .

K I -~ K i l l -~ 0
... (193)

Thermal Gradient Normal to an Insulated


Circular Disk Crack, For further information, see Ref (107).

APPENDIX HI

NOTATION

A - Crack-surface area G = Shear modulus of elasticity


a = Half-crack length of internal 9x, 9 n , ~ m = Energy rates associated
crack or crack depth of surface with each mode of cracking
crack h = Depth of a beam or plate
= Elastic compliance coefficients i = ( - 1 ) ~n
for Hooke's law of plane prob- K = K1 - iKix = Stress-intensity factor
lems of anisotropic media with complex representation
.= Elastic compliance coefficients Kx, K n , K m = Stress-intensity factors for
for the general Hooke's law of each mode (subscript "a" indi-
anisotropic media cates anisotropic type)
b = Half-width of a strip K t , K2, K3, K, =- Stress intensity at vari-
Ct, C2 = Constants ous points on a craz.k contour
r = Crack velocity K s , Ks = Plate and shell bending and
Dk = Complex differential operators shearing stress-intensity factors
( K = 1, . . . , 6 ) L = Half-length of a strip
D = Round bar diameter l = A couple-stress elastic constant
d = Notch diameter M = Applied bending moment (per
E = Modulus of elasticity unit thickness)
F = P - iQ, force with complex P = Force (per unit thickness)
representation (per unit thick- p = Crack-tip radius
ness) Pl, qi = Anisotropic elastic constants
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PARIS AND S m ON STRESS ANALYSIS OF CRACKS 77

R = R ~dius of a curved crack = Complex variable in the mapped


r = Radial coordinate from a crack plane
tip 0 = Angular coordinate measured
T = Temperature or torque from the crack plane
t = Sheet thickness (or time) K = An elastic constant for plane
U, U t , U~ = Stress functions for anisotropic stress or strain (see Eqs 162)
media ~, = Compliance of a linear-elastic
u, v, w = Displacement components body
V = Strain energy #, #k = Elastic constants for anisotropic
Z, Z I , Z n , Z m = Westergaard stress func- media (k = I, . - - , 6)
tions v = Poisson's ratio
Z, Z, Z, Z ' = Successive derivatives of a or, r = Normal and shear stress (applied
Westergaard stress function at infinity)
z = Complex variable ~o = Maximum stress at a notch
z~, z~, z3 -- Modified complex variables for anot = Net-section stress (average)
anisotropic analysis ai~ - *rz, *rU, Cr,~ Rectangular components
a -- An angle (or closing segment of a r~u, ru,, r~. J of stress
crack) ~r, ~r0, ~'r0 = Polar components of stress
/~ = An angle q~ = Airy stress function
7 = Mass density ~b = A complex stress function for
3',v, 3 ' ~ , "Yz~ = Shear strain components plane stress or strain
A = Displacement q~o = An elliptic integral
V = Gradient [(O/Ox) + (O/Oy)] Cs = A complex stress function for
V t , V4 = Harmonic and biharmonic oper-
plate bending
ators
X = A complex stress function for
= The bi-elastic constant of ~oined
plane stress or strain
half planes
~ , ~u, ~ = Normal strain components ~i = Harmonic functions
~- = A complex variable (origin at the ),g( I'} = A f u n c t i o n o f
crack tip)
h , i'~ = Modified complex variables for Re, Im - - R e a l and imaginary parts of
anisotroplc media complex functions

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PARIS A N D S m ON STRESS ANALYSIS OF C R A C K S 79

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80 FRACTImX TOUGHNESS TESTING

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PARIS AND S m oN STRESS ANALYSIS OF CRACKS 81

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STP381-EB/Apr. 1965

DISCUSSION

H. F. Bueckner~--It might be well to curvature. These values agree well with


review briefly the stress-analysis situa- those reported b y Irwin s who used the
tion regarding the notched round bar in same procedure. The results obtained b y
tension, since this geometry appears to this extrapolation method are, of course,
be i m p o r t a n t from the standpoint of only at best as accurate as the stress-
fracture testing. Several treatments of concentration factors from which they
this problem can be found in the litera- are derived. The second estimate was
ture and are compared in Table 8, which made using Neuber's formula for deep
gives the coefficient, F ( d /D ) , of Eq 57 notches in combination with a computa-
in the paper, as derived from various tion for a notch in an elastic half plane. 6

TABLE 8--COEFFICIENTS FOR COMPUTA'IION OF THE STRESS-INTENSITY


FACTOR, KI FOR A NOTCHED ROUND BAR.
[KI -- F(dlD)e~r (~rD)tl~]

Notch Depth, F(d/D) as givenby:


d/D Lubahna Irwinb Wundtc Parisd Present Solutions

0.5 0. 230 0. 224 0. 239 0. 227 0.240


0.6 0.234 0. 232 0. 252 0. 238 0.255
0.707 0. 229 0. 233 0. 258 0.240 0. 259
0.8 0. 217 0. 224 0.250 0.233 0. 251
0.9 0.195 0.199 0. 210 0. 205 0. 210

4 See footnote 2.
b See footnote 5.
c See footnote 3.
From Table 5 of the paper.
9 To be published.

references. The values used b y L u b a h n ~ Recently I completed a more rigorous


and b y W u n d t 3 represent m y first and analysisv of the problem using a certain
second estimates, respectively. The first singular integral equation, the kernel of
estimate was based on extrapolation of which is found b y means of Fourier
Peterson's published stress-concentration transforms. The coefficients derived from
factors 4 to a vanishingly small radius of this solution are shown in the last column
x General Electric Co., Large Steam Tur-
bine-Generator Dept., Schenectady, N. Y. 5G. R. Irwin, "Supplement to: Notes for
2 j. D. Lubahn, "Experimental Determina- May, 1961 meeting of A S T M Committee for
tion of Energy Release Rate," Proccsdinos, Am. Fracture Testing of High-Strength Metallic
Soc. Testing Mats., Vol. 59, 1959, p. 885. Materials."
8 B. M. Wundt, "A Unified Interpretation of e H. F. Bueckner, "Some Stress Singularities
R o o m Temperature Strength of Notch Speci- and Their Computation by Means of Integral
m e n s as Influenced by Size," ASME Paper No. Equations," Boundary Problems in Di~eren~iai
59, MET 9, 1959. Equations, edited by R. E. Langer, University
4 R. E. Peterson, "Stress Concentration De- of Wisconsin Press, Madison, Wise., 1960, pp.
sign Factors," John Wiley & Sons, lue., N e w 215-230.
York, N. Y., 1963. T To be published.
82
Copyright9 1965 by ASTM International www.astm.org
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DISCUSSION OF STRESS ANALYSIS OF CRACKS 83

of Table 8 and are considered to provide KI -- 0.414 aN (D) '/~


values of KI having an accuracy within
1 per cent. It is interesting to note that The coefficient in this equation corre-
the coefficients obtained by the present sponds to the value 0.233 in Eq 57 of
analysis agree well with those used by the paper. The present analysis yields a
Wundt, but are higher than those given value of 0.259, about 10 per cent higher
by Irwin or by Paris. Considering, for than that given by the above expression.
example, a notched round bar with
d i D = 0.707, a geometry commonly s "Screening Tests for High-Strength Alloys
used in fracture testing, the ASTM Using Sharply Notched Cylindrical Specimens,"
Fourth Report of a Special ASTM Committee,
Special Committee8 gives the following Materials Research &, Standards, Vol. 2, March~
expression ~or the stress-intensity factor: 1962, pp. 196-203.

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PLASTICITY ASPECTS OF FRACTURE MECHANICS
BY F. A. McCLINTOCK1 AND G. R. IRWIN2

Fracture mechanics, broadly speaking, yielding prevents attaining these in-


represents knowledge of the influence of finities, the leading terms still describe
loading and geometry on fracture. Fig- the stress distribution at intermediate
ure 1 shows the size range of significant distances. These will be called elastic
events involved in the crack-extension singularities or intensities. The scale
process. Until the ion and electron cloud corresponds to the next to the largest
configuration shown schematically at the configuration of the example of Fig. 1.
far left can be analyzed from wave It is the object of this paper to consider
mechanics, and the results integrated the next smaller scales of size, where the
through ten orders of magnitude, it will elastic singularity is distorted by the
be necessary to work with a series of embedded plastic zone, and plastic strain
different models, each appropriate to its is important, but the field may still be
own size range. Boundary conditions for regarded as a homogeneous continuum.
each model are found from the next In certain "ideal" situations, an elastic
largest and next smallest scales. The singularity dominates and controls the
smaller the size of the model from which enclosed plasticity. With higher stress
we can integrate through larger sizes to levels or smaller specimens, there may
obtain the fracture load for a given be no region between the plastic zone
geometry, the broader the range of and the boundaries of the specimen that
conditions which can be predicted or can be characterized by an elastic stress
correlated from given experimental data. singularity. In any event, the elastic and
From whatever level we do start, it will plastic relationships deserve careful
be necessary to introduce test data to study both as viewpoints for understand-
substitute for lack of knowledge (or cost ing phenomena at finer scale and for
of analysis) in the smaller regions. practical applications of this knowledge.
From this point of view, it is present By limiting our considerations to the
practice to correlate fracture on the basis macroscopic domain, certain relatively
of the leading term of the series expansion simple analytical models are available
of the elastic stress distribution about to serve as a basis for calculations and
the tip of the crack (1-5).3 As discussed to furnish a quantitative basis for de-
below, these terms represent mathe- scription. The discussion of such possi-
matical infinities of stress and strain at bilities is one purpose of this paper and
the very tip of the crack. Although will be treated first. Comments will then
be given relative to effects of plasticity
in crack toughness testing. In contrast
1 Professor of mechanical engineering, Massa- to linear elastic fracture mechanics,
chusetts Instititute of Technology, Cambridge,
Mass. plastic fracture mechanics is still rela-
z Superintendent, Mechanics Division, U.S. tively incomplete and so it must be
Naval Research Laboratory, Washington, D. C.
z The boldface numbers in parentheses refer
illustrated rather than treated compre
t~ the llst of references appended to this paper. hensively.
84
Copyright9 1965 by ASTM International www.astm.org
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MCCLINTOCK AND IRWIN ON PLASTICITY A S P E C T S 8S

SYMBOLS 0 = angular coordinate from the line


directly ahead of the crack
a = crack half-length
shear modulus
A, B = parameters defined by Eqs 35 # =
and 36 P* = smallest homogenous region to
r,/ which fracture criterion, Eq. 10,
= parameters in Eqs 29 and 30
describing the shape of the plastic applies
zone a = normal tensile stress at infinity
= linear elastic strain energy re- (gross-section stress)
9
lease rate cr~r = mean normal tensile stress across
k = yield strength in shear net section
K, = stress-singularity or intensity ~rr = yield strength under combined
factor for crack-opening mode stress

IONS AND SUBGRAIN GRAINS ELASTIC SPECIMEN


ELECTRON BOUNDARY INCLUSIONS PLASTIC OR
CLOUD PRECIPITATES VOI DS FIELD coMPONENT

L,o-

DISLOCATIONS SUBGRAI N LARGE ELASTIC


SLIP BAND PLASTIC, SINGULARITY
STRAINS

,, PLANE STRAIN

]1
- 'q PLANE S T R E S S ~

FIO. 1--Schematic Illustrations of Fracture Veiwed at Different Scales. For the Stress State
it Is Assumed the Specimen or Component Thickness Is One Millimeter.

KxIX = stress-singularity factor for shear ~rs = yield strength in uniaxial tension
parallel to the leading edge of r = shear stress at infinity in Mode
the crack I I I (gross-section stress)
rr = crack-size plasticity correction r~r = net-section shear stress in Mode
for the linear elastic model III.
r = radial coordinate from the crack
tip KINDS OF ELASTIC A N D PLASTIC S T R E S S
R = radial coordinate to boundary of
AND STRAIN FIELDS
plastic zone
R0 = radial coordinate to boundary of F o r a material of finite yield strength,
plastic zone d~vectly ahead of the
when the dimensions of the crack and
crack
of the component are sufficiently large
W = total width of symmetrical
notched specimen and the applied stress is sufficiently
y = shear strain small, the plastic zone m a y be regarded
7 r , ' i ' r = shear strain at yielding and as negligibly small and the simplest
fracture, respectively analytical model is the one which centers

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86 FRACTURE TOUGHNESS TESTING

attention on the elastic stress distribu- larity coefficients, K, are all that is
tion at the crack border. As has been needed to specify completely the stress
shown (1-5), this distribution can be distributions near the border of the
regarded as the sum of the leading terms crack. Consider, for example, the elastic
of the series expansion of each of three stress singularity for Mode III, longi-
stress distributions, one for each of three tudinal (or parallel) shear. Assume the
modes of deformation shown in Fig. 2. crack lies in the left half of the x,z-

MODE'ITr
k
I,

/
/
FIo. 2--Modes of Deformationof a Crack.

Mode I: Tension normal to the faces plane with the leading edge of the crack
of the crack (either plane along the z-axis. Cylindrical polar co-
strain or plane stress), ordinates around the z-axis are also used
Mode 11: Shear normal to the leading with 0 measured from the right half of
edge of the crack (plane the x,z-plane. The shear stress com-
strain or plane stress), ponents are:
Mode III: Shear parallel to the leading
edge of the crack (anti-plane
strain).
0
Aside from additive uniform stress fields, Tr~ ~ (sln ~)KII| [ ........ (1)
three scalar constants, or stress-singu- (2,',')'." ]

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McCLINTOCK AND IRwin ON PnASTICZTYAsPEcTs 87

0.5 MODE I ~6.5 \\

I"'-'"
, , I !, lF "I
t \~ t f I i f I r " , , , I ] i.

l \ f )
I I I I
x,._ / l \ l /
\ /

PLANE PLANE ~ ~ ~"


STRAIN STRESS
03 /
MoDE , ----.,,
// ~_" \ l

"--~\ .-. /l r ~k /1

ELASTIC ELASTIC
0.5 - - ~ P L A S T I C
MODE tit //"
/
/
/
/
I
I
t ! I t ',I I I I I ) !

| s
5 .0

FIG.3--Elastic Stress Singularities of the Different Crack Deformation Modes Viewed in Terms
of Mises Yield-LimitLines. Poisson's Ratio Is Assumed to Be 1/3.
The loci of fixed values of the maximum figurations are available in the litera-
shear stress are simply concentric circles ture.
around the border or leading edge of the The three elastic stress singularities
crack. are illustrated in Fig. 3 by indicating the
The constants, K , are determined by locus of points at which the Mises yield
the size and shape of the part and the criterion would be exceeded if the elastic
applied loads. For instance, for a crack stress distribution were unaffected by
of length 2a in an infinite body, yielding, assuming Poisson's ratio to be
1/3. The difference between the hypo-
KIU = 1"(~ra)11~. . . . . . . . . . . . (2)
thetical plane-strain and plane-stress
where r is the value of ru, remote from loci is not due to the stress components
the crack (gross-section stress). Values in the plane, which are identical, but to
of the K's for other shapes and con- presence or absence of transverse con-

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88 FP.ACTtmE TOUOH~SS TESTING

straint. Of course, yielding affects the intermediate between the plastic-zone


stress distribution outside the plastic size and the crack-length or part size, in
zone and thus modifies the shape of the which the elastic stress singularity is a
plastic zone itself. Such a result from good approximation to the stress, as
the analysis for longitudinal shear (5) shown in Fig. 4.
(Mode I I I ) is shown as a solid line in When the elastic stress distribution
Fig. 3. sets the boundary conditions for the
If the plastic zone is small enough plastic region within it, since the ten-

1 , i , , ' t l

2,5

2s TRAIN DISTRIBUTION~ /~.X/I(

, \ .STRESSAND STRAIN DISTRIBUTIONS


I 1.5 ./~A~ WITH NO PLASTIC FLOW
,~TRESS, \ \
STRAIN
1.0
~ STRESS DISTRIBUTION~'r/k

0.5

I I I I I

~ t 4 s 6 7
RADIUS FROM CRACK BORDER (r/Ro)
FIO. 4--Effect of Yielding upon Stress Near the Crack from Mode III Elastic-Plastic Analysis.
Yielding at Stress k of a Material with Shear Modulus, Translates the Stress Curve Away from
the Crack by the Amount Ro/2, Half the Maximum Extent of the Plastic Zone.

dency for unstable fracture in the pres-


ence of plastic flow turns out to be
relatively independent of how a given
state of applied stress and crack length
was reached, the elastic stress singu-
larities are expected to have unique
values at the onset of unstable fracture.
Thus, the intensity of the elastic stress
singularity can be used to predict the
FIG. 5--Effect of Net Section Width on Plas- fracture of the prototype from the frac-
tic Zone Shape for a Mode III Elastic Singu-
larity of Fixed Intensity. ture of a specimen.
When the crack or the notched speci-
relative to the length of the crack and men is sufficiently small, the plastic zone
to the distance to the next nearest bound- can be so large relative to the size of the
ary of the part, there will still be a region part that there is no intermediate elastic

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~VIcCLINIOCK AND IRWIN ON PI~STICITY ASPECTS 89

PLANE STRAIN PLANE STRESS

F EXTERNAL

i _ GKING

u. / .--"2k

INTERNAL
I

FIG. 6---Slip Line Fields for Fully Pbstic Tension Modes.

PLANE STRAIN

| |

| |
SHEAR

UNKNOWN

|
BAND

TRANSVERSE SHEAR LONGITUDINAL SHEAR


(MODE Tr) (MODE 3~')

FIo. 7--Slip Line Fields for Fully Plastic Shear Modes,

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90 FRACTURE TOUGHNESS TESTING

region where the stress distribution the internally and externally notched
closely resembles the stress singularity plane-strain cases in Fig. 6, the plastic
of Eq 1. This situation is illustrated by flow is fundamentally different as a re-
the noncircular Mode II1 plastic zones sult of the differences in the nearest free
shown in Fig. 5, and is expected as the boundary. With the external notch there
net-section stress for crack propagation is localized strain directly ahead of the
approaches the yield strength. There is a notch; with the internal notch there is
significant interaction between the plas- not. Under plane strain, for the external
tic zone and the boundary of the part, notch there is an infinite strain singu-
so no intermediate elastic region exists larity immediately above and below the
where the stress distribution can be tip of the notch and the equivalent
adequately described by an elastic stress strain in front of the notch is approxi-
singularity. The question now arises as mately (2/~/3) (extension/ligament
to whether there are relatively simple width) (6); whereas for the internal
analytical models for fracture in terms notch the only stain is a shear srtrain
of the next finer-scale point of view, of value unity (equivalent strain =
namely, the plastic stress and strain 1/V'3) along the 45-deg bands running
fields. Such models, if available and off to either side of the tip of the notch
appropriate, might permit prediction of (McClintock, unpublished). Further-
large-scale fracture behavior from tests more, the stress on the net section is
with much smaller specimens than are different, the maximum stress being
needed for tests of the present Kc and (1 -4- lr/2) times higher for the external
KI~ type. Unfortunately, there are as yet notch than for the internal one. Finally,
no data or calculations available for the there is a marked difference between the
plastic strain distribution at the border stress distributions in plane stress (7)
of a sharp crack for the practically im- and plane strain, since under plane stress
portant situation of plane-strain tension, the maximum stress is only 2/~r times
Mode I. In order to gain insight, we shall higher in the externally notched than
therefore turn directly to a number of in the internally notched specimen.
fully plastic configurations, illustrated Under forward shear, only the plane-
in Figs. 6 and 7. strain externally notched case has been
The chief characteristic of fully plastic solved (8). For the internally notched
flow which distinguishes it from elastic specimen some ~welve different flow
deformation is the fact that a stress or fields were considered and disproved by
strain field cannot gradually die out, but Walter (9). The result for longitudinal
must extend alt the way from one free shear (Mode III) can be readily proven
boundary to another. In mathematical from the uniqueness and rigidity theo-
terms, this is a consequence of the fact rems of limit analysis, or can be taken
that the governing equations are hyper- as the limiting case of the elastic-plastic
bolic rather than elliptic. Roughly, the solution discussed above (5). The primary
difference is analogous to the difference result from study of these shear fields,
between supersonic and subsonic flow. along with plane-stress tension, is that
The practical consequence of this differ- theoretically the plastic deformation is
ence is that in linear elasticity, the char- confined to thin bands, with a resulting
acter of a crack border stress singularity intense strain concentration. In actual
is not influenced, except in magnitude, fact, a small amount of strain hardening
by the presence or shape of the nearest will "wash out" this high strain con-
free boundary. However, as shown by centration (10). Thus, in contrast to

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MCCLINTOCK AND IRWIN ON PLASTICITY ASPECTS 91

elastic problems, the material will mark- of the laboratory specimen prior to frac-
edly influence the shape of the strain ture, the change in constraint may
singularity through its strain-hardening change the local fracture conditions
characteristics. This effect is least evi- quantitatively or even qualitatively.
dent in the plane-strain tensile mode. From such test results, determination of
Despite the complexities indicated the size of the enclosed plastic zone
above, a certain degree of unification can which must, conceptually, develop in a
be gained from a study of specimens large enough specimen is indirect and
which become fully plastic. In tensile uncertain. This information is needed to
fracture, the extremes of fully plastic predict fracture behavior for a wide
behavior correspond to ultimate strength range of crack sizes in a large service
measurements under various degrees of component.
biaxiality in plane stress or plane strain. As an escape from the disadvantage
With suitable allowance for strain hard- of small specimen, Wells has suggested
ening, the load necessary for fracture using measurements of crack-opening
can be predicted as the load necessary displacement (11). The suggestion of
for plastic instability. Wells is essentially equivalent to assum-
The toughness of a service component ing that an intensity of plastic strain,
which will fracture only after the de- critical for fracture, exists adjacent to
velopment of fully plastic instability is the crack border which can be predicted
substantial and probably adequate. from measurements of the tensile direc-
However, fully plastic behavior in the tion movement of the crack surfaces.
laboratory specimen does not permit us If deviations from the assumptions basic
to predict that fully plastic behavior to this proposal were not serious (no
will occur in a service component at differences in constraint between the
much larger scale. Dimensional influ- enclosed and fully plastic cases and
ences of various kinds are involved. The similar strain distributions), knowledge
largest one is the size of the enclosed of the crack-opening displacement might
plastic zone. Others are related to the be used with some confidence to predict
mechanisms at the tip of the crack which the size of the enclosed plastic zone
limit the size of the plastic zone. These which would be expected in a large
may include the inhomogeneous nature enough specimen. Wells's idea deserves
of plastic flow (slip lines or subgrains) further study and can be better explained
or statistical effects (flaw probability). at a later point in this paper.
There are still other dimensional factors
at smaller scale. If the crack inserted in LONGITUDINAL (OR PARALLEL) SHEAR,
the test sample is comparable in size to M O D E III
the cracks of interest in the service As noted above, there is no analytical
component, then the influence upon model of elastic-plastic deformation
crack extension of small dimensional near a M o d e I or M o d e II crack. Turn-
factors, including flaws, is modeled in ing to fully plastic situations is of limited
the test specimen closely enough for help because the connection from these
practical purposes. If the crack in the strain patterns to those in the enclosed
laboratory specimen propagates with plastic zone has not been developed.
an enclosed plastic zone, then a similar These facts greatly enhance the utility
behavior can be predicted in the larger of elastic-plastic analysis for the third
service component. However, when gen- mode, in which all displacements are
eral yielding occurs across the net section parallel to the crack border.

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92 FRACTV~. T o u o m ~ s s TESTISO

Thorough study of the Mode III concentration, and the change in stress
elastic-plastic analytical model is sup- direction as well as the incremental
ported by the following points: changes of plastic strain as the crack
advances. Consideration of the model
I. Problems can be solved in relatively
and of its limitations suggests the follow-
simple terms without loss of continuity
ing procedure for obtaining the Mode I
between the small, enclosed plastic-zone
analog from the Mode I n elastic-plastic
situation and the point of development
solution:
of fully plastic flow (4).
2. The mathematical analysis can be Applied gross-section stress
checked and supplemented by experi- T "') G
mental observations (12). Yield strength
3. Derivation of the plane-stress ten- k " ' ~ 0"y
sile-mode plastic-zone correction factor Modulus of elasticity
by assuming this factor analogous to the /~ --+ F,
same factor for Mode III, shows agree- Stress-singularity factor
ment with observations (13). Kin ~ Kx
4. With the aid of appropriate frac- Strain-energy release rate
ture criteria, the Mode III considera- 2tt~m ~ E~r (plane stress)
tions permit descriptive representation E
of instability after varying amounts of --~ 1 - - ~ ~i (plane strain)
stable crack growth (14).
5. Increasing use of th~ Mode 111 We now turn to a summary of prin-
elastic-plastic solutions to assist repre- cipal characteristics and results for the
sentation and analysis of experimental elastic-plastic crack under longitudinal
results can be expected until equally shear.
convenient and versatile analysis models
Initial Strain Distribution:
are developed which are specific to the
opening mode. For zero strain hardening, the strain
at a point r is given in terms of the radius
The applicability of Mode III solu- through that point from the crack tip
tions to tensile fracture by analogy has to the elastic-plastic boundary R, the
been discussed by McClintock (13,15) for yield strength in shear k, and the shear
plane stress and for plane strain of an modulus u, by:
anisotropic material with no displace-
ment in the x-direction. The analogies "r,e = (k/#)R/r, "r,r ---- 0 . . . . . . . (3)
hold good only when the ratio of yield
Note the increased strain concentration
strength to modulus is low enough so
in the plastic region. The strain varies
that displacements are negligible com-
inversely with the radius rather than as
pared with the size of the plastic zone.
its square root as it does in the elastic
Furthermore, the transverse stress com-
case. When the plastic zone lies in a
ponents are indeterminate in the model
small enough region to be enclosed by
so that effects of triaxial tension on the
an elastic stress singularity of the type
local ductility of the material are not
of Eqs t and 2, the elastic-plastic bound-
predicted. Within these limitations, the
ary is circular and its radial coordinate
analogy suggests a number of phenom-
from the crack tip is given in terms of
ena easily recognized in the tensile
the radius for 0 = 0 by:
problem, such as the occurrence of local
yielding, the increased plastic strain R =ffi Ro co~ 0 . . . . . . . . . . . . (4)

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MCCLINTOCK AND IRWIN ON PLASTICITYASPECTS 93

It was noted by Irwin and Koskinen other hand, a substantial slow crack
(16) that this result can be easily verified, extension usually precedes instability in
since both stress components on the crack toughness tests of high-strength
boundary of the plastic zone, required metals when the crack-border plastic
by equilibrium and the yield criterion zone is large relative to the plate thick-
within the plastic zone, exactly match ness (17,18). At a later point it will be
the elastic stress components expected shown that a tendency to either condi-
from a crack whose tip is at the center tion can be represented by appropriate
of the plastic zone rather than on its tensile analogs of Mode III problems.
circumference (see Fig. 3). Furthermore,
Loading Without Crack Growth:
the displacements on the elastic-plastic
boundary define the displacements Let us first examine the relationship
throughout the plastic zone because between the plastic-deformation work in
there is no radial shear strain. the crack-border plastic zone and the
At higher stress levels, as the plastic- strain energy release rate from the com-
zone size, R0, approaches the crack pletely linear elastic field, ~ i u , during
length or approaches a second free sur- the stage prior to movement of the
face, the plastic zone elongates, as shown crack. In a unit thickness volume element,
by the calculations of Koskinen cross- r dr dO, within the plastic zone, the in-
plotted in Fig. 5. Thus, for the same elastic deformation work is given by:
maximum extent of the plastic zone, the
strain is more concentrated on the mid- d• =* --
/z
-- 1 rdrdO ...... (5)
plane when the net-section stress is large
than when it is small. This aspect sug- The integral of df~ over the plastic zone
gests that a one-parameter character- gives the result
ization of the plastic zone will lose
accuracy as the net-section stress ap- = ~ a .............. (6)
proaches the yield strength.
General Aspects of Stable and Unstable where A is the area of the zone. If the
Crack Extension: zone is relatively small so that the shape
is circular, and we let rr = R0/2 be the
In the absence of any crack extension, radius of this circle,
the load must rise until fully plastic
yielding develops. Thus the occurrence k2
-- - ,-r r 2. . . . . . . . . . . . . . (7)
of a maximum load point prior to general /z
yielding of the net section is due to
actual crack extension. For the usual For a Mode I I I plastic zone of this kind,
crack toughness specimens, assuming we know, from the elastic-plastic solu-
constant time rate of separation of the tion, that
grips, a small crack speed of the order KIII 2 /z~tii to'
of specimen width divided by loading 21rk~ lrk~
time is sufficient for the attainment of
maximum load and the start of load As the plastic zone grows to the size
relaxation (17). In fracture tests with R0, the position of the crack border for
essentially plane strain at the crack purposes of linear elastic analysis ad-
border, observations suggest a relatively vances by the amount, r r .
abrupt onset of fast fracture from a In linear elastic fracture mechanics,
stationary crack border (18,19). On the an extension movement, a, of the crack

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94 FRACTURE TOUGHNESS TESTING

border in the presence of a crack-exten- Integration and rearrangement with the


sion force, 9, implies a stress field energy aid of Eqs 1, 7, and 8 confirm the iden-
loss (per unit of thickness or crack- tity.
border length) equal to ag. The analysis The fact that energy is consumed in
provided in Irwin's definition of ~ (3) the nonlinear dissipation process at a
represented o~3 in terms of the release rate which is twice the linear elastic 9
movement of closure forces along the value was initially surprising to the
segment a. This analysis has been shown authors. Although the result has been
to be mathematically equivalent to demonstrated only for the growth of the
representation of the stress field energy plastic zone prior to crack motion, it
loss in terms of the load and load dis- appears that in general the linear elastic
placement for the entire specimen analysis does not provide the total stress
(34,35). field energy loss. Thus, a degree of un-
From Eqs 7 and 8, ~ equals ~mrr, certainty relative to the energy balance
which suggests the movement, r r , of local to the plastic zone is inherent in
the force, ~ m , provides the stress field the linear elastic analysis. For this reason
energy loss utilized in the plastic work. the physical interpretation of K is some-
However, ~m is not constant during what easier to discuss than that of 9.
loading, but increases in proportion to In terms of interests central to this
r r . Thus, only 89 or half the neces- paper, this result enhances the advamage
sary supply of strain energy, can be of representing initiation, growth, and
found from study of the change in com- unstable acceleration of crack extension
pliance of the specimen in terms of in terms of separation mechanisms oc-
linear elastic analysis. That is, only half curring at a finer scale. This problem
the necessary strain energy would go will be discussed next.
out of the linear elastic strain field at
its singularity as the crack advanced by
Fracture Criteria:
r r . (This energy flux represents the Within the plastic zone in Mode II1,
surface energy in a Griffith-theory treat- a fracture criterion cannot be based
ment.) But the energy available for upon stress because increasing the load
plastic work is that which flows across merely enlarges the plastic zone, within
the elastic-plastic boundary in the actual which the stress level stays at the con-
material. This latter flux consists of not stant value, k. (In other modes, of
only the energy flux out through the course, different states of stress would
singularity, but also the increase in the modify the fracture criterion.) A fracture
elastic energy in that region of the linear criterion cannot be based upon strain
elastic strain field which is plastic in the alone because the analysis indicates an
actual case. The total flux across the infinite plastic strain at the crack border,
elastic-plastic boundary must equal the no matter how little the applied stress.
plastic work plus the residual elastic The limits of continuum analysis
energy of the region within the plastic suggested by Fig. 1 may now be con-
zone. To verify this, the energy balance sidered. Presumably the average strain,
can be written as: from the crack border across the small
1 f rr,* + ra, 2 dA
region containing the micro-separation
processes, is finite, and strains larger
than this in the analytical model do not
possess physical significance. Further-
=
f da +
fk,
~ eA . . . . . (9)
more, from physical considerations, frac-

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~cCLINTOCK AND IRWIN ON PLASTICITY ASPECTS 95

ture in this region will depend only on crack border reaches the critical value,
the stress and strain in this region. Ex- 7 v , which in a brittle elastic material is
ternal actions will be felt only insofar as rF/#. it is assumed the micro-separation
they affect the local stress and strain. process occurs on an atomic scale, so
The average strain in the plastic zone p, = b, the lattice spacing in a crystal
within a small distance, p,, from the or the network spacing in glass. The
crack border might therefore be estab- fracture stress, r e , can be assumed to
lished as a fracture criterion. This is have an ideally high value, say equal to
equivalent to considering a critical dis- ~/2~r.
placement across a small element of The critical stress singularity can now
width, p,, within the plastic zone. While be estimated, since, from Eq. 1,
such a criterion m a y appear similar to
Kill ~
the displacement criterion suggested re- r = 2~rr* ' or Kiiic2 = 2,rb(g/2,r)~..(11)
cently by a number of writers (20,21,22),
the displacement alone is not sufficient The surface energy, T, which is half
for a fracture criterion without stating the critical strain energy release rate,
in how small a region the fracture dis- ~ i m , m a y also be estimated:
placements are concentrated. Alterna-
tively, we could use the strain, ~'e, at a T = ~mc/2 = KIIIc2/4/a -- bla/8rr.. (12)
given point (r = p,, 0 = 0) as a fracture
For iron, taking b = 3 A and ~ = 11 X
criterion (14) :
10 e psi gives 900 ergs/cm =, compared
F r a c t u r e w h e n 7 -- "re a t r = p . . . . (10) to the 2400 ergs/cm = for tension esti-
This choice is analytically simpler and mated by Gilman (za), a plausible out-
come under the assumptions.
will be used in this discussion. Note that
this criterion m a y be applied to cases In this illustration, as in others where
the plastic or nonlinear zone is com-
where strain is uniform over a region
parable in size to the structural size,
large compared with the structural size,
p,, as in the ordinary torsion test, where p,, a fracture criterion such as E q 10
is equivalent to the Griffith crack theory.
~'e can be observed directly. The struc-
tural size, p,, is regarded here as the However, with plastic flow, the fracture
size set by grain size, inclusion spacing, work rate m a y be much greater than
theoretical estimates of surface energy
or slip-line spacing at which one can no
longer regard the material as a homo- for the solid state of the material. We
therefore turn to the plastic case, con-
geneous plastic continuum but must
sidering first the initiation of cracking.
turn to the next smaller scale model of
Fig. 1. Initiation of Crack Extension:
To illustrate this fracture criterion,
let us first apply it to the more familiar Cracking should initiate when the
case of fracture in a brittle, linearly strain distribution of Eq 3 is such as to
elastic material. Here the stress aspect satisfy the fracture criterion of Eq 10:
is significant and the criterion could be ~le = ~rRojp, ,. ......... (13)
based on either stress or strain. Prac-
tically, such Mode I I I fractures are not where the yield strain, ~ r -- k/#, is
observed, but the tensile analogy m a y introduced for convenience. For low
make such a treatment of interest. We stress levels, the extent of the plastic
assume fracture occurs when the strain zone for initiation, Rcl, can be expressed
at a certain small distance, p,, from the in terms of the stress singularity from

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96 FRACTURE TOUGHNESS TESTING

Eq 8 and the critical value of the stress estimate the plastic-zone size by in-
singularity for fracture can be found: creasing amounts as r / k increases above
0.5, and Eq 16 is implicit. We present
Km~ = k(lrRoi) 112 = (~rp,'re/'rr) 1/~. ..(14)
here an alternative representation, which
At higher stress levels these expressions is closer to theoretical solutions of the
require modification. A first approxima- problem (4,S,22). This is found by mul-
tion can be obtained by assuming that tiplying the expression for low stress
the elastic stress field is that correspond- applied to an infinite plate by a series of
ing to the crack in a purely elastic solid factors, the first of which accounts for
whose extent is greater than the actual the increase in linear elastic stress singu-
crack length, a, by the amount, r r . larity due to the finite width of a plate,

i i , , '

2
' ,EPT//
..~. REA
II
EDGE // 1+15

/CENTER II
NOTCHED
~" I 0

READA?
I I I I
o0.1 Q2 o,s o.4 o.s O0 G2 0.4 0.6 0.8
CRACK HALF LENGTH (~.) APPLIED STRESS (-~)
SPECIMEN WIDTH YIELD STRENGTH

FIG. 8--Plastic Zone Correction Factor {or Fro. g--Plastic Zone Correction Factor for
Finite Specimen Width, F ~r (Deduced from Ref. High Stress Level in Infinite Solid, F, (Deduced
24, and Eqs 4 and 11 or 19). from Refs.4, 14, or 22).

Combination of Eqs 2 and 8 then leads while the second accounts for the in-
to crease in radius of plastic zone due to
increased stress in a plate of infinite
(G JI- r Y ) T 2 •T2/Zk 2 - -
width. At the stress level, r / k --- W /
rr - -2k* ' or r r 1~ .~/2k,'" (15)
(W - 2a), equilibrium requires that the
In order to allow for the increase of the plastic zone should extend all across the
elastic singularity due to finite plate specimen so that:
width, the above equation can be modi-
fied (24) to:

27try
( ~ +--~ (k)'tan
- ~ - r ~ ' " ( 1 6 ) WW] Since this is not predicted by the above
factors, a final correction is introduced
Equations 15 and 16 tend to under- to make up the difference, giving:

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McCLINTOCK AND IRWIN ON PLASTICITY ASPECTS 97

1.0 1 I I I When fracture data are represented


in terms of K values, it seems inappro-
"~Q8"
LL~
priate to employ a complex procedure
to allow for the plastic zone because the
~Q6' linear elastic viewpoint tends to lose
meaning in the approach toward condi-

i/
3--~o., tions of general yielding. Correspond-
ingly, the equation for/C 2 from Ref (24)
~oct2 (shown here in the form of Eq 16) does
not accurately predict the size of the
o 02 0.~ O.6 Q8 plastic zone at high stress levels. Further-
LOAD , ( q:W ~ more, effects due to alteration of the
FULLYPLASTICLOAD \k(W-2o)/
plastic zone, when growth of the plastic
FIO. 10--Plastic Zone Correction Factor for zone is accompanied by slow crack ex-
Close Approach to Fully Plastic Yielding, F/p =
I - {1 - [(~/k)-(VC/Vr 2a)lq~l~. tension (discussed in the next section)

I I I I
I'01
EQ 18 AND FIG.7,8,
---- EQ 16 /
o KOSKINEM~p/,

I-..
,,, _<20.4
z3:
NO,,
_J
c ~0.2

gz
0 i i I
o oJ' 0.4 o.s o.e i.o
NET STRESS/YIELD STRENGTH (%N/k)
FIG. ll--Plastie Zone Size from Eq 18 in Comparison with Eq 16 for W - 4a. Points Are from
Koskinen (5). For W -- 4a, r -- 2,-.

have not been taken into account. How-


Ro == a FwF,
ever, one can note that modifications of
the rr correction of Ref (24), for purposes
+ L~(ZTE,F/g of empirical extension of the K value
The required factors are given in Figs. representation into the high stress level
8, 9, and 10. These two methods are range, are possible. For such purposes,
compared with the numerical results for the rr correction might be replaced by
crack half way through in Fig. 11. any allowance for plastic yielding that

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98 FRACTURE TOIIO~NESS TESTING

t I

REQUIRED STRAIN INCREMENT


FOR FURTHER CRACK GROWTH
Z
STRAIN INCREMENT
tw
F- ~kt- DUE TO CRACK GROWTH
o~
kx
r
.2
t~

.-&-, I
Re -F
- " -lk,2~
-- d(a+R o)

T COORDINATE
FIG. 12--Strain Increments Related to Crack Growth.

BOUNDARY

Y III I/

/
i...'//

ca
FIO. 13--Change in Stress Direction Related to Crack Growth.

seems more suitable. We will return to at first hope t h a t an understanding


this topic later. could be obtained directly from energy
considerations based on estimates of the
Crack Growth and Instability: work done in the plastic zone. If this
I n studying crack growth, one might work were calculated using the strain

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M C C L I N T O C K AND IRWIN ON PLASTICITY ASPECTS 99

field of the static crack, there would be would be less than the fracture strain,
no account taken of the plastic strain no further cracking would occur.
due to crack growth itself. An examina- Actually, however, there is a strain
tion of the energy balance, therefore, due to the advance of the crack. The
requires study of a moving crack to solution to the mechanics problem of a
the point where the maximum load is crack growing in Mode I I I shear in-
reached, so that the energy required dicates that at a particular point in the
can be supplied solely from the sur- plastic zone, the direction of the stress
rounding field. The condition for a load changes, as indicated in Fig. 13. This
maximum is governed in part by the produces an elastic strain which, through
conditions for local fracture. Thus it is the compatibility equations, enforces a
necessary to treat the problem so that plastic strain. From the mechanics of
the relation of stress to crack growth is the problem, it turns out that, if the

I I I !

I L

.,,...
"LNUMERICAL
CALCULATIONS
.L,./..EQ. 20
W

o.l ",,..,.

th ",. I0
W
-i
n
12..

I l I I ] I I I I f I I 1 J I I l I I I
0'01 i0 lOZ Ib 3 1'04 I0 ~ Ib 6
CRACK LENGTH (C/p_)
FIG. 14--Stress Level for Instability of Mode III Cracks after Increasing Loads and Crack
Growth. Upper and Lower Bounds to the Unstable Crack Size Are Shown by Vertical Ticks.

controlled by a specific fracture condi- crack is currently at the point a, then


tion such as Eq 10. The illustration the increment of plastic strain, d3,p, at a
which follows assumes a central crack point x ahead of the crack, due to an
in a specimen with the crack length advance of the crack by da, is (13,14,2S):
negligible in comparison with specimen
dimensions. dT~= x--a'r---~r{l +R~ +ln x--a
R~ }
Consider first whether the fracture
criterion of Eq 10 would be satisfied if At first, as indicated by the dashed line
the crack were to advance by an amount, in Fig. 12, this strain increment is not
da, without any plastic strain due to the enough to offset a decrease in strain due
advance of the crack. The strain at the to the fact that the crack is advancing
point, p,, ahead of the crack border into material with less prior strain.
would be that found from the strain Therefore, an additional increase in ap-
distribution of Eq 3, indicated by the plied stress is required. When this in-
solid line in Fig. 12. Since this strain crease has been enough to satisfy the

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100 FRACTURE TOUGHNESSTESTING

fracture criterion, an additional incre- notch. Typically, the crack-growth regioh


ment of fracture will occur, and so on. in which the shear fracture obtains its
The resulting integral equations are in- characteristic running crack size is essen-
volved and require precise numerical tially the magnitude of slow or stable
integration, carried out along the general cracking. During the stable period, the
lines of Ref. (14) but with the corrected degree of plane strain is decreasing and
form for the strain due to crack growth, the corresponding increase of oblique
Eq 19, from Ref. (13). Detail regarding shear separation must be regarded as
the numerical techniques is given in Ref. contributing in a major way to the re-
(26). The results are presented in Fig. 14. straint against instability in the onset of
As noted in preliminary calculations, fast fracture. For these reasons, a close
and as observed in foil testing (14), the quantitative comparison of the Mode III
stress level required to make a crack fracture with Kc tests in the transition
propagate at first increases rapidly, but range is not advisable. It is interesting to
then more slowly until eventually a note, however, that the ink stain slow
maximum stress is reached. At this point, crack indications show a stable crack
the crack becomes unstable. At low stress extension which is of the order of the
levels, the crack length at instability ap- formally estimated plastic-zone size at
proaches an inverse square root depend- instability, Roc, a result consistent with
ence on the applied stress. This is ex- the lower ranges of ductility shown in
pected since the plastic zone is then Fig. 14. The corresponding value of 10
surrounded by a characteristic elastic for "rpv/~'r may seem low, but is con-
stress field, described except near the sistent with the recently developed
plastic zone by Eq 1 as shown on Fig. 4. quantitative criterion for ductile fracture
Both the crack length at instability and by the growth of holes when there is a
the amount of crack growth to instability high state of triaxial tension (as in Mode
depend markedly on the ductility of the I plane strain) in front of a crack (27).
material. At high stress levels, the ap- As a second illustration of these results,
plied stress is, of course, limited by the Krafft (28) has noted that the value of
yield strength. K~c for tests of a given material at differ-
A careful examination of the curve for ent temperatures or strain rates appears
a given local ductility, (3,rV/Tr), shows to vary in proportion to the strain-hard-
the amount of crack growth prior to ening exponent, n. This might be ex-
instability to be higher at lower stress pected for two reasons. First, for viscous
levels, although it may not at first appear materials, instability (crack growth with
this way from the logarithmic scale. constant load) does not occur, since the
One would like to apply these results to strain distribution in a viscous material
tension fracture testing in which the frac- is identical to that in an elastic material
ture contains a central region of plane- and as a result there is no strain incre-
strain separation. Investigations of K~ ment due to crack growth itself. Since a
have naturally centered upon metals viscous material is in some ways analo-
with the highest strength consistent with gous to a strongly strain-hardening
a moderate degree of toughness. As a material, from the mechanics alone one
result, a high proportion of the Kc testing would expect a lower tendency to in-
experience is with tests in the fracture stability. Second, if fracture is associated
mode transition range, a region in which with the growth of holes, then the frac-
there is a gradual development of shear ture strain itself increases strongly with
lips from the corners of the sharp starting n (27). A quantitative development of

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MCCLINTOCK AND IRWIN ON PLASTICITY ASPECTS 101

these ideas is not possible at this stage equal in magnitude to the linear strain at
due to the geometrical complications dis- the ideal strength of the material,
cussed above. r~/# = 1/27r. For such small ductilities,
Because of the cost and inconvenience the apparent surface energy, T, is almost
of numerical calculations, it would be de- identical to that obtained by applying
sirable to have a closed-form solution for the fracture criterion to a linear elastic
the crack growth plotted in Fig. 14. For- solid, Eq 12:
tunately, conditions for final instability
b/,
are evaluated more easily than those for T = ~ exp [--1 + (1 + 2-reP/yr) v2]
growth, since the condition of instability
is that the rate of increase of stress be- 2.08bu
- ,.(23)
comes zero. It also turns out that one 16~
may assume that the size of the plastic
zone is nearly constant as the highly From Eqs 21 and 8, for ductile mate-
strained plastic region just ahead of the rials at low stress levels,
crack sweeps over the point in question. ~rpsk~
The validity of this approximation is ~m~ = - ~ exp [--1 + (23,~P/3,r)t/*]..(24)
checked by a detailed study of the equa-
tions or by comparing the results of the Note that again Gmc denotes not the
analysis with Fig. 14. The resulting ex- actual strain energy release rate, but
pression for the radius of the plastic zone rather that from a linearly elastic one
at instability is given in terms of its ratio having the same stress distribution at
to the crack half-length, P = Re~a, large distances from the plastic zone.
where P is a function of the stress level Equation 21 shows that at low stress
alone, in a plate of infinite width (13): levels the condition for instability can be
characterized in terms of the size of the
Rolll. ---- p. exp l--(1 + P) plastic zone. R0mc can, therefore, serve
+ [(1 + p)2 + 2(-~/v,.)]'/2} .(20) as an alternate to Kin, in describing the
tendency to unstable cracking. At high
For low stress levels, the ratio of the stress levels, however, Eq 20 shows that
radius of the plastic zone to the crack R0 depends not only on p, and ~ r , but
length will be small compared with unity, also on the stress ratio (through the plas-
and for ductile materials the plastic tic-zone ratio, P). Alternatively, rewrit-
strain at fracture will be large compared ing Eq (20) in terms of critical crack
with the yield strain, giving length, the material characteristics, p,
R0m, = a(r/k)~ and ~/j,, cannot be separated from the
test configuration in terms of a and P.
= p, exp [ -- 1 + (2-rrP/-rr) ln] ......... (21)
There is no one parameter, corresponding
For completely brittle materials with to Kmc or R0m~ (in low stress applica-
3,e ~ = 0, p, = b, Eq 20 becomes tions), which can correlate behavior over
a large variety of crack lengths at high
RoIH, = b . . . . . . . . . . . . . (22)
stress level. Thus, to extend the analysis
which is identical to the condition for of fracture (following slow crack growth)
initiation, since there is no stable crack beyond regions representable in terms of
growth in completely brittle materials. a linear elastic model, it is not only
For actual materials, it might be a better reasonable but necessary to base the
approximation to the nonlinear elastic fracture criterion upon characteristics of
force curves to assume a "plastic" strain the small critical region of the plastic

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102 FRACTURE TOUGHNESS TESTING

"" I ' I I 1

I~ vR~
(I) ("K ,,)2 = ~2 w tan + 2W ].
1.3--

"~- = 0 . 5 , R o from Eq. 18 and F i g . 8, 9

9 2 -I/'2
(2) (" g ") 2 =

i.2--
|IKII
KASTM

I.I -

I ~ I i I
' 0.8 0.9 I.o
TN/k
FIG. IS--Observations of High Stress Level Trend of Kc Values (x) Are Shown in Relation to a
Prediction, Curve (1), from Mode III Analysis Using Equation (18). Also Shown, Curve (g), Is a
Lower Bound on the Amount of the Trend Which Can Be Expected to Disappear When K~ Is
Based upon ComplianceObservations.

zone, in consistency with the local nature specimen size with 2ao/W held constant,
of the separation process. using 0.05-in. thick 7075-T6 aluminum,
shown in Fig. 2 of Ref (17). The values
Empirical Trend of High Stress Level K~ of 2a/W at the onset of instability were
Results: in the range of 0.4 to 0.5, and the latter
Under certain conditions (17), values figure was adopted in this comparison.
of K, measured as suggested in Ref. (24) Calculations were made using Figs. 8,
are not constant when the net-section 9, and 10 and Eq 18. The results, as
stress at the onset of unstable cracking, shown by Curve 1 in Fig. 15, indicate
an, exceeds 0.8 ~rs. In Fig. 15, the corrections of the right order result if we
points marked with an x represent the simply expand the r~ plastic-zone cor-
correction factors which would be neces- rection of Ref (24) in proportion to R0
sary to eliminate the high stress level from the Mode I I I analysis.
trend found in a study of the effect of In crack toughness testing of the Kc

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MCCLINTOCK AND IRWIN ON PLASTICITY ASPECTS 103

and K~r type, measurements of displace- zone upon displacements by placing the
ments near the crack or near the loading mathematical end of the linear elastic
points can be used along with a calibra- crack well beyond the center of gravity
tion to determine the effective crack size of the plastic-zone area. Both curves
(31). This procedure contains an inherent would be elevated somewhat if calculated
adjustment for the plastic zone in that for the value 2a = 0.4W of the data
the "apparent compliance" (reciprocal of rather than for 2a = 0.5W. Curves 1 and
the secant modulus) is increased by 2 furnish crude upper and lower bound
stress relaxation in the plastic zone. This estimates of the effect of using apparent
form of correcting for the plastic zone compliance to provide the effective crack
may differ appreciably from the rr cor- size for a linear elastic computation of K.
rection procedure of Ref (24) at high The correction factors of Figs. 8, 9,
stress levels. Rough estimates based upon and 10 were also applied to the data given
in Figs. 1 and 2 of Ref (29), as shown in
400 -- o, r I I I I I Fig. 16. Apparently, for small cracks in
4340, TS = 2 2 3 ksi large sheets (2a/W < 0.25) the fully
o
o plastic factors should not be applied. It
300 | o must be borne in mind that these correc-
tion techniques, applied to Mode I, are
empirical in nature. Nevertheless, so long
- 200 as test results show constancy of the
critical K values extending across from
2219-T87, TS-'69 ksi
the low net section stress range, critical
Z
"' I00
~o O e o o K values determined at high stress level
r
retain a very real physical meaning.
Crack-Opening Considerations:
0 I II I l ' I
0 2 4 6 From the Mode III elastic-plastic
GRITIGAL GRACK LENGTH (a) in. solution, the crack opening, 2n, at r =
FIG. 16--Critical Stress Singularityfrom Data 0 is:
of Ref. (29) CalculatedAccording to Figs. 7 and 8.
27 =
[~ -", 1/ '2 "y,o rdO =
k f "n
- RdO.. (25)
Mode III elastic-plastic analysis suggest IZ a - r / 2

that use of the "apparent compliance"


For the circular plastic zone, R = Ro
method should reduce the magnitude of
cos 8, and
the high stress level trend in K, measure-
ments. 2kRo
27 . . . . . . . . . . . . . . (26)
For Curve 2 of Fig. 15, values of K Iz
were estimated from the Mode III
analysis crack-opening displacement, 7. From Eq 8, the strain energy release,
Curve 2 assumes the effective crack size g i n , is related to the crack opening by
would be estimated from observation of f
crack-opening displacement at the lead- g m = ~ k(2~). . . . . . . . . . . (27)
ing edge of the real crack. At this position
the high stress level stretch of the plastic The tensile analog is
zone in the x-direction has a minimum
influence upon displacements. Curve 1
-~ 4 vr(2n) . . . . . . . . . . . (28)
overestimates the effect of the plastic

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104 FRACTURE TOUGHNESS TESTING

Neglecting the difference between k Ror-f


2,7 = . ........... (30)
~/4 and unity, one can interpret this /z
expression as indicating that 27 times
the yield stress provides a measure of where ] is the average value of f in the
the work rate for crack extension. Wells range - r / 2 to 7r/2. From Koskinen's
pointed out this interpretation (11). graphs (5), ] decreases as the plastic zone
Assuming the indicated proportionality elongates, as may be seen from the
might continue to hold when the plastic strain distributions in Fig. 17.
zone was comparatively large and even If the average radius of the plastic
for general yielding, Wells suggested zone were a constant fraction of R0,
that measurements of the plastic crack- then since R0 determines the local strain
opening displacement should be studied according to Eq 3, the displacement

9ol
4dl\ \\\ K (W:2a)

i'Y90LsTRAIN_/4 V,.. 1 ~"

Fro. 17--Strain Localization at High Stress Levels from Ref. 5, Expressed in Generalized Form.

as a possible means for permitting crack fracture criterion would be equivalent


toughness determinations using speci- to that based on the strain at a small
mens of relatively small size. This hy- distance, p,, from the crack border.
pothesis would be necessarily valid if Since ] is not constant, these two criteria
the stress and strain in front of the are not equivalent at different stress
crack were always the same for the levels. An enhancement of this difference
same crack opening. would be expected when the fully plastic
Consider next the expression for the zone is not confined to a slit as in Mode
crack opening, 2n, in Mode III analysis III deformation, but tends to spread out
when the plastic zone is no longer cir- laterally, as in plane-strain Mode I
cular. If we write deformation. Experimental data per-
mitting a comparison of these two criteria
R == Rof(O) . . . . . . . . . . . . (29)
would be quite helpful. For the displace-
then ment criterion, the data would be the

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MCCLII~OCK AND IRWIN ON PLASTICITYASPECTS 105

displacements at the crack border. For 27 = 2a,Vk# . . . . . . . . . . . (31)


the fracture strain and structural size, For unloading from rmax,
the data would be the reduction of area
of unnotched specimens, the effect of 27 = 2arm~x2/kl~ Jr 2 a ( r m ~ - ,)~/(2k)#..(32)
triaxial stress on fracture strain, and For reloading, from r = 0,
micrographs of the structure. In addition,
2,7 = a r ~ , . 2 / k # + 2 a r / ( 2 k ) # . . . . . (33)
it would be desirable to report yield
strength, tensile strength, and uniform At the face of the specimen, the elastic-
elongation so that a reasonable approxi- plastic displacements are found from the
mation to the stress-strain curve can be elastic solution for a crack whose length
obtained. is rr greater than the actual crack length,
| I 1 I ! I I

0.6"

BORDER~
0.5"

~0.4

~ Q3
o 0.2-
t.~

P_

0
0 0.2 0.4 Q6 Q8 1.0 1.2 1.4
DISPLACEMENT ACROSSCRACK(2-q/(ak//.t)
FIG. 18--Displacement Across Crack and Hysteresis Loops for Mode III.
One of the interesting by-products of as noted above. The elastic solution
Eq 26, coupled with the concept that corresponding to Fig. 2 (Mode III) can
unloading can be regarded as superim- be found, for example, by a conformal
posing a reversed load with the yield mapping (30). For the elastic case, with
strength equal to twice the initial yield the origin of coordinates at the crack
strength in shear (4), is a prediction of face, and the x-axis parallel to the crack,
the hysteresis loop on unloading and re- the z-direction displacement, w , turns
loading without crack growth. If the out to be given by:
plastic zone remains circular, the dis-
placement hysteresis loop at the crack w = (r/#) (imaginary part of [(x Jr iy) ~
border can be found from Eqs 26, 8, and - aql/9.. (34)
2, in terms of the applied stress. For
loading, where a must be replaced by a + rr to

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106 FRACTURE TOUGHNESS TESTING

allow for the shift of the stress field due effect and the finite width of the speci-
to plastic strain. The horizontal dis- men would, of course, tend to increase
placement between points at • on the the estimate of the width of the hys-
face of the elastic-plastic solid (Fig. 2) teresis loops. However, the major factor
is then found from Eqs 2 and 8 introducing the large difference may be
the shape of the crack. A loop width as
2w= ( ~ ) ( y ' q - [ a q - a r ' / 2 k ' ] ' ) in small as 30 microinches would not have
been observable within the precision of
Boyle's work. Prior to formation of the

which is of the form,


[
2_rp(Y' q- a2),n 1 -1- 2(y
a ' -2-q-
~
- - ) ~ '" (35) central tongue of plane-strain fracture,
Boyle observed no significant hysteresis.
At the comparison point where the fac-
2w --- (At/u)(1 -b Br~/k ~) . . . . . . (36) tor of 10 difference is noted, a substantial
central region of plane-strain fracture
For unloading, from rma,, had formed. Observations with a thick
2ua = (Arm~x/#)(1 + Brmax2/k2) -- [A(rm~. plate specimen in cyclic loading to lower
stress levels would provide a better
-- r)/u][1 + B(rm~.-- r)~/(2k)*]..(37) comparison because the leading edge of
For reloading, from r = 0, the crack would be in plane strain and
nearly straight through the thickness of
2w, = (3ABr~a.a/4pk *) + (Ar/#) the specimen.
9[1 + Br~/(2k)2].. (38) An interesting result of the deflection
analysis is that the crack does not close
The maximum width of the hysteresis on unloading, but a slight compressive
loop on unloading and reloading occurs stress would close the crack, first at the
at r = rmaz/2: face. Application of these results in their
present form to fatigue cracking is of
3ABrm~x 3
2(~ - w~) some interest. However, it should be
16uk2
noted that the residual stress and strain
3 a2 Tmax 3 behind the growing crack may contribute
16 (yZ q- a~)1/2 k21Z
- - .. (39)
a significant influence and this has not
yet been taken into account.
The displacement hysteresis loops for
both the face of the specimen and the EMPIRICAL REPRESENTATIONOF CRACK-
crack border are shown in Fig. 18, cal- EXTENSION OBSERVATIONS
culated under the assumption that the When the plastic zone is relatively
plastic zone remains circular. At the small, the representation of the test
stress levels shown, this assumption is of observations in terms of K values has a
marginal validity for the initial loading good theoretical basis because in this
phase of the cycle bnt is quite good for case a variety of plausible fracture
the unloading and reloading, since the criteria predict that similar behavior
yield strength in the reverse direction is will occur for similar values of K. The
double the original. Equation 39 for representation of fracture behavior in
rmax/k = 0.56, kip 0.007, a0 = 0.40 = terms of K values becomes increasingly
in., y = 1 in. indicates a hysteresis loop empirical as increases of plastic-zone size
width of 34 X 10-6 in. for the specimens modify the shape of the plastic zone by
of Ref (31), whereas of the order of 300 X significant amounts. Measurements in-
10-6 in. was observed. Any Bauschinger dicate that values of K= and KI= corn-

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MCCLINTOCK AND IRWIN ON PLASTICITYASPECTS 107

puted with the adjustment of a small indicated by Mode I I I analysis, are as


plastic-zone type correction factor re- extreme in the range 0.8 < r~ < k for
main nearly constant over a large frac- small values of 2a/W as in the range
tion of the range of ~ below the yield used in the recommended Kc test speci-
level. mens. Thus the observed success of the
However, in the upper part of this K, computation in the range 0.8 ~rs <
region and certainly above it, the char- r < ~ra, when 2a/W is small, is an
acterization of fracture behavior in empirical success not yet clearly under-
terms of K values is largely an empirical stood.
data representation formality. This is However, empirical representations of
I i j i i t

1,8

1,6 o \
~oo\\
1.484

I.Z'
_5_

1.0

0.8

D--INCHES ~"
i I .JO J I i I t
0'60 Z.O 3.0 4 I0
FIo. 19--Ratio of Net Stress to Yield Stress as a Function of Bar Diameter for Circumferentially
Notched Round Bars of Medium-Strength Steel (~rs ~ 85 ksi). The Solid Curve is Fitted to the
Data Using Adjustment of the Plastic Zone Factor. The Dashed Line Represents a Simple Inverse
Square Root Relationship.
indicated by the fact that when the fracture data in the high stress level
unstable crack length, 2a, in a sharp- range are of value and various methods
notched sheet tension test is less than have been suggested. As will be shown,
one quarter of the specimen width, the when the critical K values for large
test result expressed in terms of Kc specimens are available, the task of
does not drop below the large specimen devising a successful empirical repre-
Kc value until r exceeds errs (17). In sentation of fracture test results is
other words, the elementary plasticity comparatively easy.
correction factor derived from Eq 16 is If values of the yield strength and
much less successful when 2a/W is in ultimate tensile strength are known, then
the recommended range of 0.3 to 0.5 the stress limitations of a specimen of
than when 2a/W is smaller. However, given geometry, as the size is reduced to
the shape changes of the plastic zone, a fully plastic situation, can be estimated

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108 FRACTURE TOUGHNESSTESTING

with sufficient accuracy for most prac- The coefficient 0.233 in Eq 40 is a


tical applications. In a graph of net- function of relative notch depth which
section stress versus specimen size the has a maximum value when the net-
only remaining task is to fair a line from section diameter, d, is nearly D / x / f .
the curve representative of the constant Therefore, the coefficient can be re-
K value range to the upper stress level garded as invariant during small in-
limit across the small specimen range of creases of notch depth. The elementary
the abscissa. Presumably this would be estimate of plastic-zone influence (Eq 16)
done by drawing a line through such consists in placing the crack border (for
experimental points as are available. computational purposes) at a notch
Even in the absence of small specimen depth increased by an amount (p/21r)
size experimental results, a curve could (KIc/ars) ~, where p is a proportionality
be drawn to the ultimate strength limit factor. We can, therefore, consider repre-
based upon general experience which sentation of the data by the equation,
would have as much accuracy as per- replacing aN of Eq 40 by the net-section
tains to our understanding of how to stress, ~rN(d/daf)2:
use such data in practical applications.
The plane-strain plastic-zone correc-
tion factor suggested by Irwin (32) re-
K u I - p ~IrD~rs ] - 0.233#~r(lrD)U2..(41)
suited from an attempt at empirical data
representation and can be cited as an If p is taken as unity, the assumed
illustration of the above comments. plastic-zone adjustment is the same as
Figure 19 shows aN/ars as a function of has been employed for application to
specimen size for notched round bar plane-stress data.
tests of a rotor steel from work by From Eq 41, a~, as a function of D
Yukawa and Wundt (32). The notch root with Kic constant, has a maximum value
radius was about 0.003 in. and no slow (in the range of very small specimens)
crack growth from the notch was ob- given by:
served prior to fracture. Although a
sharper notch might have resulted in (crrrNs) 0.64
= max0.233 ~/5 (p ~,'~)U~ "'" (42)
lower values, the one used was believed
to be closely similar in all the test bars. An empirical extension of the data rep-
Thus the results are suitable for study of resentation in terms of K values can be
the plastic-zone influence under static obtained, using Eq 41, by adjusting the
crack border fracture conditions. The value of p so that the right side of Eq
material had a yield strength of 83 ksi 42 is about 1.7. A value of p of about
and in all specimens the net section at one third serves this purpose.
the notch was half the gross section. From general considerations, as shown
If the plastic zone is ignored, the in Fig. 3, the size of the plane-strain
value of K can be computed from plastic zone should be smaller than that
of the plane-stress plastic zone for equal
K = 0.233r 1/*. . . . . . . . (40)
values of (K/~rB). A size-reduction fac-
where D is the gross section diameter of tor of one third is not unreasonable. At
the test specimen. Assuming K from the present time basic considerations do
Eq 40 to be constant results in a data- not provide a definite value. Theoreti-
representation curve shown as a dashed cally, for a deep enough notch, an might
line in Fig. 19. The slope of this line is be made as large as 2.7 ars- However,
too steep to fit the data in the approach among reported results of notched-bar
to small specimen sizes. tests, where the net-section area is half

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McCLINTOCK AND IRWIN ON PLASTICITYASPECTS 109

the gross-section area, the aN/ars values CONCLUSIONS


shown in Fig. 19 are about as high as Because of its comparative simplicity,
are normally found, probably due to the Mode III elastic-plastic analysis has
yielding in the shoulders (19). We con- been used to study a number of the
clude from this that empirical considera- effects of plasticity on crack extension.
tions suggest use of a plane-strain plastic- The following conclusions are important
zone correction factor which is smaller for a general understanding of elastic-
than rr for plane stress by about one plastic fracture:
third. For numerical simplicity in Eq 41,
the value suggested by Irwin was p = 1. Only one half the strain energy re-
(2) -8/2. The solid curve on Fig. 19 shows quired for plastic flow on increase in load
the relationship of the data points to can be found from study of the change in
Eq 41, with this value of p. From the compliance of the specimen and the
suggested p value the equation for the corresponding ~ value using linear elastic
plane-strain plastic-zone correction fac- analysis.
tor becomes 2. A re-examination of Eqs 20 and 21
for instability in ductile fracture shows
K~o that at high stress levels no one param-
rr 4 X/2 ~rCr,y ~ . . . . . . . . . (43)
eter, corresponding to oo for a linear
This can be regarded as equivalent to elastic model, will characterize unstable
Eq 11 with an upward adjustment of crack growth at the scale of the model of
the yield stress by a factor of about 1.7. homogeneous plasticity. It rather ap-
Use of the plane-strain plastic-zone pears that it will be necessary to base a
correction factor has been of minor im- fracture criterion on the local stress and
portance in calculation of the crack strain in a small region just ahead of the
toughness, Kic. The same degree of crack and to predict fracture from this,
success in data fitting shown on Fig. 19 coupled with the mechanics in each case.
has not occurred with other sets of data. 3. The idea of basing the fracture
Tests of 7075-T6 aluminum and of high- criterion on the displacement across the
strength steel notched tensile bars in- leading edge of the crack is not con-
dicate ~ = 1.2 ors is about the limit of sistent with basing the fracture criterion
the range which can be characterized by on the local stress and strain iust ahead
a constant value of Kic even with the aid of the crack. Although predictions from
of the correction factor (17). Within this the two criteria are equivalent at low
range, use of the correction factor stress levels, different results would be
scarcely has a significant effect on the predicted for experiments at stress levels
resultant K~, values. Thus, from experi- near those required for general yielding.
mental studies of crack toughness cur- 4. The hysteresis in the displacements
rently available we really know very across the crack for loading and unload-
little about the Mode I plane-strain ing have been evaluated at low stress
plastic zone beyond certain general levels. For a stress-zero-stress cycle, the
aspects which might be derived from width of the hysteresis loop is propor-
intuitive considerations. tional to the cube of the stress.
On the other hand, knowledge of the With specific reference to tension frac-
nature and extent of the Mode I plastic ture testing:
zone is of basic importance if we are to
advance our understanding of crack 5. A more complete study of the stress
toughness beyond the linear elastic and strain distribution for cracks under
viewpoint. tension is needed, not only under in-
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110 FRACTURE TOUGHNESSTESTING

creasing load, but also for increasing zone correction factor based in an em-
length. pirical way upon Koskinen's calculations
6. To assist in further basic under- of the high stress level shape of the
standing of the problem, work intended Mode 11I plastic zone (Figs. 8, 9, and
for research rather than for acceptance 10 and Eq 18). Alternatively, a sub-
testing should not only include data stantial part of the high stress level K,
recommended in Ref. (29), but also trend may disappear if effective crack
metallographic and micrographic ob- length is based upon the apparent com-
servations to indicate the mechanisms of pliance of the specimen at fracture.
fracture and the structural size, p,,
below which the homogeneous theory Acknowledgment:
cannot be applied. In addition, for more The support of part of this work by
information on the strain hardening, the the National Science Foundation through
uniform elongation of unnotched speci- Grant G-14995 is deeply appreciated.
mens should be reported, even if only The work of J. Mahoney on digital
that obtained by measuring the reduction computations for the Mode III insta-
of area away from the neck in an ordinary bility was invaluable. These were carried
tension test. out through the courtesy of the Compu-
7. Pending more exact solutions, the tation Center, Massachusetts Institute
tendency of K, measurements to fall of Technology. The experience and back-
below the characteristic large specimen ground obtained from fracture studies
value when , , exceeds 0.8 *rs might he at the U.S. Navel Research Laboratory
removed by the adoption of a plastic- were equally helpful.
APPENDIX

SUMMARY OF RELATIONSHIPS BETWEEN LINEAR-ELASTIC AND


PLASTICITY VIEWPOINTS
The first report of the ASTM Special major influences of local plastic deformation"
Committee on Fracture Testing of High- Specifically, the Mode III elastic-plastic
Strength Metallic Materials (24) suggested treatment states that, when the plastic zone
allowance for the plastic zone at the crack is small relative to crack size and net sec-
border could be made by adding to the tion, the plastic-zone boundary is circular
half-length, a, of the crack, an adjustment, (as shown in Fig. 5) and the radius of this
r r , given by: circle, r r , is given by:

rr --- 2~r \crr] . . . . . . . . . . (AI) rr --- 27r - - " ........ (A2)

This adjustment was intended to assist This treatment assumes a perfectly plastic
accuracy of the stress-fieldrepresentation in material (zero strain hardening). The re-
a region where the plastic zone, although sistance to plastic shear is k. At and outside
enclosed by a surrounding elastic stress the boundary of the plastic zone, the elastic
field, was not small enough to be ignored stresses and strains are identical to those
in the test analysis. given by a linear elastic Mode III solution
For conditions of this nature no direct elas- in which the leading edge of the crack is
tic plastic treatment of opening mode cracks placed, for analysis purposes, at the center
isavailable at the present time. W e can, how- of the circular plastic zone.
ever, utilize the tensile analog of a M o d e III Clearly Eq A1 is the tensile analog of Eq
elastic-plastic solution as indicative of the A2. Thus the plastic-zone correction factor.

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McCT.n,rrocyr AND I R w i n ON PLASTICITY ASPECTS 111

r r , suggested in Ref (24), is identical to the Eq A1. In plane-stress Ko testing, ~ r has


first-order correction one finds by taking the been commonly given the value of the 0.2
tensile analog of the Mode I I I elastic-plastic per cent offset uniaxial ter~ile yield strength,
treatment. A simple account of the actual ~ r s . For plane-strain KI~ tests, the rr
ideas initially employed in "correcting" for adjustment tends to be less important.
the plastic zone is given in Ref (32) of the Section I I I of this paper discussed a plane
paper. strain, r r , which was equivalent to taking
The Mode I I I plastic zone is only circular ~rr = (8)~/*~r8. These particular values of
in the limit as its dimensions approach ~ry for plane stress and plane strain are
negligible size in comparison with the crack arbitrary. Plasticity considerations indicate
length and the net section. Numerical cal- these choices are plausible but do not in-
culations of the size and shape of the plastic dicate how to modify or improve them. For
zone at high values of net-section stress, this reason the employment of moderate
where the shape is no longer circular, have alterations of rr in order to obtain a better
been made by Koskinen (5) as discussed in fit of fracture data to a constant critical K
the paper. Simple inspection of these results value can be justified. A recent paper by
suggests that, when the net-section stress, Getz, Pierce, and Calvert (36) provides an
rN, is less than 0.8 k, the plastic zone is example. On the other hand, in Ko and KIo
sufficiently enclosed and nearly enough like testing using the customary specimens, use
a circle in shape so that a close fit of the of the r r values noted above seems desirable
adjusted linear elastic treatment to experi- for consistency in reporting of test results.
mental results would be expected. Corre- From the linear elastic viewpoint, the K
spondingly, Ko testing experience with 2a/W factor characterizes the level of tensile
in the range of 0.3 to 0.5 suggests that Ko stress acting near the crack to cause separa-
values remain constant with decrease of tion, and critical values of K provide a basis
specimen dimensions until the net-section for predicting unstable fracturing in a serv-
stress, a~z, becomes greater than 0.8 ~rs ice component as a function of stress level
(17,Z9). For 2a/W < 0.25, the test data and crack size. From a plasticity viewpoint,
show no high stress level trend in the values the counterpart of the K factor consists in a
of Ko until cr~r > ~rs (17). representation of the critical condition of
When the plastic-zone size is a large frac- plastic strain in a small portion of the plastic
tion of the net section or of the crack size, zone adjacent to the leading edge of the
the adjusted linear elastic analysis does not crack. The paper provides specific illustra-
represent the stress field near the crack with tion of this idea by stating the critical con-
realistic accuracy. Use of this viewpoint in dition in terms of a strain, 3'p, at a fixed
such regions is semi-empirical rather than small distance, p , , from the leading edge
empirical. So long as testing experience of the crack. Calculations have been made
shows negligible difference between a critical of the consequences of this assumption using
K value measured at low stress level with a the Mode I I I elastic-plastic analysis.
large specimen and a critical K value meas- Application of this type of analysis can
ured for the same material at high stress be made to fracture experiments either
level with a small specimen, then the Ko or assuming unstable crack extension starts
KI~ parameter has a useful significance over immediately, as if from a stationary crack
the entire size and stress range investigated. border, or that unstable crack extension
Some indication of the accuracy limits of the develops only after a significant amount of
linear elastic treatment, adjusted for plas- stable crack growth. Results corresponding
ticity using Eq A1, can be obtained by to the latter have been obtained by Me-
elastic-plastic analysis. However, the prac- Clintock using a step-wise or incremental
tical usefulness of the adjusted linear elastic calculation plan and are summarized in Fig.
model, when applied semi-empirically to 14. The amount of stable crack growth before
fracture tests in the high stress level range, instability is an increasing function of the
must be determined from testing experience. ratio, Ro/p,, where Ro is the straight-ahead
The tensile analog of k in Eq A2 is Grr in size of the plastic zone. As Ro/p, drops

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112 FRACTURE TOUGHNESS TESTING

below 10, the stable growth approaches a extension was implicit in the analysis of the
negligible amount. r r crack-length adjustment given previously.
The implications of these results depend Under similar terms, the Mode I I I elastic-
upon how one interprets the structural plastic analysis provides a simple analytical
length factor, O~. Previously in this paper basis for definition of length factors which
grain size or inclusion spacings were sug- can be regarded as characterizing crack-
gested as indicative of the magnitude of p, 9 extension behavior. The crack-opening dis-
Larger estimates are possible. For example, placement, ~/, is an example of such a length
microscopic examination of the leading por- factor. The use of this length factor as a
tion of a segment of plane-strain extension, fracture criterion in a proposal by Wells
marked by heat tinting, permits examination (11) was discussed in the paper.
of the sizes of the crack front irregularities. Plasticity aspects of fracture necessarily
If the major irregularities are accepted as connect with linear elastic fracture me-
giving the magnitude of p,, then P, must chanics in a smooth way. When the condi-
be comparable in size to plastic zone for tions for unstable fracture are stated in
plane-strain conditions. This would support terms of a critical strain, 3'r (at r -- O,), or
the idea of regarding abrupt crack extension in terms of a critical opening displacement,
instability from a stationary crack border as ~Te (at the crack border), it is desirable to
normal behavior for plane-strain conditions. bear in mind that these are simply and
When shear lips are present, the central directly related to critical values of K and
tongue of plane-strain fracture tends to grow when the plastic zone is relatively small.
in steps of varying size, and choice of a
These connections are of practical impor-
particular value for O, is rather difficult.
tance. In investigations of the service frac-
Although uncertainties of interpretation re-
main which deserve additional study, the tures of primary interest, those which occur
results of calculations can be regarded as in prior to general yielding, an adjusted linear
agreement with experimental observations. elastic analysis is still the most convenient
The simplification of neglecting the in- method for connecting any specific fracture
fluence on the plastic zone of stable crack criterion with the stress level and crack size

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MCCLIN'rOCK AND IRWIN ON PLASTICITY ASPECTS 113

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Containing Slits," Journal of Mechanics (33) B. M. Wundt, "Unified Interpretation of
and Physics of Solids, Vol. 8, 1960, p. 10. Room Temperature Strength of Notched
(21) F. A. Field, "Yielding in a Cracked Plate Specimens as Influenced by Their Size,"
in Longitudinal Shear," Transactions, Am. Am. Soc. Mech. Engrs paper 59-MET-59,
Soc. Mechanical Engrs, Vol. 30, E, 1963, 1959.
p. 622. (34) H. F. Bueekner, "The Propagation of
(22) B. A. Bilby, A. H. Cottrell, and K. H. Cracks and Energy of Elastic Deforma-
Swinden, "The Spread of Plastic Yield tion," Transactions, Am. Soc. Mech.
from a Notch," Proceedings Royal Society, Engrs., Vol. 80, 1958, p. 1225.
A, Vol. 272, 1963 p. 304. (35) J. L. Sanders, Jr., "On the Griffith-Irwin
(23) J. J. Gilman, "Cleavage and Ductility in
Fracture Theory," Transactions, Am. Soc.
Crystals," Proceedings, Int. Conference
on Atomic Mechanisms of Fracture, Techn. Mech. Engrs, Vol. 27, Series E, 1960,
Press, Mass. Inst. of Tech., Cambridge, p. 352.
Mass. and John Wiley and Sons, New York, (36) D. L. Getz, W. S. Pierce, H. F. Calvert,
N.Y., 1959, p. 193. "Correlation of Uniaxial Notch Tensile
(24) "Fracture Testing of High Strength Sheet Data with Pressure-Vessel Fracture Char-
Materials," First Report of Special ASTM acteristics," Am. Soc. Mech. Engrs Paper
Committee, ASTM Bulletin, Jan. 1960. No. 63-WA-187, Nov. 1963.

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CRACK-VELOCITY CONSIDERATIONS

BY J. M. K ~ r F T 1 Am) G. R. IRWIN1

SYNOPSIS
If resistance to crack growth always increased with crack velocity, then its
measure at nil velocity, ~c or ~]xo, would always represent minimum toughness
and thus a safe criterion. The practical difficulty arises if an increased crack
speed, or loading rate of a fixed crack, results first in a decrease in R, possibly
to some minimum, prior to its increase for the "stable" propagation balance.
Arrest of such a crack will require reduction of the crack driving force, ~, at
least to minimum R. In strain-rate and temperature-sensitive materials this
minimum can lie far below initiation levels. Even in relatively high-strength
materials, speed4hermal effects can be large.
The onset and arrest of rapid fracture provide relatively abrupt measure-
ment points suitable for crack toughness evaluation. An understanding of
these behaviors can be sought through study of the influence of plastic flow
properties. Use of strain-rate sensitive materials over a wide range of tempera-
tures and strain rates permits study of the influences of flow properties without
alteration of the inherent flaws. A correlation of rising-load Kic values with
the strain-hardening exponent, n, suggests that the onset of fast fracture is
controlled to a substantial degree by a tensile instability with a simple relation-
ship to the strain-hardening exponent. The limited information available sug-
gests that crack-arrest conditions can be predicted on the basis of adiabatic
values of n at high strain rates.

Measurements of crack motion during elastic strain energy with crack exten-
brittle fracture of various metallic and sion (the crack driving force, 9) is nearly
glassy solids result in maximum speeds balanced against the inelastic fracture
no greater than about half the elastic work rate (the crack resistance, R) even
shear wave velocity (1)2 and correspond- during fast propagation; and (2) if R
ingly ~ - of the Rayleigh wave limit (2) is a continuous and increasing function of
for propagation of the linear elastic crack velocity. Such rapid crack exten-
crack stress field. Below this limiting sion can be regarded as essentially stable
velocity, the speed of a running crack in the sense that an increase of the crack-
appears to rise and fall in phase with the extension force, 9, is required to produce
crack driving force, 9. Such behavior an increase of the speed.
can be expected: (1) if the release of In practical evaluation of material
1 Section head and superintendent, respec- toughness, behavioral characteristics
tively, Mechanics Div., U. S. Naval Research which lead into or from this stable
Laboratory, Washington, D. C. range of crack speed are most important:
2 The boldface numbers in parentheses refer
to the list of references appended to this paper measurements of the stress conditions
114
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KP.AFFT AND IRWIN ON CRACK-VELocITY CONSIDERATIONS 115

for initiation or for arrest of the rapid are of practical as well as of basic im-
crack-extension process. If resistance to portance in crack toughness measure-
crack growth always increased with ments.
crack velocity, then its measure at nil
velocity, ~c or g~c, would always repre- RUNNING CRACKS
sent minimum toughness and thus a In studies of fracture surfaces, ob-
safe criterion. The practical difficulty servation of small cracks adjacent to the
arises if an increased crack speed, or main fracture indicate that a locally
loading rate of a fixed crack, results discontinuous behavior is characteristic

FI6. 1--Arrest of a Running Crack in Plexiglas Sheet Modulated by 80-kc Shear Wave, Typifies
Finite Velocity up to Arrest Point for Rate-Sensitive Materials. (From Unpublished Results of
A. B. J. Clark.)

first in a decrease in R, possibly to some of crack extension, regardless of the


minimum, prior to its increase for the crack speed (3). At any stage, the separa-
"stable" propagation balance. Arrest of tion process is contingent upon a supply
such a crack will require reduction of the of crack driving force sufficient to over-
crack driving force, 9, at least to mini- run localized regions of greatest fracture
mum R. In strain-rate and temperature- strength. However, in the fast propaga-
sensitive materials, this minimum can tion range, such tough regions are
lie far below initiation levels. Even in quickly overrun so that the attachment
relatively high-strength materials, speed- of an average speed to forward movement
thermal effects can be large. For these of the separation process seems an
reasons, crack-velocity considerations appropriate simplification. Observations

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116 FRACTURE TOUGHNESSTESTING

of crack propagation with such an section decreases by a factor of 20 prior


averaging scale, or as a continuous to crack arrest. The central region is
process, are illustrated first. bordered by regions of greater roughness,
To observe a running crack in regions presumably related to plane-stress yield-
where its speed is changing rapidly, the ing at the plate surfaces. As the speed of
ripple-marking method of Kerkhof (4) crack extension in the central region
is a useful technique. A running brittle decreases, these regions grow in size and
crack tends to remain normal to the accept larger fractions of the (decreas-
direction of greatest tension. If a vibra- ing) crack driving force until arrest
tion is introduced with a shear compo- occurs.
nent on the plane of the crack normal to Plexiglas is composed of a linear

FIG. 2--Initiation of a Crack in a Glass Rod Modulated by 500-kc Shear Wave, TypifiesGradual
Velocity Change for Materials of Low Rate-Sensitivity.Taken from Kerkhof (5).

the crack border, the fracture surface polymer, polymethyl methacrylate, and
tilts in a periodic manner, producing the tendencies toward preferred orienta-
shallow ripples easily visible with specu- tion in regions of large strain make its
lar lighting. As an example of such an behavior somewhat visco-elastic and
experiment, Fig. 1 shows the last 5 mm strain-rate sensitive. It will be noted that
prior to arrest of a fracture segment 7 its ripple markings (Fig. 1) do not ap-
mm long produced in a plate of Plexi- proach zero spacing at the arrest line,
glas at the Naval Research Laboratory but at a finite one suggestive of thres-
(NRL) by A. B. J. Clark. The super- hold velocity minimum for crack arrest.
imposed wave frequency was 80 kc, On the other hand, the less rate-sensi-
traveling counter to the direction of tive epoxies (cross-linked polymers),
crack propagation. In the region shown, particularly glass, tend to exhibit a
the crack speed in the central smooth terminal ripple spacing more nearly like

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KRAFFT AND IRWIN ON CRAcK-VELoCITY CONSIDERATIONS 117

that of a mathematical limit point of an stabilizes the process. Unless abrupt


infinite series. acceleration occurs earlier, the maximum
A corresponding graduality is ob- load point will be reached when the
served in the initiation of a crack in crack speed is about equal to W/t, where
materials of low rate sensitivity. Figure W is the specimen width and t is the time
2, from a paper by Kerkhof (5), shows a to reach maximum load at constant head
tensile fracture through a glass rod. The speed (7). Concurrently with this, the
successive crack-border positions are increase of crack growth resistance, R,
outlined here by ripple markings of 500 and of the crack driving force, 9, are
kc traveling perpendicular to the crack just matched with the load constant.
surface. The highest velocity reached For example, in early crack toughness
was half the limiting crack speed. In testing at NRL, examinations of 24
the lower part of the figure, the frac- frame per second motion picture records
ture may be seen to exhibit markings of tests of 12-in. wide sheets of high-
which approach zero spacing toward the strength aluminum alloy (s) indicated
position of the initial crack. The latter that a crack speed of about W/t de-
was not sufficiently co-planar with the veloped in coincidence with the maxi-
main fracture surface to be illuminated mum load point. The sheet thickness
in the photograph. was 0.050 in. or less, and most of the
One can see traces of Wallner-line slow growth was full oblique-shear
ripples curving across the main pattern separation. The majority of these tests
of ripple markings in Fig. 2. These showed complete separation in one frame
originated from vibrations related to of the film close to the maximum load
local irregularities of separation, particu- point. Evidently the gradual develop-
larly at the intersection of the crack ment of the maximum load point was a
border with the free surface of the rod. marginal thing.
Indeed, it was the use of Wallner lines It is possible to use a gradually de-
by Smekal (6) for measurements of veloped maximum load instability, of the
crack speed which suggested the use of above kind, to explain a tendency of
ultrasonic vibrations. K, to decrease with decrease of specimen
size and increase of net-section stress.
CRACK BORDER INSTABILITY If one assumes, somewhat inaccurately,
IN K~ TESTINC that the rate of increase of resistance to
In studies of the running crack, it crack extension with growth of the crack
seems natural to discuss behavior pri- is not influenced by specimen width,
marily in terms of the stable balance then the match between the constant
between the supply of stress field energy load increase of ~ with crack length and
and the energy dissipated in the separa- the increase of resistance can be expected
tion process. In contrast, when we dis- to occur at lower values of resistance,
cuss onset and arrest of crack propaga- the smaller the specimen (9). The pat-
tion, it seems more appropriate to tern of resistance growth corresponds
center attention upon factors which to the development of the shear lips
would introduce instability and would with crack growth. Alternatively, this
lead to rapid acceleration or deceleration trend of K, can be explained using the
of the crack movement. Mode III elastic-plastic analysis to
When slow cracking is observed in a provide an enhanced plastic-zone cor-
K~ test, the crack growth is accompanied rection factor. Not only the magnitude
by a steady increase of resistance which of the trend, but also the observed disap-

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118 FRACTUR~ TOUGHNESS TESTING

pearance of the trend when the net- enough for a pop-in type of K~c deter-
section stress is less than 0.8 ~rrs, can mination (lZ).
be explained in this way (10). If the Of course, slow stable plane-strain
latter is accepted, then the former is crack extension may occur in the pres-
unnecessary and this, in turn, leaves in ence of stress corrosion or with cyclic
doubt the crack speed at the point of loading. Gross weakness of internal
rapid acceleration. planes normal to the crack border may
In terms of strain rates near the crack introduce small internal shear lips to
border (11,12), there is a quite large postpone instability by providing a local
difference between assuming that accel- region of plane stress. In the absence
eration is abrupt from a stationary of such factors, however, it is difficult
crack border and assuming that the crack to understand how even small amounts
speed at instability is Wit. The W/t of plane-strain crack-border motion can
crack speed, although small for usual occur without immediate development
test conditions, increases the strain rate of rapid, progressive fracture. Thus one
by an amount equivalent to several can assume that, in normal behavior,
orders of magnitude of increase in the onset of fast separation at a plane-strain
loading speed. Thus the questions dis- crack border results from a development
cussed above on the nature of the Kc of critical conditions in advance of the
instability are of importance when the border during a final loading period in
crack toughness of the material is known which the crack border is essentially
to be sensitive to strain rate. stationary. The assumption of a sta-
tionary crack border simplifies the task
INSTABILITY AT A PLANE-STRAIN of studying the relationship of plastic
CRACK BORDER flow properties upon K~c over a range
Consider next the development of of temperatures and strain rates. The
instability in a Krc test using either a success of correlations resulting from
notched round bar or a plate specimen these studies, in turn, tends to justify
thick enough so that the shear lips do the assumption of a stationary crack
not delay the initial unstable accelera- border prior to initiation.
tion of the crack border. At one stage,
such small separations as may have GENERAL STRAIN-RATE INFLUENCES
formed near the border of the initial The Fifth Report of the ASTM
crack are surrounded by areas of stronger Special Committee states that slow test-
material which accept the increase of ing speed crack-toughness evaluations
tensile load. At a later stage, the spread- are adequate for most applications when
ing and joining of the initial separations the strain-rate sensitivity of the material
surround and overload the local regions does not exceed that found in martensitic
of highest strength so that these no longer steels heat-treated to a yield strength,
block the forward movement of the a r s , of 200 ksi or more (13). Measure-
separation process. At this point, the ments of the plastic yield properties of
process is quite unstable and must accel- various steels provide a reasonable basis
erate rapidly. Even when the stabilizing for this attitude. There is a tendency for
influence of the shear lip is large enough the absolute sensitivity of yield strength
so that substantial amounts of plane- to strain rate to remain at about the
strain separation precede the develop- same value independent of large changes
ment of final rapid separation, the first in trys. For example, the 3 per cent
plane-strain instability is often abrupt (strain) flow stress of both low- and

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K1LA:FI~TAND IRWIN ON CRACK-VELOCITY CONSIDERATIONS 119

high-strength steels typically exhibit an this in a consistent and appropriate way,


increase of about 6 ksi for a tenfold in- one must assume either that the crack
crease in strain rate. Thus a factor of 10~ border is stationary prior to instability or
in strain rate, corresponding to a change that the crack motion has a known value.
from static testing to impact speeds, The complexities associated with the
causes about a 30-ksi increase of the flow latter choice are quite formidable. Fur-
stress. This is a change of nearly 100 per thermore, the simpler, stationary crack-
cent for a plain carbon steel. The corre- border assumption seems justified by
sponding decrease of crack toughness is factors previously discussed.
quite large. On the other hand, for the An additional assumption is necessary
class of steels defined above as relatively which is equivalent to stating the de-
insensitive to strain rate, a 30-ksi eleva- pendency of plastic strain upon distance
tion of the flow stress is no more than a from the crack border. One can make
15 per cent effect. this choice without actual knowledge of
the exact dependency because the effects
INFLUENCES OF TEMPERATURE AND of different reasonable hypotheses on the
LOADING RATE UPON KI= calculated strain rate are scarcely signifi-
VALUES cant in their influence upon plastic flow
Information currently emerging from properties. For example, if we assume
studies of effects of temperature and that the strain, e, at distance, d, ahead
loading rate upon Kit values suggests of the crack border has the inverse
that it may be possible to understand first-power dependency suggested by the
onset of fast fracture and crack arrest Mode I I I elastic-plastic solution 0s),
on similar terms. These terms center then
attention upon plastic flow properties
of the material and their influence upon = ~r -- , ........... (1)

resistance to plane-strain extension of a


crack (14). From the point of view where 2rr is the formal calculation of
adopted, K~c is jointly determined by plastic-zone size from
inherent flaws, such as poorly bonded I(KI,~'
2rr = - - - 9. . . . . . . . . . (2)
inclusions or grain-boundary impurities, lr \ ~ r /
and by plastic flow properties. Although In a rising load test such that K is pro-
the inherent flaws in various plates of portional to the loading time, t,
metal may differ depending upon fabrica-
--- 2~/t .............. (3)
tion and other factors, tests using speci-
mens from a single plate over a wide Equation 3 neglects the variation of ar
range of temperature and strain rate, with time rates, this factor being of
which alter the plastic flow properties, minor importance.
permit a study of the influence of these If we assume, in place of Eq 1, that
properties upon the crack toughness.
It is desirable to restrict these in-
vestigations, initially, to plane strain for
various reasons, one of which is analyti- this assumption is equivalent to an
cal. The analysis requires association of elastic strain dependency. Using K ~o t
results from plastic deformation tests and Eq 4, one finds
(performed with tension or compression = ,/t ............... (s)
specimens) with plastic strains and strain
rates adjacent to the crack border. To do which differs from Eq 3 by a factor of 2.

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120 F~CTU~.E TOUGHNESS TESTING

Equation 5 is preferred here for the University of Illinois wide-plate series,


following reasons: (1) rounding of the as shown in Fig. 3. Here one may com-
crack tip by plastic strain as well as work pare the critical stress-intensity factor,
hardening would tend to reduce the KI~, with the time rate of increase in
strain gradient of Eq 1; and (2) as noted this factor, K, computed as Kio/t. In
later, Eqs 4 and 5 permit definition of a this graph, both coordinates are divided
process zone-length factor which is by Young's modulus for comparison
invariant with temperature and strain with plastic strain measurements.
rate. Now it is evident that the range of
Nevertheless, when we center atten- validity for linear elastic analysis of the
tion on a particular strain, e~, at a dis- tests is limited to rather low tempera-
tance, d~, we can bear in mind that Eqs tures with this mild steel. One can, in
4 and 5 are, to some degree, schematic. principal, raise this restriction by testing
The length, dl, may require a propor- suitably large specimens, as for example
tionality factor or a special starting the large beams and spin disks tested
B
/
I n(T, ISOT'HERMAL'e-~-g'ADI~,BATIC n n ] I MATCH/
_"~ 0.4
$30 _
o.3

IS 0.2

~,o7~ ,
"- " " ,J~-,2o.- ~/
iI 5 - - ~ 0,06

,Lo ,'o-, ,'o-, / ,'o-,


l 9 (SOLID POINTS] ~CRACK TIP STRAIN RATE FACTOR (~] v~'~lsec
l
I I I I I
10-3 10-2 iO-J I I0 I00
- - (HOLLOWP~INTS) PPLASTIC STRAtN RATE (~) I/$ec

FIG. 3--Correlation for Setting Proportionality Between Isothermal Fracture Toughness, KIo(T)
and IsothermalStrain-HardeningExponent, n(r), the Crack Re-initiation Values for University of
Illinois Mild Steel P'ate.

point for measurement. In any case, t in the rotor steel investigations (11).
examine whether values of KIc correlate However, there are situations where
with values of flow stress, af, or strain- this would be impossible and, in any
hardening exponent, n (corresponding case, large specimens are inconvenient,
to a strain, e0, the appropriate values of expensive, and even more difficult to
~! and n can be obtained from plastic load rapidly. This difficulty augments
flow studies, assuming the strain rate interest in finding correlations between
applicable to the Kic test is (el/t). Exami- plastic flow properties and crack tough-
nations of this type show a strong correla- ness, since such correlations might be
tion tendency indicative of a direct
used to extend the crack toughness data
proportionality between KI~ and n over
into a range otherwise impractical be-
a wide range of temperatures and strain
rates (13). Two examples will be shown. cause of the required specimen size. The
correlation of plane-strain crack tough-
INITIATION /~Ir IN A MILD STEEL ness, Kic, with the strain-hardening
Consider first the data on a mild steel exponent, n, appears to be suitable for
plate, a part of Specimen No. 39 of the such purposes, and is shown in Fig. 3 for
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KRAF]?T AND IRWIN ON CRACK-VELOCITY CONSIDERA'IIONS 121

the mild steel plate material (17). Here field. The dimples seen in electron fracto-
the strain-hardening exponent was meas- graphs are thought, as suggested by
ured with small compression specimens Beachem (11)~ to represent the broken
i in. in outside diameter and ] in. long, ends of these ligaments. Second, it is
the Kr~ with single-edge notch specimens assumed that the tensile plastic strain
as reported in Ref 08). distribution approaching the real crack
tip can be regarded as increasing con-
MODEL FOR BRITTLE FRACTURE BY
tinuously up to the elemental cell in
TENSILE INSTABILITY
accordance with the inverse square root
Now the observation of a similarity of d.
between K~ and n in their dependency With these assumptions, it is seen that
upon temperature and strain rate merits a constant proportionality between Kt,

12-

~'10 -

m
~S-- -
_

c
i

0 4 __ _
O::
l,l
>
Z

0--
-320 -220 -120 -70 -12 +80
TEST TEMPERATURE T ( ~

FIr 4--Thermal Correction of Strain-Hardening Exponent, An, Versus Test Temperature, "1",,
for University of Illinois Plate of Fig. 3.

some sort of rationale. The basis used and n suggests that the instability is
in Ref (14) was perhaps oversimplified, closely related to a length factor at the
but it still appears to suffice for all data crack border given by:
available at this writing:
The model requires two assumptions.
. . . . . . . .

First, the process of tensile instability


and rupture actually occurs in a small
element adjacent to the crack border. where ~1is regarded as the critical strain.
This can be regarded schematically as The length factor is constant if n/~l is
composed of minute short, uniaxial constant. From the fact that instability
tensile ligaments, freed from the sur- of a tension bar occurs when ~1 = n, it is
rounding triaxial state of stress by the natural to try this assumption with the
free surface of the crack tip and by other data. In this event, the strain rates for
holes growing under the influence of the the K~o and n determinations should be
dominating crack border tensile stress properly matched when
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122 FP~CTUP.E TOVGmcESS TESTING

k
_ = -. . . . . . . . . . . . . . (~) petition between the thermal softening
KIc rJ and the normal strengthening of iso-
thermal work hardening. The effect is
That the data can indeed be matched greater at very low temperatures. Be-
while this constraint is imposed may be cause of the vanishing specific heat ,ear
seen in Fig. 3 for the University of absolute zero, the temperature rise for
Illinois plate (17), as in other data previ- a given plastic deformation er.ergy is
ously reported (14). higher. The extent of the effect on the
280 I I i ~, ] I

~-~ .220"F
260

~g

, ,, ,4130~
IO t I0 I IO IO IO
K / K I t - - SOLID POINTS
RECIPROCAL LOADING TIME - - l ~ I r l - - HOLLOW P O I N ' I 3 - - see-'

FIG. 5--For a High-Strength Titanium Alloy, Flow Strength, al:(~, Increases with Speed Versus
Temperature but so Does Initiation Crack Toughness, K l a ~ , unlike BCC steel shown in Fig. 3.
Precracked Charpy W/A, after Hartbower (22,23), shows the same trend.

ADIABATIC HEATING strain-hardening exponent, n, is typified


by the correction curves for the Univer-
It was pointed out by Zener and sity of Illinois plate which are shown in
Hollomon (2o,21) that adiabatic heating Fig. 4, taken from Ref (17).
could greatly augment the tendency for In general, the time of straining, which
local shear instability by diminishing will become too short for conduction of
the strain-hardening tendency. This the generated heat to the surrounding
effect is relevant to the tensile instability, metal, will increase as the square of the
regarded here as the governing process linear dimension of the deformed enclave,
for onset of rapid Mode I plane-strain d, and decrease as the coefficient of
separation. The process is one of com- thermal diffusivity, a,

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KRAFI~T AND IRWIN ON CRACK-VELOCITY CONSIDERATIONS 123

t ~ d'/~ . . . . . . . . . . . . . . . (8) tests were larger for impact than for


For an enclave as small as the plastic static loading. These are superimposed
zone, 2rr, or the still smaller process on the K~c plot of Fig. 5, reduced to K
zone, dr, the crack-initiation process in coordinates as [E(W/A)] ~12, with the
the K~o test is seen to be fully isothermal Charpy blow put in at 1/t ~ 1.5 • I(P
throughout the available loading-speed as estimated elsewhere (11). A 50 per cent
range. Thus it is proper to compare increase is reflected in both [E(W/A)] ~
isothermal strain-hardening values, n(r), and K~o(r) measurements with the 10~
with the K1c(n 9 This has been done in increase in loading speed. The Charpy
the n data shown in Fig. 3 by correcting energy result might be expected to be
n values obtained at strain rates greater somewhat higher than K~o, as it includes
some contribution from surface shear lip
than isothermal, using Fig. 4.
energy which is not included in the
ImTIATION KI~(T) IN 6A1-4V plane-strain process.
TITAmUM ALLOY
INFLUENCE OF FLOW STRENGTH SPEED
For mild steel, a decreasing trend of VERSUS TEMPERATURE SENSITIVITY
crack toughness with increasing loading The isothermal flow stress at 3 per cent
speed (Fig. 3) is quite typical. However, strain ~I3(T) is also plotted in Fig. 5 and
this behavior is not observed in all typesa strengthening with speed increase and
of metals. For example, hard titanium temperature decrease is observed, except
(6A1-4V) shows just the opposite trend at --120 F. This behavior is also found
as may be seen in Fig. 5. Here isothermal in mild steel as may be seen by looking
values, Ki~(n and n(r) X (Kit/n) are forward to Fig. 6; yet the fracture
displayed on a linear scale against log toughness versus speed tendencies in the
1/t, where the ratio of KiJn was previ- two materials are directly opposite. It
ously determined from a logarithmic seems pertinent to note an observation
matching plot similar to that of Fig. 3. of Beeuwkas (23), who pointed out that
In testing the titanium alloy, a procedurethe absolute slope of the stress-strain
of step-wise straining-quenching cycles curve, 0, for body-centered cubic (BCC)
provided a direct measure of isothermal metals tends to remain constant with
flow properties even at high strain rates,changing temperature and speed. For
as described in Ref (1~). mild steel of this class, n (and thus K~o)
At room temperature, K~ was also would vary inversely as the flow stress,
evaluated with a part-through crack ~s, since (n ~ 0/~I). For face-centered
specimen by Hartbower (z2) and an cubic (FCC) metals, Beeuwkas observed
agreement may be seen in Fig. 5. increasing with speed/temperature
COMPARISON WITH PRECRACKED which, if a stronger effect than the in-
CH~P.PY creasing ~z, would necessitate a rising n
or KI,. Since the titanium alloy is
It would be expected from the n-value partially i~-phase and thus non-BCC, it
trends shown at room temperature and might well possess characteristics similar
below for this titanium alloy, that to the FCC metals consistent with the
initiationof crack propagation would be result shown in Fig. 5.
easier for static than for dynamic load-
ing. Indeed, the authors' study of this EQUI~ ALENCE OF LOADING RATE
material was an investigation of just TO CRACK SPEED
such a finding by Hartbower, whose Crack-arrest K-value measurements
W/A values from precracked Charpy require relatively large specimens and
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124 FRACTURE TOUGHNESSTESTING

are generally more complex than rising speed necessary for an adiabatic fracture
load tests based upon onset of crack process zone may be obtained by dividing
propagation. Correspondingly there has the length factor, q d r , by the time,
been less experimental work. No more (qdr)2/a, where a is the thermal-diffusion
than a brief summary will be attempted coefficient. Thus,
here.
o~
A series of possible length factors can acrit = - - 9. . . . . . . . . . . (12)
be derived from analysis of the crack- qdr
border plastic zone. These are, in addi-
tion to the length factor, dr, already Inserting this value into Eq 11 gives a
discussed: result consistent with Eq 8, within a
factor of 2. Thus, with a sufficient in-
(1) The opening displacement, 2~/, at crease of loading speed, one might expect
the crack border, based upon analogy a continuous trend of strain rate and
with the Mode III elastic-plastic analy- thermal conditions from high-speed
sis: rising load tests into the moving crack
range. From this one might conclude no
= ......
4 ( * 1 ) 2- d r , . . . . . . (9) difference will be found between values of
~y
K~ at crack arrest and values of K~ in a
rising load test, fast enough to match
(2) The distance, tiN, from the crack
the velocity of the crack just prior to
border to the point where e = el, based
arrest if). However, reservations must
upon Eq 1:
be made to allow for the fact that the
d~r -- [(2dr)(2rr)]~/s. . . . . . . . (10) temperature distribution around the
moving crack border differs substantially
(3) The plastic zone size, 2 r r , as from that near the stationary crack
given by Eq 2. border prior to instability. From the
Discussion will be based upon use of general nature of the difference, it can be
the length factor, dr. However, since argued that crack-arrest values of KI
dr is the smallest of the four length might correspond to a larger adiabatic
factors and the analysis is schematic effect and a lower toughness than the
only, we will refer to the length factor as K~c values which would be found even
q d r , where q might be an order of magni- in the most rapid types of rising load
tude larger than unity, or smaller, d ~ , / d r , testing.
as in Ref (14). This discussion cannot resolve un-
The strain rate of interest in advance certainties thus introduced. However, it
of a moving crack approaching arrest is is clear that, for a typical strain-rate
presumably the strain rate, where e has sensitive steel, an abrupt arrest should
the critical value, el. This, in turn, we occur when the crack speed drops below
would tend to associate with the strain- the value given by Eq 12. The process
hardening exponent, n, under ambient zone at crack arrest is therefore adia-
conditions of temperature and time rate. batic. Furthermore, unless ways can be
From Eq 4, this strain rate is given by: found to shorten greatly the load rise
time in Klo evaluations, these will gen-
i = el 2qdr . . . . . . . . . . . . (11) eraUy correspond to isothermal cond-
tions in the process zone and thus to
where a is the crack speed. higher values of Kx~ and n than for crack
An approximate estimate of the crack arrest.

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KRA~FT A N D IRWIN O N CRACK-VELOCITY CONSIDERATIONS 125

9 1 I [ i I I l Fe f c,020%; Mn, 0,76; SE, o,03~ P, 0.o{4;


S; 0.040; Ni,0.I6
CvqS~ZlaF;Crys 9 34.KII; UTS, 9 62;R&65~
. -T_:.o. dT "Z~ ( tN
~r )Z " ,23.6 x lO'Gin..
~ 120 KIC=~E2V~dT 9 3,66x ]05n
=~=t " V l 2dT~tc ~-- t~ 1~ft/$e~
B + 30~ '
~ 80 + 180 o ( for KIC 9 37'esi I~T~n.
~)
~o~
u
,~ ~ 20~- NRL DYNAMICUNIVERSAL _|_89 x 60" _L 03 x 6 ~ j | _WIOiEPLATE DI~ x
> u~ ,I ~ '=- " } L(~AOER ] -~AR BLOCK-VBAR-BA,~ J F" R E S U L / - ]
o~
o ~ PLASTIC STRAIN RATE (~) SEC-I

< z .0
I00~

I} -I?'~
-70 o
~ ~0 -- -I20 ~
-----...~.-sE~ .._~__----~
I I I 'l ] I 1 I 1
IO~ I0=~ 106 107 tOe IO9 10la
CRACKTIP STRESSRATE FACTOR K psi i~'~n/$ec
I I I I .I
0'.001 O.Ot 0.1 l I0 lO0 I000 IO,O00
CRACK VELOCITY [V] fl/sec

FIG. 6--For the Freely Propagating Crack or Its Arrest, Adiabatic n(Q) and Thus Kz~(o) Values
from Compression Tests Are Compared with K Calculated for Propagating Cracks in the Wide
Plates. Adiabatic 3 per cent Flow Stress, cr18(o), Is Shown on Upper Plot.

[ 1~-'~6~S"'-~ J., ESTIMATES ON NORDELL-HALL A 2128

~''',.-"~--~'/ RECKARREST K VALUESA PLATE

I00-

80" i -- " ).PLATE THICKNESS


~ ;,//~F )NFLUENGE

~' 60 O ~
K
ksi'(T~ ISOTHER A L ~ .----, ....., --" """W~
4C
R
ESTIMATES ON EARLY U ILL PLATE
20'

o -8~ -8~ -4b -~of ~ 2'o ,*o 6'0 ;o


TEMPERATURE ~

FIO. 7--Comparison of Various Estimates of K for Crack Arrest for Two Mild Steels.

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126 FRACTURE TOUGHNESS TESTINO

VELOCITY PRIOR TO CRACK ARREST distribution from separate studies of


From the preceding discussion, it is residual stress in similarly welded speci-
of interest to compare K~ estimates from mens. The results show very little tem-
adiabatic n determinations with values perature sensitivity in the range from
of K approached by a decelerating crack. --50 to +20 F. Above this temperature,
This can be done using values of K for estimates of the relative size of the plastic
low crack speeds derived from University zone predict a significant plane-stress
of Illinois strain-gage data for the mild influence upon the results and a major
portion of the upward trend of the K
steel of Fig. 3.
An attempt of this sort for the Uni- values above 20 F must be due to this
versity of Illinois plate material is repro- influence.
duced from Ref (17) in Fig. 6. Added to The nil-ductility temperature (NDT)
flow data from Fig. 3 (fast enough to be values from tests of the Pellini-Puzak
adiabatic) are points some 10 and 100 drop-weight type were reported as in
times higher in strain rate obtained with the range of 20 to 30 F for the test plates.
Hopkinson-Kolsky type bar loaders. The Estimates of KI can be derived for com-
K value scales are based upon the corre- parison from the nature of the small-flaw
lation between KI~ and n, established in drop-weight test as suggested in Ref (7).
The results of this comparison shown in
Fig. 3.
A consistent pattern of speedwise be- Fig. 7 indicate that the drop-weight
havior is evident. Regions of minimum NDT test can be regarded as controlled
K~ may be seen to o c c u r at very low by the same toughness as pertained to
speeds for temperatures of --70 F and the crack arrests. The degree of numeri-
down; then, at much greater speeds, for cal agreement is encouraging but not
--12 F and up. A corroborative pattern definitive. The numerical work contains
for 301 stainless steel crack-propagation a number of uncertainties which were
results (that is, Kc tests, of Witzel) is resolved by arbitrary rough estimates. In
reported by Christian and Hurlick (24). addition, some ambiguity exists as to
At the right side of Fig. 6 are shown whether the small-flaw drop-weight test
the K values estimated from strain-gage should be regarded as controlled by crack
observations at various crack speeds. arrest or by onset of plane-strain frac-
The trend of the data indicates a K-value ture.
range for crack arrest which is consistent SUMMARY
with the minimum toughness level for 1. The onset of rapid fracture and
- 1 2 F. crack arrest provide relatively abrupt
measurement points suitable for crack-
CRAcK-ARREST MEASUREMENTS
toughness evaluation.
Figure 7 shows estimates of K at crack 2. An understanding of these be-
arrest from wide-plate tests at the Uni- haviors can be sought through study of
versity of Illinois (2s). In these tests, the the influence of plastic flow properties.
crack ran outward from a vertical weld 3. Use of strain-rate sensitive mate-
residual stress zone of high tension. From rials over a wide range of temperatures
the value of the moderate tensile stress and strain rates permits study of the
applied to the plate, the crack length, and influences of flow properties without
an assumed distribution of residual alteration of the inherent flaws.
stress, it was possible to estimate values 4. A correlation of rising-load K~
of K for the observed arrests. It was values with the strain-hardening expo-
necessary to assume the residual stress nent, n, is found which suggests the

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KRAI*Fr AND IRWIN ON CRAcK-VELOCITY CONSIDERATIONS 127

onset of fast fracture is controlled to a 5. T h e limited information available


substantial degree b y a tensile instability suggests t h a t crack-arrest conditions
with a simple relationship to the strain- can be predicted on the basis of adiabatic
hardening exponent. values of n at high strain rates.

REFERENCES
(1) G. R. Irwin, "Fracture," Encyclopedia of plement), Vol. 27, No. 9, September, 19o2,
Physics, Springer, Berlin, Vol. VI, 1958, p. 428.
pp. 551-590. (13) "Progress in Measuring Fracture Tough-
(2) E. H. Yoffe, "The Moving Grit~th Crack," ness and Using Fracture Mechanics,"
Philosophical Magazine, Vol. 42, 1951, p. Materials Research & Standards, Vol. V,
739. No. 3, March~ 1964, p. 107.
(3) J. A. Kies, A. M. Sullivan, and G. R. (14) J. M. Krafft, "Correlation of Plane Strain
Irwin, "Interpretation of Fracture Mark- Crack Toughness with Strain Hardening
ings," Journal of Applied Physics, Vol. 21, Characteristics of a Low, a Medium and a
1950, p. 716. High Strength Steel," Applied Materials
(4) F. Kerkhof, "Analyse des Spr6den Zug- Research, Vol. 3, April, 1963, p. 88.
bruches van Gl~tsern mittels ultraschall," (15) F. A. McClintock and J. A. H. Hult,
Naturwiss, Vol. 40, 1953, p. 478. "Elastic-Plastic Stress and Strain Distri-
(5) F. Kerkhof, "~ber den Bruchvorgang butions around Sharp Notches in Re-
beim Manteldruckversuch," Glastechnis- peated Shear," Ninth International Con-
che Berichte, Vol. 33, H.12, 1960, S. 456--459 gress on Appl. Mech., Brussels, 1956.
(6) A. Smekal, "Verfahren zur Messungvon (16) D. H. Winne and B. M. Wundt, "Applica-
Bruchfortpflanzungs geschwondigkeitan an tion of the Griffith-Irwin Theory of Crack
Bruchflasehen," Glastechnische Berichte, Propagation to the Bursting Behavior of
Vol. 23, 1950, p. 57. Disks," Transactions, Am. Sec. Mechani-
(7) G. R. Irwin, "Crack Toughness Testing of cal Engrs., Vol. 80, 1958, p. 1643.
Strain Rate Sensitive Materials," ASIDE (17) J. Eftis and J. M. Krafft, "A Comparison
Paper 63-WA-g17, Am. Sac. Mechanical of the Initiation with the Rapid Propaga-
Engrs., November, 1963. tion of a Crack in a Mild Steel Plate,"
(8) H. L. Smith, J. A. Kies, and G. R. Irwin, Paper 64 MET 16, Am. Sac. Mechanical
"Fracture Toughness of Materials for Engrs., May, 1964.
Aircraft and Missiles," Proceedings, 3rd (18) A. M. Sullivan, "New Specimen Design
Navy Science Symposium on Materials for Plane Strain Fracture Toughness
Research in The Navy, Office of Naval Tests," Materials Research & Standards,
Research, Washington, ASTIA Report Vol. 4, January, 1964, p. 20.
217823. Philadelphia, March, 1959. (19) C. D. Beachem, "An Electron Fracto-
(9) J. M. KraffL A. M. Sullivan, and R. W. graphic Study on the Influence of Plastic
Boyle, "Effect of Dimensions on Fast Strain Conditions upon Ductile Rupture
Fracture Instability of Notched Sheets," Processes in Metals," Transactions, Am.
Crack Propagation Symposium, Cranfield, Sac. Metals, Vol. 56, September, 1963, p.
1961. 318.
(10) G. R. Irwin, Discussion of paper by M. F. (20) C. Zener and J. H. Hollomon, "Effect of
Koskinen, Transactions, Am. Sac. Me- Strain Rate upon Plastic Flow of Steel,"
chanical Engrs., Vol. 85, Series D, 1963, p. Journal of Applied Physics~ Vol. 15,
591. January, 1944, p. 22.
(11) J. M. Krafft and A. M. Sullivan, "Effects (21) T.A. Read, H. Marcus, and J. McCaughey,
of Speed and Temperature on Crack "Plastic Flow and Rupture of Steel at
Toughness and Yield Strength in Mild High Hardness Levels," Fracturing of
Steel," Transactions Quarterly, Am. Sac. Metals, Am. Sac. Metals, Cleveland, Ohio,
Metals, Vol. 56, No. 1, March, 1963, p. 160. 1948.
(12) R. W. Boyle, A. M. Sullivan, and J. M. (22) G. M. Orner and C. E. Hartbower, "Sheet
Krafft, "Determination of Plane Strain Fracture Toughness Evaluations by Charpy
Fracture Toughness with Sharply Notched Impact and Slow Bend," Welding Journal,
Sheets," Welding Journal (Research Sup- Vol. 40, 1961, p. 405s.

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128 FRACTURE TOUGHNESS TESTING

(23) R. Beeuwkas, Jr., "Plasticity and Frac- Vessel Materials for Application in a
ture," Proceedings, Third Sagamore Ord- Cryogenic Environment," ASD TDR
nance Materials Research Conference, 63-258, It. II, February, 1965.
Duke University, Durham, N. C., Decem- (25) W. J. Nordell and W. J. Hall, "Two Stage
ber, 1956, p. 89. Fracturing in Welded Mild Steel Plates,"
(24) J. L. Christian and A. Hurlick, "Physical University of Illinois Report, October
and Mechanical Properties of Pressure 1963, to be published in Welding Journal.

DISCUSSION

CARL E , HARTBOWERL-One observa- was ring-rolled to a section thickness of


tion that may be overlooked in reading in., solution-treated and machined to
this excellent paper is the quantitative 0.1-in. wall thickness. Aging resulted
correlation found between the part- in a 0.2 per cent offset yield strength of
through crack (PTC) and the single- 156.5 ksi. The individual test results
edge notched (SEN) tension specimens from five PTC tension specimens are

TABLE 1--PART-THROUGH-CRACK (PTC) T E N S I O N DATA.


(6AI-4V Titanium Alloy at 156.5 ksl Yield Strength)

Surface Crack, Gross


Fracture Fracture
la. Specimen Toughness
Specimen a/2c P/Fy Shape, ]
No.
Wide, A~n
~, Strew,
Depth Length L•d, ksi KI9 GIe

I. .. 0.030 0.110 0.273 0.998 0.I00 14 376 143.8 0.92 1.36 41.3 93.0
2. . . . . . 0.040 0.100 0.400 0.996 0.100 14 150 141.5 0.90 1.82 40.7 90.2
3. .. 0.040 0.140 0.286 1.000 0.100 12 500 125.0 0.80 1.44 40.4 88.5
~.. 0.060 0.220 0.263 0.998 0.100 9 850 98.5 0.63 1.42 39.3 83.6
5. .. 0.060 0.220 0.273 1.002 0.100 10 875 108.8 0.70 1.43 43.2 101.2

T A B L E 2--VARIATION IN STRESS- presented in Table 1. The PTC tension


INTENSITY FACTOR WITH STRAIN
specimen was 8 in. long and t in. wide
RATE, KI~ (ksi%/~..)
in the gage section. Note that in spite of
SEN Test Charpy [(W/A)IXJta an appreciable (deliberate) variation in
45/see 10-1/see Impact 0.02 i../sec crack length and shape, the computed
values of fracture toughness were essen-
60 38 106 55 tially constant.
The authors have observed that both
in 0.1-in. thick 6A1-4V titanium alloy. the stress-intensity factor and the strain-
The fracture toughness values obtained hardening exponent increased with in..
from the two test specimens were, for all creased loading rate. Increasing fracture
practical purposes, the same: the stress- toughness with increasing rate d loading
intensity factor, Kic (ksi %/~.), was 36.4 has been observed in several metals
for the SEN specimen, and 41.0 for the using the precracked Charpy test (see
PTC specimen. The 6A1-4V titanium Figs. 16 and 17 in Orner and Hartbower2
t G. M. Orner and C. E. Hartbower, "Sheet
1Research engineering specialist, Aerojet- Fracture Toughness Evaluated by Charpy
General Corp., Solid Operations, Sacramento, Impact and Slow Bend," Wdd/nr Journa/,
Calif. VoL 40, No. 9, September, 1961, p. 405-s.

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Discussio~ oN CRACK-VELOCITYCONSmV.~TmNS 129

and Table 4 in Hartbower and Orner.* degree as shown by the precracked


The data obtained by Irwin and Krafft Charpy. However, the values obtained
show the upward trend of K~r and n with from the precracked Charpy tests in
speed to be quantitatively of the same slow bend and impact (Table 2) are
higher than those obtained from the
a C. E. Hartbower and G. M. Orner, "Metal- SEN tension specimen. This effect would
lurgical Variables Affecting Fracture Toughness be expected considering that the pre-
in High Strength Sheet Alloys," Air Force cracked Charpy involves both plane-
Technical Documentary Report No. A,SD-TDR-
6~-868, October, 1962. strain and plane-stress fracture.

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Test Methods

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FRACTURE TOUGHNESS T E S T I N G METHODS
BY JOHN E. SRAWLEY1 AND WILLIAM F. BROWN, JR. 1

SYNOPSIS
A comprehensive survey is presented of current methods of fracture tough-
ness testing that are based on linear elastic fracture mechanics. General princi-
ples are discussed in relation to the basic two-dimensional crack-stress field
model, and in relation to real, three-dimensional specimens. The designs and
necessary dimensions of specimens for mixed mode and opening mode (plane-
strain) crack toughness measurements are considered in detail. Methods of
test instrumentation and procedure are described. Expressions for calculation
of crack toughness values are given for the common types of specimens.

In keeping with the purpose of the cepts and methods of linear elastic
symposium of which it is a part, this fracture mechanics and to evaluate
survey of fracture toughness test meth- objectively the usefulness of these con-
ods will be restricted to those methods cepts and methods for rational engineer-
that have their basis in linear elastic ing analysis of fracture problems. From
fracture mechanics, or that can be a practical point of view, the arbitrary
treated satisfactorily by the methods of empirical procedures (the most familiar
linear elastic fracture mechanics at the being notched-bar transition tempera-
present time. This restriction of scope ture testing) are most useful for evaluat-
carries with it no implication that there ing structural steels in the lower range
are not other methods worthy of con- of yield strengths. The application of
sideration. In the opinion of the authors, steels in the higher range of yield
some of the arbitrary empirical proce- strengths and of titanium and aluminum
dures for evaluating fracture toughness alloys calls for much more discriminating
are, and will continue to be, of great evaluation to the point of being able to
value, having been proved by correlation estimate the strength of structural ele-
with service-failure studies. In this ments containing cracks. Thus, it is
connection reference can be made to the desirable that fracture toughness testing
reviews by Tipper (1,2),~ and in particular of such materials shall be based on the
to the work of Pellini and his colleagues principles of mechanics as applied to
at the U.S. Naval Research Laboratory cracked bodies.
(3,,t). The prime purpose of the sym- Because of its rapid development over
posium, however, is to clarify the con- the last decade or so, fracture mechanics
1 Head, Fracture Section, and chief, Strength has seemed confusing to many interested
of Materials Branch, Lewis Research Center, parties (and we do not exclude ourselves).
National Aeronautics and Space Administration, It is, therefore, useful to keep in mind
Cleveland, Ohio.
2 The boldface numbers in parentheses refer the simple essentials of the discipline
to the list of references appended to this paper. as we proceed to develop the subject
133
Copyright9 1965 by ASTM International www.astm.org
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134 FRACTURE TOUGHNESS TESTING

in the later sections. In the simplest provided with cracks of graded sizes to
terms, the fracture toughness of a mate- determine an empirical relation between
rial determines how big a crack the strength and crack size. But the problem
material is able to tolerate without frac- is not simply a matter of crack size. In
ture when loaded to a level approaching addition, crack shape, bulk of the mem-
that at which it would fail by excessive ber (that is, thickness of a plate), orienta-
plastic deformation. For example, how tion of the crack in relation to the fibering
big a crack could be tolerated in the of the material, temperature, and rate
wall of a pressure vessel manufactured of loading all may affect the fracture
from Brand X steel when the nominal strength of a structural member of a
hoop stress is raised to 90 per cent of the given material. To take into account
yield strength? all these factors in a purely empirical
Naturally, every reasonable effort test program would require very large
would be made to avoid having any numbers of specimens for each material
cracks or like defects in the structure. evaluated. The burden of testing can be
But grievous experience tells us un- considerably reduced, however, by apply-
mistakably that it would be quite un- ing knowledge of the mechanics of frac-
realistic to depend upon the total absence turing, which is best represented at the
of crack-like defects, however good our present time by linear elastic fracture
intentions. If something fairly quantita- mechanics.
tive about the crack tolerance of mate- We shall assume familiarity with the
rials were known, we could be more concepts, assumptions, and stress-analy-
realistic and could take more effective sis aspects of current linear elastic frac-
measures with regard to inspection, ture mechanics, since these are reviewed
quality control, proof testing, and avoid- in considerable detail in other contribu-
ance of development of cracks in service. tions to the symposium. For additional
For one thing, that material having the information, reference can be made to
greatest crack tolerance at the stress the reports of the ASTM Special Com-
level contemplated could be selected out mittee on Fracture Testing of High-
of those having adequate yield strength Strength Metallic Materials (5-9), here-
and that were satisfactory in other re- inafter referred to as the ASTM Special
spects. Or we could decide, according Committee on Fracture Testing. In these
to the application in mind, how far we references, the discussion is often in
could go in reducing weight and bulk by terms of K, the stress-intensity factor
employing materials of greater yield of the elastic stress field local to the
strength at the expense of reduced crack crack, rather than in terms of 9, the
tolerance. In this connection, the dimen- crack-extension force, or strain-energy
sions of cracks that have been discovered release rate with respect to crack exten-
to be the origins of fracture failures of sion. For reasons that will become appar-
critical structures range from a few ent, it is more convenient in this disserta-
thousandths of an inch in the case of tion to develop our subject primarily in
some steels with yield strengths ap- terms of 9 rather than K. This should
proaching 250,000 psi up to more than a cause no difficulty if the simple relations
foot in diameter in the case of at least between these two quantities are kept
one low-strength steel casting. in mind: K 2 = Eg for plane stress, and
The most direct way of evaluating the K S = E g / ( 1 - ~ ) for plane strain~
crack tolerance of a material apparently where E is Young's modulus and v is
would be to test a series of specimens Poisson's ratio.

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SRAWLEYA N D BROWN O N TESTING METltODS 135

A satisfactory fracture toughness specimens are necessarily more compli-


test, in the present context, is simply a cated than the simple expression E9 =
model fracture experiment designed to 7rata, which applies to a straight,
satisfy two essential requirements, through-thickness crack of length, 2a, in
namely: (1) the specimen dimensions a flat plate of width, W, greater than
and loading arrangement must be such 20a, under uniform tensile stress, ~.
that the value of the crack-extension Sufficiently accurate expressions have
force, 9, can be calculated with sufficient been obtained by mathematical or
accuracy at any stage of the test at experimental methods for a number of
which the values of the load and the useful types of specimens, which are
crack dimensions are known; and (2) discussed later. These include specimens
the values of the load and the crack that are loaded in bending as well as
dimensions at the point of instability of tension.
crack extension can be measured with While linear elastic fracture mechanics
sufficient accuracy. As will be shown is probably about the simplest form of
later, it follows from the first of these strength of materials approach that
requirements that the crack dimensions, could be taken in the study of fracturing
and therefore the dimensions of the speci- phenomena, it is nevertheless quite a
men in which the crack is contained, complex subject. This results from the
must exceed certain minimum values inherent complexity of the fracture
that increase as the ratio of E~, to the behavior of actual materials. Conse-
square of the yield strength of the mate- quently, the subject of fracture tough-
rial. Since there is a general tendency ness testing will be developed in stages,
for ~, to increase as the level of yield starting with a simple, idealized model
strength of structural materials is de- of a fracture toughness test specimen
creased, it follows further that the mini- that is referred to as the quasi-two-
mum necessary dimensions of a specimen dimensional prototype specimen. This
of a given type increase very rapidly as is an abstraction of the wide-plate speci-
the yield-strength level of the materials men referred to in the preceding para-
to be tested decreases. To illustrate this graph in which the thickness of the
point, whereas the over-all diameter of plate is ignored. This will allow develop-
the smallest circumferentially crack- ment of the important concepts of crack-
notched round bar necessary to measure extension resistance and fracture insta-
the plane-strain crack toughness, ~ , of bility in essentially two-dimensional
a steel having a yield strength of 300,000 terms. Next we consider the complica-
psi would probably be less than 0.2 in., tions associated with finite thickness and
the smallest diameter necessary for a the change in fracturing behavior and
steel having a yield strength of 150,000 apparent toughness as the thickness is
psi might exceed 5 in. varied through the transition from slant,
In order to minimize specimen dimen- or plane-stress, fracture mode to square,
sions as much as possible, thereby mak- or plane-strain fracture mode. This leads
ing most effective use of available test to consideration of the measurement of
material and testing machine loading plane-strain crack toughness, ~ , , which
capacity, types of specimens have been is of particular importance in that it
developed in which the dimensions of represents a practical lower limit to the
the simulated crack are appreciable fracture toughness of a material under
fractions of the over-all specimen dimen- given conditions. At this point we are in
sions. The expressions for ~ for such a position to consider practical specimen

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136 F ~ c r u m ~ Tovr TESTING

types that require reasonable amounts engineering method for dealing with the
of material and loading capacity. The risk of fracture.
narrow symmetrical plate types of speci-
men for general ~c testing are discussed SYMBOLS
first, and then several types of specimens length, half-length, or depth of
suitable only for gi~ testing are discussed crack according to type of speci-
in sequence. In these sections, the ques- men, Figs. 29-30; subscript 0
tion of ~ measurement capacity in refers to initial value; m refers
relation to specimen size is discussed for to measured value at instability
each type of specimen. A summary table A -- net cross-sectional area ot
is provided for comparison of the various cracked Charpy specimen
types of 9io measurement specimens. In B -- thickness of plate or bend speci-
men
the remaining sections the topics of test C half-length of surface crack,
instrumentation and procedure and Fig. 30(a)
certain aspects of specimen design and C, Co = compliance of selected gage
preparation are taken up. An appendix length of specimen, that is,
provides ready reference information on reversible change in gage length
the various types of specimens, giving per unit load; subscript 0 refers
proportioned sketches and appropriate to initial value of C for specimen
expressions for 9 in compact form in each without crack
case. Ca, Cxo = ~r or ~x, measurement capacity
We have one final comment before of specimen, that is, estimated
maximum value of ~ or ~ c
proceeding to the body of the disserta-
that could be measured with
tion. Some readers may tend to become acceptable accuracy for speci-
impatient with the complexity of the men of given dimensions made
subject and its incomplete status as they of material of given yield
proceed through the text. We would strength and elastic modulus
remind them that other branches of d, do = average diameter of crack-
applied mechanics of structural materials notched section of round
are no less complex nor more complete notched bar, Fig. 30(e); sub-
(for example, inelastic distortion of struc- script 0 refers to value without
tures). In his classic treatise (lo), Love plastic-zone correction
says "The conditions of rupture are but D = major diameter of round
notched bar, Fig. 30(e); also,
vaguely understood, and may depend distance of axis of loading from
largely upon these and other accidental cracked edge of single edge-
circumstances. At the same time, the notched tension specimen
question is very important, and a saris- e = displacement, that is, change in
factory answer to it may suggest in many selected gage length of specimen
cases causes of weakness previously E = Young's modulus; also, electri-
unsuspected, and, in others, methods of cal potential difference between
economizing material that would be two sdected positions on speci-
men; E0 refers to value of the
consistent with safety." The problems
electrical potential difference
that fracture mechanics sets out to solve for specimen without crack
are still somewhat vaguely understood, ~, ~i ___strain-energy release rate with
yet the progress that has been made in crack extension per unit length
recent years is most encouraging, and of crack border, or, crack-exten-
surely justifies what further effort is sion force; subscript I refers to
required to provide us with a sound opening mode of crack exten-

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SRAWLEY AND BROWN OK TESTING METHODS 137

sion; without subscript, mode is crack tip for a single edge-


unspecified notched tension specimen or
.~c, ~ic ffi critical value of ~ or ~z at point bend specimen
of instability of crack extension, O"N == net-section stress for round
taken to be measure of fracture notched bar
toughness of material O'y8 --uniaxial tensile yield strength
K, K~ --- stress-intensity factor of elastic (0.2 per cent offset)
stress field in vicinity of crack
front; subscript I refers to open- GENERAL CONSIDERATIONS
ing mode of crack extension;
without subscript, mode is un- The Quasi-Two-Dimensional Prototype
specified Specimen:
K~,Kx~ ffi critical value of K or K~ at It is desirable to discuss the general
point of instability of crack
concepts that apply to all fracture
extension, taken to be an alter-
native measure of crack tough- mechanics type toughness tests before
ness of material considering in detail the various types
L = effective length of fracture of fracture toughness test specimens that
toughness specimen; also, mo- are in common use. To do this we shall
ment arm length of bend speci- start with a simple, idealized model and
men, that is, half the difference then introduce systematically the various
between major and minor spans complications encountered with real
M = dimensionless coefficient in ex- specimens. We refer to this model as a
pression for 9 for round notched quasi-two-dimensional prototype speci-
bar men, and it m a y be visualized as a flat
P ffi load applied to specimen
r r , rlr = plastic-zone correction term sheet of width W, under uniform uni-
added to measured crack axial tension ~, and containing a straight,
length; subscript I applies to ideal crack of length 2a, less than W/IO,
plane-strain conditions and rtr in the center and normal to the direction
is taken to be rr/3 of the applied stress. The thickness is
R = crack-extension resistance of regarded as vanishingly small and the
material at crack tip that op- length sufficient so that the stress-field
poses ~] disturbance due to the crack is insignifi-
U = loss of pendulum energy in im- cant at the ends.
pact test, or, area under load- This model is an idealization of an
deflection curve of test of
otherwise similar plate specimen of finite
cracked Charpy specimen
W = width of plate specimen or thickness, B. For such a real specimen,
depth of rectangular section as we shall discuss later, the crack-front
beam specimen configuration m a y be quite complex,
v = Poisson's ratio and g (the crack-extension force per
$, ac ffi gross stress applied to specimen unit length of crack border, or strain-
in tension, that is, applied load energy release rate with crack extension
divided by WB in case of plate per unit length of crack border) has,
specimen, or 7rDi/4 in case of in general, a different value at each posi-
notched round bar; subscript c tion along the crack border. With the
refers to the point of instability
quasi-two-dimensional model we need
of crack extension
~t -- average net-section stress for a consider only a single value of 9, which
symmetrical plate specimen in we m a y regard as a sort of average value
tension for the real crack in the plate of finite
cnu,n = nominal stress at position of thickness. The state of the stress field is

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138 FRACXtlRE TOU6HNESS TESTING

assumed to be one of generalized plane less, they do have useful quantitative


stress, and the appropriate expression significance as measures of fracture
for ~ is E~ = Irg~a (11). toughness.
Criterion of Fracture Instability--In a In some of the literature on fracture
typical fracture toughness test, the load mechanics, ~, is defined in different
on the specimen is raised continuously terms, for instance, as the value of the
until a point is reached at which unstable crack-extension force at onset of rapid
crack extension occurs. In order to define crack propagation. Such a definition is
this more precisely, it has to be appre- too vague as an operational definition
ciated that the load is not the independ- for testing purposes, and may be even
ent variable in the test. The variable somewhat misleading in seeming to
that is actually most nearly under the imply that continuing slow crack exten-
control of the operator is the separation sion is to be expected at constant levels
of the heads of the testing machine. For of ~ less than ~c. Such behavior, fortu-
our purposes, this can be regarded as nately, is unusual and, when observed,
equivalent to the over-all extension of indicates a need for careful investiga-
the specimen, e, which will be taken as tion of the material and the environment
the independent test variable. (In the in which the test is conducted. To avoid
case of a bend specimen, e would be the ambiguity in conducting and interpreting
specimen deflection.) The criterion for fracture toughness tests, the precise
the point of instability of crack exten- operational definition of 9o is to be
sion in the test is, then, that the load, preferred.
P, as a function of e, reaches a stationary Crack-Extension Resistance and Occur-
value, that is, either a maximum or a fence of Instability--To appreciate the
point of inflection of zero slope. In conditions that must be satisfied in valid
mathematical terms, dP/de = 0. At fracture toughness tests, and to under-
this point, the ability to control the stand properly the results that are ob-
load is lost, at least temporarily, and tained, it is necessary to be familiar
that is why the load cannot be regarded with the current concept of the growth of
as the independent variable. resistance to crack extension during a
The value of ~ at the point of insta- test. This concept was originated by
bility can be calculated from measure- Irwin (12), and is mentioned in the first
ments of the load and the instantaneous report of the ASTM Special Committee
crack length at that point and is desig- on Fracture Testing, but has not been
nated 9~. Either ~ or K~ (equal to the given much emphasis heretofore. The
square root of E~o for plane-stress condi- most extensive previous discussion is
tions) is taken as a measure of fracture probably that given by Krafft et al (13).
toughness of the material. The essence of this concept is that, as
This operational definition of the the crack-extension force, 9, is increased
point of instability of crack extension, during a test, it is opposed by an in-
and the corresponding definitions of creasing resistance to crack extension,
~ and Ko, correspond to those adopted R, of the material at the crack tip, so
by the ASTM Special Committee on that equilibrium between ~ and R is
Fracture Testing (5). To correct a com- maintained up to the point of instability.
mon misapprehension, ~c and K~ are The crack-extension resistance, R, may
not necessarily independent of specimen be thought of as analogous to the increas-
dimensions other than thickness, as will ing resistance to plastic deformation due
be shown in the next section. Neverthe- to work hardening, which opposes the

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SRAWLEY AND BROWN ON TESTING METHODS 139

applied stress in an ordinary tension test. At instability, d(r/de = 0 by definition,


In this case also, there is a point of and Eq 1 reduces to
instability at which d P / d e = O.
By definition, ~ is equal to the value of (0910o),=,o = (aRIo~),_,~ . . . . . . . (2)
R at instability and beyond this point where g~ is the stationary value of o" at
increases more rapidly with e than does instability.
R. Now, although the values of ~ and R The significance of this is illustrated
are equal up to the point of instability, in Fig. 1, which shows a plane section
these quantities represent distinctly through the surface representing 9 as a
different physical entities and have function of ~ and a for the constant
different functional relations to the value of ~ equal to ~,. In the simple
subsidiary test variables, r and a. For case of the prototype specimen, the

==

~=
o~

t~
= f
R

Crack half-length, a
Fro. 1--Representation of the Crack-Extension Instability Condition as a Tangency Between
the 9- and R-Curves at a Unique Value of Applied Stress.

the prototype specimen, as noted earlier, trace of the ~ surface is the straight line,
= lr,T2a/E, but the dependence of R -= 7 r ~ 2 a / E , as shown. In general, it
on these variables has yet to be dis- would be an upward-sweeping curve.
cussed. Before doing this, it should be The curve representing R in the figure is
noted that there is a condition which a projection onto the plane section of a
must be satisfied at the point of in- three-dimensional curve representing a
stability that may be derived as follows. relation, as yet unspecified, among R, a,
Since (9 -- R) is equal to zero up to and a. This three-dimensional curve must
the point of instability, d(g - R) is also lie in the ~-surface up to the point Of
equal to zero up to this point. Expressing instability if R is equal to ~ up to this
this in terms of the subsidiary variables, point. Equation 2 expresses the condi-
and a, yields: tion that the trace of the g-surface in
d(~- R)/de = 0 = (O~/O~)(dzr/de) Fig. 1 must be tangent to the projection
o~ the R-curve at the point of instability.
+ (09/~a)(da/de) -- (OR/Oa)(d~/de) A similar figure for a constant value of
- (OR/Oa)(da/d~) (1) a less than , , would show the g-surface
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140 FRACTURE TOUGHNESS TESTING

trace intersecting the projection of the one point on the crack-extension resist-
R-curve. ance curve is determined, namely, the
In a fracture toughness test, as instability point for the particular
normally conducted, the value of only specimen used, which is called 9~. This

1000--

801}--
a.

.~ o
~.--q

A
f
D

i: 0

A Sharply defined instability.


I

I I
Crack extension, - a0

B Representative of actual behavior of A1 7075-T6, according to Krafft (13).


I

C Transient instability due to sudden extension in openhlg mode (pop-in) followed by further,
mixed-mode, stable crack extension.
D Discontinuous growth of crack-extension resistance characteristic of real materials to some
degree. Other examples are actually smoothed versions of this sort of behavior.
Fro. 2--Some Conceivable Types ol Crack-Extension Resistance Curves.

Parameter,
o C,
ksl
t 8o0 _ ,45 18

-//
~dT
" LOCUS
u=..
L - C~ 400
O

.2

-/V/
I
4 6 8 10
Crack half-length, a, in.
Fro. 3--Crack-Extension Instability Condition for Various Crack Lengths in a Brittle Material.

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SRAWLEY AND BROWN ON TESTING METHODS 141

is something like determining only the forms of R-curves and the factors upon
ultimate tensile strength in an ordinary which they depend. Krafft and co-
tension test. How nearly independent workers, however, have proposed a very
of crack length ~ will be for a group of plausible working hypothesis that is
tests on the same material, but using consistent with their observations (z3)
specimens with different initial crack and which will be utilized here. The
lengths, will depend upon the form of the hypothesis can be stated as follows: for a
R-curve for the material. To characterize given material in an inert environment
the fracture toughness of a material under given conditions of testing speed
thoroughly, it would be necessary to and temperature, the resistance to crack
determine the entire R-curve. Fortu- extension, R, is primarily a function of

Parameter,
1000 0 C,
ksi

US
~T
~d
t-'--

~162 40(]
o 0

i
o~

~: 20(

(.3

4 6 8 10
Crack half-length, a, in.
FIG. 4---Dependence of ~, on Initial Crack Length for Material Having Crack-Extension Re-
sistance Curve of Type B, Fig. 2 (A1 7075-T6).

nately, experience suggests that ~ is the magnitude of crack extension,


sufficiently independent of crack length (a- a0), and is independent of the
to provide a single-valued representation initial crack length, 2a0. This implies
of the fracture toughness of most ma- also that R is not directly a function of
terials for most practical purposes. Where ~, only indirectly in that both R and
this is not the case, the R-curve can be are related to (a -- a0). This hypothesis
determined by using a sufficiently large refers to an ideally sharp starting crack
specimen, and then used for a more and, in effect, assumes that an invariant
detailed study of a potential fracturing sequence of development of crack-front
situation than would be possible from configuration and associated plastic
a knowledge only of a single ~ value9 zone occurs as (~ - a0) increases, what-
The only published data on R-curves ever the value of 2a0. Study of the
seem to be those given in Ref. (is) for fracture surfaces of specimens having dif-
7075-T6 aluminum. Consequently, very ferent initial crack lengths lends con-
little is known, in general, about the siderable support to this concept of an

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142 FRACTVRX TOIICHNESS TESTING

invariant pattern of development for type B in Fig. 2. This curve is a good fit
specimens of the same thickness. At this to the data for 7075-T6 aluminum re-
point, the question of thickness is still ported in Ref (13). The dependence of
neglected, but will be dealt with in a 9o on initial crack length is quite con-
later section. siderable in this case, compared with
If this is accepted as a working hypoth- that shown in Fig. 3. When specimens
esis, the approximate form of the are used for which 2ao is about 0.3W
R-curves for a variety of materials can or greater, the situation is further com-
be inferred from unpublished data ob- plicated and ~ may have a maximum
tained by the present authors. Figure 2 value at some value of 2ao, as will be
shows some examples, Curves A, B, and shown later.
C, representing smoothed versions of To summarize thus far, some of the
actual behavior. The curves for real general aspects of fracture mechanics
materials are always more or less erratic toughness testing have been considered
on a fine scale, as indicated by Curve D. by referring to a quasi-two-dimensional
Curve A represents a case approaching prototype model specimen that has

r" Trace of plane of originating crack (under normal stress)

Slant V-slant 100 x/B, percent square Square


Fro. 5----RecommendedDescriptive Terms for Types of Fracture Surfaces Observed in Plate
Specimens Illustrated by SectionViewsTaken Normal to Direction of Propagation.

ideal brittle behavior, in which case ~, enabled us to defer consideration of some


would be virtually invariant. This point of the complexities involved when real
is illustrated in Fig. 3 which shows the specimens are considered. An operational
points of tangency of ~-traces to R- definition has been given of the point of
curves of type A for several different instability of crack extension in a test,
initial crack lengths. This figure and and ~c has been defined as the value of
others that follow are representations of the crack-extension force at that point;
the same kind as Fig. 1. In Fig. 3, the K~ is defined similarly. The concept of
R-curves are identical except for lateral crack-extension resistance, R, has been
displacements of the origins to different discussed, and the working hypothesis
values of the initial crack half-length. that R is primarily a function of the
For this type of R-curve, 9~ is almost magnitude of crack extension, (a - a0),
constant, the locus tending to slightly independent of initial crack length, has
lower values for shorter initial crack been assumed. On this basis, it has
lengths. In practice, behavior of this been shown that 9o may depend to some
sort is to be expected when the specimen extent on the initial crack length, the
breaks with a square, brittle-appeazing extent of the dependence varying accord-
fracture. ing to the form of the R-curve for the
Figure 4 is a plot similar to Fig. 3 material. Thus, ~ is not to be regarded
except that the R-curve is that shown as as an invariant property of the material,

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SRAWLEu AND BROWN ON TESTING METHODS 143

but rather as a somewhat arbitrary roughly flat, it is clear that the front of
underestimate of the limiting value of R an extending crack in a real plate is not
for a long crack in a wide plate of the even roughly represented by a straight
material. line, except possibly in the extreme cases.
Actually, as is well known, the front of a
Actual Cracks in Specimens o.f Finite square fracture is roughly parabolic with
Thickness: the most advanced point at mid-thick-
We are now in a position to consider ness. For a fully developed slant fracture,
real, wide-plate specimens of finite thick- the front is almost straight, as shown in
ness, B, in other respects similar to the Fig. 6(a). This has been established by
quasi-two-dimensional prototype. Any- terminating tests of steel specimens at a
one familiar with fractures of plate point short of instability. In each case.

ing ~ \.! I I

front
(a) Fully devetopedslant fracture.

Start- ~\\
,2 '3
\\\\ \\ \\\ 7 \\ X,, x\\
4 5 6
ing ,x I ~ t I , e) I
crack i J I / / / / / /
front // / ,/ / / / / /
// ,1 ii / I / / // // i / /
I/~f~'~ l t i. ~ i. !
r // r

(b) Predominantly square fracture.


FIG. 6--Schematic Drawing of Various Successive Positions of Crack Fronts, Shown as Dashed
Lines, in Specimens Having (a) Fully Developed Slant Fracture or (b) Predominantly Square Frac-
ture (about 70 per cent Square).

specimens knows the common forms the specimen was removed from the
that they might take, as illustrated by testing machine, heat-tinted to mark
schematic section views in Fig. 5. The the crack boundary (the use of a liquid
two extreme types of fracture are here staining medium for this purpose is not
referred to by the terms "slant" and reliable), then loaded again to complete
"square" in preference to the more the fracture. In the general case of a
usual terms "shear" and "flat." The mixed fracture consisting of a central
term "shear" is misleading because this square strip with slant borders, the crack
type of fracture does not necessarily front must be a nonplanar curve. A good
occur by relative displacement of the example of this case, obtained by the
two surfaces in their common plane, heat-tinting procedure, is illustrated in
and the term "flat" is ambiguous be- Ref (14).
cause a slant fracture can be as flat as a The value of 9 for a given load varies
square fracture. with position along the crack front
Since only the extreme slant and according to the curvature at that posi-
square types of fracture surface are tion. Unfortunately, no detailed analysis
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144 FI~ACTV~.E TOUGHNESS TESTING

has been made for a curved front of a It also involves the use of a plastic-
through-thickness crack in a plate, zone correction term, also discussed
though some insight can be gained by later. At this point it is sufficient to
reference to Irwin's discussion of the note that uncertainty about the value
case of a semi-elliptical part-through of 2a at instability is the largest source
crack (IS). Consequently, it has to be of error in 9c measurements.
assumed that a single average value of Dependence of 9o and Fracture Appear-
9 can be taken to apply to the whole ance on Thickness--For a given material
crack front with sufficient accuracy for at a given temperature and testing speed,
practical purposes. Essentially, the finite both the appearance of the fracture of a
thickness plate is treated in the same plate specimen and the 9, value will
way as the quasi-two-dimensional proto- depend upon the thickness. This de-

IQ0- 1000--

d
e do,z ~k~ I---B --d

I qxc
I
O.8
}
1.0
O 0,2 0.4 0.6
Thickness, B, In.
FIo. 7--Dependence of gc and Fracture Appearance (in Terms of Percentage of Square Fracture)
on Thicknessd Plate Specimens.Schematic,but Based on Data for Aluminum7075-T6.

type specimen, and it is important to pendence is not the result of the metal-
realize this because the generalized plane- lurgical processing involved in reducing
stress model is only an approximation to the plate to various thicknesses, be-
the real specimen, even in the case of a cause the effect can be demonstrated by
thin sheet specimen fracturing with a testing specimens of different thicknesses
fully developed slant fracture. Where obtained by machining from plate stock
apparent inconsistencies in test results of the same initial thickness. Metal-
occur, the adequacy of this model to lurgical processing effects may also occur,
represent the actual test specimen should but these should not be corffused with
be carefully reconsidered. the intrinsic effect of thickness.
The assumption of an average value The intrinsic effect of thickness is
of 9 involves some assumption about the illustrated in Fig. 7, which is based on
value of the effective crack length, 2a, data for 7075-T6 aluminum from Ref
to be used in calculating 9. This will (16). The curve is qualitatively typical of
depend on the method of measurement many high-strength metallic materials.
and will be discussed in a later section. The quantitative aspects, such as the

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SRAWLEY AND BROWN ON TESTING METNODS 145

peak value of ~,, the lower limiting value fracture toughness. In the case of square
for large thickness ~ , the thickness at fracture, it is usually assumed that the
which ~ is greatest, and the range of layer of associated plastically deformed
thickness over which the major part of material extends for a constant distance
the fracture mode transition occurs, are from the fracture surface, independent
all dependent upon the material and the of the plate thickness. On the assump-
testing temperature (and, in some cases, tion that the density of plastic-deforma-
on the speed of testing). For a particular tion energy depends only upon the
material at a particular temperature, distance from the fracture surface, then
these aspects depend upon the yield- the plastic work per unit thickness per
strength level when this is varied by unit crack extension, gi, will be inde-
thermal or mechanical treatment. pendent of thickness for a completely
The initial, ascending portion of the square fracture (13,17).
curve of ~, versus thickness is associated The subscript I refers to the first of
with fractures that are fully slant or three component modes of crack ex-
V-slant, and is commonly explained by tension distinguished by Irwin (1s-2o).
assuming that the volume of associated In this mode, the mating crack surfaces
plastically deformed material per unit separate as the crack extends so that
length of fracture is proportional to the their relative displacement is normal to
square of the thickness. This follows the fracture plane; hence, it is called
from the assumption that the patterns of the opening mode. It corresponds to the
plastic deformation for different thick- intuitive concept of cleavage separation
nesses in this range are geometrically (but should not be confused with cleav-
similar, which agrees with observation. age in a microcrystalline sense). Modes
If it is further assumed that the density II and III are referred to as the edge-
of plastic-deformation energy is constant sliding mode and the screw-sliding mode,
throughout the plastically deformed respectively (analogous to the concepts
volume, the plastic work per unit thick- of edge and screw dislocations in crys-
ness per unit crack extension, which is tals). In the two sliding-component
equated with ~,, is directly proportional modes, there is no relative displacement
to the thickness. Actually, the available of the mating crack surfaces in the direc-
data are only sufficient to confirm that tion of their normal, the surfaces are
g, does increase with thickness in this supposed to slide over one another either
range, not to confirm any particular in the direction of crack extension or
form of the relation. It seems unlikely normal to it. Any arbitrary mode of
that there should be a simple linear crack extension can be represented as a
dependence. linear combination of these three com-
The descending portion of the curve ponent modes, and the three quantities,
of ~, versus thickness is associated with ~i, ~ u , and ~ux, are the corresponding
the occurrence and progressive domi- rates of transfer with crack extension of
nance of square-fracture surface in the energy from the surrounding elastic
center of the plate thickness. At suffi- strain field to other forms 08).
ciently large thicknesses, the slant frac- From a macroscopic point of view,
ture borders occupy a negligible propor- square fractures are usually considered
tion of the total fracture surface, and to result from simple mode I crack ex-
~ approaches a lower limiting value, tension in a gross sense. In microscopic
,qIc, referred to as the plane-strain frac- detail, they are quite complex and may
ture toughness, or the opening-mode involve a variety of fracture modes, as

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146 FRACTURE TOUGHNESS TESTING

discussed in another contribution to this given temperature and rate of testing.


symposium. In practice, 9ic refers to the The possibly lower values of ~ for
gross average toughness value for macro- very small thicknesses are only rarely of
scopic opening-mode crack extension. practical importance, and apparently no
Slant fractures that occur when speci- such values have yet been measured for
mens are loaded in tension (in contrast any material. There are many practical
to torsion) are not the result of pure applications where the fracture, if it
sliding-mode crack extension in a gross occurred, would be virtually completely
sense. As can be deduced by observing square, and the relation of load-bearing
such specimens during tests, the corn- capability to crack dimensions would be

18xlO
3

16~ /

14
A

.Q

12 - -

4 t'-
10 ~_

oT ~.,-10~av - . (- O.07-in., crack extension)~ I


Electric otential change
Fro. 8--Typical Examples of Load Versus Electric Potential Records for Single-Edge-Notched
Specimens of a Maraging Steel Aged 3 Hr at 600 F, A; 1000 F, B; and 800 F, C.

ponent of relative displacement normal governed by 9i~. Even when the section
to the crack surfaces is considerable. of the load-bearing member is thin
Fractographic examination confirms that enough so that the fracture would be
this must be so because the ductile partly or entirely slant, the load-bearing
dimples observed on slant-fracture sur- capability might be governed by ~
faces of specimens broken in tension are rather than by the value of 9~ measured
not generally pronouncedly elongated in for the actual thickness, unless the ratio
one particular direction (21). 9~/~io exceeded some value that would
The plane-strain, or opening-mode, depend upon the shape and size of the
crack toughness, ~i~, is of special im- initial crack. More detailed discussion
portance in that it represents a practical of this point can be found in Refs (6)
lower limit to the fracture toughness of a and (20). From the point of view of
material in a given condition and at a having a single value representing the

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SRAWLEY A N D :BROWN ON TESTING METHODS 147

fracture toughness of a material, 9~o of the importance of 9i~, a number of


is independent of the dimensions of the different types of specimens have been
specimen (provided that these are suffi- developed for measuring it. At this point,
ciently large for a proper ~o measure- it is convenient to discuss the concept of
ment) in contrast to ~o, which depends metainstability and the so-called pop-in
strongly on thickness and to some extent method of measuring ~r,, which applies
on crack length, as we have seen. Of to several of these types of specimens and
course, materials exhibit nonuniformity which makes it possible to use thinner
and anisotropy with respect to 9~o, specimens than would be required to
just as they do for other properties, and obtain an almost entirely square fracture.
this has to be taken into consideration in The pop-in method of ~ determina-

lO001-

8OO- qr

40O

03

<..)
a I
O.Z 0.4 0.6 0.8 1.0
Crack half-length, a, in.
FIO. 9--Meta-instability (~ic) and Ultimate Instability (go) for Wide Plate Specimen Exhibiting
Pronounced Pop-In Behavior.

evaluating a material. In general, in the tion was first proposed by Boyle et al


absence of more specific information, it (22) who observed in tests of sheet speci-
will always be a safe practice to use a mens of 7075-T6 aluminum that the
properly determined value of ~ c as first appreciable extension of the crack
the measure of the toughness of a ma- occurred as a distinct burst or pop-in
terial, except possibly in some cases of that was then followed by a stage of
very thin sheet or foil. gradual crack extension as the load was
~c Measurement at Meta-instability further increased. The same phenomenon
or Pop-in--The most obvious way to had been observed by numerous other
measure ~ c would be to test a sufficiently investigators in the form of an audible
thick plate specimen of the material. ping or click at the pop-in load, but its
This might not always be convenient, significance had apparently not been
or even possible, and certainly would not appreciated. Boyle and co-workers were
be very economical of material. Because able to show that the value of 9 at

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148 FRACTURE TOUGHNESS 'rESTING

pop-in was essentially the same as the ambiguous, and example A is apparently
value of 9~,, which would be determined not interpretable in terms of pop-in at
with a sufficiently thick plate specimen. all. In the case of example C, the heat-
The term "pop-in" is descriptive of tinting procedure showed that the shape
what actually occurs, namely, an abrupt of the crack front after pop-in was ap-
extension of the crack front from its proximately that shown as position 5 in
initial position to some position such Fig. 6(b), although the fracture in this
as that labeled 5 in Fig. 6(b), while the case was less than 50 per cent square.
load remains constant or even drops These three examples serve to make the
slightly. The crack movement can be further point, to which we return later,
followed during a test by using the out- that distinct pop-in behavior is not

=:
qc
r
_.o ~

r ~..
~o

Crack half-length, a0 in.


A Short crack, specimen breaks at load corresponding to ~I,.
B Long crack, ultimate load is considerably higher than that corresponding to ~19 Significance
discussed in text.
FIc. 10--Instability Behavior of Wide Plate Specimens Having Different Crack Lengths.

put from either an electrical potential always observed and, therefore, cannot
measuring device or a displacement gage be depended upon for ~z~ measurement
to drive an X - Y recorder, as discussed in all cases.
in a later section. Figure 8 shows three When pop-in does occur, it satisfies
contrasting examples of electric poten- the instability condition d~/de = O, but
tial change (at constant current) versus the instability is only temporary, so
load for specimens of restaging steel 0.2 that it is referred to as meta-instability.
in. thick. Example A represents material It will now be considered in terms d the
aged 3 hr at 600 F, B aged at 10O0 F, crack-extension resistance curves that
and C aged at 800 F. The arrows indicate were discussed earlier. Figure 9 shows
interruption of the tests for heat-tinting a projected curve d R versus a which is
to mark the crack-front positions. derived from the records of tests of the
Whereas example C exhibits very distinct maraging steel aged 3 hr at 800 F, the
pop-in behavior, example B is somewhat records being similar to example C d

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SRAWLEY AND BROWN O~ TESTING METHODS 149

Fig. 8, but carried to more advanced force of the excess elastic strain energy
stages. As the specimen is extended, the of the system. This may be referred to as
slope of the ~ versus a trace increases in the ultimate instability point of the test
proportion to ~. The g-trace intercepts as distinguished from the meta-instability
the R-curve so that equilibrium is main- that occurs at 9I*.
tained until the step in the R-curve is One of the consequences of the hypoth-
reached. At this point, the value of R esis that the value of R is a function
over a certain interval of (a - a0) is less only of (a -- a0) is illustrated in Fig. 10.
than the value of ~ corresponding to the This represents two wide-plate speci-
stress at the point, ~,o. Thus, the balance mens, supposedly identical except that
between ~ and R is temporarily upset the initial crack lengths are different.

o=
.m 9

-~7
~.---

"5
J
k B

hin Thick
,peclmen specimen
R
Crack half-length, a, In.
A Thin specimen, no well-defined pop-in.
B Thick specimen, pop-in occurs at maximum load.
FIG. ll--Extreme Cases of Pop-In Behavior.

until the crack has extended to the point The R-curves are, therefore, identica,
al, or somewhat beyond. The extent to but originate at different values of a0.
which the load drops in this interval is a The behavior of the specimen with the
function of several variables. However, longer crack, case B, is the same as that
and R will again become balanced at described in connection with Fig. 9.
some value of a slightly greater than The behavior of the specimen with the
al, and will remain so, on the average, shorter crack, case A, will be different
until the point ~c is reached. Beyond in that ultimate instability will be
this point, the load cannot increase reached at 9ic, that is, the load cannot
further, and, even though extension of increase beyond the value reached at
the specimen is halted at this point, the pop-in. If extension of the specimen is
excess of ~ over R will continue to in- maintained at a steady rate, the load
crease with increasing a, so that crack will drop at pop-in, then may increase
extension accelerates under the driving again slightly, but the load at which

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150 FRACTURE TOUGHNESS TESTING

g and R are equal at any subsequent Example B in Fig. 11 represents the


stage of crack extension will always be other extreme, in which the developed
less than the pop-in load. Thus, the load- fracture of a plate specimen is almost
bearing capability of the specimen is entirely square, the pop-in is very pro-
controlled by ~i, and not by some higher nounced, and the subsequent increase in
value of ~,, even though a higher value R is very gradual because there is very
could be measured by using a specimen little development of slant-fracture bor-
with a longer crack, as in case B. This ders. For any practical initial crack
comparison emphasizes the point that length, the load cannot increase beyond
was made earlier about the controlling the value at pop-in, so that ~ic is well
significance of 9Io in some cases, bearing defined by the maximum load value and
in mind that test specimens are nothing the initial crack length. The record of
more than simple examples of structural load versus crack length in this case will
members. show a sharp peak at the load correspond-
Two contrasting examples of schematic ing to ~ic, followed by a rapid decrease
R-curves are shown in Fig. 11. Example of the load.
A represents a relatively thin specimen In this section an attempt has been
in which the developed fracture is fully made to describe and explain the pop-in
slant and the initial, triangular region of phenomenon and its use for gio measure-
square fracture (see Fig. 6(a)) is quite ment by reference to the Krafft hypothe-
small. The magnitude of the pop-in is sis of an invariant curve of R versus
reduced to the point where it cannot be (a - a0). It is worth repeating that this
detected with confidence, and 9~c cannot hypothesis, while probably a good first
be measured with any confidence of approximation, may require some modifi-
accuracy. In a case like this, it may be cation in the light of future experimental
possible to obtain a well-defined pop-in information. In fact, it will be an im-
measurement of 9i, if a specimen of portant aspect of fracture mechanics
sufficiently greater thickness can be research in the immediate future to
tested. But it should not be assumed that conduct experiments designed to test
this will always be the case. The authors and extend this hypothesis. It seems
have found, by using SAE 4340 steel likely that, while the dominating factor
specimens, for instance, that well- upon which R depends for a given ma-
defined pop-ins do not always occur terial, thickness and testing conditions,
even when specimens are used that are is indeed (a - a0), there may well be a
sufficiently thick for the developed secondary influence of initial crack
fractures to be more than 50 per cent length. This might be quite significant
square. This raises the question of how when the initial crack length is suffi-
9~ might be measured for such materials, ciently short so that the net section
but there is no satisfactory answer to stress at gc approaches the yield strength
this question yet. It is hoped that re- of the material. This is a situation that
search currently in progress may resolve might be avoided in fracture mechanics
the matter. While it is sometimes as- testing but that is not always avoidable
sumed that 9io measurements can always in practical fracture problems.
be satisfactorily made by testing round
notched bars of sufficient size (which are PRACTICAL SPECIM[EN TYPES
discussed later), there is really no con- The discussion has so far centered
clusive evidence at the present time around fiat tension specimens having
that this assumption is warranted. transverse cracks of length less than one

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SRAWLEY AND BROWN ON T~STINO METHODS 151

tenth the specimen width. These are introduced to represent the maximum
conveniently simple for the purpose of value of 9~ that could be measured with
discussing general concepts. In subse- acceptable accuracy with a specimen of
quent sections, various types of speci- given dimensions made of a material of
mens will be considered that are more given yield strength and elastic modulus.
suitable for practical testing purposes, This will allow a summary comparison
~ither because they require less material to be made of the different types of
and lower testing load capacity, or specimens for 9r, testing, which indi-
because they provide conditions of cates the merits and limitations of each
greater elastic constraint. First, two type.
types of specimen will be considered
that are primarily intended for general Symmetrical Plate Specimens for General
9c (mixed mode) toughness testing but 9o Measurement:
that may sometimes be used for 9i, These two types of specimens are
measurement by the pop-in method. illustrated in Fig. 29 (see the Appendix).
Then those specimen types that are re- The center-cracked type (a) is provided
garded as suitable only for 9i~ measure- with a simulated central transverse
ment will be considered. While the crack of initial length, 2a0, equal to
specimen types discussed here are those about 0.3W, where W is the width; it is
having the most general application, obviously a modification of the wide-
there are numerous other types that have plate specimen having a longer crack
been, or could be, devised for special for a given width. The symmetrically
purposes, the only qualification being edge-cracked type (b) is provided with
that a satisfactory specimen design equal transverse edge cracks of initial
must be amenable to a sufficiently length, a0, equal to about 0.15W. These
accurate stress analysis to obtain an two specimens are essentially equivalent
accurate expression for 9. This could be except for a slight difference in the
obtained either mathematically or ex- expressions for 9, and the choice be-
perimentally, as illustrated by Refs tween them is mainly a matter of con-
(23) and (24), respectively. In particular, venience in preparation. The discussion
Winne and Wundt (25) have discussed will, therefore, be confined largely to the
the use of notched rotating disks, and center-cracked specimen with the under-
Ripling et al (26) have discussed speci- standing that it applies in general equally
mens for measurement of fracture tough- to the symmetrically edge-cracked speci-
ness of adhesive joints. men.
In connection with each of the prac- The elastic strain energy field in the
tical specimen types we shall discuss the vicinity of the ends of the crack is
appropriate expression for ~ and the appreciably influenced by the proximity
value of the effective crack length to be to the free edges of the specimen when
used in calculating 9, including the 2a/W exceeds about 0.1. Consequently,
plastic-zone correction term that is added 9 is then no longer given with sufficient
to the observed value of the actual crack accuracy by the equation, E 9 = lr~2a.
length. We shall also discuss the capaci- The appropriate expression recom-
ties of the various types of specimens mended by the ASTM Special Com-
for measurement of 9o or ~i~ in relation mittee on Fracture Testing (5) is the
to specimen size. For this purpose, an tangent form derived by Irwin (12,18)
unfamiliar symbol representing the 9c from an analysis by Westergaard (27):
measurement capacity, namely Co, is E9 = g2W tan (Tra/W). An earlier

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152 FRACTUP,t TOUGHNESSTESTINO

expression was derived by Kies (28) 0.2 per cent offset tensile yield strength.
from the work of Greenspan (29), and For a state of plane strain, usually as-
is known as the Greenspan or poly- sumed for ~ measurements, rzr may
nomial form. While this form is occasion- be taken as one third of the plane-stress
ally still used, it is preferable to use the value, that is, E~/6r~rs ~. The basis
tangent form in the interests of con- for these correction terms has been
sistency with the majority of investiga- thoroughly discussed in the literature
tors. To show that the difference between (5,12,30) and is also discussed in other
these expressions is not inconsequential, papers in this symposium, so that no
they are compared in Fig. 12 on a di- extensive discussion is needed here. It is
mensionless basis, E~/Tra2a, which is important for our purpose, however, to
equal to the configurational or geometric emphasize the point that this method of
3.0

,.,Ix I/
2.5
//
2.0
~176 //
1.5

1.0 - I I I
0.2 0.4 0.6 0.8 1.0

Fzo. 12--Comparison of the Irwin Tangent Expression and the Greenspan Equation for Sym-
metrically Center-CrackedPlate Specimens.

factor in each case, being plotted versus correcting an assumed elastic stress
za/w. analysis to take account of inelastic
Effective Crack Length and Plastic- strain in a limited region is somewhat
Zone Correction Term--The value of the arbitrary and approximate. For this
effective crack length, 2a, which should reason, calculated values of ~ should be
be used in calculating ~ from the tangent regarded as increasingly inaccurate, the
equation given above, is not simply the greater the ratio rr/a. This is one factor
estimated average length of the actual that should be considered in deciding
crack at instability, 2a.., but also how large a specimen is needed for an
includes a term, 2rr, to correct for the accurate measurement of go, but the
stress-relaxing effect of the plastically basis of the current recommendation of
deformed zones at each end of the crack; the ASTM Special Committee on Frac-
that is, a = am + r r . When a state of ture Testing on this point is somewhat
generalized plane stress is assumed, as different, as is discussed later.
in the case of a 9~ measurement at The cMculation of ~ is complicated by
ultimate instability, r r is taken to be the inclusion of the plastic-zone cor-
equal to Eg/2~r~rvs~, where ~rs is the rection term, which itself is a function of

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SRAWLEY AI~D BROWN ON TESTING METHODS 153

9. Except in the simplest case of the cracked specimen of a given width, W.


wide-plate specimen, ~ cannot be ex- For this purpose the ASTM Special
pressed as an explicit function of the Committee on Fracture Testing has sug-
load and the specimen dimensions, and gested the criterion that the go measure-
must be calculated from the implicit ment will be sufficiently accurate if the
equation by either a graphical or an average net-section stress at instability
iteration procedure. The graphical pro- does not exceed 80 per cent of the 0.2
cedure for the symmetrically cracked per cent offset tensile yield strength,
plate specimens is described in Ref (s). ~r8 0). This is a tentative recommenda-
The iteration procedure is simply a mat- tion, based upon a limited number of
ter of first calculating a first approxima- tests of specimens having different
tion to ~ by neglecting r r , next a second widths and crack lengths which indicated
approximation to 9 entailing a value of that 9o was independent of width and
rr based on the first approximation to crack length when this condition was
9, and so on. Convergence will normally satisfied. It would appear that the ma-
be very rapid, and the iteration pro- terials used for these tests must have
cedure is the natural one to use for a R-curves of a type that would result in
digital computer calculation program. 9o being insensitive to crack length,
9o Measurement Capacity in Relation that is, like type A in Fig. 2 rather than
~.o Specimen Size--If the width of a like types B or C. It should be noted
center-cracked plate specimen is less that there is a distinction to be made
than some value that is directly propor- here between an intrinsic dependence of
tional to the value of 9, to be measured, ~c on crack length due to the shape of
the average net-section stress at insta- the R-curve, which exists even when the
bility will exceed the uniaxial tensile test is well represented by the linear
yield strength of the material. A test of elastic stress field model, and an apparent
this sort is not represented even approxi- dependence of g~ on crack length that
mately by a linear elastic stress field occurs when the average stress is too
model, and therefore does not provide a close to yield to be properly represented
useful measurement of 9~ Even when by the linear elastic model.
instability occurs at an average net- Substituting the condition, crn,t =
section stress less than the yield strength, 0.8~rs, in the tangent equation yields,
the accuracy of ~ measurement is lower, for Cg, the maximum value of 9, that
the greater the value of rr/a, as men- could be measured with acceptable
tioned above. The ratio rr/a increases in accuracy for a given yield strength,
proportion to the square of the ratio of elastic modulus, and specimen dimen-
the average net-section stress to the sions:
yield strength for a given value of 2a/W.
It follows that the larger the specimen G -~ 0.64(qrsVE)
that is tested, the more accurate the 9W [ 1 - (2a,./W)] 2 t a n (~ra/W)
measurement of 9o is likely to be. Similar
considerations apply to the specimens where am is the estimated average half-
for gr~ testing, which will be discussed length of the actual crack at instability,
later. anda= am+ft.
It is of considerable practical impor- This expression for Cg can be regarded
tance to be able to estimate how large a as the product of four distinct factors,
value of gc could be measured with ac- each having a particular significance:
ceptable accuracy by using a center- (1) the numerical constant 0.64 repre-

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154 F~cTtrR~ TOUGHNESS TESTING

sents a factor of utilization based upon varied over a considerable range for a
experimental results; (2) ,rs~/E repre- given value of W, as indicated in Fig.
sents the dependence of Cg on the 29, and will be discussed later.
properties of the material under test; From the expression for Cg given
(3) the width, W, is the characteristic above, it follows that the most efficient
dimension representing specimen size; value of 2am/W will be that for which
and (4) [1 - (2a,,/W)]~ tan (za/W) is a the quantity 0.6411 - (2a,~/W)]2 tan
dimensionless factor representing the (Tra/W), which is equal to ECJ~rs2W,
effect of ratio of crack length to width. is greatest. This is plotted versus 2am/W
The length of the specimen should be in Fig. 13, showing that the maximum
proportional to W, and chosen to be occurs in the range of 2am/W between

~f
0.20

~176
0.0I/O'M
5~ {I "Zarn/W)Ztan (~a/W)"ECq~S W

| I I I I J
0 0.2 0.4 0.6 0.8 1.0
2an
FIG. 13--Measurement Capacity of SymmetricallyCenter-Cracked Specimensas a Function of
Relative Crack Depth.

sufficient so that there is a region of 0.3 and 0.4. This is the basis for the
uniform stress distribution between the recommendation that 2a0 should be
crack and each of the end regions of the about 0.3W for the center-cracked
specimen through which the load is specimen. The useful range of 2a,,/W
applied. Photoelastic studies have con- extends up to about 0.6; beyond this
firmed that the proportions of the point, the accuracy of the expression for
specimens shown in Fig. 29 of the appen- ,q becomes increasingly dubious (12).
dix are just about sufficient for the Furthermore, the accuracy of the esti-
pin-loading method shown. With pro- mate of ~ becomes increasingly depend-
portionately shorter specimens, the ent on the accuracy of the value of a
interference between the stress field of that is used, and this is the least accurate
the crack and that of each of the loading of the several measurements from which
pinholes would be appreciable. Specimen 9 is calculated. Thus, if 2a,~/W exceeds
thickness for ~c measurement may be 0.6 in any test, the result should not be

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SRAWLEY AND BROWN ON TESTING METHODS 155

used for anything more than a rough exceed about 0.2, so that any associated
estimate of ~ . Additional tests of error in 9 would be likely to be less than
wider specimens are necessary for 5 per cent.
accurate ~, measurement in such cases. Bearing in mind these considerations
For values of 2a,~/W much less than regarding accuracy, we may estimate
0.3, limitation of the average net-section the ~ measurement capacity of a center-
stress to 80 per cent of the yield strength cracked specimen, Cg, by referring to
may not be a sufficient indication that Fig. 13. The value of the ordinate for a
an acceptably accurate determination of given value of 2am/W is equal to the
~ will result. The reason for this is value of ECJ~rs2W. When 2a,~/W is
that, for crnet = 0.8~rs, the ratio rr/a between 0.3 and 0.45, Cg is slightly
increases as 2am/W decreases, as shown greater than 0.2Wgr~/E, and this value
in Fig. 14. To a first approximation, if may be regarded as the maximum 9~

ryla O.2

0.1~

I I I
0.2 0.4 0.6 0.8 1.0
2.dw
Fro. 14---Ratio of Plastic-Zone Correction to Effective Crack Half-Length as Function of rr/a
f o r Crne, -- 0.8 a r ~ 9

the estimate of r r as E~/21rgrs2 is in measurement capacity of the center-


error, the consequent error in the calcu- cracked type of specimen. The maximum
lated value of ~ will be proportional K~ measurement capacity is, therefore,
to rr/a multiplied by the error in r r . about 0.45~rsW 1/~. The same figures
In Ref (3o), it is suggested that the value can be used in estimating the toughness
of rr is unlikely to differ from the esti- measurement capacities of symmetrically
mate E~/21r~rs ~ by more than about edge-cracked specimens.
4-25 per cent, so that the consequent Variation of ~c with Crack Length and
error in the calculated value of ~ would Specimen Width--The preceding discus-
be expected to be no greater than 25rr/a sion of ~c measurement capacity involved
per cent. The value of this limit in- the implicit assumption that ~ would
creases from 4.4 per cent at 2am/W equal be independent of initial crack length,
to 0.3, to 8 per cent as 2am/W approaches as would be the case for a material with
zero (from Fig. 14). In general, it would an R-curve similar to type A in Fig. 2.
seem desirable that rr/a should not Assuming ~r to be independent of initial

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156 FRACTURE TOUGI~NESS TESTING

crack length enabled us to avoid an in. in each case. These g-traces are no
unduly complicated discussion of ~ longer straight lines, as in Fig. 4, but are
measurement capacity, and the con- constructed from the equation, E~ =
clusions reached are not substantially a~W tan (za/W), the appropriate values
different from those that would have of . required to satisfy the tangency
followed from a more general discussion. condition being obtained by graphical
Having dealt with the question of ~c interpolation. As discussed earlier, the
measurement capacity in this manner, points of tangency represent the values
it is now necessary to return to the of ~. that would be measured according
question of how ~ might depend upon to our criterion of instability. The main
crack length and specimen width in the point of Fig. 15 is that, for a given initial

qc for W of 12

.~ 30(3-- q curves
~'~" for W ofl2~, // / I
~= 6~,',

J
0 0.2 0.4 0.6 0.8 LO 1.2
Crackhalf-length, a, In.
FIG. 15--Dependenceof 9~ on SpecimenWidth, W, for Center-CrackedPlate SpecimensHaving
the SameInitialHalf-Crack Length.

case of a material having a different crack length and an R-curve of this type,
kind of R-curve, for instance, type B of the measured value of 9o decreases as
Fig. 2. This question was discussed the specimen width is decreased. Further-
earlier with reference to center-cracked more, the dependence of ~c on W is
plate specimens for which 2a/W was stronger, the larger the value of 2ao/W.
less than 0.1 (Fig. 4); we now extend These conclusions are, of course, drawn
the discussion to consider specimens for from a construction on the basis of the
which 2a/W is greater than 0.1. hypothesis that R is a function of
Figure 15 shows an R-curve that is (a -- ao) only (13). The results given in
identical with those in Fig. 4 apart from Ref. (13) for 7075-T6 aluminum are
scale. The particular g-traces that are generally consistent with Fig. 15, the
tangent to the R-curve for specimens R-curve in that figure having been ob-
of widths 2, 3, 6, and 12 in. axe also tained from those results, but the agree-
shown, the initial crack length being 1 ment between measured and predicted

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SRAWLEY AND BROWN ON TESTING METHODS 157

values of ~, is no more than fair. This two effects oppose one another when the
simply means that more extensive specimen width is kept constant and
experimental investigation of the hy- the crack length varied, as in Fig. 16.
pothesis is needed; the fact that ~ The crack-length effect dominates for
may depend upon specimen width in the the smaller values of 2at~W, resulting
manner shown by Fig. 15 is not in in an initial increasing trend of ~ with
question. However, the degree of the 2ao/W. For values of 2ao/W greater
dependence will depend upon the ma- than about 0.35, however, the effect of
terial, its thickness, and upon testing the restricted specimen width dominates
speed and temperature, and may be and the trend is reversed. Of course,
imperceptible in some cases. this is just one example, and it is to be

=
o .
'~,~
~'~
40(

~.-~
z_

.o
~ 200

~_~~
"

0.2 0,4
n.4 ~ 2adwJ I
0.6 0.8 1.0 1.2
Crack half-length, a, in.

FIO. 16---Dependence of gc on Relative Initial Crack Length for a Finite Width Specimen Having
an R-Curve Identical to That of Figs. 4 and 15.

Figure 16 shows the predicted de- expected that the form of the g-locus
pendence of 9c on 2ao/W for a fixed will vary with the form of the R-curve,
specimen width of 3 in. when the R-curve but the opposing effects will exist to
is identical with that of Fig. 15. The some degree in any case. Perhaps the
value of ~ does not vary greatly over the most important point to make about
range of 2ao/W between 0.2 and 0.5, this is that it is possible to obtain a
and the locus has a maximum at 2ao/W false impression of the degree of inde-
equal to about 0.35. The contrast be- pendence of ~, from a series of tests in
tween this figure and Figs. 4 and 15 which the specimen width is kept con-
is rather surprising. The explanation is stant and the initial crack length is
that ~, increases with increasing crack varied.
length, as in Fig. 4, but decreases as Since the measured value of ~, will
2ao/W increases for a given value of the depend upon both ~nitial crack length
initial crack length, as in Fig. 15. These and specimen width to a greater or

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158 FP.ACTtrRE TOUGHNESS TESTING

lesser degree, depending upon the form materials to a preferred few. These
of the R-curve for the material and would then be subjected to more ex-
thickness under investigation, there is tensive testing involving a range of
some question as to how to make use of crack sizes, perhaps even to determina-
particular ~, measurements. This ques- tion of the entire R-curve for the thick-
tion cannot be satisfactorily answered ness of interest. What is most important
until the R-curves of a sufficient variety is that it should be appreciated that
of materials have been determined and neither the planning nor the interpreta-
evalm~ted in sufficient detail. At the tion of 9o tests is a routine matter.
present time it would seem only prudent Before leaving the subject of ~c test-
to evaluate g, for several crack lengths ing to take up 9~* testing, we need to
in the case of any material and thickness discuss the question of specimen thick-
th:-t is intended to be used in a particular ness. This will lead naturally into a
application. general discussion of 9~c measurement
As far as evaluating the fracture and then to consideration of other types
toughness of materials in general is of specimen for this purpose.
concerned, ~ , is apparently independent Thickness of Symmetrical Plate Speci-
of any specimen dimension and thus mens-The ASTM Special Committee
provides an invariant fracture charac- on Fracture Testing has recommended
teristic for many of the materials of that the specimen thickness, B, for
engineering interest. This is the main mixed mode or slant mode 9, measure-
reason why effort on ~c testing has in- ment should be between W/45 and
creased in recent years at the expense of W/16, except that the lower limit need
effort on ~, testing. not apply if proper measures are taken
We do not wish to leave the impres- to prevent buckling around the crack
sion, however, that 9o testing should be when B is less than W/45 (5). In the
abandoned in favor of 9io testing ex- experience of one of the authors, buck-
clusively. Rather, we would suggest ling of symmetrically edge-cracked speci-
that 9, tests should be conducted pri- mens is less apt to occur than is the case
marily in relation to specific structural with center-cracked specimens. In any
components and should be conducted in case, supporting the specimen between
sufficient detail that the 9~ values de- lubricated face plates is an effective
termined are relevant to circumstances method of preventing buckling of thin
of failure that are pertinent to the com- specimens and ensuring that accuracy
ponent in question. For example, in an of ~ measurement is not impaired
airplane skin, tolerance for a crack thereby.
several inches long is desirable, if not The restriction that B should not
mandatory, but in a rocket casing it may exceed W/16 applies only when it is
be necessary to use materials that cannot desired to measure ~,, as distinct from
tolerate cracks that are only a fraction of ~ o , by the pop-in method. It has to do
an inch long. These different cases call with the change in crack-front configura-
for different approaches to 9o testing. tion as the crack extends from the initial
Material selection in relation to risk fatigue crack front, which is nearly
of fracture should entail at least two square and straight, in the stable range
stages. The first, screening stage would preceding instability. It is useful at this
utilize a standardized specimen appro- point to refer to Fig. 6. With the assump-
priate to the application and would tion that the crack will eventually
serve to reduce the number of candidate develop into the slant type (the most

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SRAWLEY AND B R O W N ON TESTING METHODS 159

extreme case), the distance over which of any additional information, we shall
the development takes place will be make use of the conclusion from Ref (22)
roughly proportional to B, and of about that B should not be less than 2E~J
equal magnitude (Fig. 6(a)). For 2ao/W 7r~r82, as a necessary condition for a
equal to about 0.3 and B not greater satisfactory pop-in ~ c measurement. It
than W/16, development of full slant should be appreciated, however, that it
fracture should be completed at some is not necessarily also a suffcient condi-
value of 2am/W less than 0.6. For tion in all cases. As mentioned earlier, it
greater thicknesses, there is a possibility appears that some materials may not
that development of full slant fracture exhibi* an:~ distinct ~o meta-instability.
may not be complete when 2am/W In Ref (22) it is also suggested that the
equals 0.6 and instability might occur specimen width for ~Ie measurements
at some value of ~ lower than that can be as small as lOE~i~/zr~rs2. This
appropriate to the thickness and width. corresponds to a restriction of the average
While no specific data are available on net-section stress to be less than the
this point, general experience indicates yield strength, rather than less than 80
that there is good reason to respect this per cent of the yield strength as recom-
restriction. mended by the ASTM Special Com-
For materials of such thickness that mittee on Fracture Testing for ~
the specimen will exhibit a predomi- measurements. Until more data become
nantly square fracture, the restriction available to support the less restrictive
could be less severe, as implied in Ref. estimate of Ref (22), it appears advisable
(5). For ~ie measurements, there appears to adhere to the ASTM committee's
to be no basic reason to impose any recommendation for ~ pop-in measure-
upper limit on the thickness, but there ment as well as for ~ testing, and we shall
is an optimum value of the ratio B/W, do so here.
as we shall now discuss. From these considerations, we are led
In their original study of the pop-in to suggest that the optimum range of
method of 9I~ measurement, Boyle et al B/W for symmetrically cracked plate
(22) observed distinct pop-in indications specimens used for pop-in ~o measure-
with 7075-T6 aluminum specimens that ment is between ] and ~o. This does not
had thicknesses no less than 2E~i~/~r~r~~, mean that specimens of width greater
that is, not less than four times the value than 10B should not be used when it is
of rr corresponding to ~io. Distinct convenient to do so, only that the ~i~
pop-in indications were not observed measurement capacity in that case will
with specimens that were thinner than be limited by the thickness, not by the
this. The qualitative explanation of width. Also, specimens having W less
these observations is that, when the than 5B could be used, but when the
plane-stress plastic-zone size approaches available form of the material to be
one half the specimen thickness, the tested makes this desirable, it is both
component of stress in the thickness more convenient and more efficient to
direction will be relaxed along the major use single- edge- notched specimens,
part of the crack front so that a state of loaded either in tension or bending, as
plane strain no longer prevails. It is to will be discussed in subsequent sections.
be expected that the limiting value of With one exception, it will be assumed
the ratio rr/B for distinct pop-in detec- that the 9x~ measurement capacities of
tion would differ somewhat from one all types of plate specimens are limited
material to another, but in the absence to the same extent by thickness, namely,

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160 FRACTURE TOUGHNrESS TESTING

CI~ = ~'~rr~B/2E, according to the from this assumption could not exceed
preceding discussion. The exception is about 5 per cent and is probably much
the surface-cracked type of plate speci- less.
men in which the crack propagates
initially in the thickness direction of Specimen Types Suitable for ~o Measure-
the specimen, not in the width direction ment Only:
as in the other types. The types of specimens in this cate-
Plane-Strain Plastic-Zone Correction gory that will be discussed are illustrated
Term--~zc and Krc Calculations--Before in Fig. 30(a-e) (see the Appendix) as
considering the other types of speci- follows:
mens that are intended for plane-strain (a) single-edge-notched plate specimen
crack toughness testing, there are two loaded in tension
general points that are relevant to all (b) notched rectangular section bend
such tests. First, in calculating values of specimen, three-point loading
9~,, a plastic-zone correction term may (c) notched rectangular section bend
be added to the estimated average value specimen, four-point loading
of the actual crack length, just as in the (d) surface-cracked (or part-through
case of ~, calculations. There are two cracked) plate specimen
differences, however: (1) it is assumed (e) circumferentially notched round bar
that no stable crack extension occurs, specimen
and the initial crack length is used in
the calculation; and (2) the plane-strain While these specimens are referred to
plastic-zone correction term is taken to for brevity as notched specimens, it is
be one third of tlae plane-stress term, to be understood that the notches should
that is, r,r = rr/3 = Egi~/6rar82 always terminate in sharp cracks, usually
(22,3o). This term can often be neglected provided by fatigue stressing.
entirely without significantly affecting Single-Edge-Notched Tension Speci-
the accuracy of the ~c measurement. mens-This type of specimen was first
When it is taken into account, the ~ , introduced for the purpose of plane
calculation is most readily carried out strain crack toughness measurement by
by the aforementioned iteration proce- G. R. Irwin, J. M. Krafft, and A. M.
dure. Usually, only one iteration is Sullivan in an unpublished memorandum
necessary. to the ASTM Special Committee on
The other point concerns the relation Fracture Testing in August, 1962. Sub-
between K~, and ~ c . As mentioned sequenfly, Sullivan published a discus-
earlier, for plane-strain conditions: K1~ = sion of the particular design of the
E~I(1 -- v~). However, for pop-in ~t~ single-edge-notched specimen used by
tests, there is an unresolved question as these investigators (31).
to the degree to which the stress field in A single-edge-notched tension speci-
the vicinity of the middle of the crack men can be regarded as derived from
front approaches a state of plane strain either type of symmetrically cracked
(24). As in Ref (22), it is usual to calcu- plate specimen by bisecting along the
late K~, from the plane-strain relation longitudinal centerline and shortening
given above simply because there is no accordingly. Since this operation affects
basis at present for estimating the degree neither the thickness nor the simulated
to which the stress state deviates from crack size (a0 remains the same), it
one of plane strain. The possible error might be expected that the gi, measure-
in the calculated value of K~ resulting ment capacity of each half would be

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SRAWLEY AND BROWN ON TESTING METHODS 161

about the same as that of the symmetri- single-edge-notched tension specimens.


cal specimen from which it was derived. Approximate expressions of very good
If this were the case, the amount of ma- accuracy have been obtained, however,
terial required for a single-edge-notched by a mathematical procedure of bound-
specimen of given 9ic measurement ary collocation applied to a suitable stress
capacity would be only one fourth the function (23) and by the experimental
amount required for a symmetrically compliance measurement procedure (24).
cracked specimen of equal capacity, The experimental method was originally
with the assumption of the same ratio suggested by Irwin and Kies (32), and,
of length to width for the two types of in principle, is of general utility. The
specimens. Actually, the size advantage expression for ~z~ given in Fig. 30(a) is

25-- ~oh.-
._,._..

I 0
0h

114 ~3

a / //

5
O.1 0.2 0.3 0.4 0.5

Fro. 17--Relation Between the Calibration Factor and a/W for Single-Edge-Notched Tension
Specimens for Several Locations of the Load Axis.

of the single-edge-notched specimen is taken from Ref (24) and applies strictly
probably not nearly this great, but it only for the given values of D/W and
does have another advantage in re- L/W, where D is the distance of the
quiring considerably less load to deter- axis of loading from the cracked edge of
mine a given ~ic value than does a sym- the specimen and L is the distance be-
metrically cracked specimen. This could tween loading pinholes. In Fig. 30(a),
be a determining factor in the choice of D/W is 89 and L/W is ~.
specimen type when it is necessary to It is convenient to express the results
test very large specimens of materials of collocation computations or of experi-
having high ratios of toughness to yield mental compliance measurements in the
strength. form of dimensionless factors that are
Up to the present time, no expression functions of ~, the applied load, P, and
for 9 in closed form has been derived for the pertinent specimen dimensions. In

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162 FRACTURE TOUGHNESS TESTING

the case of single-edge-notched tension value of a/W depends very strongly on


specimens for given values of D/W and D/W, as shown in Fig. 17. The curves
L/W, the appropriate dimensionless shown in this figure for various values
factor is E~B2W/P~, which depends of D/W are derived from unpublished
only upon a/W. That is to say, if the work by B. Gross of NASA, who used
proportions of the specimen dimensions the boundary-collocation procedure men-
other than thickness are kept constant, tioned earlier. The figure is intended to
the value of E~B2W/F2for a given value be illustrative only, not for calculation
of a/W will be the same regardless of purposes. The main point to be made
the size of the specimen, its thickness, from it is that once a value of D/W
or the material from which it is made. has been decided upon and an accurate
This factor can therefore be expressed expression for E~B2W/1n versus a/W
universally as a function of a/W in the obtained for that value of D/W, it
form of a table, a curve, or a suitable should be held within close tolerances in
polynomial in a/W obtained by least- order to avoid errors that would result
squares best-fit procedures applied to from deviations from the nominal value.
the tabulated results. The polynomial There is actually no good reason to
form is a convenient way to express the choose a value of D/W different from
relation between E~B2W/1n and a/W {, for which an expression for EgB2W/tn
compactly, as in the Appendix. Ex- of adequate accuracy already exists
perience has shown that a third-degree (Fig. 30(a) and Refs (23) and (24)). It is
polynomial is suff• to provide an true that the loa d required to measure a
adequate fit, as discussed in more detail given value of 9i~ will be lower the
in Ref. (24). smaller is D/W, but this load could be
The ratios L/W and D/W are addi- reduced even more by using a bend
tional parameters that cannot be com- specimen instead of loading in tension.
bined with E~B2W/tn into a more On the other hand, the sensitivity of
general dimensionless factor in any 9 to a small error in the measured value
simple way for the single-edge-notched of a0 is greater the smaller is D/W, so
tension specimen. (It will be shown later, that 9io measurement accuracy decreases
however, that a rather more general as D/W is decreased. It would seem that
dimensionless factor can be devised for having a choice between a bend specimen
bend specimens.) Providing L/W is (requiring lower load) and a single-edge-
sufficiently large, the effect of small notched tension specimen with D/W
variations of L/W on E~B2W/tn is equal to { (providing better accuracy)
negligible, and the expression for would be sufficient without complicating
E91cB~W/tn given in Fig. 30(a) can be the issue by considering tension speci-
used with confidence provided that L/W mens having other values of D/W.
is held to ~ within 5 per cent. If circum- Having discussed the essential features
stances make it necessary to use a of the design of single-edge-notched
shorter specimen, such as that described tension specimens, we can now consider
in Ref (all an experimental calibration the 9io measurement capacity of this
should be conducted for the specific type. The criterion that we use for this
specimen proportions to be used. In this purpose is that the nominal stress at the
case it would be advisable to read the crack tip should not exceed the yield
discussions relating to specimen length strength. This is admittedly somewhat
that are to be found in Refs (23) and (24). arbitrary, but is analogous to the cri-
The value of EgB~W/tn for a given terion discussed previously for the sym-

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SRAWLEY AND BROWN ON TESTING METttODS 163

metrically cracked specimens, except from which Fig. 17 was plotted, we can
that the maximum value of the average formally calculate values of E~/Crrs214'
net-section stress was limited to 0.8~rs that correspond to ~,om = ars. The three
in that case. In the case of the single- curves shown in Fig. 18 for values of
edge-notched specimen, the decrease of D / W of 88 ~, and 89are plotted from the
nominal stress with distance from the results of such calculations. These
crack tip justified using a somewhat curves represent the dependence of the
higher limit for the nominal stress at the quantity ECig/~rrs~W on a / W for the
crack tip. three different D / W ratios, and have the
What is meant by the nominal stress same significance as the curve shown in
at the crack tip is the tensile stress that Fig. 13 for the center-cracked specimen
0.30--

O.2P

~V2

010

O.05

I I I I .]
~I 0.2 0.3 0.4 0.5

FIC. 18--Dependenceof Measurement Capacity of Single-Edge-NotchedTension Specimens on


a/W for Three Positions of the Load Axis (See Fig. 17).

would exist at the edge of a strip of (with the assumption that the respective
width ( W - a), under an eccentric criteria on which they are based are
tensile load, _P, acting at a distance equivalent). The shapes and relative
(D -- a) from that edge, obviously de- positions of the three curves in Fig. 18
rived from a single-edge-notched speci- would not be changed by taking the
men by removing a longitudinal strip ratio ~rnom/~rS as having some value
containing the notch without changing different from unity; only the ordinate
the position of the loading axis. This scale would be changed in proportion to
stress is given by: the square of this ratio; therefore, the
figure shows two things. First, that the
~nom = P/B(W -- a) maximum efficiency depends very little
+ 3P(W + a -- 2D)/B(W -- a)2 on D / W , being somewhat higher the
lower the value of D / W . The slight
From this, together with the results advantage in efficiency when D / W is

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164 FRACTURE TOUGHNESS TESTING

low is unlikely to be worth the decrease was necessary to provide a notch that
in accuracy of ~j, measurement. Second, terminated in an actual crack, nor that
regardless of the value of D/W, the the specimen, while suitable for ~xc test-
efficiency is greatest ~'hen a/W is about ing by pop-in measurement, was not
0.25, but varies only about 5 per cent in suitable for accurate gc testing under
the range of a/W between 0.15 and 0.35. circumstances where the fracture was not
With the assumption that the ~ , predominantly square. Consequently,
measurement capacities of the center- many of the early data obtained with
cracked specimen type and the single- notched bend bars are only useful in a
edge-notched tension specimen type are semiquantitative sense.
reasonably well represented respectively There is no essential distinction be-
by Figs. 13 and 18, it is apparent that tween a notched rectangular section bend
the single-edge-notched type has only specimen and a single-edge-notched plate
a marginally greater capacity for a given specimen tested in tension. The notched
width than the center-cracked type. rectangular section bend specimen is
Thus, it would appear erroneous to make simply the extreme case of the single-
the simple assumption that bisecting a edge-notched plate specimen when the
symmetrically cracked specimen would loading results from a couple without
result in two single-edge-notched speci- any additional tension component. For
mens each having the same ~c measure- one of several practical reasons, it may
ment capacity as the symmetrically be more convenient to test specimens in
cracked specimen. Actually, the analysis bending rather than in tension, and, in
we have just presented is open to ques- particular, the load needed to measure a
tion, and it will probably require con- given value of gic is less for a bend speci-
siderable experimental work to arrive men than for any other type. On the
at good estimates of the 9~ measure- other hand, it is to be expected that the
ment capacities of the various types of accuracy of 9jc measurement is in-
specimens. In the interim, in order to herently lower for the bend specimen
have some basis for deciding upon than for any other type because the
specimen dimensions, we make use of sensitivity of the calculated value of 9
this and similar analyses that appear to to a small error in a0 is greater than for
be predicated upon reasonable assump- any other type.
tions. Recommended dimensions for bend
There is no reason to suppose that the specimens are shown in Figs. 30(b) and
limitation imposed by thickness would (c). The symbol, W, is used for the beam
be different for the single-edge-notched depth because this dimension corre-
type than for the center-cracked type sponds with the width of a single-edge-
of specimen. Hence we deduce that the notched tension specimen. The beam
optimum range of B/W for the single- thickness is B and L is the moment arm
edge-notched type should be about 88 length, that is, half the difference be-
to -~ as contrasted to -~ to i!a, which were tween the major and the minor spans,
derived earlier for the center-cracked which reduces to half the span for three-
type. point loading. The total applied load, P,
Notched Bend Specimens--The notched is assumed to be equally distributed. The
rectangular section bend specimen was bending moment within the minor span
one of the earliest types of specimen to is, therefore, PL/2.
be used for fracture toughness testing. The most general dimensionless factor
It was not at first appreciated that it that can be used to express ~ as a func-

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SRAWLEY AND BROWN ON TESTING METHODS 165

tion of a/W for a bend specimen is are in satisfactory agreement with pub-
EgB~WS/P~L~, that is, W~/L2 times the lished results of experimental compliance
less general factor, EgB2W/Ps, which calibrations by Irwin et al (16) for three-
was used for the single-edge-notched point loading and by Lubahn (33) for
tension specimen. This simply takes four-point loading, as will be discussed
into account the fact that EgB2W/P~ is in a forthcoming publication.
proportional to L2/W~ for bend speci- If the expressions for three-point and
mens having a given value of a/W. This four-point loading given in Figs. 30(b) and
was deduced originally by G. R. Irwin (c) are compared, it will be seen that for
in an unpublished note and later con- a given a/W, the value of EgB~WS/P~L*
firmed by a different method by B. Gross is always less for three-point than for
0.30 m

0.25

0.15
R

" g o.zo

0.05

I I I I I
~1 ~2 ~3 ~4 E5
,,/w
Flo. 19--Dependence of the Measurement Capacity on a/W for Bend Specimens.

of NASA (also unpublished to date). four-point loading, an average of about


Gross has computed tables of values of 10 per cent less. Comparison of the ex-
EgB2WS/P2L* for both three-point and perimental results shows the same thing
four-point loading by using the procedure (15,33). The difference arises in the
of boundary collocation of the Williams mathematical treatment because the
form of the Airy stress function, which computations for four-point loading con-
was mentioned earlier. The expressions sidered the region within the minor span
for E~I,B~W3/P2L~ as cubics in a/W, as subjected to a bending moment only,
which are given in Figs. 30(b) and (c) whereas the computations for three-
for the three-point and the four-point point loading took into consideration
loaded specimens, respectively, were ob- the shearing stress that changes from
tained by applying least-squares best-fit P/2BW t o - - P / 2 B W at the center
procedures to these results of Gross. It loading poir~t.
is worthy of note that Gross's results The shearing stress is independent of

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166 F~d~CTU~ TOIIGHN~SS TESTING

L, whereas 9 is proportional to L~/W 2, From comparison of Fig. 19 with Fig.


as mentioned above. The influence of 18, it is seen that a single-edge-notched
the shearing stress upon ~ should, there- specimen loaded in four-point bending
fore, diminish with increasing L/W. is apparently about 15 per cent more
For this reason, it is recommended that efficient than a single-edge-notched ten-
the span of a three-point loaded speci- sion specimen of equal width and thick-
men should not be less than 8W, which ness and having D / W equal to 89 For a
is an unpublished estimate by G. R. specimen loaded in three-point bending,
Irwin. In the case of a four-point-loaded however, the efficiency is about the
specimen, the shearing stress is zero same as that of the tension specimen.
within the minor span, but it appears This, of course, involves the assumption
desirable that the major span should that the same limiting condition ap-
not be less than 8W in this case also. plies to both types of specimens, which
Furthermore, it is recommended that appears to be reasonable in the absence
the minor span should not be less than of experimental data to the contrary.
2W on the basis that the part of the It should be noted that if the recom-
strain energy field that is appreciably mendations regarding specimen length,
affected by the crack length is contained which are given in the Appendix, are
within that part of the specimen that followed, then the bend specimens would
extends a distance W on either side of have to be about twice as long as the
the crack. Thus, with a minor span not tension specimen of equal width.
less than 2W, ~ should not be appre- Cracked Charpy Specimens--Consider-
ciably influenced by either the magnitude able use has been made of cracked
of the shearing stress outside the minor Charpy specimens for the intended pur-
span or by the concentrated stresses at pose of 9x~ and even ~ measurement
the loading points. From these con- (34). The cracked Charpy specimen is
siderations, it is reasonable to expect simply a small, three-point-loaded bend
that somewhat more accurate ~ meas- specimen and is subject to exactly the
urements could be made with a bend same limitations as we have discussed
specimen in four-point loading than with for three-point bend specimens. The
the same specimen in three-point loading. usual dimensions are as follows: W =
In order to estimate the 9i, measure- 0.394 in., B is variable between about
ment capacities of notched bend speci- 0.04 and 0.8 in. (for standard Charpy
mens, the same criterion was used as in specimens, it is 0.394 in.), a0 is variable
the case of the single-edge-notched between about 0.1 and 0.2 in. (normally
tension specimen discussed previously. slightly greater than 0.1 in.), and the
Values of Eg/~rra2W corresponding to span is 1.574 in. The specimen is pro-
~rnom = 3 P L / B ( W - a)~ = errs were duced by machining to normal Charpy-V
calculated from the expressions given dimensions except that the thickness
in Figs. 30(b) and (c), and used to plot can be varied, then generating a fatigue
the curves of ECiJ~rrs2W versus a/W crack at the bottom of the V-notch. It
that are shown in Fig. 19. From these is tested either with a pendulum-type
two curves it is seen that the bend impact testing machine, in which case
specimen is apparently used more efll- only the loss of pendulum energy is
ciently in four-point loading than in usually measured, or in slow bending
three-point loading. This, of course, is to obtain a load-deflection record.
simply a reflection of the fact that the It would be possible to determine
values of EgB2W3/P~L 2 are greater for ~i~ values within the limitations of
four-point than for three-point loading. measurement capacity imposed by the
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SRAWLEY AND BROWN ON TESTING METHODS 167

dimensions of the Charpy specimen fracture of a plate specimen would be


(C~g would be about ars*/lOE), by predominantly slant. In any case, in
measuring the pop-in load and proceed- the opinion of the authors the results
ing as for any other three-point bend of cracked Charpy tests should not be
specimen. Although the ratio L/W is used for any other purpose than pre-
only about 2 for the Charpy specimen, liminary screening of materials, at least
rather than 4 as we recommend for until such time as the interpretation of
three-point-loaded bend specimens, a the results is much better understood
~ measurement that was accurate than at present. It is particularly im-
enough for some purposes, such as a portant that U/A values should not be
materials screening program, might be used in an attempt to calculate critical
obtained. However, this is not the way crack dimensions for structures since
the specimen is usually treated. Instead, this might be dangerously misleading.
the loss of pendulum energy in an impact Surface-Cracked Plate Specimens--De-
test, or the area under the load-deflection tails of this type of specimen, sometimes
curve in a slow bend test, is measured. called a part-through crack specimen,
This energy value is usually denoted W, are shown in Fig. 30(d) (see the Ap-
but here it will be called U in order to pendix). It was originally introduced in
avoid confusion with the symbol for order to investigate directly the effects
specimen width. of cracks similar to those from which
It is assumed that U can be equated fractures had often originated in service
with the energy required for the forma- (36-38). Cracks of controlled size, ap-
tion of new fracture surfaces only, and proximately semi-elliptical in shape with
that no part of U is dissipated in any the major axis at the surface, were
other way. Then a further assumption formed in plate specimens by fatigue
is made, essentially that the crack-ex- stressing (3s,39), or by static stressing
tension resistance is constant during the in a suitable environment (37). It became
propagation of the crack through the possible to calculate ~c values from the
specimen. With these assumptions, it is results of tests of surface-cracked speci-
concluded that ~o, or ~ if the fracture mens when Irwin (is) derived an ap-
is square, can be taken to be equal to propriate expression for ~i (originally a
U/A, where A is the area of the frac- private communication in 1960) by
tured cross section, B(W -- ao). Both making use of earlier work by Green
of these assumptions are open to con- and Sneddon (4o). Irwin's expression is
siderable question, and do not appear given in Fig. 30(d) for the value of ~i
to have been thoroughly investigated. in the central region of the front of a
In fact, it can be inferred from recent semi-elliptical surface crack that is no
work by Krafft (3S) that the second deeper than one half the plate thickness.
assumption is definitely not generally The expression as given includes a plas-
valid. tic-zone correction term. The magnitude
It is true that there is qualified evi- of ~i varies with position along the
dence of correlation between U/A and crack front and is greatest at the central
results of some ~, tests to a degree that position (15). The crack extends first in
suggests that U/A may be a useful this region and the magnitude for ~ at
measurement for screening purposes. other positions along the crack front
This is more likely to be the case when is of no consequence to this discussion.
the fractures are predominantly square, Reference (IS) does not deal with the
and ~ approaches ~i~, than when the question of how narrow the plate speci-
thickness is such that the fully developed men could be without appreciably in-
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168 FRACTU~ TOTJ6~NESS TESTING

fluencing the value of g~ at the middle mum load and is not preceded by a
of the crack front. We shall assume, metastable crack extension at some lowel
rather arbitrarily, that W should not be load. While the experience of the authors
less than 6c, where 2c is the surface and examination of data obtained by
length of the crack, assumed to be the others suggest this assumption is not
major axis of an ellipse. This restriction seriously in error, at least as far as high
is almost certainly on the safe side since strength materials are concerned, it
the length of the pertinent central region ought nevertheless to be subjected to
of the crack front, where the crack critical investigation. It is recommended
first extends, is a small fraction of 2c. that crack extension should be moni-
Extended discussion of the 9i~ meas- tored during all tests of surface-cracked
urement capacity of surface-cracked specimens, just as for other types of
specimens as a function of the various specimens, by using one of the methods
dimensions of the cracked section, W, B, discussed later. Results obtained with-
a, and c (Fig. 30(d)) would be unwar- out this sort of instrumentation should
ranted since the selection of this type of be regarded as somewhat uncertain, the
specimen would be governed by con- more so the less brittle the material.
siderations other than measurement ca- Circumferentially Notched Round Bars
pacity. Instead we shall estimate the --Tension testing of notched round
9x, measurement capacity of a selected bars has an extensive history, and it was
example in which the crack dimensions natural that this type of specimen should
are as large as the aforementioned re- have been one of the earliest used for
strictions permit, namely, a = B/2 and 9x~ measurement. As in the case of
2c = W/3. We also assume a/c = 89 notched bend specimens, it was not at
which is a likely ratio for specimens first appreciated that notch sharpness
fatigue-cracked in bending, and that equivalent to that obtained by fatigue
the average net-section stress at in- cracking was necessary for accurate
stability should not exceed ~rs for a 9~* measurement, so that many of the
valid 9,* test. Using these conditions earlier 9~, data are of somewhat doubtful
in the expression for oo~ given in Fig. value.
30(d) gives C,o = 1.09 ars2B(1 - v~)/E, There is at present no highly accurate
which is equal to ar~B/E when Pois- expression for 9~ for a round notched
son's ratio is 0.3. Here, Cig is given in bar. In their contribution to this sympo-
terms of B rather than in terms of W, sium, Paris and Sih discuss this case in
as for other types of plate specimen. some detail and conclude that an ac-
The reason for this difference is that it curate solution would require an analysis
is the depth of the crack that determines of the type suggested by Sneddon (41).
the 9~, measurement capacity of a The mathematics involved in this type
surface-cracked specimen, and the crack of approach is quite formidable. Ap-
depth is limited to a maximum of one proximate expressions for ~ are available
half the specimen thickness. from unpublished work by H. Bueckner,
In 9~ tests with the surface-cracked which are discussed by Lubahn (~) and
type of specimen, it has been the usual by Wundt (42), or can be derived from
practice to measure only the maximum stress-concentration factors as discussed
load sustained in the test and the initial in Ref (16). The results obtained by these
crack dimensions and to calculate 9~, approximate methods can be expressed
from these measurements. This practice conveniently in the form Egl/(1 --
assumes that instability occurs at maxi- v2) = Ma,2D, where M is a dimension-

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SRAWLEY AND BROWN ON TESTINO METHODS 169

less function of d/D, D is the major for using a value oi d/D much different
diameter, d is the diameter of the crack- from 0.7, so that the expression for
notched section, and a~ = 4P/,r# is the ~zc need only be used over a very limited
average net-section stress. range of diD. In the range of diD from
Figure 20 shows values of the dimen- 0.65 to 0.7, the assumption that M has
sionless factor, M, plotted versus d/D. the constant value 0.17 is probably all
One set of plotted points is derived from that is warranted by the accuracy of the
results given in Ref (33) and the other available estimates.
set was obtained by the method of The value of d that should be used
Ref (15). It is difficult to judge the ac- in calculating a value of 9zc is less than
curacy of these values, but the extent of the measured value of the initial crack
the agreement between them may give diameter, do, by a plastic-zone correction
some indication of this. A fitted curve term, E~z~/3~rav82.This is equivalent to

0,20

0.18

•l:i
z 0' 16

: v 0.14

0,12
A Bueckner-kul~hn (ref. 33)
0 Method of Irwin (ref, 15)

El0 I I I I I }
0'4 0'5 0.6 0'7 0.8 0.9 1.0
d/o
Fro, 20--Values of Dimensionless Factor, M, for Round Notched Bars Versus d / D . Egx ==
M ~ u t D ( 1 - - v2).

corresponding to a simple expression for increasing the initial crack depth (D --


M is also shown in the figure. Within do)~2 by the same plane-strain plastic-
the range of did shown, which is greater zone correction term used for other
than would normally be of practical types of specimen. It is worth mentioning
interest, the simple, compact expression that there is some arbitrariness about
for M appears to fit the plotted points the choice of the value used for this term
adequately. Consequently, in the ex- (3o), which is apt to cause confusion in
pression for ~zc given in Fig. 30(e), the reading the literature unless one is aware
factor M has been replaced by [0.172 - of it. The practical effect of this, how-
0.8(d/D -- 0.65)2]. Figure 20 also shows ever, is negligible since it amounts to a
that the most efficient value of d/D is small variation of a small correction
about 0.7, which corresponds to a term.
notched cross-sectional area equal to The ASTM Special Committee on
about one half the shank cross-sectional Fracture Testing has recommended that
area. There would be no good reason the size of a round notched bar for

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170 FRACTURE TOUGHNESS TESTING

~t, measurement should be sufficient to that this estimate implies that the
ensure that the average net-section magnitude of Cig is just about the same
stress at fracture does not exceed 1.1 for a notched round bar as for a sym-
times the uniaxial tensile yield strength metrically cracked plate specimen of
(9). The reason that the maximum recom- width equal to the diameter of the
mended ratio of ~N/~rs can be greater notched round bar. The experimental
in this case than the ratio of crnot/r for results reported in Ref (22) are consistent
symmetrically cracked plate specimens with this conclusion, and it is also
is, of course, that the effective yield intuitively apparent if one regards a
strength of the notched section of the symmetrically edge-cracked plate speci-
round bar is correspondingly higher than men as equivalent to a longitudinal slice
~rs. A state of triaxial tension exists from the center of a round notched bar.
within the notched section and, on the The round notched bar requires a
basis of either a maximum shear stress considerably greater amount of material

T A B L E 1 - - C O M P A R I S O N OF D I M E N S I O N S OF VARIOUS P L A N E - S T R A I N C R A C K
T O U G H N E S S S P E C I M E N S H A V I N G CIa EQUAL TO e r s 2 / E , a

Symmetrl- Single-Edge-Notched
cally Surface Notched
Cracked Tension Bend, Bend, Cracked Round
Plate D/W = 1/2 three-point four:point
(
Relative dimensions
of initial cracks . . . . 2ao/W ao/W ao/W ao/W ao/B = 1,i do/D
= 0.3 = 0.3 = 0.2 = 0.2 2c0 = W / 3 = 0.7
W or D, in . . . . . . . . . . . 5.0 4.0 4.0 3.5 6.0 5.0
B, in . . . . . . . . . . . . . . . . 0.65 0.65 0.65 0.65 1.0
M i n i m u m length, in ... 20 16 36 32 24 20
L o a d / a r s , in3 . . . . . . . 1.8 0.8 0.14 0.16 5.4 11.2
Accuracy--order of
merit . . . . . . . . . . . . . 1 1 3 2 potentially potentially
high high

a Specimens of the dimensions given would be large enough to measure values of ~t, up to ~ t, s2/E,
according to the criteria discussed in the text. For other values of ~ , , the m i n i m u m dimensions are
directly proportional, and the loads are proportional to the square of the values given in the table.

or an octahedral shear stress criterion, and considerably more loading capacity


the average net-section stress at which than any of the other types of specimen
yielding occurs will exceed ~rs to an for ~c measurement that we have con-
extent depending upon diD. For d/D sidered. To compensate for this, the
equal to 0.7 or less, the effective yield potential accuracy of 9~c measurement is
strength will be high enough to justify probably relatively higher, but it would
~i~ measurements with values of ~ at not be easy to attain the full potential
least up to 1.1 ~rs. accuracy. Apart from the need for a
Applying this limitation and taking the more accurate expression for 9 than is
maximum value of M as 0.17 yield the now available, it would be necessary to
estimated ~ measurement capacity of ensure almost perfect concentricity of
a notched round bar: C~g -- 0.22 fatigue cracking and uniformity of load-
~rvs2D(1 -- v2)/E, or 0.2 ~rs~D/E when ing. No study has yet been made of the
Poisson's ratio is 0.3. This calculation errors that would result from small
takes into account the plastic-zone cor- deviations from the assumed perfectly
rection term. It is interesting to note uniform tensile loading of notched round

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SRAW~EY AND BROWN ON TESTINO METHODS 171

bars, but the study of single-edge- have been accumulated, but it is un-
notched plate specimens discussed earlier likely that the revised values will be
indicates that unavoidable nonuniform- appreciably smaller than those given
ity of loading could be a considerable in Table 1, more likely they will be
source of error in testing notched round greater. To estimate minimum dimen-
bars. At the present time, the best sions for different values of ~ , , the
accuracy of ~ measurement with linear specimen dimensions should be
notched round bars is probably no better taken in direct proportion to the values
than with plate specimens. given in Table 1, and the required load
As in the case of surface-cracked proportional to the square of the value
specimens, it is usually assumed that given in the table. The safest course in
instability occurs at maximum load in a deciding upon the size of specimen to be
notched round bar test, and ~i~ is used is to overestimate substantially the
calculated from the maximum load and largest value of E~ic/~r~ among the
the average diameter of the initial materials that are to be tested and to
cracked section. In this case also, the calculate the specimen dimensions ac-
assumption ought to be subjected to cordingly. For most purposes it is best
adequate experimental verification uti- to select from a graded series of specimen
lizing crack-extension monitoring instru- sizes, in which the linear dimensions
mentation. increase by a factor of 2 from one size
Summary Comparison of Specimens to the next. Following the ASTM
for ~ic Measurement--In selecting a Special Committee on Fracture Testing,
particular type of specimen for ~i~ one size of each type of plate specimen
measurement, the following factors may would be 3 in. wide. Hence, a graded
need to be considered: (1) the magnitude series of plate specimens could con-
of the highest value of E~Ic/ara2 ex- veniently have widths of 3 times 2"
pected among the materials to be tested; in., where n has the values --2, - 1 , 0,
(2) desired accuracy of ~ , measurement; 1, 2, etc.
(3) loading capacity of available testing While it is somewhat premature to be
machines; (4) economical usage of avail- very definitive about accuracy, experi-
able test material; and (5) form of the ence so far suggests that the best
test material. accuracy of ~ic measurement that is
Table 1 provides guidance regarding likely to be achieved is of the order of
necessary dimensions and load require- :k2 per cent. A clear distinction should
ments, and s--'uggests an order of merit of be made between testing accuracy and
accuracy for the various types of speci- material variability. The variance of
men we have considered. The proportions ~c for a given stock of material may be
given for each specimen type are con- of the order of 10 per cent or more, that
sidered to be about optimum so far as is, the standard deviation of the results
can be estimated at the present time. from a large number of accurate
The dimensions given are estimated as replicate tests would be of the order of
the smallest that could be used for 10 per cent or more of the average value.
determination of a value of ~Ic equal to However, it is important to know the
ars~/E, based on the criteria discussed in variability of the toughness of a ma-
the preceding sections and subject to terial as well as its average toughness.
the qualifications stated therein. These In fact, a lower confidence limit is more
values may need to be revised when important than the average value. For
sufficient pertinent experimental data this reason, it is desirable that the ~ ,

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172 FRACTURE TOUam~IESS TESTINC

measurement precision should be sub- loading capacity required to measure a


stantially better than the variance of given level of Eg~. Both also require
g~ resulting from inherent material considerably more material than the
variability. The main factors that in- other types of specimen. It is pos-
fluence the accuracy of 9i, measurement sible, though not yet established, that
are the accuracy of the expression used either the surface-cracked plate speci-
for calculating 9 and the degree of un- men or the notched round bar might be
certainty in the estimate of the effective useful for 91~ measurement in cases
crack length, including the plastic-zone where definitive results could not be
correction factor. The other necessary obtained by the pop-in measurement
measurements can be made with rela- procedure. In this case, of course, sym-
tively high accuracy (provided that the metrically cracked or single-edge-notched
9ic instability is clearly defined). The plate specimens of sufficient thickness
authors believe that the accuracy of the could also be used, but then the ad-
expression for 9 for the single-edge- vantage of lower bulk would largely be
notched tension specimen (Fig. 30(a)) lost. This is a question that has yet to be
is of the order of -r per cent when settled by careful experiment. It is of
2ao/W is about 0.3 (24). This is consider- considerable practical importance in con-
ably less than the 4-2 per cent suggested nection with materials of high tough-
for best attainable 9~* measurement ness and low yield strength that require
accuracy, and the potentially more large specimens.
accurate expressions for 9 that might be Sometimes the controlling factor in
obtained for the symmetrically cracked selecting a specimen type will be the
plate, the surface-cracked plate, and form of the stock of material to be
the notched round bar are, therefore, tested and its texture in relation to
probably only of academic interest. the directions of the nominal principal
The order of merit for accuracy given stresses in service. For a given stock of
in Table 1 is based on these considera- material, ~xo may depend considerably
tions and on other points discussed in upon the orientation of the crack in
connection with bend specimens. relation to the principal textural direc-
Reference to Table 1 shows that if the tions deriving from the ingot structure
loading capacity of available testing and subsequent deformation into prod-
machines is the major limiting factor, a uct form. Alternatively, the measure-
notched bend specimen will have a ment of toughness of welds and asso-
distinct advantage in the level of E~ic ciated heat-affected regions may be of
that can be measured with a given load. prime importance in a particular ap-
On the other hand, if material economy plication. This requires very careful
is of major importance because the location of test cracks in relation to the
amount of test material available is variable structure of the weld region.
limited, then the single-edge-notched For the common case of plate stock,
tension specimen requires only about the nomenclature of Ref (5) is convenient
half as much material as the bend speci- in referring to the six principal systems
men because it is proportionately shorter. of crack propagation. The plate-thick-
It is also somewhat more accurate, but ness direction is labeled T, the major
requires about five times as much load. rolling direction R, and the width direc-
Both the surface-cracked plate and tion, W. The six principal systems of
the notched round bar types of specimen crack propagation can then be dis-
have a considerable disadvantage in the tinguished by pairs of letters, the first

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SRAWLEY AND BROWN ON TESTING METHODS 173

letter representing the normal-to-the- required in pop-in plane-strain ~t, test-


crack plane and the second letter the ing. In special circumstances, however,
direction of propagation. For example, it may be desirable to follow crack ex-
R W would represent a crack normal to tension from pop-in to final fracture and
the rolling direction propagating in the in such cases the instrumentation must
width direction. It would be convenient combine adequate sensitivity with the
to use either symmetrically cracked plate necessary measurement range.
specimens or single-edge-notched speci- Before proceeding with a description
mens of full plate thickness for tests of of the various types of instrumentation
either WR or RW, but surface-cracked that have been employed for crack-
plate specimens would be more con- extension measurement, it is desirable to
venient for WT or RT. Bend specimens discuss the use of staining fluids for this
could conveniently be used for any of purpose. In the first report of the ASTM
these four systems of crack propagation. Special Committee on Fracture Testing
Tests of TW and TR present difficulties, (S), it was suggested that a useful in-
but, fortunately, high tensile stresses dication of crack length at fracture in-
in the thickness direction are usually stability could be obtained by introduc-
avoided by good design. Sometimes ing a staining substance, such as India
heavy forgings may have to be used in ink, into the notch or crack before start-
such a way that the maximum nominal ing the test. The assumption was made
tensile stress is normal to the fibering that the ink would follow only the stable
direction, however, and in such cases it crack extension. At fracture instability,
is most important to test appropriately the crack velocity would suddenly in-
oriented fracture toughness specimens. crease to a point where the ink would
If necessary, extension pieces could be no longer move inward fast enough to
welded to test sections taken from the keep pace with the crack tip. Even if
forging. In this case, the obvious pre- this assumption could be proved cor-
cautions should be observed. rect, there are very good reasons for
avoiding the use of staining agents. Thus,
INSTRUMENTATION AND PROCEDURE there is no way to determine, in advance,
From the foregoing sections, it is how much fluid must be introduced into
clear the determination of ~c or ~ic the crack. An excess of fluid will splatter
requires a knowledge of the crack length or run after fracture so that the crack
corresponding to the load at fracture length can be greatly overestimated. An
instability. Essentially, two cases may be insufficient amount of the staining agent
distinguished: namely, an appreciable will, of course, have the opposite effect.
amount of crack extension takes place For these and other reasons, the com-
before unstable fracture, or fracture mittee no longer recommends the use of
instability occurs immediately from the staining fluids in crack toughness tests
initial crack front. The first case is (9).
frequently encountered in plane-stress In the following section, several crack-
testing and the method of crack detection extension measurement methods po-
employed must be capable of following tentially capable of yielding unam-
substantial amounts of stable crack biguous results will be described.
extension up to the maximum load. On Particular attention will be given to
the other hand, the major requirement practical applications and proper han-
in the second case is high sensitivity to dling of the data. It should be emphasized
initial crack movement as would be that with the exception of cinema-

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174 FRACTU~E TOtYCH~SS TESTING

tography, all the techniques have been mended since the apparent extent of the
recently developed and only limited data dimple will vary with the prevailing
are available. For these reasons, some lighting conditions.
areas of uncertainty exist in the applica- The data are generally represented as
tion of the new methods. It is also the a plot of crack length and applied load
purpose of this section to define these (or gross-area stress) against time (or
areas clearly. frame number). Examples of such plots
are shown in Fig. 21 for wide sheets of
Cinematography: 4330M steel provided with center fatigue
Synchronized motion-picture cameras cracks (unpublished data from C. F.
may be used to photograph simul- Tiffany, The Boeing Co.). From repre-
taneously the load dial of a tension sentations of this type, the crack length
testing machine and the plane surface at maximum gross stress may be se-

713

12

1~ r- 1E

.~a" 1 ~ - ~ 1 ~ Ill
~ v

10
0//*~'/Tcl,I
L ' fr~ure.~/
. . . . . . . -,

80_ 60 ) J
Time, sec

Fro. 21--Examples of Stress and Crack-Length Measurements Using Cinematography.

of a specimen containing a through-the- lected for use in calculating the frac-


thickness crack. Satisfactory resolution ture toughness. However, some ~nvesti~_
of the crack requires adjustment of the gators select the stress at a crack length
lighting for the particular surface condi- judged to correspond to the onset of
tions of the specimen being tested. "fast crack acceleration." Obviously,
Unwanted reflections can be minimized such a criterion for selection of crack
by use of polarizing screens (9). The length permits considerable latitude in
film is examined frame by frame and the judgment when behaviors such as
the crack length directly measured. those shown in Fig. 21 are encountered.
Some investigators have made this meas- For this reason, it is recommended that
urement to include the apparent extent the stress and crack length at maximum
of the dimple ahead of the crack with load be used in the fracture toughness
the idea of taking into account directly a calculations, in accordance with the
plastic-zone correction; however, this recommendations of the ASTM Special
procedure cannot be generally recom- Committee on Fracture Testing (5).

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SRAWLEY AND BROWN ON TESTING METHODS 175

This photographic method has been The potential distribution will be a


widely employed by the aircraft in- function of the specimen geometry,
dustry in tests on very wide thin-sheet crack size, and location of the current
specimens containing long through-the- leads. As shown previously (44), it is
thickness slots or cracks. The materials possible to obtain a calibration curve
of interest in these tests are quite tough that relates E/Eo to the crack size,
and generally exhibit considerable stable where E is the potential difference be-
crack extension. Under these circum- tween the probe points measured as a
stances, the technique has considerable function of load and E0 is the value at no
flexibility in that it may be readily load for a specimen without a crack. A
adapted to tests at both low and high calibration curve of this type will be
temperatures provided that the speci- independent of the material and speci-
men surface is visible. The method is men size provided that all specimen
unsuitable for pop-in detection, since it dimensions are changed in proportion,
provides no indication of crack extension including the locations of the current
below the surface. As presently used, it and potential leads. For specimens con-
is relatively insensitive to small crack taining through-the-thickness cracks, it
extensions; however, there is no funda- is convenient to make a pattern of the
mental reason why considerable increase specimen geometry by using an elec-
in sensitivity could not be obtained by trically conductive analog paper. These
suitable refinements in the optical sys- paper patterns are useful not only for
tem. obtaining the calibration curve, but also
for general potential mapping of a
Electrical Potential Measurement: particular specimen geometry in order to
If a body carrying a current contains determine optimum locations for the
a discontinuity, there will be a disturb- current leads and potential probes. A
ance of the potential field in the region sufficiently constant current can be
of the discontinuity. If the disconti- maintained if the paper is connected
nuity is a crack, the potential difference across a 90-v dry battery through a
between two fixed points spanning the resistor having a value about 100 times
crack will increase as the crack extends, the resistance of the paper pattern. A
provided that the total current does not razor blade may then be used to cut the
decrease. This is the basis for crack- desired crack lengths and shapes, and
extension measurement by the electric a vacuum tube voltmeter employed to
potential method. In practice, a con- map the potential field. The recom-
stant current is supplied to the speci- mended current input and probe loca-
men, and potential probes are fastened tions as well as the calibration curves
at suitable points on either side of the to be described were obtained in this
crack. The potential change with crack manner.
length may be measured with a double Testing Procedure--The specimen
Kelvin bridge as used by Steigerwald should be electrically insulated from the
and Hanna (43), or by electronic instru- tension testing machine by some suit-
ments such as the milliohmeter em- able means, such as Teflon sheet spacers
ployed by Anctil et at (44), or a highly or electrical insulating tape. It is de-
sensitive voltmeter amplifier described sirable to locate the current leads suf-
later. These electronic instruments have ficiently far from the crack plane so that
the advantage that an output is provided small variations in their position would
which is suitable to drive an X-Y plotter. not influence the results. This distance

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176 FRACTURE TOUGHNESS TESTING

should be greater than one half the ternatively, wet storage ceils connected
width or diameter of the practical speci- in parallel can be used with a suitable
men types illustrated in the Appendix. ballast resistance (high relative to the
For high sensitivity to initial crack specimen) in series with the specimen. If
extension, the potential probes should the current output drifts appreciably
be located as close to the crack tip as during a test, additional batteries should
possible, the actual location depending be connected in parallel to reduce the
on the method of attachment. The probe current drain per ceil. The current supply
positions shown in Fig. 22 for plate cable can be connected to the specimen
specimens were established for use with by damps or by bolts through small
a particular set of slotted yokes that holes. With the latter arrangement, the
span the specimen thickness and refer- holes should be at least one specimen
ence the specimen edges. Opposing width or diameter away from the crack
pointed screws in each yoke serve as to avoid interaction of stress tides. The

4000 (' I, Ai2a)-0.2in.


J =i~
~ 3000 StageIIl

Sta~eI ._
I I I
10 20 3O 4O 5O 10 20 30 40 5O
E- Ei, pv E-Ei, tlv
FIG. 22--Typical Load Versus Potential Records IllustratingPop-In and Crack Extension to
Maximum Load.

probes contacting the front and rear amount of current required for a given
surface of the specimen. Leads from each crack-extension sensitivity will, of course,
yoke connect to the potential measuring depend on the resistivity of the speci-
device. It will be noted that the yokes men, its cross section, and the sensitivity
locate the probes slightly behind the of the potential measuring device em-
nominal initial position of the crack ployed. As an example, the authors
tip of the practical plate specimens using the potential sensing and record-
shown in the Appendix. This horizontal ing equipment described below, obtain
location is chosen so that the tip of the the desired sensitivity to crack extension
shortest crack (within the expected when supplying 10 amp to a steel singie-
tolerance) will be at or beyond the probe edge-notched specimen 3 in. wide and
points. in. thick.
The constant current may be obtained As mentioned previously, an elec-
from a regulated power supply. These tronic potential measuring instrument
are commercially available in capacities can be used to advantage. The milllohm-
u• to 100 amp with high stability. A1- eter described by Anctil et al (44) has a

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SRAWI,EY AND BROWN ON TESTING METHODS 177

built-in power supply which is limited channel, a plot of potential against load
to 100 ma. This instrument, therefore, is obtained directly. Examples of two
lacks sufficient sensitivity to make it such plots for single-edge-notched speci-
generally useful in fracture testing. A mens are shown in Fig. 22, illustrating
recently developed (45) voltmeter-am- both a relatively small initial crack
plifier combination can be used with an movement and a very distinct pop-in.
external current supply such as described The initial potential, E~, is suppressed
above and has an output of 10 v for and the potential change with load,
full-scale meter deflection on any one of (E - E~), may be considered as con-
13 input ranges, the most sensitive of sisting of three stages. During stage I
which is 0 to 0.1 gv. Zero suppression is there is a rapid increase in potential at
available up to 100 times full scale on low loads due to separation of the

' J0.35 W ' |

~_~w13 -'-""//"'"/;
L --w = //

0" ' ' '

0,1 0.2 O.t 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Za/W
FIG. 23--Electric Potential Calibration Curves for SymmetricallyCenter- and Edge-Cracked
Plate Specimens.

any range. In order to minimize the fatigue-crack surfaces. The potential


influence of thermal emf, it is necessary during stage II increases linearly with
to avoid, where possible, dissimilar metal load and corresponds only to elastic
junctions in the input circuit to the strain. The beginning of stage III, E~,
voltmeter. Difficulties due to these is marked by a nonlinear increase in
thermocouple effects and stray fields potential resulting from crack extension
limit the useful working range of the or crack-tip plasticity (the contribution
voltmeter to 30 gv or higher, unless of plasticity is usually considered negligi-
elaborate precautions are taken in the ble), or both. The accuracy with which
experimental setup. the load corresponding to initial crack
Reduction of Data--If the output of movement can be established depends
the voltmeter-amplifier is fed to one on the sharpness of the division between
channel of an X - Y recorder and the stage II and stage III. In the two cases
signal from a load cell to the other shown, this is quite distinct; however,

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178 FP,ACT~U~ Totlom~ss TESTmO

as will be discussed later (see Fig. 28), Ei)/A, where A is the value of E/Ec
small amounts of crack extension may obtained from the calibration curve
occur early in the test before a distinct corresponding to the measured initial
pop-in, and, in such cases, acoustic crack length and width, and E, is the
measurements are of assistance in in- potential at crack initiation (see Fig. 22).
terpretation of the potential records. If When calibration curves of this type
plane-strain toughness determinations are used, it is important to keep in
are to be made, the load at pop-in is mind certain restrictions on their ap-
read directly from the load-potential plication. For the probe positions and
records and used in the appropriate connections described, the calibration
9~ equation. Also the load-potential curves for symmetrically cracked plate
records may be converted to a plot of specimens will yield the average of the

_J__

0.317W

~.~0
~-----
- W - - - ~

3----
I I i

T ...li
.. :
0 0.05 0.10 0.15 0.20 0.25 O.3O 0.35 0.40 0.45 0.511

FIG. 24---Electrical Potential Calibration Curve for Single-Edge-Notched Specimen.

crack extension as a function of load by crack extension occurring at each crack


the use of calibration curves. tip. Independent measurements are of
Calibration curves for several practical course possible, if separate pairs of
fracture toughness plate specimen types probes are used at these locations. The
are given in Figs. 23 and 24. These have calibration curve corresponds to a crack
been determined for the potential probe front normal to the specimen surface
postions shown and with the current and load axis. As discussed previously
input attachments far enough removed (see Fig. 6) in an actual specimen, the
that the measured potential is influenced front is always curved and this curva-
only by the crack. When these curves ture in mixed mode fractures may occupy
are used, the value of E0 could be meas- a region about equal to the plate thick-
ured on a dummy specimen without a ness. For this reason, crack extensions
notch. Alternatively, E0 for a particular calculated from the calibration curves
test may be calculated as Eo - (E, + will closely approximate the actual values

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SRAWLEY AND BROWN ON TESTING METHODS 179

only when the curved region is a small increasing amounts of potential change.
fraction of the total crack extension. In The specimens are then heat-tinted to
~ tests, the effect of curvature on outline the crack front, and broken. A
measured crack length may be neglected plot may then be made of E/Eo at
if the total crack length, 2am, is large interruption against some measured
in comparison with the thickness. value from the heat-tinted crack indica-
When studies are made of the pop-in tion. A few results of this type have been
phenomenon, it is instructive to de- reported in Ref (43). Some data obtained
termine the extent of crack movement by the authors are shown in Fig. 25 for

l~a - ~115 Eo (from calibration curve)

3.

3.35L
000 / ~ 9
~148 Eo

~o~.24

3.05

3.oo I I I I l "1
0 0.02 0.04 0.06 0.08 0.10 0.12

FIG. 25--Ratio of Potential Change to Initial Potential as I:unction of Actual Crack Extension
Determined by Means of Interrupted Tests.

associated with a given indication of single-edge-notched tests on 18Ni-Co-


pop-in (for example, the magnitude of a Mo steel aged to a wide range of strength
step in the loading curve). As discussed levels. In this case, Aa represents the
above, the calibration curves are not maximum extension from its initial
particularly useful in this case, since the position of the most advanced point on
major portion of the crack extension is the crack front. Within the scatter, there
occupied by the curved fracture front. is roughly a linear relation between Aa
To obtain a more direct indication of and E/Eo that is useful in estimating
crack extension under these circum- the amount of crack extension repre-
stances, interrupted tests of a series of sented by a given potential change at
specimens may be made representing pop-in. The general trend of these

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180 FRACTURE TOUGHNESS TESTING

points may be compared with the slope maximum response speed is of the order
of the calibration curve for the particular of 89 sec. The use of an oscilloscope is
value of ao/W used in these tests. As apparently not possible because input
might be expected, the calibration curve amplifiers are not available that have
would give estimates of &a corresponding sufficient gain combined with fast re-
to a straight crack front and therefore sponse, high stability, and low noise.
considerably smaller than the actual
values. Displacement Gages:
Advantages and Limitations of Po- The displacement per unit load be-
tential Method--This technique appears tween two points spanning a crack will
to be readily adaptable to all practical increase with crack length. For elastic
fracture toughness specimen types. The loading, this ratio is defined as a com-
necessary instrumentation is com- pliance and, for given specimen dimen-
mercially available to permit automatic sions, depends only on the distance
recording of the potential change. Cali- between the points (gage length) and
bration curves relating potential change the elastic modulus of the material.
to crack extension may be easily de- Measurement of displacement is the
termined for through-cracked speci- basis for use of so-called compliance
mens by use of analog paper. With gages in measuring the crack extension
optimum location of the potential probes, in fracture toughness specimens. In
a very high sensitivity to crack extension practice, a test specimen is provided
may be obtained. For example, it may with a gage that measures the displace-
be reasonably assumed that 0.050-in. ment as a function of applied load as the
chart-pen movement on the X-Y re- crack extends. It is usually assumed that
corder is easily discernible and that a the compliance corresponding to any
gain of 100,000 is possible through the point on the curve may be obtained
voltmeter-amplifier with good stability. from the slope of a line connecting this
This corresponds to a sensitivity of 0.5 point to the origin.
#v. With this sensitivity, a crack ex- The crack length at a given load is then
tension of 0.0025 in. is obtained from determined with the aid of a calibration
the calibration curve for an aluminum curve. For example, in the case of sym-
center-cracked specimen (W --- 3 in. metrically loaded plate specimens, this
and B -- 89in.) provided with 50 amp. curve gives the ratio of 2a/W as a func-
The current requirements can con- tion of C/Co, where C is the assumed
stitute a definite limitation on the use of compliance corresponding to a particular
the method. Thus, the resistivity of most point on the load extension curve, and
metals decreases very rapidly at tempera- Co is the compliance at zero crack length.
tures below about - 3 0 0 F, and at The value of Co may be calculated from
liquid-hydrogen temperature, the cur- the elastic modulus as is described later.
rent required for normal specimen sizes The calibration curve in this form will
would be prohibitively large. At elevated apply to any material, provided that all
temperatures, the resistivity increases dimensions of the specimen under test
but appreciable thermoelectric effects and the gage length are proportioned to
become difficult to avoid. The speed of the calibration specimen. Calibration
testing is limited by the response of the curves are obtained by machining
potential measuring device employed. progressively longer slots (simulating
When the high sensitivity electronic the crack) into a calibration specimen
voltmeter described above is used, the and determining the compliance for the

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SRAWLEY AND BROWN ON TESTING METHODS 181

selected gage length at each known slot This requires that the gage length be
size for conditions of elastic loading. adjustable to accommodate various
This method of determining crack specimen sizes. This, in turn, requires
extension is well suited to tension-loaded the signal output as a function of dis-
plate specimens containing through-the- placement to be linear over a sufficiently
thickness cracks, although in principle wide range to accommodate the largest
it applies to any specimen. However, displacements anticipated. On the other
application to other specimen types offers hand, the main requirement of the dis-
as yet unresolved problems either in the placement gage in 9x~ testing is that of
experimental procedure or in the inter- high sensitivity to initial crack move-
pretation of the results. For example, ment. For either type of testing the gage
the method has been applied to circum- length should be as short as possible as
ferentially notched round bars as de- an aid in obtaining maximum sensitivity.
scribed in Ref (33) and more recently by Linear response to displacement com-
Van der Sluys (45). The data obtained bined with high sensitivity and adequate
indicate that the change in compliance range for ~, testing is provided by linear
with crack extension is relatively small differential transformers. A recent paper
for this specimen type and that ec- by Boyle (47) describes a fixed gage
centricities of loading (which are difficult length (2 in.) adapter that permits the
to avoid) can have an appreciable effect use of a standard releasable extensometer
on the accuracy. for displacement measurements between
Before proceeding to a discussion of gage points spanning the center notch
the practical application of displace- in plate specimens. A magnification
ment-gage techniques for crack-extension factor of 2 is provided by a lever system
measurement, it should be mentioned with spring-loaded knife edges. The
that the strain energy release rates can adapter is not completely separable,
be determined from the rate of change and the gage points suffer rather badly
of compliance with crack length. This when testing hard specimens to fracture.
technique for determining ~ values for It is difficult to construct a trouble-free
a particular specimen geometry was displacement gage with a variable gage
suggested in Ref (32) and was used in length. A design of this type for center-
Ref (33) to obtain an experimental rela- notched specimens used by Jones and
tion between strain energy release rate Brown (4s) consists of an upper and
and crack depth in bend specimens and lower split yoke. These are attached
circumferentially notched round bars. A independently to the specimen so that
more recent publication (24) describes a the gage is completely separable. One
very precise method for measuring the yoke contains the differential transformer
compliance of tension-loaded plate speci- and the other serves as a reference surface
mens as a function of crack length and for the transformer core. The yokes are
gives results for a single-edge-notched provided with gage points that span the
specimen. notch at the specimen center. A particu-
Gage Types and Testing Procedures-- lar gage length is established by use of a
The requirements for a displacement positioning jig that is removed after
gage to be used in ~ tests are somewhat clamping the yokes to the specimen. This
more difficult to meet than those for gage is adaptable to any specimen thick-
~,, testing. For the former application, it ness and, in principle, could be made to
would be desirable to use a single cali- accommodate a range of specimen
bration curve for a given specimen type. widths. In order to permit its use on

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182 FRACTURE TOUGHNESS TESTING

specimens having an appreciable bow, types of transformer are used in the


an additional linear differential trans- displacement gage, additional circuits
former should be incorporated so that may be required to obtain .the desired
the strains on the two flat surfaces of magnification factor. If the transformer
the specimen may be averaged. In an output is to be fed to an X - Y recorder,
arrangement used by Bulloch and Fergu- it is necessary to employ a suitable
son (49) a linear differential transformer converter.
and a suitable reference surface are As indicated previously, requirements

iilmmyspecimen

~,T / ")-Beamgages

estsp~imen H

Differential gages

Beam9qeoutput
Fzo. 26--Load-Displacement Records for Single-Edge-Notched Specimen Obtained by Using
Single Beam Gage and Differential Beam Gage.

fastened to the specimen by means of regarding the measuring range and


pins fitted through small holes. This linearity of output may be relaxed in
method of direct attachment appears to 9z~ testing. Relaxation of these require-
be limited to situations where the speci- ments gives more freedom in the design
men thickness is sufficient to support of displacement gages that are frequently
the pins; however, it does have the ad- optimized for a particular specimen type.
vantage of flexibility. The linear differential transformer gages
It is possible to drive the load-strain described above are, in general, also
recorder of some tension testing machines suitable for ~ , testing. In the case
directly from a linear differential trans- of single-edge-notched specimens, a
former output. However, when some standard releasable or separable ex-

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SRAWLEY AND B~OWN ON TESTING METHODS 183

teusometer may be clamped at the speci- sensitive gages of this type is given in
men edge across the notch; however, an Ref (~). Beam gages are readily adapt-
extensometer used in this way can be able to a variety of testing situations.
damaged if the specimen halves are For example, the gage may be located
allowed to rotate freely about the load- by edge grooves machined on either
ing pins after fracture. Excessive rota- side of the notch in single-edge-notched
tion can be prevented by placing soft specimens. Krafft (51) has used pins
metal blocks in the yokes under the glued to the surface to position a beam
specimen ends. For bend tests, Romine gage across the center notch of a plate
(5o) has described the use of a conven- specimen. The output of a beam gage

Potential
/
/
I P2" P2
, .d,P /
/
W/lO rPl W16 /
/
'2V'13~--L-----~" P2 I /
~J
/ /l
/
& 9 .d,P / / PI" P1
/ /J
/ r/
/ l/J
i: J//!/ d-djDisplacement
J
//~ / ,.t

0.1 0.2 0.3 0.4 0.5 0.6 0.? 0.8


2a/W
Fro. 27--Comparison of Displacement-Gage Calibration Curve with Several Calibration Curves
Obtained by Using Electric Potential Measurements Illustrating Influence of Gage Length.

tional deflectometer to measure deflec- will be a nonlinear function of its end


tions at the point of load application. deflection; however, this is of no particu,
Frequently, it is possible to use a lar consequence in ~c testing, where a
relatively simple beam gage (or clip pop-in indication is the only information
gage) that consists of a metal strip required.
with wire resistance or foil strain gages A differential beam gage is under
on opposite faces. The beam gage is then development by the authors to detect
bent to bear against two reference pop-in in single-edge-notched specimens.
surfaces at the extremes of the gage The principle is to buck out that part
length. Sensitivity of a beam gage in- of the gage output that is not due to a
creases with the ratio of beam thickness change in crack length. The arrangement
to length and the ratio of gage length used in Fig. 26 consists in loading the
to beam length. A description of highly test specimen in tandem with a dummy.

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184 F ~ c r u m z TouGm~ss T~-s~Nc

Both specimens are provided with beam the previously discussed potential
gages spanning the edge cracks, the out- method. The displacement-gage cali-
put of these gages being opposed in a bration is given as C/Co versus 2a/W,
suitable bridge arrangement. The where C is the compliance corresponding
dummy specimen is identical to the to any point on the load-displacement
test specimen except that its edge slot curve and Co is the compliance for zero
is terminated in a hole rather than a crack length. This calibration curve
fatigue crack, so that no crack extension applies to all center-notched specimens
in the dummy occurs during the test. provided that the displacement gage
A schematic X-Y recorder plot of gage used has a gage length of 2W/3 and is
output versus applied load, shown in located symmetric to the crack plane at
Fig. 26 for a single-edge-notched speci- the specimen centerline. Under these
men, illustrates results obtained with a conditions, C = e/P, where e is the total
differential beam gage and a single gage. measured deflection at the load, P.
Two advantages of the differential beam The value of Co for this gage length may
gage as compared with a single gage are be calculated as Co = 2/3EB, where B
evident. Because the differential gage is the thickness and E is the elastic
mxtput is obtained only with crack modulus of the test specimen.
extension, pop-in indications will be This procedure for use of the calibra-
more distinct and considerably higher tion curve assumes that the unloading
gain may be used without exceeding line corresponding to any given amount
the limits of the chart paper before of crack extension on a load-displacement
pop-in occurs. curve will be linear and will pass through
The instrumentation necessary for the origin. Actually, as shown in Ref
beam gages is the same as that normally (47), the unloading curves are not exactly
employed with wire resistance strain linear and do not pass through the origin.
gages. The gage outputs can be used to This is attributed to the action of a
drive conventional tension testing ma- crack-tip plastic zone that acts to prop
chine load-strain recorders either directly open the crack on unloading. By ad-
or through commercially available adap- justing the unloading curve to pass
tors. If an X-Y recorder is used, the gage through the origin, it is assumed that
bridge output may be connected directly this propping effect is subtracted out
to one axis with the output from a load and that the "true" compliance at load
cell bridge on the other. is determined.
Reduction of Data--If plane-strain It should be noted that the displace-
toughness determinations are to be ment measurements will be increased
made, the load at pop-in is determined by crack-tip plasticity as well as by
from records such as those shown in Fig. crack extension. For this reason, it has
26 and used with the appropriate ~x~ been suggested that the crack lengths
equation (see Appendix). If the load- calculated from the displacement-gage
strain record has been determined with calibration curves be used directly in the
gages designed for 9r testing, the deflec- 9c equations since, in effect, they already
tions may be converted to crack lengths contain a plasticity correction. While
by using a suitable calibration curve. A this procedure should probably be
calibration curve given in Ref. (47) for followed, it is difficult to establish it on
center-notched specimens is shown in a firm basis due to the previously dis-
Fig. 27, along with some curves for the cussed complexities introduced by the
same specimen geometry obtained by nonldeal unloading curve behavior.

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SRAWLEY AND BROWN ON TESTING METHODS 185

When interpreting displacement-gage high strain rates because the output may
data in terms of crack extensions, it be easily displayed on conventional
should be remembered that, at best, only oscilloscopes. The authors have used
average values can be determined unless these gages on single-edge-notched speci-
the crack extension is large in comparison mens fractured in the order of a few
with the thickness. Measurement errors milliseconds. Care must be taken to de-
associated with small crack extensions sign the gage and arrange the mounting
due to the curved nature of the crack so that the rapid application of load does
front were previously discussed in con- not cause resonance vibration in the
nection with data reduction from po- beam.
tential measurements. There appears to be no inherent limita-
Advantages and Limitations of Dis- tion to the application of displacement
placement Gages--This method in prin- gages in fracture toughness testing. As
ciple is adaptable to a wide variety of compared with the electrical potential
testing situations, but the particular technique, however, the method of
gage design will depend on both the adapting the sensing element to the
specimen type and the testing conditions. specimen is frequently more difficult.
If linear differential transformers are This is particularly true of the linear
employed, the gage may be immersed gages desirable for ~ testing, which may
directly in a cryogenic bath. The authors require carefully machined and some-
have used differential transformers at times complex mounting and linkage
liquid-hydrogen temperatures with no systems. Another disadvantage lies in
difficulty, provided that the trans- the fact that unwanted bending deflec-
former windings were sealed against tions will cause nonlinear response and
moisture. By employing conventional require the use of double sensing ele-
extensometer extension-arm arrange- ments to cancel the bending effects.
ments, linear differential transformer Sensitivity of Displacement Gages--
displacement gages could be used for Before leaving the subject of displace-
high-temperature tests. ment gages, some comment should be
A beam-displacement gage for 9~ test- made regarding their sensitivity. It has
ing at high temperatures with center- been generally assumed that this crack-
notched plates was described by Morri- measurement method is inferior to the
son et al (Sz). The gage is mounted electrical potential technique regarding
between extension arms that contact the the sensitivity available. This observa-
edges of the specimen near the heads and tion is probably based on the rather
extend out the sides of a split infrared large apparent difference in slopes be-
lamp furnace. Because of the fact that tween the calibration curves that have
the gage points are far removed from the been published for these two methods.
crack, this gage has rather low sensi- In order to define more clearly such dif-
tivity. Beam gages with foil-resistance ferences, a calibration curve for the
sensing elements could be used at cryo- center-notched plate displacement gage
geuic temperatures. A discussion of the described in Ref (47) is compared (Fig.
most suitable types of foil gages for use 27) with calibration curves obtained for
in liquid hydrogen and special precau- the same specimen type by using po-
tions regarding their application has tential measurements. From this repre-
been presented by Kanfman (~,S4). sentation it is quite evident that the
The beam-displacement gage is par- slope of the calibration curves depends
ticularly well suited to 6i, testing at on the gage length and position selected.

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186 FRACTURE TOUGHNESSTESTING

In this respect, the potential measure- on an aluminum single-edge-notched


ment has an advantage since the probes specimen and assuming the same mini-
can be located very close to the crack mum pen deflection for a pop-in indica-
tips; however, it should be noted that, tion. These calculated sensitivities, of
for identical locations and gage lengths, course, are not directly comparable in a
Boyle's displacement-gage calibration quantitative sense and should not be
curve has a definitely greater slope than taken as limiting values. They do indi-
that obtained by electric potential meas- cate, however, that both the displace-
urements. From this displacement-gage ment-gage and potential method can
14, 000 - -
18NI-Co-Mosteel
_ 3"?n -
12,000
f ACoustic record~ j " "~

10,000

8,0QO

_ Potential U
"-Potential
4,0(]0
Single-e~je-
notch
specimen
2,000 m

J
of"l I i I /
Potentialchange
FIo. 28--Load-Potentialand AcousticRecords from Single-Edge-NotchedSpecimensIllustrating
Oifferent Pop-In Behaviors.
calibration curve, an estimate was made have very high sensitivity to crack exten-
regarding the absolute sensitivity to sion.
crack extension that could be obtained
in a typical case. Acoustic Method:
The case selected as an example is Disturbances within a material that
represented by a load-deflection curve result in the sudden release of elastic
given in Ref (47) for a 7075-T6 center- energy can frequently be detected by
notched specimen x~-in, thick and 3 in.- using a transducer that will convert an
wide. With the assumption that a chart- elastic vibration into an electrical signal.
pen deflection of 0.050 in. is easily Thus, if a piezoelectric crystal is placed
discernible at a magnification of 2000, a in contact with a specimen containing a
total crack extension of 0.006 in. should propagating crack, the crystal will pro-
be detectable at the pop-in load, which duce signals that may be amplified and
was about 16,000 lb. This may be com- recorded or used to drive a loud-speaker.
pared with the 0.003-in. crack-extension The acoustic method of detecting crack
sensitivity previously mentioned for the propagation has been described in a
electrical potential method when used paper by Romine ($5) and in Ref (48).

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SRAWLEY AND BROWN ON TESTING METIIODS 187

The latter paper contains a detailed de- tinted to outline the fracture area, and
scription of the method including the then pulled to failure. Two rather differ-
electronics required for recording load ent behaviors are represented by these
and crack sounds. tests.
In practical application, a crystal The specimen aged at 800 F exhibited
transducer such as a slightly modified an abrupt large potential change at about
phonograph pickup is clamped to the 10,000 lb, and this corresponds to a large
specimen or to the loading train. A tape burst of sound. Preceding this burst,
recording is made of the load and speci- there were very weak acoustic indications
men acoustic output simultaneously on possibly due to crack movement in
separate channels. The tape record may fatigue-damaged metal. Approximately
then be transferred to a recording oscillo- 0.1-in. total crack extension was repre-
graph or simply audited with the tape sented by this pop-in, and the plastic-
load channel working a counter. The zone size at pop-in was less than one
method is extremely sensitive to small tenth the thickness. Under these circum-
crack extensions and may give definite stances, there seems to be little doubt
indications of crack movement before that the load at fracture instability in
either an electrical potential or a dis- the opening mode has been measured.
placement gage gives a discernible out- The behavior of the specimen aged at
put. While the amplitudes of the acoustic 725 F appears more complex. There is a
signals probably increase with the distinct step in the load-potential curve
amount of material involved in a given at about 13,400 lb, and this corresponded
increment of crack movement, there is to about 0.025-in. total crack extension.
no known way of estimating the amount The plastic-zone size at this pop-in was
of crack extension from acoustic records. approximately one eighth the specimen
For this reason, the acoustic technique thickness. It will be noted that rather
is best used in conjunction with either strong acoustic indications start at about
potential measurements or displacement 9500 lb and continue with increasing
gages. Employed in this way, it provides load. Using the acoustic indications as a
additional information concerning the guide makes it possible to detect a slight
initial stage of the crack propagation departure from linearity in the potential
process. record also starting at about 9500 lb.
Examples of Data--As shown in Ref Apparently, a substantial portion of the
(48), the acoustic method is capable of 0.025-in. total crack extension at pop-in
indicating pop-in loads that agree well took place at considerably lower loads.
with those obtained by using displace- There is a question as to whether the
ment gages. In some cases, the acoustic pop-in load observed for the specimen
method may also be helpful as an aid in aged at 725 F can be used to calculate a
interpreting a load-potential or displace- K~ having the same meaning as that
ment record. In order to illustrate this calculated from the pop-in obtained
point, two examples are shown in Fig. 28 from the specimen aged at 800 F.
for single-edge-notched tests on an Advantages and Limitations of Acoustic
18Ni-Co-Mo steel aged at 725 and 800 F. Method--The major advantage of the
In this representation, load-potential acoustic method lies in its relative sim-
records are given along with correspond- plicity and adaptability to a variety of
ing indications from oscillograph traces specimen types and testing situations.
of the acoustic output. These tests were For example, if the specimen is enclosed
interrupted at the point indicated, heat- in a furnace or low-temperature bath,

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188 FRACTURE TOUGHNESS TESTING

the pickup may be mounted on some and is applied to the specimen surface so
part of the loading train external to the that the elements are normal to the direc-
specimen enclosure. Special precautions tion of crack propagation. The elements
must be taken, however, to eliminate the are longer the farther they are from the
introduction of extraneous sounds that notch tip. This arrangement provides
might mask or be confused with crack- approximately linear resistance change as
movement indications. As a general rule, successive elements are fractured by the
it is desirable to establish independently extending crack.
the background-noise character and level In its present form, each gage is about
before conducting a series of tests. Fre- 89in. wide and has 20 elements with a
quently, this may be accomplished by spacing of approximately 0,01 in. If
loading a smooth specimen under the crack extensions beyond 0.2 in. are ex-
same conditions as to be used for the pected, additional gages are placed in the
notch tests. As mentioned previously, a line of crack extension. Conventional
major disadvantage of the acoustic strain-gage instrumentation may be used
method is the fact that there is as yet no with each gage being part of a bridge
way of quantitatively relating the signal circuit. The output of the bridge is re-
characteristics to the extent of crack corded on a light-beam galvanometer
movement. oscillograph along with a load trace from
a load-cell-bridge circuit. A step appears
Continuity Gage: in the output for each ribbon element
fractured and the crack length at maxi-
A recent paper by Kemp (s6) describes mum load can be determined by count-
the use of a "continuity" gage to measure ing these steps.
crack extension. Essentially, this is a The main advantage to this type of
special type of foil-resistance strain gage gage is its adaptability to crack-growth
and is constructed in the same general studies in tank tests at cryogenic tem-
way. It consists of regularly spaced metal peratures. The gages are rather expensive
ribbon elements all connected in parallel and, of course, are not re-usable.
APPENDIX

PRACTICAL FRACTURE TOUGHNESS SPECIMENS--DETAILS


OF PREPARATION, TESTING, AND DATA REPORTING
This section presents a convenient sum- Fig. 30(~-c) for the single-edge-notched
mary of the geometries of the recommended plate and bend specimens. The sources of
practical fracture toughness test specimens. these expressions are discussed in the text. It
Included also will be comments on specimen will be noted that the factor (1 - vs) has
preparation, testing precautions, and data been used in the equations relating ~ to K for
reporting. plane strain. This factor is an approximation
The various practical fracture toughness in relation to the stress state in an actual
test specimens are shown in Figs. 29-30. The plate specimen. This point was discussed
proportions given are those developed in further in the text, and as mentioned, it is
previous sections of this paper. Relations for difficult to judge the accuracy of the pub-
and K are given in the usual closed form lished approximate solutions for ~i for
for symmetrically cracked tension specimens circumferentially notched round bars. The
(Figs. 29(a) and (b)), and for the surface- form shown in Fig. 30(e) represents an aver-
cracked plate specimen (Fig. 30(d)). Poly- age of several results in the d/D range be-
nomial expressions in a/W are shown in tween 0.55 and 0.9.

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SRAWLEY AND BROWN ON TESTING METHODS 189

Specimen Machining: Where loading pinholes are shown, these


The most critical features of specimen should serve as reference surfaces for ma-
machining are concerned with the prepara- chining the crack starter notches. In this
tion and location of the fatigue crack starter way, symmetry of the notches about the
notches and the means for transmitting the loading axis is easiest to achieve. It should be
load to the specimen. Details of the starter noted that the pinhole position in relation
notches for plate tension specimens are to the width is an important parameter in
shown in Fig. 31. The dimensional limits the single-edge-notched plate specimen and
given will ensure that the influence of the that the ~i expression shown applies to the
shape of the notch does not extend to the W/2 position with the limits indicated. No
tip of the fatigue crack. The angle at the means for gripping the surface-cracked plate
slot end is not critical and the notch-tip specimen or the circumferentially notched
radius shown may be easily produced by round bar are shown in Fig. 30(a-e). Pin-

For tlc tests


5 <-WlB < I0
Eq= Eqic - (i - u2)KIc
9

(See fig. 3!.1 -<:"-'- , ""'""-" 1 -E~-E~-qEqc EqIc


--. . a. am + 2-'~ 5 a - am + u,,~y~'ZS
p2 ~'a [
EG'~ tan "~

(a) Symmetrical center-cracked plate.


A - Surfaces must be symmetric to
specimen centerline within
WllO~

' ,ol
W + 0.1 sin ~ - J

(b) Symmetrical edge-cracked plate.


Fro. 29--Practical Fracture Toughness Specimen Types. Specimens for General Use. (The Fac-
tor (1 -- v~) Is an Approximation. See Text of Appendix.)

slightly extending the ~-in. slot with a loading of the surface-cracked specimen will
0.010-in. jeweler's saw. If the starter notches require a head wider than the test section, or
shown in Fig. 31 cannot be accommodated the use of doubler plates around the pin-
because of insufficient specimen width, it is holes. Alternatively, the specimen may be
best to produce narrow slots by using an gripped in the tension testing machine jaws.
electric-discharge machining process. An The circumferentially notched round bar is
indentation made with a sharp chisel having normally provided with buttonheads al-
a rounded end will serve as a crack starter though, as described in Ref (8), a threaded
for the surface-cracked specimens. Alterna- specimen with special alignment surfaces
tively, a surface notch may be produced by may be used. In either case, precision ma-
an electric-discharge process. The V-notch chining of all cylindrical surfaces is necessary
in the circumferentially notched round bar to ensure that the notch section is perpendic-
should have as sharp a tip radius as possible ular to and concentric with the loading axis.
in order to minimize the stress necessary to The edges of the plate tension specimens
produce fatigue cracks in a reasonable do not have to be machine-finished unless
length of time. they serve as locating surfaces for positioning

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190 FRACTURE TOUGHNESS TESTING

V,< "-b,o.W~, ~+,~ <t<


AU/
(a) Single-edge-notchedplateItension), l " Surfacesmustbetrue to specimen
centerlinewithin W/lO00

2<W[8<8
L2

L-4W ~ L-4W
(h) Notchbendspecimen(three-pointloaded).

2<W/B<8

/
E~,Ic./P) 2 L2 a~.55 2 a2+196 ~)
Eqlc9(I - v2) K~C
L,4W-- -,- L-4W
(C)Notchbendspecirnen(four-pointloaded}.

W/B> 6

P W a~< B/2

l -
1.~.P2,o F 1 ]

/r12~ c2"a2
<~- 1-~~ "Osin2edo

(d) Surface-crzckedplate.

3O0/600
A - Surfacesmustbeconcentric

d'"o'k F,/
(el Circumferentially notchedznd fatlgue-cracked
round bar,
FiG, 30--Practical Fracture Toughness Specimen Types. Pla~e-Stra~ Tests. (For. All SpecLme~s
a =. ao + E g l 6 x ~ r ~ ; the factor (1 -- ~) Is an Approximation. See Text of Appendix.)

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SRAWLEY AND BROWN ON TESTING METHODS 191

of the notches and pinholes. The flat sur- duces "wing cracks" starting from the
faces of these specimens are machined only surface and joining at the center of the thick-
when necessary to remove warping or to ness. These cracks are sometimes difficult to
eliminate an unwanted surface layer. Rec- keep in one plane and form a crack front
tangular cross-section bend specimens (Figs. with considerable curvature. Further studies
30(b) and (c)) should provide no special of these crack shapes are required before
machining problems whatsoever. Surfaces in this method of producing fatigue cracks can
contact with the loading and support pins be recommended.
should be ground to reduce friction. These Surface fatigue cracks may be produced
surfaces can then serve for reference put- by cantilever bending of the specimen over a

Specimen loading hole r


1/4 in *V32 ~
diam. \ q-.,..,, 90+2o
'~ ~. - r 0 005-in red. max
~,f ~%k_~ / (seetext)

Fatigue ~
crack

[ ' ~ I A 9 B within 0.010 in.


== 2a0 - =,

(a) Fatigue crack starter for center-cracked plate specimens ON _>2 in.).

/-0.00P-In. rad. max (see text)

L ~ / / r Fatigue crack
1/16 nax
Single edge notch W20.6 in.
rain ' min ' Notchbend W_>l.0in.

(b) Fat ue crack starter for edge-notched plate specimens.


FI6. 31--Fatigue-Crack Starter Notches for Center-Cracked and Edge-Notched Plate Speci-
mens.

poses when machining the fatigue crack support that tapers to a point. Details of this
starter notch. technique are given in Refs (38,39). Cracks
are initiated more easily and may be located
Fatigue Cracking and Heat Treatment: at the desired spot on the specimen surface
Details concerning the fatigue cracking of if a small sharp indentation is provided as a
the symmetrically cracked tension specimens crack starter. As mentioned previously, this
(Figs. 29(,7.) and (b)) and the circumferen- starter notch may be produced by a chisel or
tially notched round bar (Fig. 30(e)) have by electric-discharge machining. The sur-
been given in Refs (5,8). It was recommended face cracks produced by this method are
that tension-tension loading be used to pro- semi-elliptical in shape with the ellipticity
duce fatigue cracks in the symmetrically usually increasing with the depth; however,
center-cracked specimens; however, some it is possible to control the crack shape if
investigators have cracked this type of speci- the starter notch is produced by electric-
men in bending with the moments perpen- discharge machining by using specially con-
dicular to the sheet plane. This method pro- toured electrodes.

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192 FRACTURE TOUGHNESS TESTING

Fatigue cracking of single-edge-notched (8), when preparing circumferentially


plate specimens may be conveniently ac- notched round bars, it may be necessary to
complished by cantilever bending with the finish machine and fatigue crack after full
bending moment in the plane of the speci- heat-treatment in order to correct for warp-
men. The stress at the notch tip is kept in age and to avoid quench cracks. These con-
tension with the minimum stress set just siderations may also be important for thick
sufficient to ensure smooth operation of the plate specimens.
fatigue machine and satisfactory alignment
during the fatigue cycling. This method Testing Procedure:
poses no special problems, and the cracks Testing procedures for symmetrically
are relatively easy to control since they are cracked sheet tension specimens and circum-
running into a decreasing stress field. ferentially notched round bars have been
There are very few data regarding the discussed in Refs (5) and (8). As described in
effect of the maximum stress used in produc- these publications, special care should be
ing fatigue cracks on the measured fracture taken to minimize eccentricity of loading by
toughness. Some results given in Ref (39) for using pin-yoke assemblies for sheet speci-
surface-cracked specimens of a brittle steel mens and by using special loading devices
indicate no significant difference in average for notched round bars. Details concerning a
KI~ values for nominal bending stresses of concentric buttonhead loading fixture for
about 30, 40, and 60 per cent of the yield notched rounds are given in a paper by
strength. The scatter of data, however, ap- Jones and Brown (57). When testing thick
peared to be greater as the nominal bending pin-loaded specimens in tension, it is ad-
stress increased. In view of these results, it visable to make use of double pin yokes in
would seem best to keep the nominal net- order to minimize bending moments acting
section stress below 50 per cent of the yield both perpendicular and parallel to the sheet
strength when fatigue cracking. plane. These yokes must be carefully ma-
The question of whether heat-treating chined so that they do not in themselves
should precede or follow fatigue cracking is introduce bending due to misalignment of
difficult to resolve with the limited amount the pinholes. When pin yokes are used, it is
of data now available. The center-crack desirable to lubricate the pinholes with
strength of a relatively brittle steel ~) was molybdenum disulfide.
the same whether sheet specimens were As mentioned previously, surface-cracked
heat-treated before or after fatigue cracking. specimens, if pin-loaded, will require a head
The results of a few surface-crack tests (38) larger than the test section or the use of
appear to confirm this behavior. It would doubler plates around the pinholes. By using
seem reasonable to assume that any differ- the tension testing machine jaws for grip-
ences in fracture toughness due to the crack- ping, a uniform width and thickness speci-
ing and heat-treating sequence would tend men may be employed. It might be expected
to be minimized by stable crack extension. that loading in the jaws of a tension testing
For this reason, the effects of this sequence machine would introduce considerable
should be more pronounced in ~tc than in eccentricity, which would vary from test to
~c tests. In this respect, recent experiments test and produce excessive scatter. However,
in the authors' laboratory showed that more data from a large number of replicate tests
distinct pop-in indications were obtained on jaw-loaded surface-cracked specimens of a
for 18Ni-Co-Mo single-edge-notched tests brittle steel have been reported (39) and
when specimens were aged after fatigue these data exhibit very small scatter. In
cracking rather than before. In the absence addition, a few results (38) for pin-loaded
of more definite information, it would seem specimens indicate that surface cracks ec-
reasonable to heat treat after fatigue crack- centric with respect to the specimen center-
ing where possible. This procedure should line do not result in lower strengths. On the
assist in reducing any effects that might basis of the data available, it would appear
arise from differences in the fatigue stressing that jaw loading for this type of specimen is
condition% however, as pointed out in Ref permissible. However, the data should be ex-

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8RAWLEY AND B R O W N ON TESTING METHODS 193

amined for scatter that could be attributed testing techniques, but also on the proper
to variation in eccentricity from test to test. identification of the reported data. All too
In the case of heat-treated martensitic frequently fracture toughness information
steels, crack extension can occur due to appearing in the published literature and in
stress corrosion under a constant load in the company reports is so poorly identified that
presence of water vapor. Plane-strain frac- no judgment can be made concerning its
ture toughness values for such materials can validity nor its applicability to the particu-
be influenced by the amount of water vapor lar problem at hand. I t must be remembered
in the air and this effect will depend on the that fracture testing and fracture mechanics
testing speed. Results are given in Ref (46) analysis are new approaches to a very com-
for circumferentially notched round bars of plicated problem and that in the formative
SAE 4340 (errs = 225,000 psi) tested at stages of any engineering science it is neces-
three levels of relative humidity using nor- sary to provide the maximum amount of
mal loading rates. Because of the limited information to the person attempting to use
amount of data available from this investi- the data. With this in mind, the Fifth Report
gation and the scatter encountered, no of the ASTM Special Committee on Fracture
quantitative relation could be established Testing (9) listed required supplementary
between the amount of moisture present and information that should be reported with
the fracture toughness; however, the notch fracture toughness data.
strength decreased with increasing relative Care should be exercised to avoid using
humidity. In view of the uncertainties in- the designation "fracture toughness" or the
volved, it is not possible to make any recom- symbols ~ or K in connection with data that
mendations at this time concerning control do not meet the basic requirements for
of the humidity during a test; however, when fracture toughness testing. A particularly
testing low-alloy tempered martensites or dangerous practice is the reporting of calcu-
other alloys subject to stress corrosion in lated critical flaw sizes as a function of
the presence of water, the temperature and applied stress when the calculations are
relative humidity of the air surrounding the based on poorly established fracture tough-
specimen should be recorded. ness data. Information of this type should
always be carefully qualified regarding the
Data Reporting: basis of calculation and the manner in which
The usefulness of fracture toughness data the fracture toughness parameters were ob-
depends not only on the selection of proper tained.

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194 FRACTURE TOUGHNESS TESTING

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SRAWLEY AND BROWN ON TESTINO METHODS 195

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Am. Soc. Testing Mats., Vol. 59, 1959, pp. July, 1960.
885-915. (46) W. A. Van der Sluys, "Effects of Repeated
(34) G. M. Orner and C. E. Hartbower, "Sheet Loading and Moisture on the Fracture
Fracture Toughness Evaluated by Charpy Toughness of SAE 4340 Steel," T dr AM
Impact and Slow Bend," Welding Journal Report 245, University of Illinois, May,
(Research Supplement), Vol. 40, Septem- 1963.
ber, 1961, pp. 405s-416s. (47) R. W. Boyle, "A Method for Determining
(35) J. M. Krafft, "Fracture Toughness of Crack Growth in Notched Sheet Speci-
Metals," Report of NRL Progress, U.S. mens," Materials Research dr Standards,
Naval Research Lab., November, 1963, Vol. 2, No. 8, August, 1962, pp. 646-651.
pp. 4-16. (48) M. H. Jones and W. F. Brown, Jr., "Acous-
(36) C. D. Beachem and J. E. Srawley, "Frac- tic Detection of Crack Initiation in Sharply
ture Tests of Surface Cracked Specimens Notched Specimens," Materials Research dr
of AMS 6434 Steel Sheet," Memorandum Standards, Vol. 4, No. 3, March, 1964, pp.
Report 1097, U.S. Naval Research Lab., 120--129.
September, 1960. (49) D. F. Bulloch and R. Ferguson, "Thick
(37) J. E. Srawley and C. D. Beachem, "Frac- Section Fracture Toughness, Exhibit B,"
ture of High Strength Sheet Steel Speci- Quarterly Progress Report 1, Boeing-North
mens Containing Small Cracks," ASTM American, Los Angeles, Calif., October,
STP 302, Symposium on Evaluation of 1963.
Metallic Materials in Design for Low-Tem- (50) H. E. Romine, "Plane Strain Fracture
perature Service, Am. Soc. Testing Mats., Toughness Measurements of Solid Booster
1962, pp. 69-83. Case Materials," RTD-TDR-63-4048,
(38) C. S. Yen and S. L. Pendleberry, "Tech- Third Maraging Steel Project Review, AF
nique for Making Small Cracks in Sheet Materials Lab., November, 1963, pp. 185-
Metals," Materials Research dr Standards, 211.
Vol. 2, No. 4, November, 1962, pp. 913-916. (51) J. M. Krafft, Unpublished note to the
09) J. E. Srawley, "Small Fatigue Cracks as ASTM Committee on Fracture Testing of
Fracture Origins in Tests of High-Strength High Strength Metallic Materials, Aug. 29,
Steel Sheet," Proceedings, Am. Soc. Testing 1963.
Mats., Vol. 62, 1962, pp. 734-741. (52) J. D. Morrison, P. C. Jenkins, and J. R.
(40) A. E. Green and I. N. Sneddon, "The Kattus, "An Investigation of the Crack-
Distribution of Stress in the Neighborhood Propagation Resistance of High-Strength
of a Flat Elliptical Crack in an Elastic Alloys and Heat-Resistant Alloys," Sum-
Solid," Proceedings, Cambridge Philosophi- mary Technical Report, Dee. 23, 1960--Oct.
cal Sot., Vol. 46, January, 1950, pp. 159- 23, 1962, Southern Research Inst., Nov. 21,
163. 1962.
(41) Ian N. Sneddon, "Crack Problems in (53) Albert Kaufman, "Performance of Electric-
Mathematical Theory of Elasticity," Re- Resistance Strain Gages at Cryogenic Tem-
port ERD-126/1, North Carolina State peratures," NASA TN D-1663, 1963.
College, May 15, 1961. (54) A. Kaufman, "Investigation of Strain
(42) B. M. Wundt, "A Unified Interpretation of Gages for Use at Cryogenic Temperatures,"
Room-Temperature Strength of Notched Experimental Mechanics, Vol. 3, No. 8,
Specimens as Influenced by Their Size," August, 1963, pp. 177-183.
Paper 59-MET-9, Am. Soc. Mechanical (55) H. E. Romine, "Determination of the
Engrs., 1959. Driving Force for Crack Initiation from
(43) E. A. Steig~'wald and G. L. Hanna, "Initi- Acoustic Records of 9o Tests on High
ation of Slow Crack Propagation in High- Strength Materials for Rocket Motor
Strength Materials," Proceedings, Am. Soc. Cases," NWL Report 1770, U.S. Naval
Testing Mats., Vol. 62, 1962, pp. 885-913. Weapons Lab., Oct. 4, 1961
(44) A. A. Anctil, E. B. Kula, and E. DiCesare, (56) R. H. Kemp, "Characteristics and Applica-
"Electric-Potential Technique for Deter- tion of Foil Strain Gages at --423 ~ F."

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196 FRACTURE TOUGHNESS TESTING

Paper presented at Western Regional (57) M. H. Jones and W. F. Brown, Jr., "An
Strain Gage Conference, Denver (Cole,), Axial Loading Creep Machine," ASTM
Sept. 30-Oct. 1, 1963. Bulletin, No. 211,January, 1956,pp. 53-60.

DISCUSSION
W. W. GEI~ERICH~--The amount of the plastic-zone size becomes much
information presented in this paper is greater than the plate thickness, the
too extensive to comment on in detail so energy absorbed by plastic deformation
I will limit my remarks to two points. becomes significantly large, so that it
First, I was very interested in the cannot be estimated using elastic con-
determination of maximum energy re- siderations. Using experimental stress
lease rate measurement capacity, Co, analysis techniques,* it has been strongly
as typified in Fig. 13 since this approach indicated that the plastic energy release
is practically identical to the one I rate exceeds the modified Griffith-Irwin
presented in a relatively uncirculated energy release rate at a value of *net/*r~
report3 The only difference should be somewhere between 0.8 and 1.0. To be
the utilization factor which stems from conservative, the 0.8 value is a valid
using ~net = 0.8 ~rs as an upper limit limitation for obtaining exact quantita-
for accurate measurements. However, tive design information.
my results are still 20 per cent higher J. D. MORRISONS--I simply wish to
even with the inclusion of the 0.64 congratulate the authors on their excel-
factor. For example, at the maximum lent presentation, which so effectively
which occurs at 2a/W of about 0.35, summarizes the current state of develop-
Fig. 13 gives a value of 0.21, whereas I ment and the significance of fracture
obtained a value of about 0.25. This toughness testing in terms of fracture
later value agrees with the maximum mechanics. The further refinement of
value obtained by Irwin 3 if the 0.64 methods for evaluating plane-strain
factor is included. Although this dis- fracture toughness, continuing at the
crepancy is small, I wonder if the authors authors' laboratory, is certainly to be
have some explanation for this differ- applauded. It is to be hoped that those
ence? In general, th~a approach can be individuals engaged in the design of
very useful in specimen design and the highly stressed structures, and those
authors are to be congratulated in ex- developing "new" structural materials
tending it to a number of test specimens for such applications, will follow the
and formulae. evolution of these methods and will
Secondly, the point that accurate apply them in terms of the recommenda-
measurements of ~c should be limited to tions of the ASTM Special Committee
cases where the a~et/~rs ratio is less than on Fracture Testing of High-Strength
or equal to 0.8 is very realistic. When Metallic Materials.
A. A. WI~LLSe---As an exposition of
~ Research Laboratories, Aeronutronie, Div. linear fracture mechanics from the view-
of Phileo Corp., Newport Beach, Calif.
2 W. W. Gerberieh, "Theoretical and Prac- 4W. W. Gerberich, "Current Trends in
tical Aspects of Correlating Percent Shear-Lip Testing Methods, Design, and Material for
to Relative Plastic Zone Size in Brittle Fracture," Fracture Toughness," presented at Joint
TR 3~-11~, Jet Propulsion Lab., California ASM-ASTME Meeting, March, 1964 and to be
Institute of Technology, September, 1962. published in Metals Engineerina Quarterly.
3 G. R. Irwin, "Advanced Fracture Strength Research Metallurgist, Southern Research
Measurement Techniques," Contributions to Institute, Birmingham, Ala.
1950 Lecture Series of Washington, D. C., 6 Dept. of Civil Engineering, The Queens
Chapter of ASM, 1959. University, Belfast, Ireland.

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DISCUSSION ON TESTING METHODS 197

point of its technological exploitation, Unfortunately, the analytical tools


the paper by Srawley and Brown offers for the assessment of triaxiality varia-
an exceptionally well-balanced judgment. tions under partly or fully plastic condi-
It gives loyal support to the ASTM tions are as yet rather crude, although
presentation, while indicating fully and the presence of these triaxiality varia-
with care the uncertainties and weak- tions is clearly revealed in the plastic
nesses. It will be widely read abroad rigid analyses for plane strain. As far as
and may favorably influence the com- the experiments are concerned, the re-
mittal of opinion there, where the pio- sults obtained on 36 by 3-in. edge-
neering achievements of ASTM have notched, mild steel tension specimens
been watched so far with great interest may be of interest (see Table 2). For
but also, it may be said, without wide- the purpose of this comparison the crack-
spread committal. opening displacement at fracture, ~, may
In view of the qualifications so ex- be taken as proportional to fracture
pertly presented, there is little to criticize toughness, 9~ The method of determin-
in the paper. It might, however, be useful ing the plastic stress-intensification or
to add a qualification which relates to triaxiality factor is described in a paper
the sources of variance of fracture tough- to the recent Royal Society Symposium
ness with crack length, and of the plane- in London which is to be published. The
strain values in particular. I refer to the highest triaxiality and lowest ~ values
T A B L E 2.

Notch depth, in . . . . . . . . . . . . . . . . . . . . . . . . 11/~ 3 6


Test temperature, deg C . . . . . . . . . . . . -10 -40 -10 -40 -10 -40
Crack-opening displacement at fracture, 5, mils . . 20.5 9 17 3 28 17
Observed plastic stress-intensification f a c t o r . . 2.14 2.22 2.10

influence of triaxiality, which may most fol ~ach temperature arise at 3-in. notch
succinctly be described in terms of the deph', the over-all variation correspond-
prevailing superimposed uniform stress ing with a transition temperature shift
field in the direction of crack travel, as of 20-40 C. There is reason to believe
foreshadowed many years ago by Irwin that the triaxiality falls right off for
in his elucidation of crack-tip stress fields. shallow notches. Of these results, most
Effects of this type have been high- were at general yield, but the 3-in.
lighted by our recent work in the United notch result at --40 C gave a low stress
Kingdom, aimed at the extension of fracture. Thus one would expect to see
linear fracture mechanics into the general these effects in high-strength steels too.
yielding range, for the benefit of utilizing It is tentatively suggested that the
the tougher low-strength materials. ASTM Special Committee might con-
Readers of the paper will recognize that sider the encouragement of linear me-
experiments based on low-strength steels chanics investigations into this field.
require use of large specimens, and in J. E. SRAWLEYAND W. F. BRow~, JR.
their analysis one is hemmed in with (authors)--The authors wish to thank
boundary effects. The triaxiality varia- the discussers for their comments. With
tions in these experiments are mainly regard to the first point raised by Mr.
exposed by the magnifying effect of the Gerberich, the apparent discrepancy
temperature transition, and its move- that he finds results from an under-
ment up or down by changing other standable oversight on his part. The
dimensions than the plate thickness. value of Co is an implicit one, not an

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198 FRACTURE TOUGHNESS TESTING

explicit one. The factor, tan(va/W), We will follow with interest Mr. Wells's
is equal to tan (~am/W + ECJ2*r*rs2) efforts at using crack-opening displace-
where a,, is the measured crack half- ment measurements in toughness evalua-
length and ECa/2~*rs~ is the value of tion of low-strength (high-toughness)
the plastic-zone correction term when constructional steels, and we look for-
is equal to Ca. Values of Co have to be ward to studying his discussion of tri-
calculated by graphical or iterative axiality effects in the paper to be pub-
procedures, just as do other ~ values. lished by the Royal Society. 7
When this is done there is no discrepancy Mr. Morrison hopes that those en-
between our values of Ca for a utilization gaged in the design of highly stressed
factor of 0.64 and Gerberich's or Irwin's structures, and those developing new
for a utilization factor of unity. On his materials for such structures, will apply
second point, we are encouraged to know fracture toughness test methods. In the
that Mr. Gerberich has obtained addi- authors' experience there is a steadily
tional evidence which supports the choice increasing demand for this type of test-
of a utilization factor of 0.64 as being ing and most alloy producers are now
realistic and conservative. There is a set up to make one or more of the tests
definite need for information of this described in our paper as a matter of
sort which will permit us to make more routine.
confident estimates of specimen-size 7 Further discussion of these subjects appears
limitations. in the panel discussion, see p. 373.

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EVALUATION OF PROPOSED R E C O M M E N D E D P R A C T I C E FOR
SHARP-NOTCH T E N S I O N T E S T I N G

BY R. H. HEYER1

SYNOPSIS
The objectives and limitations of the proposed recommended practice for
determining sharp-notch strength of high-strength sheet materials are given.
Two specimen designs are used: 3 in. wide with sharply machined edge notches,
and 3 in. wide with a center slot extended in both directions by fatigue cracking.
Evaluation test results are reported for sharp-notch strength of four materials:
aluminum alloy 7075-T651, titanium alloy 4A1-3Mo-IV, maraging steel
18Ni-9Co-5Mo, and precipitation-hardening stainless steel PH 14-8 Mo.
Test data from seven laboratories are analyzed for differences among lab-
oratories and between the two specimen designs. Agreement among labora-
tories is generally satisfactory considering inherent difficulties in preparing
sharply notched specimens to the close tolerances required. Data from speci-
mens out of tolerance after machining or after fatigue cracking were rejected.
Center-cracked specimens have significantly higher sharp-notch strengths than
edge-notched specimens in tests on the aluminum alloy and the precipitation-
hardening stainless steel.
Test specimens 8 in. long are suggested as alternates for the recommended
12-in. long specimens when insufficient material is available. Significant differ-
ences in test results were obtained for the two lengths of specimens.

A proposed Recommended Practice analogous to the ultimate tensile strength


for Sharp-Notch Tension Testing has of a standard tension-test specimen,
recently been drafted by the ASTM which is based on the area of the speci-
Special Committee on Fracture Testing men before testing.
of High-Strength Metallic Materials. Sharp-notch tension tests were pro-
The present paper is a report on evalua- posed as screening tests in the first
tion tests made according to the proce- committee report? The effects of notch
dures given in the proposed recom- angle, notch radius, width, and thickness
mended practice. were considered in the design of the test
The sharp-notch strength of an ap- specimens. The specimen width of 1 in.
propriate specimen is determined by has been increased to 3 in. in the recom-
dividing the maximum load sustained mended practice. This has been found to
in a slow tension test by the initial be necessary to reduce the tendency to
area of the supporting cross section in the yield plastically on the notched section
plane of the notches or cracks. This is
2 "Fracture Testing of High-Strength Sheet
Supervising research metallurgist, Armco Materials," A S T M Bulletin, No. 244, pp. 18-28
Steel Corp., Middletown, Ohio. (1960).
199
Copyright9 1965 by ASTM International www.astm.org
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200 FRACTURE TOUGHNESS TESTING

when testing the newer alloys having strength is less than the tensile yield
improved toughness. strength, and the discrimination increases
The objectives and limitations of the the lower the notch strength is with respect
recommended practice are further de- to the yield strength.
fined in the scope as follows:
1.3 This test is restricted to sheet materials
1.1 This recommended practice covers ap- not exceeding 0.25 in. in thickness. Since the
paratus, specimens and procedures for the notch strength may vary with the sheet
determination of a comparative measure of thickness, comparison of various material
the resistance of sheet materials to unstable conditions must be based on tests of speci-
fracture originating from a very sharp stress- mens having the same nominal thickness.

l.oo"dlo, ref. o.oo2"mox, cleoronce


with Iooding pin
:- Surfaces must be symmetric to center
line within 0.002"
/ ~ V~_ A A--Bwithin--"0~

. . . . + "r ..

| . _A'
/I
Notch radius_/ i~ --B -
O.O007"max. L ,4.2,$-~ _._~
i-
/~. o'~,- S.#" -j

*This dimension is 2.25" for


the ~'x 8" specimen.
Fro. 1--Machlned Sharp Edge-Notched Specimen (EN).

concentrator or crack. It relates specifically 1.4 The sharp-notch strength may depend
to fracture under continuously increasing strongly upon temperature within a certain
load and excludes conditions of loading which range depending upon the characteristics of
produce creep or fatigue. The quantity de- the material. The recommended practice is
termined is the sharp-notch strength of a suitable for use at any appropriate tempera-
specimen of particular dimensions, and this ture. However, comparisons of various ma-
value is determined by these dimensions as terial conditions must be based on tests con-
well as by the characteristics of the material. ducted at the same temperature.
The test is intended to serve the fol-
1.2 This recommended practice is restricted
lowing purposes:
to one specimen width which is generally
suitable for evaluation of high strength ma- I. In research and development of
terials (yield strength to density ratio above materials, to study the effects of the
700,000 psi/lb, in. -a. The test will dis- variables of composition, processing,
criminate differences in resistance to un- heat treatment, etc.
stable fracture when the sharp-notch 2. I n service evaluation, to compare

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HEYER ON EVALUATION OF PROPOSED RECOMMENDED PRACTICE 201

Edges must be equidistant,from longitudinal


centerline within 0.005
~ f.oo"dia, ref. o.ood'max, clearance
with loading pin

\
/
~~ e_F~.3
~/
p. 1 . O " d e t o
___ t
l

~r
/~..0 or 8.0" rI

~This dimension m 2.25" for the


3"X8"specimen.
Fro. 2--Fatigue Center-Cracked Specimen (CC).

.~'~ ~t" D/a~. - - ~ ~____Specimen/~l~ hole

'-~ __2@/__~"Required envelope


~
/ t / 1 0 f JL
"~---"A - -'M22
I
/.10" Limits of crock extension (20~

A = B within o.olo"
FIG. 3--Suggested Design for Center Fatigue-Crack Starter.

the relative crack-propagation resistance 3. For specifications of acceptance


of a number of materials which are and manufacturing quality control when
otherwise equally suitable for an applica- there is a sound basis for establishing
tion, or to eliminate materials when an a minimum acceptable sharp-notch
arbitrary minimum acceptable sharp- strength. Detailed discussion of the basis
notch strength can be established on for setting a minimum in a particular case
the basis of service-performance correla- is beyond the scope of this recommended
tion, or some other adequate basis. practice.

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202 FRACTURE TOUGHNESS TESTING

TEST SPECII~[ENS shown in Fig. 3. The machining may be


Two specimen designs are used. The done before heat treating, and the cyclic
machined, sharp-edge notch specimen stressing to extend the center cracks
(EN) is shown in Fig. 1, and the fatigue may be done after heat treating; how-
center-crack specimen (CC) in Fig. 2. ever, this order of operations is not
The preferred length is 12 in.; however, mandatory.
8-in. specimens are also provided so that Both specimens are pin-loaded. Clevis-
tests transverse to the rolling direction type loading devices and reinforcing
T A B L E 1 - - T R A N S V E R S E T E N S I L E P R O P E R T I E S OF M A T E R I A L S U S ED IN ASTM
T E S T P R O G R A M F O R E V A L U A T I O N OF P R O P O S E D R E C O M M E N D E D P R A C T I C E
FOR SHARP-NOTCH TENSION TESTING.

Material Thickness, in_ Lab. Tensile Yield Elongation


No. Strength, Strength, in 2 in.,
psl psl per cent

A - - A l u m i n u m alloy 7075-T651 . . . . . . 0.25 1 84 800 74 200 13.0


3 84 000 74 200 13.0
5 85 200 75 900 10,0

84 700 74 800 12.0

B - - T i t a n i u m alloy Ti-4A1-3Mo-IV.. 0.062 1 176 000 156 500 8,0


3 179 400 158 800 6.8
5 175 700 162 800 6,1

177 00O 159 400 7.0

C - - M a r a g i n g steel 18Ni-9Co-5Mo... 0,100 1 319 700 311 700 3.0


3 324 800 312 000 3,0
5 326 800 323 600 ~..0

323 800 315 800 2.3

D--Precipitation-hardening stainless
steel PH 14-8 Mo . . . . . . . . . . . . . . 0.090 I 242 300 215 400 8,0
3 236 800 217 000 5.5
5 247 500 233 300 4.7
7 236 400 212 200 6.5

240 800 219 500 6.2

may be made in laboratory-roiled sheet, plates which may be required to prevent


which is often limited in width. cracking at the pinholes are illustrated
It is important to meet the notch- in the proposed recommended practice.
radius specification of 0.0007 in. maxi- Methods for temperature control in tests
mum for the EN specimen. A method of at other than room temperature are also
machining these specimens has been given.
published by March et al.3
PROCEDURE
The CC specimen requires machining
of suitable crack-starter notches. Various The test is conducted in a similar
methods are permissible provided the manner to an ordinary tension test, at a
cuts are contained within the envelope loading speed such that the increase of
nominal stress in the notched or cracked
J. L. March et al, "Machining of Notched
Tension Test Specimens," A S T M Bulletin,
section does not exceed 100,000 psi per
No. 244, p. 52 (1960). minute. The maximum load is recorded.

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HEYER ON EVALUATION OF PROPOSED RECOMMENDED PRACTICE 203

TABLE 2 - - S H A R P - N O T C H S T R E N G T H .
(Values are given in ksi.)
Edge-Notched (EN) and Center-Cracked (CC) specimens taken transverse to the rolling direc-
tion. Specimen length is 12 in. except for indicated tests on 8-in. long specimens.

Lab 1 Lab 2 Lab 3 Lab 4 [ Lab 5 1 Lab 6 Tests on 8-in.


Ma~
Long Specimens
l I
terial
EN EN CC EN I CC CC
_2- CC EN EN

LAB 3
I CC

A .... 36.0 35.4 38.1 35.8 39.9


39.9 37.7 I 39.9 31.4
33.9 33.7 40.4 34.2 39.8
39.8 40.0 I 39.8 32.2
36.7 33.8 42.6 35.1 41.3
i1.3 41.9 40.3 31.6
32.7 34.3 37.5 36.7 4i1.6
16 __42"0 40.1 33.6
32.9 36.4 38.0 32.5 ]
i0.9 40.0 40.4 31.5
40.3
34.4 34.7 39.3 34.9 40.5 [ 40.1 32.1

LAB 6
B... 80.1 76.1 64.8 I 68.3 69.4 59.9 65.7 55.1 55.8
59.0 81.4 72.1 70.3 67.8 77.9 66.4 52.9 68.0
68.0 87.3 68.81 62.6 77.1 70.3 86.7 48.9 58.5
66.2 80.0 79.8 i 62.0 58.0 73.1 81.3 44.7 69.7
67.7 78.9 70.3 60.9 64.6 76.7 54.4 55.6 69.5
I 75.4 . . . .
68.2 80.7 71.2 71.6 70.9 51.4 64.3
68.7

C... 100.0 .02.9 89.1 92. I 90.7 86.6 85.6 78.4 106.1
97.5 88.0 91.5 90.3 98.5 84.4 88.0 84.2 105.2
96.2 L07.3 90.1 92.7 90.9 91.3 87.2 84.7 ~ 99.7
96.8 92.0 92.6, 93.2 98.6 88.7 89.0 83.0 100.5
86.7 .11.6 90.8 89.2 89.5 80.3 82.7 98.6
87.1 87.8 ----
95.4 .00.4 I 90.8 93.6 86.0 82.6 102.0
90.8

LAB 7
D... 154.1 55.0 64.9 .45.2 162.0 1144.7 169.7
158.6 54.5 64.5 .41.1 156.6 1157.3 171.0
154.2 [58.8 64.2 ,44.1 158.2 153.8 171.8
150.7 .58.6 61.5 .45.1 157.3 153.7 172.5
151.1 ~61.4 62.1 39.7 155.7
153.7 .57.7 I 63.4 43.0
" I

The net cross-sectional area of the E N the net sections are based on the area of
specimen is determined from the distance uncracked metal before testing, and do
between notch-root radii measured be- not take into account possible reduction
fore testing. In the case of the CC speci- in this area due to slow crack growth
men, the width of the net section is before fracture.
determined after fracture by subtracting The proposed recommended practice
the distance between the most advanced outlines a procedure for estimating and
points of the fatigue cracks from the reporting fracture appearance.
specimen width. I t should be noted that The tensile yield strength is de-

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204 FRACTURE TOUGHNESS TESTING

SN__ES MATERIALA
psi Aluminum alloy
50,000
CC

40,000 J

EN

30,000

20,000

Laboratory
1 2 3 4 5
FIG. 4--Comparison of Sharp-Notch Strength Tests of Material A.

SNS MATERIAL8
psi Titanium alloy
90,000 EN

CC
80,000

t
!
i
70,000
!_

60,000

50,000

Laboratory m

1 2 3 4 5 6
FIG. 5--Comparison of Sharp-Notch Strength Tests of Material B.
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HFYER ON EVALUATION OF PROPOSED RECOYrM~.NDED PRACTICE 205

SNS MATERIALC
psi Maraging stee!
EN
120,000 I

110,000

100,000

90,000
II

W
80,000

Laboratory
70,000 1 2 3 4 5
FIG. 6--Comparison of Sharp-Notch Strength Tests of Material C.

.SNS MATERIAL D
psi
Precipitation- hardeningstainless steel
170,000
CC

160,000

150,000
i
140,000

1 2 3 4 5 7
130,000
FIG. 7--Comoarison of Sharp-Notch Strength Tests of Material D.
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206 FRACTURE TOUOmCESS TESTING

termined using a standard tension-test The data for the 12-in. long specimens
specimen processed in the same manner are represented in Figs. 4-7 as mean
as the sharp-notch specimen. The ul- values -4-2 r limits. The mean sharp-
timate tensile strength, the yield strength, notch strengths and standard deviations
and the ratio of the sharp-notch of the four test materials are summarized
strength to the tensile yield strength are in Table 3. The ratios of sharp-notch
reported. strength to yield strength are also given
in the table. All of the materials were
EVALUATION TESTS
heat-treated to a relatively high strength
The test materials and their standard for the grade, and the sharp-notch
tensile properties are given in Table 1 strengths are well below the yield
and the sharp-notch strength data are strengths.
listed in Table 2. The aluminum and Data for each material were tested
titanium alloys were sent to the cooperat- for differences in precision and in mean
ing laboratories in the hardened condi- values among laboratories, and for
tion. The steels were supplied as solution- differences between the means of EN
annealed. The maraging steel was aged and CC specimens.

TABLE 3--MEAN SHARP-NOTCH STRENGTHS (SNS) A N D S T A N D A R D


D E V I A T I O N S (a).
(Values a r e g i v e n in ksi.)

EN CC
Material Pooled Ratio,
Me~.~l r Mean ~ r SNS/YS

A ............. 34.7 1.6 40.1 1.4 a 1.5 0.50


B ............. 71.2 8.1 70.5 6.1 7.2 0.44
C ............. 93.0 5.8 ~ 92.0 4.1 5.1 0.29
D ............ 151.5 2.9 158.2 3.0 3.0 0.70

T h e r e w e r e s i g n i f i c a n t differences in p r e c i s i o n a m o n g l a b o r a t o r i e s .

by the testing laboratory, while the Significant differences in precision,


precipitation-hardened steel was re- using the chi-square test, or in means,
turned to the supplier for heat treatment using the Student's t test, could not be
after machining. All tests were made in established at the 95 per cent confidence
the transverse-to-rolling direction. level except for the instances cited
Specimen preparation for sharp-notch below.
tension testing is inherently more difficult
than for conventional tension testing, Material A:
and the test results are more sensitive to The precision of the CC tests of
deviations from standard tolerances. Laboratory 5 is higher than for other
Three sets of test results, two edge-notch tests of this material, or for tests of
and one center-cracked, were rejected any of the materials. The mean values
because the specimens were out of toler- of EN tests are lower than those of CC
ance, either in machined dimensions or tests (see Table 3).
after fatigue cracking. This was the first
attempt by most of the participating Material B:
laboratories to produce these specimens, The precision of the EN tests of
and the number of successful tests Laboratory 6 is lower than for other
indicates that the procedure can be tests of this material. The mean value
carried out and useful results obtained. of the EN tests of Laboratory 2 is
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HEYER ON EVALUATION OF PROPOSED RECOMMENDED PRACTICE 207

higher than the grand mean (80,700 the differences are small and are signifi-
compared to 71,300). cant only at reduced confidence levels,
as low as 80 per cent.
Material C: These differences are believed to be
There are differences in precision related to stress-distribution patterns as
among laboratories making E N tests influenced by pin loading. In the case of
(also for CC tests at the 90 per cent the E N specimens, relatively higher
confidence level). The mean values of stresses would be expected in the vi-
EN tests of Laboratories 2 and 6 are cinity of the notches of the shorter
different from the grand mean (100,400 specimens, resulting in lower sharp-notch,
and 86,000 compared to 93,000). strength. In the case of the CC speci-
mens, relatively lower stresses would be
Material D: expected in the central region of the
The mean value of the CC tests of shorter specimens, resulting in higher
Laboratory 2 is higher than the grand sharp-notch strength. An exception to
mean (163,400 compared to 158,200). this pattern is the data for CC tests of
TABLE 4--SHARP-NOTCH STRENGTH TESTS OF 12-IN. AND 8-IN. SPECIMENS.
(Values are given in ksi.)

Material Specimen 12-in. Length 8-in. Length Difference Confidence


Type Mean ~ Mean r Levelsb

B ......... CC 71.1 -4-3.8 64.3 -4-2.1 -6.8 98


C ......... CC 95.0 "4-5.9 102.0 -4-3.4 +7.0 91~
D ........ CC 157.6 -4-1.7 171.3 -4-1,2 +13.7 99,

A ......... EN 34.9 -4-3.4 a 32.1 =t=0.9 a -2.8 80


B ......... EN 70.9 +13.0 ~ 51.4 -4-4,6 a -19.5 95
C ......... EN 86.0 :t=3.4 82.6 -4-2.5 -3.4 80

Significant difference in v a r i a n c e .
b T h e differences b e t w e e n 12-in. a n d 8-in. t e s t s are significant a t t h e i n d i c a t e d confidence levels.

The mean values of the E N tests of Material B. It is interesting to note that


Laboratories 2 and 3 are different from the variance for the 8-in. tests is smaller
the grand mean (157,700 and 143,000 than for the 12-in. tests in every case.
compared to 151,500). However, only in two instances were
The mean values of the E N tests are these differences in variance shown to be
lower than for the CC tests (see Table 3). significant at the 95 per cent confidence
level.
All Materials:
SUMMARY
There were no significant differences
in precision between E N and CC tests; The general agreement among labora-
however, the CC test results are higher tories in determining the sharp-notch
than the E N for Materials A and D. strength of four typical high-strength
More deviation in test values was materials is quite satisfactory. It was
observed in tests of Materials B and C not expected that the precision or the
than for tests of Materials A and D (see accuracy of the test would be equal to
Table 3). that of conventional smooth-bar tension
Tests on the proposed alternate 8-in. tests, and the results obtained in this
long specimen and the 12-in. specimen first trial of a new test specimen are
are compared in Table 4. In some cases gratifying.
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208 FRACTURE TOUGHNESS TESTINO

On the other hand, not all laboratories should be used only as an expedient when
were able to prepare the specimens within insufficient test material is available for
the proposed tolerances. While no action the 12-in. specimen.
has been taken by the committee, the
task group will recommend that the Acknowledgment:
proposed specimens and procedures be The evaluation tests were made in
used as a recommended practice without the laboratories of the following compa-
substantial modification until more ex- nies: Allegheny Ludlum Steel Corp.,
perience is gained. Aluminum Company of America, Armco
A statement should be added to the Steel Corp., The Boeing Co., Douglas
recommended practice noting that dif- Aircraft Co., Titanium Metals Corp.,
ferences may be expected between results Thompson Ramo Wooldridge Inc., and
of EN and CC tests. It is stated in the at Lewis Research Laboratories of
draft copy that the 8-in. long specimen NASA.

DISCUSSION
J. G. K~ur~N.1--At the Alcoa Re- possible, the thickness should be con-
search Laboratories, we use edge-notched sidered a variable in the tests.
tension specimens of the design in Fig. 8 R. H. I~Y'~R (author).--The Alcoa
for sharp-notch tension tests of alumi- sharp-notch tension specimen, Fig. 8, is
num alloy sheet and I-in. thick plate. I ~ _ i 7"
This design meets all of the require-
ments of the ASTM specimen (Fig. 1,
EN), but has wider grip ends so that it
may be loaded through a single pin at
each end, without the need for the stiff- _ d
ener plates and without fear of fracture
at the loading holes. Data obtained with 0
the two designs of specimen are given in d
Table 5. There is no significant difference
in values of notch tensile strength. ~S
We wish to emphasize the point made
by Mr. Heyer that the results of sharp- (~.
notch tension tests are extremely de-
pendent upon the thickness of the ma-
"1-
terial. For example, data in Fig. 9 for I-- -

7075-T6, -T651 and 7079-T6, -T651, Z


show the magnitude of the effects over
the thickness range from 0.063 to 0.250
in. Therefore, for valid comparisons of
different compositions or tempers of sheet
or thin plate, the thickness should be
maintained constant, or when this is not [ .oo:1 .oo'L
4.00" ,,-

l Assistant chief, Mechanical Testing Div.,


AlcoaResearchLabs,, NewKensington,Pa. FIo. 8--Sharp-NotchTension Specimen.

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DISCUSSION OF EVALUATION OF PROPOSED RECOMMENDED PRACTICE 209

TABLE 5--SHARP-NOTCH TENSILE distribution at the notch. On the other


STRENGTH, psi.
hand, tests by Laboratory 3 on aluminum
ARL Design, Fig. 8 ASTMDesign, Fig. 1, EN alloy 7075-T651 using the short speci-
36 200 35 S00
men (8-in. length) were 8 per cent lower
34 600 34 200 than for the regular (12-in. length)
34 300 35 100 specimen, as shown in Table 2. The short
32 400 36 700
34 200 32 500 specimen will not be designated as a
standard specimen in the recommended
34 300 34 900
practice.

60

o 50
0 7 o . s - T 6 . -T65,
0

~ 40
Z
W
\
~ 50
W
_-I 3#
60 ~ V,

~,
W
2o NOTCH -TIP
RADIUS
k .

I.-- O.O005-1N,

F-
0
Z

0
0 0.I 0.2 0.5
THICKNESS, IN.

FIo. 9--Effect of Thickness on Notch Tensile Strength of 7075-T6, -T651, and 7079-T6, -T651
Sheet and Plate.

longer over-all and between loading The effect of specimen thickness on


holes than the regular 12-in. long speci- sharp-notch strength was not included
men used in the committee's evaluation as a variable in the evaluation program.
program. Since no difference in test We appreciate Mr. Kaufman's data,
results was obtained using the two speci- Fig. 9, which call attention to this
men designs, the 12-in. specimen appears important variable in sharp-notch ten-
to be sufficiently long to give good stress sion testing.

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E L E C T R O N F R A C T O G R A P H Y - - A TOOL FOR T H E STUDY OF
M I C R O M E C H A N I S M S OF F R A C T U R I N G PROCESSES

BY C. D. BEACttEM1 AND R. M. N. PELLOUX2

SYNOPSIS
Uses of the electron microscope for the study of fracture surfaces and the
subsequent formulation of models of fine-scale fracture mechanisms are
demonstrated. Electron fractography is shown to be a valuable tool in ob-
taining a better understanding of fracture and in the analysis of service
failures.
Various types of fracture surfaces produced by single-cycle overload and
by fatigue in various materials are discussed in order to indicate the useful-
ness of this relatively new tool.
The scope of application in the general field of fracture research is indicated.

Visual and low-magnification observa- volumes of material associated with each


tions of fracture surfaces have for a long increment of fracture which determine
time aided engineers in their fracture the resistance to fracture. The strength
analyses. The "rock-candy" appearances of interfacial bonds between constituent
of burnt steel, the concentric growth particles and between grains, the cleav-
rings of fatigue, and the chevron mark- age strength of intermetallics, the
ings of brittle fractures are examples of residual stresses around constituent
the use of low-power optical microscopy particles, and the location, shape, size,
in the study of fracture surfaces. A density, and properties of constituent
powerful means of investigation has particles and grains are a few of the
recently been added with the advent of factors that determine what will occur
the use of the electron microscope. at the tip of a crack. To understand
The electron microscope has shown fracture, one must be able to measure
conclusively that the large majority of and predict all the forces and properties
materials, including engineering ma- in the entire system, whether they be
terials, fracture by the nucleation and such large-scale factors as the stiffness
growth of minute submerged free surfaces of the testing equipment, intermediate
(cracks or voids) to form incremental scale factors such as stress concentration
advances of fracture. It is frequently the at the root of a notch, or fine-scale fac-
properties of, and conditions at, the tiny tors such as the forces necessary to move
dislocations.
1Head, Micromechanical Metallurgy Sec- Research work with simple materials
tion, Physical Metallurgy Branch, Metallurgy
Div., U.S. Naval Research Laboratory, Wash- such as ionic crystals and metallic
ington, D. C. single crystals has resulted in some
2Head, Materials and Proeesses Unit, understanding of the basic mechanisms
Turbine Div., The Boeing Company, Seattle,
Wash. of fracture. On ~*~'~+her scale, numerous

Copyright9 1965 by ASTM International www.astm.org


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BEACHEM AND PELLOLrX ON ELECTRON FRACTOGRAPHY 211

mechanical tests of engineering materials provides a much more general and com-
have been done by engineers in order to plete view of the features of the fracture
evaluate and select materials for the surface. For instance, if one wishes to
design of useful structures. Thus research determine the relative proportions of
is progressing at both ends of the pres- intergranular and transgranular frac-
ently known spectrum--from bonding ture, it would be far easier to observe
strength between two atoms to plane- the fracture at an angle normal to the
strain fracture toughness. Though prog- macroscopic plane of the fracture than
ress is being made in both the metal it would be to make a large number of
physics and the continuum mechanics fracture-profile studies. The difference
approaches, researchers in the two in amount of time and work necessary
fields have not been able fully to benefit to find out the shape, size, and distribu-
from each other's results. This is partly tion of intergranular constituents on an
due to the microstructural complexities intergranular fracture is even more
of the structural materials investigated striking.
in fracture mechanics and partly because The electron microscope---with a large
there is a large difference in scale (size) depth of field, a high resolving power,
between some of the factors investigated and a large range of magnification--is
in the two approaches. an ideal tool for use in the study of
Observations and studies of fracture fracture surfaces. Fractures should be
surfaces at high magnification with the studied on all scales, and electron frac-
electron microscope (often called electron tography does not replace optical micros-
fractography) include studies of the copy or observations with the unaided
relationships between the surface topog- eye. An electron fractograph by itself,
raphy and the microstructure, as well as for instance, cannot always indicate
studies of the chronological order of fine- whether the macroscopic fracture was
scale events taking place during frac- brittle or ductile. Electron fractography,
ture. The use of this new technique shows then, should be considered as a comple-
promise of helping bridge the gap be- mentary tool for fracture studies and
tween the metal physics and continuum failure analyses.
mechanics approaches by providing Two types of electron microscopes ar~
qualitative assessments of micron-scale presently being used to study fracture
fracture processes and quantitative surfaces. The scanning microscope per-
measurements of some of the fracture mits, with limited resolution, the direct
variables that are not measured in study of the fracture surface itself. This
either of the above approaches. has the advantage that one can observe
changes on the fracture surface as they
USES OF ELECTRON FRACTOGRAPHY
occur. For instance, Jacoby3 has de-
Fracture surfaces are usually studied scribed the ionic etching of fatigue frac-
by using the following procedures: (1) tures in the scanning microscope while
observing cross sections of the fracture the surface was being observed. The
to relate the fracture surface to the conventional electron microscope has a
structure of the underlying metal; and higher resolving power than the scanning
(2) observing the fracture surface along microscope, but has the disadvantage
a direction normal to the macroscopic that the fracture itself is not directly
plane of fracture. Though both methods
3 Private communication from Gerhard
are necessary for the study of some Jacoby, Institut far Festigkeit, Mtilheim/Ruhr.
aspects of fracture, the second method Germany.

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212 FRACTURE TOVGI~NESS TESTING

observed. Very thin replicas of the frac- the fracture surface. This shadowing
ture surface must be prepared and trans- brings out the relative heights and depths
terred into the microscope for study. of the features of the fracture surfaces.
Though there are some inherent dis- When a detailed study of the three
advantages to such an indirect method dimensions of the fracture features is
of study, replica techniques offer so needed, stereo pairs of photomicrographs

FIG. 1--Cleavage Fracture in an Alnico Alloy. A Typical Cleavage Step Is Indicated by the
Horizontal Arrow.
The circle shows where two steps converge to form part of a river pattern. The river markings
along ABC, probably originating at a twist-boundary, are clearly due to cleavage along a secondary
cleavage plane. Local propagation direction is shown by the upper arrow. Two-step replica. (Re-
printed from Ref (~).) 6000• Reduced one-third in reproduction.

many advantages that they are used can be taken. After enlargement, the
almost exclusively in electron fractog- stereo pairs are studied at leisure with a
raphy. stereo viewer.
One of the main advantages of the During the preparation of the replicas,
replica technique results from shadow- the direction of shadowing can be selected
ing. In order to have a better contrast, in such a way as to coincide with the
the replicas used in electron microscopy macroscopic direction of crack propaga-
are shadowed with a heavy metal evap- tion. In this manner, the orientation of
orated under a low angle with respect to each micrograph with respect to the

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 213

FIo. 2--Cleavage Fracture Surface of a Low-Carbon Steel Broken by Impact at 78 K.


A B C is a grain boundary; B D is a typical river marking. The long arrows indicate local crack-
propagation directions and the circled arrow indicates a cleavage step. The facet F is due to cleavage
along a deformation twin. Direet carbon replica. (Reprinted from Ref (2).) 5500X. Reduced one
third in reproduction.

general direction of crack propagation responsible for the local initiation and
will always be known. propagation of the fracture.
Finally, in many cases the replicas When fracture surfaces are observed
can be prepared in such a way as to at increasingly higher magnifications,
extract in situ some of the second-phase the extremely complex nature of the
particles present on the fracture surface. fracture features becomes more and more
With these extraction replicas it is apparent. Electron fractographs show
possible to analyze by electron diffraction clearly that structural materials generally
the nature of the second-phase particles cannot be considered as homogeneous

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214 FRACTURE TOVGHNESS TESTING

FIG. 3---Typical Cleavage Fracture Through Many Grains of an Alnico Alloy.


The grain boundaries E F and G H are clearly at the origin of the formation of cleavage steps. In
grains A and B, fracture was intercrystalline. Two-step replica. (Reprinted from Ref (2).) 5600X
Reduced one third in reproduction.

continual and that no simple disloca- work done by electron fractography has
tion models can b y themselves entirely been to study and classify the fine-scale
explain the fracture processes. However, features present on the fracture surfaces
in spite of the complex appearance of a of known materials broken under con-
fracture surface, it is possible to see, at trolled conditions. I t is not possible, in
high magnification, that a given mecha- general, to account for the formation of
nism of fracture is associated with a these features in terms of the simple
certain number of characteristic fracture models of fracture. However, the topog-
features (I).4 So far, the major part of the raphy of the fracture surface and the
4 The boldface numbers in parentheses refer fine-scale features can frequently be
to the list of references appended to this paper. related to the microstructure of the

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 215

FIG. 4---Overload Fracture in a 7075-T6 Aluminum Alloy, Showing Cleaved Intermetallic Be-
tween Horizontal Arrows, Dimples Between Oblique Arrows and Intergranular Fracture Through
Intermetallic Particles (vertical arrows). Direct Carbon Replica. 15,000X. Reduced One Third in
Reproduction.

material. Since the fracture path is the FRACTURE ~IECHANISMS STUDIED BY


path of least resistance, a close stud)" of ELECTRON FRACTOGRAPHY
the fracture surface should reveal some As observations are made at varying
of the structural weaknesses of the magnifications, specific features become
materials. This type of systematic study either less or more prominent. Just as an
of the local origin of fracture shows the astronaut in orbit may see a whole
importance of electron fractography in mountain range while a prospector on
the analysis of service failures. It is foot may see the types of minerals con-
presently one of the major applications tained in individual rocks, unaided visual
of this new tool. An example will be observations of fracture surfaces reveal
given later. .~ome features not seen in the electron

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216 FRACTURE TOUGHNESS TESTING

microscope. Of course the same is true in terminology. The terms "silky,"


reverse, since many of the features dis- "woody," "fibrous," "rock-candy, .... in-
covered in the electron microscope can- tergranular," "transgranular," "ductile,"
not be resolved at lower magnifications. and "brittle" are still useful in describing
Various materials and various fracture fractures, but they are wholly insufficient

Fro. 5--Quasi-Cleavage and Dimpled Rupture in AISI Type 410 Stainless Steel, Quenched,
Tempered, and Broken at Room Temperature.
Examples of quasi-cleavage facets are shown between the small arrows, and groups c,f dimples
are indicated by large arrows. Palladium-shadowed direct carbon replica. (Reprinted from Ref (6).)
9200• Reduced one third in reproduction.

conditions result in a large variety of to rep,~rt and explain the fine-scale


different fracture-surface features. These features of fracture surfaces. The ter-
features, viewed at higher and higher minology used to describe the character-
magnifications, could be differentiated istic fine-scale features of fracture
again and again and classified into surfaces has been selected after a careful
groups, subgroups, etc. This would lead consideration of what is presently known
to a complex but necessary svstem of about the mechanisms of fracture.

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 217

FIo. 6--Fine-Scale Markings on a Quasi-Cleavage Facet in Quenched and Tempered Type 410
Stainless Steel Broken at Room Temperature.
The fracture-initiation region for this facet is seen just to the lower right of the center of the
facet. The large arrows point out the boundaries of the facet while the small arrows indicate river
patterns which lead away from the center of the facet. Pa]ladium-shadow~t two-stage carbon replica.
(Reprinted from Ref (6).) 9200• Reduced one third in reproduction.

T h e fracture m e c h a n i s m s selected for CLEAVAGE


discussion in this p a p e r are classified as Cleavage is defined as the s e p a r a t i o n of
follows: (1) cleavage; (2) micro-void a crystal along certain crystallographic
coalescence; (3) quasi-cleavage; (4) planes. A typical example of a perfect
i n t e r g r a n u l a r separation; a n d (5) fatigue. cleavage fracture is the fracture of
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218 FRACTURE TOUGHNESS TESTING

crystals of mica which split along their crystal is never perfect and so the cleav-
weakly-bonded basal planes. 5 Many age crack does not follow a single plane
other crystalline substances including through the entire crystal. Its actual
metals with body-centered cubic or path is usually broken up along parallel
hexagonal structures fracture by separa- sets of cleavage planes. The steps be-
tion along planes of high atomic density. tween the parallel planes (horizontal
Cleavage fracture of metal crystals is arrows in Figs. 1 and 2) have been shown
always preceded and accompanied by to form by cleavage along a secondary

I:1(;. 7--Quasi-Cleavage in H-11 Steel Broken at Liquid-Nitrogen Temperature. Under Such


Conditions Many Steels l:racture with a Tendency to Shatter, Producing Secondary Cracks Seen
Here as Dark Bands (Arrows). (Reprinted from Ref (6).) 12,000X. Reduced One Third in Repro-
duction.

some plastic deformation. This means set of planes or by plastic shearing


that it is not a simple process of separa- (3,4). These steps converge as the fracture
tion along atomic planes and some of the propagates, and the resulting fracture
fracture features will be related to this surface exhibits "river patterns" which
small amount of plastic deformation. are typical of most cleavage fracture.
Examples of cleavage fracture surfaces When the steps between cleavage planes
are shown in Figs. 1-4, One might expect converge they nsually combine to form a
the two fracture surfaces created by larger cleavage step (as shown in the
cleavage to be perfect planes, but a single circled area on Fig. 1). Screw dislocations,
~Portions ~f the text and certain fracto-
either present in the crystal or created by
graphs in this paper are taken from l/el (2). plastic deformation at the tip of the

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FIG. 8--Matching Quasi-Cleavage Facets from the Two Halves of a Hardened and Tempered
AISI 410 Stainless-Steel Wire Broken in Tension at 50 F.
Stereo viewing showed three features of quasi-cleavage which are indicated between numbers.
Between numbers 1-1 and between numbers 2-2 are steps, similar to those in true cleavage, seen as
dark lines. The numbers 3-3 and 4-4 indicate examples of tear ridges and the 5's show where three
tear ridges eonverge. "Tongues," similar to those found in true cleavage, are seen in the regions
bounded by 6's. Between the numbers 7-7 is an example of a step merging with a tear ridge. Cellulose
acetate replica technique. (Reprinted from Ref (6).) 14,500• Reduced one third in reproduetion.
219

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220 FgACTU~ TOUGHNESS TESTING

advancing crack, are considered to be the cleavage fracture of metals and


responsible for the formation of cleavage alloys, other fine-scale features of the
steps on the fracture surface. The best microstructure such as precipitates and
illustration of this explanation is the nonmetallic inclusions, may also play an
sudden increase in the number of cleav- important role and can lead to rather
age steps that occur when the crack complex mixtures of fracture modes.
crosses a region of high screw dislocation Thus, in quenched and tempered steels

FI6. 9--Simplified Sketches of Three Distinctly Recognizable Features of Quasi-Cleavage.


M a t i n g fracture surfaces show steps and tongues which m a t e as in true cleavage, and tear ridges
which protrude from both surfaces and therefore do not resemble true cleavage. Tear ridges are
similar to the chisel edges t h a t result from stretching apart very ductile tension specimens. (Reprinted
from (Ref (6).)

density such as at a twist boundary (line containing fine dispersions of carbide


A B C in Fig. 1) or at a grain boundary. particles, several fracture modes may be
Other features of cleavage are seen in distinguished.
the fan-like cleavage of, for example, the In many of these steels, fracture
intermetallics in 7075-T6 aluminum surfaces created at temperatures con-
alloy (Fig. 4) and the feather-like ap- siderably above the ductile-to-brittle
pearance of cleavage fracture in a tung- transition temperature range are made
sten single crystal (s). up of dimples, while those created at
temperatures considerably below the
QUAsi-CLEAVAGE transition range are mainly composed of
In addition to the influence of grain flat facets and other features that some-
boundaries and subgrain boundaries on times strongly, and sometimes weakly,

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BEACHENI AND PELLOUX ON ELECTRON FRACTOGRAPHY 221

resemble cleavage. At temperaturse


within, and near, the transition tempera-
ture range, various percentages of both
dimples and flat facets are found. No
abrupt change in fracture mode has been
found.
I t has been observed that the flat
facets that resemble cleavage are far
larger than the discrete, fine-scale fea-
tures of the tempered martensite, and
that the orientation of the facets cannot
definitely be related to cleavage planes
in the ferrite matrix. Therefore, Srawley ~
suggested that the term "quasi-cleav-
age" be used to distinguish these facets
from true crystalline cleavage planes.
Since it is necessary to discuss the fine-
scale features of low-energy fracture in
quenched and tempered steels, ter-
minology must be coined which describes
adequately the newly observed features.
Quasi-cleavage is admittedly unprecise,
but most accurately describes this type
of fracture.
I n quenched and tempered mar-
tensites, quasi-cleavage is defined as a
fracture mode which produces individual
planar, or nearly planar, fracture facets
which are transgranular with respect to
the prior austenite grains. Examples are
shown in Figs. 5-8, 7 and sketches of some
of the features are shown in Figs. 9 and
10. Figure 5 shows a number of quasi-
cleavage facets while Fig. 6 delineates
the boundaries of a single facet. Figure
5 shows dimples which are often observed
between facets.
Figure 6 shows river patterns which
indicate that the fracture origin for this
facet was within the facet rather than FIG. 10---Sketch of a Frequently Observed
at the edge where fracture would orig- Feature of Quasi-Cleavage.
Three submerged cracks, lying in approxi-
inate in true cleavage. This figure pro- mately the same plane, grow together from top to
vides clear indications that quasi-cleav- bottom in the sketch. Plastic deformation at their
age fractures propagate in a step-wise tips, as they approach one another, causes the
formation of tear ridges on both fracture surfaces.
Though three submerged eraeks are sketched--
e Private communication from J. E. Srawley. with three resultant tear ridges intersecting one
~This subject is discussed more fully in another--other configurations of joined ridges
Ref (6). Some of the illustrations here are re- develop from other combinations of submerged
printed from that reference, cracks. (Reprinted from Ref (6).)

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222 FRACTURE TOVOmeESS TESTING

FIG. ll--Typical Shear-Rupture Dimples on Surface of Shear Lip in a Steel Specimen. 3000X.
Reduced One Third in Reproduction.

FIG. 12--Equiaxed Dimples in 7075-T6 Fracture. Direct Carbon Replica. 30,000X. Reduced
One Third in Reproduction.

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BEACHEM AND PELLOUX ON ELECTRON FRACTOORAPHY 223

manner by the linking up of submerged up of the micro-cracks. The proportion of


cracks with one another or with the these two modes of fracture observed in
major fracture front. Figure 7 shows a quenched and tempered steels depends
high proportion of secondary cracks, upon the composition (for example,
often found in the more brittle fractures. carbon content), heat treatment, and the
Precisely matched fracture surfaces are test conditions (for example, tempera-
shown in Fig. 8. Stereoscopic viewing of ture).

FIo. 13--Tear Dimples Formed During the Early Stages of Internal Fracture of a Necked 4340
Steel Smooth-Bar Tension Specimen. Two-Step Replica. 12,000X. Reduced One Third in Reproduc-
tion.

many such matching surfaces shows three COALESCENCE OF MICRO-VOIDS


distinct features which are indicated
Fracture surfaces of many metals and
with numbers in Fig. 8. These features
are as follows: steps, ridges, and tongues. alloys exhibit evidence of severe localized
They are sketched in Fig. 9. The forma- plastic deformation. Tear ridges in
tion of tear ridges is believed to occur quasi-cleavage fracture already have
by the mechanism shown in Fig. 10. been mentioned. However, in most
In quenched and tempered steels, ductile or tougher materials, another
quasi-cleavage exhibits some of the fracture mode involving the formation
features of crystalline cleavage in the and coalescence of internal micro-voids
initiation of the facets and some of the is of major importance (7-11). The initia-
features of plastic rupture in the linking- tion of the micro-voids is dependent upon

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224 F~CTUP.E T o v o m ~ s s TESTING

Fro. 14--Tearing at the Root of a Fatigue Crack in a Ti-2.5AI-16V Specimen,


The fatigue crack was intentionally introduced as a stress raiser for the later crack-propagation
test. The tear dimples (arrows) were formed in the early stages of crack growth during the test.
T h e fracture progressed from right to left. Palladium-shadowed direct carbon replica. (Reprinted
from Ref (6).) 6000X, Reduced one third in reproduction.

the existence of some heterogeneities or and plastic properties between the


defects originally present in the material matrix and second-phase particles, micro-
or created during plastic deformation. cracks or free surfaces are created at the
For example, during plastic deformation interface between the particles and the
and as a result of differences in elastic matrix.

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FIo. 1S--Dimpled Rupture Surface in a 7078 Aluminum Alloy. Two-Step Replica. FIG. lfv--Dimples on a Fracture Surface in a
(Reprinted from Ref (2).) 6600)<. Reduced One Third in Reproduction. 2219 Aluminum Alloy. Note the Range of Sizes
of the Dimples. Two-Step Replica. (Reprinted b,9
form Ref (2).) 0000X. Reduced One Third in t,O
r
Reproduction.

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226 FI~ACTUgE TOUGHNESS TESTING

The highly complex mechanics of hemispherical or equi-axed and were


plastic flow during the growth of these called "cupules" by J. Plateau et al; and
internal free surfaces is not fully under- 2) those that have parabolic shape and-
stood. It is known that the free surfaces (were called "dimples." The term "dim
tend to develop into rounded holes as ples" has come to be used in reference to
they grow. Each one of the holes, or all such half-voids on fracture surfaces.
voids, is a fracture surface in itself, Examples of equi-axed dimples are shown
initially completely isolated from the in Figs. 12, 16, and 17, and they are
other voids. During increasing plastic sketched in Fig. 18(a). The parabolic

FIO. 17--Example of Dimples in a Maraging Steel. Two-Step Replica. (Reprinted from Ret
(2).) 6400X. ReducedOne Third in Reproduction.

low these voids continue to grow. If a dimples can form in two different man-
void is near another free surface it may ners: (1) by shear rupture (Fig. 18(b));
grow until the material between the two and (2) by tearing (Fig. 18(c)). Examples
free surfaces thins down and separates of shear-rupture dimples are shown in
by rupturing; this is termed coalescence. Figs. 11 and 15, and tear dimples are
the fracture surfaces created by the shown in Figs. 13 and 14. Parabolic
coalescence of voids is made up of dimples resulting from a shear fracture
rounded concave depressions as shown in are practically always present on all of
Figs. 11-17. the shear surfaces that one sees with the
The half-voids are easily divided into unaided eye, such as on shear llps and the
two distinctly different groups according sides of cup-and-cone fractures. Tearing
to their shape: (1) those that are roughly frequently occurs at the tip of sharp

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 227

cracks that are opening up under tension. the initial internal free surface; and (2)
Unfortunately no characteristic features the amount of plastic growth permitted
have yet been recognized that enable one before the void coalesces with another
to distinguish between tear dimples and free surface. The first factor is deter-
shear-rupture dimples. However, it is mined primarily by the size of the

o.!

~,,o"2
I o:o
(o)

o" l
X,,j3
(b)
lccc [

(c)

FIG. 18--Three Observed Basic Modes for the Coalescence of Voids.


For each mode the sketches show, from left to right: (1) material stressed almost to the point
of local rupture; (2) local rupture; and (3) the directional sense of dimples on the rupture surfaces.
(a) Normal rupture; coalescence under the influence of uniform plastic strain in the direction of the
applied stress. (b) Shear rupture; coalescence under the combined influences of plastic strain in the
direction of the applied stress and shear strain on a plane of maximum shear stress. (c) Tearing;
coalescence under the influence of nommiform strain in the direction of the applied stress. Plastic
strain is greatest on the left side of the element. (Reprinted from Ref (6).)

evident that tear dimples, once they are inclusions, precipitate particles, etc.
identified, can be used to determine the The second factor is mainly dependent
local direction of crack propagation, just upon the distance between neighboring
as in the case of the river patterns in voids which in turn is frequently deter-
cleavage. mined b y the density of precipitate
The size of dimples is determined particles. However, there is not neces-
primarily by two factors: (1) the size of sarily formation of a micro-void at each

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228 FRACTURE ToIJGm,mSS TESTING

precipitate lying along or near the frac- metal attack, quenching stresses, and
ture surface. In general, the density of stress corrosion in the presence of gases
precipitate per unit of fracture surface and liquids sometimes has been observed
is much larger than the number of to propagate along grain boundaries in a
dimples observed on the same surface. large number of metals and alloys.
The work-hardening behavior of the Lattice irregularities at and near
surrounding matrix probably plays an grain boundaries will in general have a
important role in controlling the amount tendency to make these boundaries
of plastic growth which can take place inherently weaker than the grain in-
teriors. In addition, grain boundaries
0.4
are often favorable sites for the segrega-
DEPTH MEASUREMENTS ON 5 % Cr DIE STEEL
-o- AVG, D~-PTH OF RUPTURE OIMPLES
tion of various impurity or alloying
--x-- AV6, HEIGHT OF RIDGES BETWEEN
QUASI-CLEAVAGE FACETS
elements to form either composition
gradient zones or precipitate particles
(or continuous films) of secondary phases.
0.5 - - The presence of these segregated zones
or the second phases cause the mechani-
cal, physical, and chemical properties of
the grain-boundary regions to be dif-
ferent from those of the grain interiors.
g If the constituent particles are nu-
:~0.2 -- Ix
merous enough or large enough and
possess properties that are sufficiently
different from the grain interiors, frac-
u/
/ ture may nucleate or propagate along
/x the grain boundaries to produce inter-
0,l -- /
/
/
granular fractures.
Some alloys that contain extensive
brittle grain-boundary constituents may
fail entirely along the grain boundaries.
However, a lower amount of grain-
o P - ,lI 0 0 01
-200
I i I I l [
I00 2 0 0 SOO 4 0 0 5 0 0 6 0 0 7 0 0 boundary constituents may result in
TEST TEMPERATURE (=F'I
failures which are partly intergranular
FIG. 19--Plot of Average Depth of Dimples and partly transgranular.
and Height of Tear Ridges Between Quasi-Cleav-
age Facets as a Function of Temperature in H-11 Depending upon how much the ad-
9 . o
Steel. (Reprintedfrom Ref (12).) joining grains deform during inter-
granular fracture, the exposed grain
before coalescence of the micro-voids. facets may vary from quite flat to some-
In this connection it has been found that what convex or concave in over-all shape9
the depths and sizes of dimples increase The electron microscope has permitted
with the testing temperature in several
detailed studies of intergranular fracture
materials. For example, Fig. 19 shows the
surfaces and a number of interesting
variation of dimple depth versus tem-
features have been found9 Depending
perature for H-11 steel (12).
upon the shape, size, distribution, and
INTERGRANULAR SEPARATION properties of the weak phases which
Fracture due to static overload, initiate local internal free surfaces along
fatigue, hydrogen embrittlement, liquid- a single grain boundary, and depending

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BEACIIEM AND PELLODX ON ELECTRON FRACTOGRAPHY 229

FIO. 20--Intergranular Fracture, due to Micro-void Coalescence, in a 2219 Alloy.


The difference in orientation of the grain-boundary facets is well marked and the shear direction
is given by the direction of elongation of the dimples. Two-step replica. (Reprinted from Ref (2).)
5500 X. Reduced one third in reproduction.

upon the test conditions, the two sep- 25 shows a feature which is often ob-
arated grain facets may exhibit no served in quenched and tempered steels.
markings (fiat and featureless as in Fig. These markings (arrows) have been
4), dimples (Figs. 20 and 21), cleavage observed on static overload, stress corro-
steps (Fig. 22), fatigue markings (Fig. sion, and hydrogen-embrittlement frac-
23), various corrosion pits and products, ture surfaces, and are thought to be
or other markings. At times only a few formed (13) by the thinning down and
markings are seen, as in Fig. 24. Figure rupture of material between neighboring

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230 FRAC~rURE TOUGHNESSTESTING.

internal grain boundary cracks (as optical microscopy shows dull and bright
sketched for quasi-cleavage in Fig. 10). regions. The dull zones are depressions
The recognition of all the different usually with a large intermetallic par-
kinds of fine-scale markings on grain ticle visible at the bottom of the depres-
boundary facets is by no means complete. sion. The bright zones show a series of

FIG. 21--Dimples Along Grain-Boundary Facets in a Weld-Heat-AffectedZone in a Steel.


2400X ReducedOne Third in Reproduction.

In addition, with the present limitations regular striations as illustrated by Fig.


of replication techniques and replica 26. The examination of the same surface
fidelity it is probable that a large number by electron microscopy shows that the
of significant markings will remain un- depressions are made up of dimples
detected. characteristic of a rapid, plastic fracture.
The striations of the bright zones are
FATIGUE clearly resolved (Fig. 27) and in the case
The examination of the fatigue frac- of a fatigue test under a constant stress
ture surface of an aluminum alloy by level, the spacing of the striations is

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BEACHEM AND PELLOUX ON [ELECTRON FRACTOGRAPHY 231

locally very uniform. The examination alloys. Two general types of striations
of program-loaded fatigue fractures has have been recognized, the brittle and the
demonstrated that each of the character- ductile types. Figure 28, taken in part
istic fatigue striations first observed by from Forsythe, illustrates the differences
Zapffe and Worden (14) is produced by a between the two types of striations. The

Fio. 22--Cleavage Fracture and Separation Along the Interface of a Large Particle in an Alnico
Alloy.
The smooth and hexagonal steps are growth markings present on the particle before agglomera-
tion. Two-step replica. 6600• Reduced one third in reproduction.

single cycle of stress (15), thus the stria- brittle striations are connected with what
tions (also called crack-front arrest lines) seems to be a cleavage fracture along
represent the successive positions of a sharply defined facets. Numerous river
transgranular front at each load cycle. line markings separating these facets run
Forsythe (16) has recently given an normal to the striations as shown on Fig.
excellent survey of the mechanisms of 29.
fatigue-crack propagation in aluminum The profile of a brittle striation is

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232 FRACTURE TOUGHNESS TESTING

shown in Fig. 28(d). As far as it is known, striations. Smith and Laird (19) and
brittle striations have been observed McEvily (20) have shown that in the case
only in high-strength aluminum alloys, of high-stress fatigue, the profiles of the
and they are usually indicative of the two fracture surfaces do not match.
presence of corrosive media. Under conditions of low stress fatigue,
The ductile striations are more cam- it is not clear at this stage, whether the

FIO. 23--Fatique Striations on Grain Boundariesin a Ti-2.5AI-16VAllay. 6000X. Reduced One


Third in Reproduction.

man and they have also been observed in profiles are of the type II or type III
polymers which would show that their represented on Fig. 28.
formation is not necessarily related to the Grain boundaries play an important
crystallographic nature of metals. Figures role in fatigue-crack propagation. The
27 and 30 give some good examples of different figures presented here show that
ductile fatigue striations. The exact in aluminum alloys, the crack front is
mechanism of formation of these stria- held up along grain boundaries, and the
tions is not clearly understood. Figure orientation of the striations changes
28(c) presents different profiles of fatigue from one grain to the other. This could

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 233

be accounted for by the fact that in high- the calculated crack-growth rate. How-
stacking fault energy materials, fatigue ever, in general, brittle fracture of inter-
cracking is the result of deformation by metallic particles and ductile tear around
cross slip which is more extensive inside large constituent particles result in a
the grains than along the grain bound- rapid and localized advance of the crack
aries. front. This is shown on Fig. 31(a) and

FiG. 24--Intergranular Fracture Through Sintered Tungsten. Grain Facets Have Only a Few
Features Visible. 2800X. Reduced One Third in Reproduction.

Under uniform load, the height and the 31(b). Consequently, the spacing of the
spacing of the striations increase with observed striations is, in general, smaller
the crack length. The spacing of the than the spacing expected from the
striations as measured by electron mi- macroscopic measurements of crack
croscopy is not always equal to the growth rates. Naturally the spacing of
calculated spacing or crack-growth rate the striations is also markedly dependent
derived from macroscopic measurements on the load. Figure 32 shows that under
of crack length v e r s u s number of cycles. a varying load, the spacing of the stria-
If at each cycle the crack front does not tions may vary considerably. It can also
advance in a uniform manner over its be seen from this figure that the well-
whole length, the average spacing of the defined fatigue striations provide us with
observed striations will be larger than an ideal marker which should be used to

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o
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Fie. 2 5 - - I n t e r g r a n u l a r Fracture in a 4340 Steel. FIo. 2 6 - - O p t i c a l Micrograph of a F a t i g u e


Fracture in a 7178 A l u m i n u m Alloy. Some Re-
This intergranular fracture at the origin of a service failure was gions Are out of Focus due to the Small D e p t h
probably due to stress corrosion and hydrogen embrittlement. Note of Field of t h e Optical Microscope. 3200X. Re-
the tear ridges along t h e grain-boundary facets and t h e dimples in A duced One Third in Reproduction.
and B. Two-step replica. (Reprinted from Ref (2).) 6 0 0 0 X . Reduced
one third in reproduction.

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BEACHEM AND PELLOUX ON ELECTRON FRACTOORAPHY 235

measure the true influence of a peak discontinuous. Very often, according to


overload on the rate of crack propaga- the ratio of the maximum to the mini-
tion. This kind of work would be very mum stress, the details of the fracture
useful in the formulation of a proper surface have been destroyed by the
theory of fatigue damage. rubbing action of the two fracture faces.

FIG. 27--Electron Micrograph of a Fatigue Fracture in a 7178 Aluminum Alloy.


By contrast with Fig. 26, this micrograph shows the larger depth of field of the electron microscope.
The fiat regions where the crack propagated in a cyclic manner are connected by ductile regions where
fracture took place suddenly around inclusions or by shear. Two-step replica. 5800• Reduced one
third in reproduction.

Other examples of fatigue striations This is often the case with service failures
are shown in Figs. 33-35. In general, where a fatigue mode of fracture is
the striations in different materials are identified by the presence of a few stria-
not as sharply defined as they are in tions on a flat surface and the absence of
high-strength aluminum alloys. In steels other characteristic fracture features.
for instance, the successive positions of Fatigue-crack propagation is not always
the crack front do not appear clearly a transgranular mode of fracture with
defined; the striations are short and well-defined crack-front arrest lines. In

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Oo
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Fro. 28--Different T y p e s of Ductile and Brittle Fati:.ue Striations; (a) and FIG. 2 9 - - E x a m p l e of Brittle Fatigue Striations in a Service Fail-
(b) Are T a k e n from Forsyth (16). ure of a 2014 A l u m i n u m Alloy.
Note t h e cleavage steps running parallel to the direction of crack
propagation a n d normal to the fatigue striations. Two-step replica.
5000X. Reduced cne third in reproducticn.

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 237

FIG. 30--Examples of Ductile Fatigue Striations in a 7178 Aluminum Alloy.


Bottom photo shows clear~ the role of grain boundaries in slowing down the progression of the
crack front. Two step replica. (top) 10,000X. (bottom) 6000X. Reduced one third in reproduction.

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238 FRACTURE TOUGHNESS TESTING

FIG. 31--Examples of Ductile Fatigue Striations and Brittle Fracture of a Second-Phase Particle
in a 7178 Aluminum Alloy. Two-Step Replica. 12,000X. Reduced One Third in Reproduction.

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FI~. 3 2 - - F a t i g u e F r a c t u r e in a 7178 A l u m i n u m Alloy.


Under a random load the spacing of the striations is not uniform. Fro. 3 3 - - F a t i g u e Striations[ n a 4340 Steel.
The influence of peak overloads on the rate of advance of the front are
clearly indicated. Two-step replica. 7600X. Reduced one t h i r d in re- The striations are never well defined over the whole fracture sur-
face. Two-step replica. II,O00X. Reduced one t h i r d in reproduction.
production.
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240 F~cTuP.J~ TOUG~m~SS TESTING

Fro. 34--Fatigue Striations in a Welded Zone of a 2219 Aluminum Alloy.


The large second-phase particles are probably eutectie p~.rticles of AI~Cu. Two-stage replica.
6800X. Reduced one third in reproduction.

many cases, fatigue cracks propagate observed in very brittle materials; they
along grain boundaries. This type of are the result of an interaction between
fracture was observed in 70-30 brass by the advancing crack front and an elastic
one of the authors and it also takes place wave propagating at the same time. They
in high-strength steels such as 4340. appear as uniformly spaced striations
Very often a misinterpretation of some but with an occasional criss-crossing
fracture features can lead to some con- network of lines (Fig. 36). I t also often
fusion. For instance, Wallner's lines happens that in a composite material,
(19) should not be confused with fatigue fracture takes place at the interface
striations. Wallner's lines are usually between large second-phase particles and

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BEACHEM AND PELLOUX ON ELECTRON FRACTOGRAPHY 241

a matrix. Such a case is shown in Fig. 22. tions of material, stress, and environ-
The sharp lines and facets which are ment. Successful failure analyses with
growth markings on the surface of the this tool depend on the prior knowledge
second-phase particles should not be of the appearance of the fracture surfaces
confused with fatigue striations. of a given material broken under specific

FIG. 35--Fatigue Striations in a Zirconium Alloy. Two-Stage Replica. 6400N. Reduced One
Third in Reproduction.

FAILURE ANALYSES conditions, both in the laboratory and in


Electron fractography has become a service. A proper analysis of a service
very useful tool in the analysis of service failure with this technique also depends
failures. Although it does not replace the on the preservation of the fracture sur-
other failure-analysis tools, it frequently faces.
permits the unambiguous identification As an example8 of service failure
of fatigue striations, intergranular frac- analyses, Figs. 37 and 38 show the
tures, dimples, or cleavage facets which macroscopic and electron microscopic
are known to be caused by specific condi- s Unpublished work, W. R. Warke.

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242 FRACTURE TOUGHNESS TESTINC

FIG. 36--Examples of Wallner's Lines Resulting from the Brittle Fracture of a Silicate Particle
in an Aluminum- Silicon Alloy. Two-Stage Replica. 6800)<. Reduced One Third in Reproduction.

FIG. 37--Photomacrograph of a Fractured ,Muminum Forging Showing Five Small Cracks Which
Formed During Service. 3X. Reduced One Third in Reproduction.

features of a 2014-T6 aluminum alloy case the techniques of electron fractog-


forging which developed cracks in raphy easily and quickly gave informa-
service. The cracks were found during a tion which would have been very difficult
routine inspection and the part was or impossible to obtain in any other
removed from service and submitted for way.
analysis. The part was broken in the
SUS~ARY
laboratory to reveal some of the cracks.
Figure 38 shows the primary origin to The direct or indirect observations of
be stress-corrosion cracking with subse- fracture surfaces at high magnification
quent crack growth by fatigue. In this permit the study of the path of least

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BEACIIEM AND PELLOUX ON ELECTRON FRACTOGRAPIIY 243

FIo. 38--Composite Electron Microscope Fractograph of One of the Cracks in Fig. 37 Showing
Striated Fatigue Fracture Originating from a Minute Intergranular Surface Flaw. Two-Step Replica.
2400X. Reduced One Third in Reproduction.

resistance to fracture in much more can help fill the research gap between
detail, and much more easily, than can continuum mechanics and mechanical
be done with polished cross sections. metallurgy on the one hand and the
Detailed studies are revealing a new metal physics approach on the other
class of information which permits a hand. It should be emphasized that the
fuller knowledge of the complexities of small amount of information accumu-
fracture and a better understanding of lated to date is immediately useful to
fracture processes. Electron fractography those who are working with high-strength

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244 FRACTURE TOUGHNESS TESTING

engineering m a t e r i a l s - - h e l p i n g them members of the s u b c o m m i t t e e on Frac-


u n d e r s t a n d fracture toughness a n d to tography a n d Microstructure in Relation
perform critical failure analyses. to F r a c t u r e B e h a v i o # for their contribu-
tions to the body of this report a n d their
Acknowledgment:
helpful suggestions a n d c o m m e n t s con-
The authors extend their t h a n k s to the cerning the text.

REFERENCES
(1) C. A. Zapffe and M. Clogg, Jr., "Frac- (12) A. J. Edwards, "Depth Measurements on
tography--A New Tool for Metallurgical Fracture Surfaces," Report of NRL
Research," Transactions, Am. Soc. Metals, Progress, November, 1963.
Vol. 34, 1945, p. 71. (13) E. P. Dahlberg and D. B. Lytle, "Fatigue
(2) R. M. N. Pelloux, "The Analysis of Frac- Crack Propagation in High-Strength 4340
ture Surfaces by Electron Microscopy," Steel," NRL Memorandum Report 1471,
Boeing Scientific Research Laboratories November, 1963.
Report D1-82-0169-R1, December, 1953. (14) C. Zapffe and C. Worden, "Fractographic
(3) J. R. Low, Jr., "A Review of the Micro- Registrations of Fatigue," Transactions,
structural Aspects of Cleavage Fracture," Am. Soc. Metals, Vol. 43, 1951, pp. 958-
Swampscott Conference on Fracture, John 969.
Wiley & Sons, Inc., New York, N. Y., 1959. (15) P. J. E. Forsyth and D. A. Ryder, "Fa-
(4) J. R. Low, Jr., "Dislocations and Brittle tigue Fracture: Some Results Derived from
Fracture in Metals," Madrid Colloquium the Microscopic Examination of Crack
on Deformation and Flow of Solids, IUTAM, Surfaces," Aircraft Engineering, Vol. 32,
Springer-Verlag, Berlin, 1956. 1960, p. 96.
(5) E. P. Dahlberg, "Characteristics of Twin- (16) P. J. E. Forsyth, "Fatigue Damage and
ning on Fracture Surfaces of Single and Crack Growth in Aluminum Alloys,"
Polycrystalline Tungsten," Paper J-5, Acta Maallurgica, Vol. 11, July, 1963,
Fifth International Congress for Electron pp. 703-715.
Microscopy, Academic Press, New York, (17) C. Laird and G. C. Smith, "Crack Propa-
N. Y., 1962. gation in High Stress Fatigue," Fhilo-
(6) C. D. Beachem, "Electron Fractographic sophical Magazine, Vol. 7, 1962, pp. 847-
Studies of Mechanical Fracture Processes 857.
in Metals," Transactions, Am. Soc. Mc- (18) A. J. McEvily, R. C. Boettner, and T. L.
chanical Engrs., to be published. Johnston, "On the Formation and Growth
(7) C. Crussard et al, "A Comparison Be- of Fatigue Cracks in Polymers," 10th
tween Ductile and Fatigue Fractures," Sagamore Army Materials Research Con-
Swampscott Conference on Fracture, John ference, 13-16 August, 1963.
Wiley & Sons, Inc., New York, N. Y., 1959. (19) H. Schardin, "Velocity Effects in Frac-
( ) H. C. Rogers, "Tensile Fracture of Ductile ture," Swampscott Conference on Fracture,
Metals," Transactions, Met. Soc. Am. John Wiley & Sons, Inc., New York,
Inst. Mining Metallurgical Engrs., Vol. N. Y., 1959.
218, June, 1960, p. 504.
(9) G. T. Hahn et al, "Initiation of Cleavage
Microcracks in Polycrystalline Iron and 9 G. S. Ansell, Rensselaer Polytechnic Inst.;
B. R. Bannerjee, Central Research Lab., Cruci-
Steel," Swampscott Conference on Fracture, ble Steel Co.; C. D. Beachem, U.8. Naval
John Wiley & Sons, Inc., New York, Research Laboratory; A. J. Brothers, Large
N. Y., 1959. Steam Turbine-Generator Dept., General Elec-
(10) C. D. Beachem, "An Electron Fracto- tric Co.; C. M. Carmen, Frankford Arsenal;
graphic Study of the Influence of Plastic R. W. Hertzberg, Lehigh University; M. Hill,
Strain Conditions Upon Ductile Rupture Research Center, Republic Steel Corp.; M. S.
Processes in Metals," Transactions, Am. Hunter, Alcoa Research Laboratories; N. A.
Soc. Metals, Vol. 56, September, 1963, pp. Nielsen, Engineering Research Lab., E. I.
DuPont de Nemours & Co.; G. E. Pellissier,
318-326. Applied Research Lab., U.S. Steel Corp. (sub-
(11) P. J. E. Forsyth and D. A. Ryder, "Some committee chairman); R. M. N. Pelloux, Tur-
Results of the Examination of Aluminum bine Div.. The Boeing Co.; W. R. Warke,
Alloy Specimen Fracture Surfaces," Metal- Battelle Memorial Inst.; and B. V. Whiteson,
lurgia, Vol. 53, March, 1961, pp. 117-124. Douglas Missile and Space Systems Div.

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STP381-EB/Apr. 1965

DISCUSSION

T. G. Roc~owl--The title and scope confined to the fractography of metallic


of your excellent paper are broad enough materials. Do you mean to include
to include fractography of resins, poly- resinous materials--at present or in the
mers, and their products--amorphous as future ?
well as crystalline. Yet your observa- C. D. BEACnEM (author).--We are not
tions and interpretations seem to be presently using fractography to study
fracture mechanisms in resins and
1 Research felh)w, American Cyanamid Co., polymers. However, the techniques are
Stamford, Conn. applicable and are being used by others.

245
Copyright9 1965 by ASTM International www.astm.org
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Practical Applications

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APPLIED FRACTURE MECHANICS

BY C. F. TIFFANY l AND J. N. MASTERS'

SYNOPSIS
Procedures for applying fracture mechanics to typical engineering problems
are reviewed. Particular emphasis is placed on plane-strain fracture of ma-
terials used in fabrication of pressure vessels and booster cases. The major
areas considered are: (1) material selection; (2) the estimation of structural
life; and (3) the determination of nondestructive inspection acceptance limits.
In order to treat these items properly, a brief discussion on the character of pre-
mature structural failure is presented, followed by a discussion on the selec-
tion of a fracture toughness specimen.
In the area of material screening and selection, it is shown that the required
design tool is related, not to toughness alone, but also to the design stress level
and the size of the structure. In the estimation of structural life and determina-
tion of nondestructive inspection acceptance limits, emphasis is placed on the
use of fracture specimen test results and the stress-intensity concept to predict
critical flaw sizes and subcritical flaw growth. Both cyclic and sustained stress
flaw growth are discussed and comparisons made between specimens and
pressure vessels. The value of the proof test is discussed with regard to deter-
mining the maximum possible initial flaw sizes in a pressure vessel.

While the primary purpose of this time at sustained load before the flaw
paper is to review the application of attained a size sufficient to cause failure.
fracture mechanics to the design and In that the gross stress field is generally
life p~ediction of structures, it appears elastic at the operational loads, the
appropriate first to provide some back- failed component is normally charac-
ground as to the character of premat,:re terized by an absence of a large amount
structural failure. of plastically deformed or yielded ma-
Examination of structural components terial. This is of fundamental importance
which have failed during service opera- and points out the danger involved in
tion typically indicates that the failure assuming that the strength and opera-
origin was a small crack or crack-like tional life of the structures can be esti-
flaw. The initial flaw size may have been mated using conventional strength anal-
sufficiently large to cause fracture upon yses which are predicated upon the
initial loading, or it may have been absence of flaws and large amounts of
small enough such that the component plastic yielding prior to fracture. Clearly,
withstood a number of load cycles and it must be recognized that fabricated
structures and, indeed, even the raw
1 Chief, Pressure Vessel Development Unit, materials contain defects and flaws of
end research engineer, Pressure Vessel Develop-
ment Unit, respectively, The Boeing Co., Aero- various kinds. The lives of these struc-
Space Div.. Seattle, Wash. tures are controlled by the flaw sizes
249
Copyright9 1965 by ASTM International www.astm.org
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250 FRACTURE TOUGHNESS TESTING

]FIG. 1--Landing Gear Cylinder.

FIG. 2--SteelPressure-VesselFailure.

FIo. 3--Alumlnum Pressure-VesselFailure(LiquidHydrogen Temperature).

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Tn~rANY A N D MASXERS ON AI,PLmD FRACtUrE MECHANICS 251

Fla. 4--Turbine-Rotor Failure.

required to cause fracture (that is, categorized as surface flaws, embedded


critical flaw size) at the operating stress flaws, and through-the-thickness cracks.
levels, the initial flaw sizes and the sub- For surface and embedded flaws, the
critical flaw-growth characteristics of the degree of constraint at the crack leading
materials. border is high and plane-strain conditions
As pointed out in the fifth report of generally prevail. The initial flaws may
the ASTM Special Committee on Frac- or may not reach critical size prior "to
ture Testing of High-Strength Metallic growing through the thickness depending
Materials (1),* the types of flaws en- upon the plane-strain fracture toughness
countered in fabricated structures can be (Kxc value), the applied stress levels, and
J T h e boldface n u m b e r s in parentheses refer the material thickness. If the calculated
to t h e list cf references appended to this paper. critical flaw size is small with respect to

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252 FRACTURE TOUGEN'ESS TESTING

the wall thickness, the formation of a the thickness is increased the plane-
through-the-thickness crack prior to strain (Kit) values should be used. This
fracture is not likely. If fracture does is discussed in more detail in Ref (l) in
occur prior to growing through the conjunction with the probable types of
thickness, the flaw at time of fracture flaw growth that can lead to structural
very often approximates an elliptical or failure.
semi-elliptical shape. This is illustrated
in the fractographs of several typical THE SELECTION OF A FRACTURE-
component fractures shown in Figs. 1-5, TOUGHNESS SPECIMEN
and is of basic importance since the In that Refs (I) and (2) discuss the
mathematical model used in predicting various types of fracture specimens and

FiG. S--Structural Stiffener Failure.

critical surface and embedded flaw sizes the requirements for valid toughness
assumes this shape (1). measurements in considerable detail, it
For through-the-thickness cracks, the is not considered necessary to repeat
mode of fracture for a given material, them in this paper. However, it does
strength level, and test temperature is appear appropriate to point out the
dependent upon material thickness. If significance of end-hardware application
the material is relatively thin, plane- and material anisotropy on specimen
stress conditions are generally predomi- selection and to show fracture-toughness
nant. With increasing thickness, the correlations between several of the more
fracture appearance changes from that of common specimens.
full shear to an essentially flat or plane- Since conventional mechanical prop-
strain fracture. Thus, for thin sections erties generally vary to some degree
containing through-the-thickness cracks, among various forms and grain directions
the plane-stress fracture toughness (Kc) in a given basic alloy, it is reasonable to
values are of primary importance and as expect that fracture toughness values

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TIFFANY AND MASTERS ON APPLIED FRACZU'P.E M E C H . ~ C S 253

POSSIBLEDIRECTIONSOF 9STRESSFIELDAND
FLAW PROPAGATION, AND GRAIN DIRECTIONS
GRAIN DIRECTIONS
Longitudinal*-~
Longitudinal*~Transverse* ./ " ~ ~ /---Long"
.~" # ~ . . ' ~ Y T ~// Transverse

P ~

Transverse ~'~o' Transverse "~'k~X /~'~


A - F: Directionsof
Flaw Propagation
*Grain Direction
(a)
Fzo. 6--Stress Field, Grain Directions, and Possible Directions of Flaw Propagation.

220 (100) ( I 0 0 ) ?(65)~% Shear


SPECIMENSUSED

,'+\ ! O CenterCrackr Kc Values


180 9 CenterCrack, K. Values
I ~7 SurfaceFlaw, Kll: Values
v

e~ I RoundNotch Bar, Kic Values


v 14C 4L
I
l (4o)
1~ I . l [ j I. . . . .
I I ~ ~'.,..,. Plane Strain .r~-
e--;--li ......
60,- "Pop-In" -
KIc
I I I o)4o I I l I I I I I
0.20 0.60 0.80 1.00 1.20
THICKNESSI IN.

Fzo. 7--Specimen Correlations, 18 Per Cent Nickel (300) Steel.

also vary. This assumption appears to be applied stresses in the hardware. For ex
borne out by results of fracture tests ample, in a motor-case cylindrical shell.
performed to date on various materials. the stress field is biaxial in the plane of
In a rolled plate or forging, six direc- the plate. Stresses are applied in both
tions of flaw propagation are possible (3), the longitudinal and long-transverse grain
and plane-strain toughness (KIe) values directions, indicating the Kzc values of
may differ in each of these directions (see interest are those relating to the A, B,
Fig. 6(a)). The need to determine the K,c C, and D directions of propagation. In
values in each of these directions is di- such forgings as roll-forged Y rings
rectly dependent on the direction of the (Fig. 6(b)) stress is applied in all three

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254 FRACTDRE TOUGHNESS TESTING

grain directions, thus indicating the measures the lowest of either the A or
additional need for K~ measurements in B directions, or the lowest of either the
the E and F directions. C or D directions. For material where
Considering the banding and delami- there are no pronounced directional
nation problems in some thick plates, it effects, the same toughness should be
appears intuitively that the Kxc values obtained regardless of which of the
can be different between the A and B specimens is used. This is illustrated for
directions and, likewise, the C and D 18 per cent nickel (300) vacuum-melted
directions. This has been found to be maraged steel in Fig. 7. Figure 8 shows a

180
1
i
|

~pteecirnalelYFlawed ~;Ucn,deNnOtchedBar
160 0" oN

v
LJ g:i:Z2w., &..j
~ ]120

100 - ~ D = 1.0" (BothSpecs) R< 0.001"


.<

180 ~ j - - KIc = 32.6 KSI IY~ from Round Notch Bar Data
i ~ a w e d Sf~'c'JmenDataPoints

60

I I I I I I I I I i I I I I I
0.05 \0.]0 0AS
CRITICALFLAWSIZE, acr./Qcr ~ IN
Fro. 8--Internal Flaw Correlations.

the case (4) and tends to explain the comparison of internally flawed 17-7PH
differences in Kxc values obtained using steel pressure-welded specimen data with
surface-flawed and round notched bar or that obtained from round notched bar
single-edge-notched fracture specimens. tests. The internal flaws were introduced
The surface-flawed specimen is normally by placing tungsten flakes on the edge
used to measure the toughness in either preparation prior to welding. It is noted
the A or C directions, while the single- that in addition to illustrating specimen
edge-notched or center-cracked (pop-in) correlation, the data tend to support the
specimens measure the toughness in the basic relationship between failure stress
B or D directions. The round notched and flaw size. The term, a/Q, as used to
bar (removed so that its longitudinal describe flaw size is discussed in Ref (1).
axis is parallel to the plate surface) In the short transverse direction, there

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TIFFANY AND MASTERS ON .APPLIED F~CTm~E MECHANICS 255

appears to be no reason for believing the surface-flawed specimen in the A and


that there should be a significant differ- C directions. The arbitrary use of a very
ence in KIo values between the E and F large diameter round notched bar fabri-
directions; however, to our knowledge, cated from material other than that to be
there has been no experimental sub- used in the hardware is questionable
stantiation of this. Likewise, for weld- because of possible differences in tough-
ments, we know of no major differences ness between the specimen material and
existing in Kic values for a flaw propagat- the hardware material.
ing parallel to the plate surface (B or D In short, it is the authors' opinion
directions) as compared to a flaw propa- that there is no single "best fracture
gating normal to the surface (A or C specimen" to use in all situations where
directions). However, it is known that toughness values are needed--nor is
there can be differences in fracture such a specimen required. Of primary
toughness between the weld centerline importance is that the specimen selected
and the heat-affected zone. In addition, provide toughness data which are repre-
it is considered probable that there are sentative of the toughness of the material
differences in fracture toughness as well as it is used in the hardware application.
as subcritical flaw-growth characteristics As such, the toughness values must not
within the heat-affected zone, and, if be obscured by specimen-size effects,
realistic allowable flaw sizes are to be specimen-preparation effects, and loading
established, the minimum KI~ values procedures which are unique to the
must be determined. laboratory test.
Measurement of the actual K~o values
and variations in KI~, which occur T H E APPLICATION OF FRACTURE
due to material anisotropy, direction of MECHANICS
flaw propagation, and metallurgical In the selection of a material and the
differences, requires the use of fracture design of a tension-loaded structure such
specimens designed to yield valid data. as a pressure vessel, one must consider
The actual specimen selection is de- the following questions:
pendent on the direction in which the
K~ measurement is desired and the 1. What are the critical flaw sizes
ability to design a large enough specimen (that is, sizes required to cause failure)
out of the material gage to prevent in the various portions of the vessel at
general yielding prior to fracture. While the expected operational stress levels?
round notched bar specimens might be 2. What are the maximum initial
considered to be desirable because they flaw sizes that are likely to exist in the
automatically obtain the lowest tough- vessel prior to its being placed into
ness value in either the A or B directions, service?
or the lowest in either the C or D direc- 3. Will these initial flaws grow to
tions, it may not always be possible to critical size and cause failure during the
use the specimen type because of ma- expected service life of the vessel?
terial thickness limitations (that is, the Quite obviously, the answers to these
specimen diameter needed to get a valid questions are heavily dependent upon
K~, value exceeds the hardware ~all the inherent fracture toughness and
thickness). subcritical flaw-growth characteristics of
In such a case, the single-edge-notched the pressure-vessel materials, but in
specimen might be used to obtain the addition, are dependent upon such items
toughness in the B and D directions and as deslgn-safety factors, proof-test fac-

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256 F R A C T ~ TOUGHNESS TESTING

EmbeddedFlaw--(a//Q)'cr = ~ x(--~) 2

Qcr
_L
t- l-

CRITICALFLAW SIZE (a//Q'~cr

FzG. 9--Applied Stress Versus Critical Flaw Size.

b.-2c--q a
0,50

External Intema /~N~=~,~, . _

0.40

0.30

0/2a
0.20
o !o,=l l l
j r #/" ~" ~ " Q = Flowshapeparameter
~'/~'/ (~ = Completeell|ptiaal integral
0.10 ,~ j/" f / of the secondkind "
/ / / / O' = G,O,$stress

iiii 1.0 1.5


...o
2.0 2.5
Q

Fic. 10---Flaw-ShapeParameter Curves for Surface and Internal Cracks.

tars and the nondestructive inspection subcritical flaw growth, and estimating
procedures that are used. structural life have been discussed in
The use of fracture-toughness data some detail in Ref (l). Also, Ref (1)
and fracture mechanics analysis in pre- points out the use of the conventional
dicting critical flaw sizes, evaluating proof test as a means of determining the

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TIFFANY AND MASTERS 0N APPLIED F~CTUm~ MECHANICS 257

FIG. 11--The Significanceof Flaw Shape.

maximum possible initial flaw size in a additional experimental data and to


pressure vessel. In the following para- point out the significance of fracture
graphs a portion of the Ref (I) discussion toughness data in material selection and
is repeated, but expanded to include the use of fracture mechanics to arrive

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258 FRACT~r.~ T O ~ C ~ S S TESTING

ALL VALUES ARE YIELD CORRECTED


I i

MEASURED FROM PREDICTED FROM


MEASURED TANK ROUND NOTCH BAR
FLAW SIZE
DATA
KIc ac/Qcr KIc
|1

2a =10.1670 In.
cr
a c r =0.0835 In. 51,300 0.0632 48,700 0.0564
2c ='0.355 In.
=
I II

FIo. 12--Comparisonof Measured and PredictedCritical Flaw Size.

at rational nondestructive inspection the most dangerous condition in that


acceptance limits. Primary emphasis is both the subcritical flaw growth and
placed upon surface and embedded flaws final critical flaw size are controlled by
which can attain critical size prior to plane-strain conditions and in the case
growing through the thickness. This is of high-pressure tanks, there is no ad-

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TIFYANY AND MASTERS ON APPLIED FRACTURE MECHANICS 259

ALL VALUES ARE YIELD CORRECTED


i

MEASURED FROM PREDICTED FROM


FLAW TAN K ROUND NOTCH BAR
i
SIZE "
DATA K Ic a cr/Qcr KIc a cr/Qcr
i i t

O
cr = 0.075 In.
2c = 0.15 In. 54,000 0.033 53,000 0.031
cr

Qcr =2.26
i

FIG. 13--Comparisonof Measured and Predicted Critical Flaw Size.

vance warning (such as leakage) of for a given hardware operating stress.


failure. For convenience, the relationship of
flaw size to stress is usually plotted as
The Prediction of Critical Flaw Sizes and shown in Fig. 9. Note that we have
Their Role in Material Selection: elected to use the term, a/Q, to describe
As noted in the previous sections, flaw size as is discussed in Ref (1). The
Klc values can be obtained from several plot of Q versus the depth-to-length
types of specimens. Having developed ratio (a/2c) of surface and embedded
valid data for a given material form flaws is given in Fig. 10. With regard to
(that is, plate, forging, weldment, etc.), this point, it is noted that a considerable
heat-treat level, and test temperature, amount of data has been published in
the critical flaw size can b e calculated which surface-flaw sizes have been

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260 FRACTURE TOUG~N~ESST~STZNG

ALL VALUES ARE YIELD CORRECTED


MEASURED MEASURED FROM PREDICTED FROM
FLAW SIZE DATA TANK ROUND NOTCH BAR

CRACK NO. 1 CRACK NO, 2 KIc %r/Qcr KIr acr/Qr r


i

a| = 0.041 In. al = acr =0.045 In


2ci= 1.02 in. 2c,=2c =0.99 In.
I cr 44,900 0.0454 49,500 0.055
Q|= 0.9 Oi = Qcr = 0.9
al/Qi =0.0414 In a i//Qi = acr/Qcr
=0.0454 In.
FzG. 14--Comparison of Measured and Predicted Critical Flaw Size (External Artificial Semi-
Elliptical Flaw).

plotted in terms of flaw length, depth, or areas were tested, yet both failed at
area versus gross failure stress. While approximately the same stress. Both had
such data can have a useful meaning ff approximately the same a/O. ratio, and
the a/2c ratios are held constant, the thus the same KI~ values.
a/2c values are usually absent in the The engineering usefulness of the
published reports. basic stress-intensity concept in the
The fallacy of such a presentation is prediction of critical flaw sizes and the
obvious after reviewing the test data use of a/Q to describe flaw size has been
shown in Fig. 11. Here, two specimens supported by a number of hardware
with different flaw depths, lengths, and correlations. Some such correlations are

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T~FANY AND MASTERS ON APPLIED FRACTURE MECHANICS 261

ALL VALUES ARE YIELD CORRECTED

MEASURED FROM TANK PREDICTED FROM


FLAW SIZE DATA ROUND NOTCHED BAR
CRACK NO, 1 CRACK NO. 2 Kic acr/Qcr Klc o c/Qcr
tt

a. = a =t0.051n.
al =0.05 In. J cr
2c| =1.05 in. 2c|=2Ccr = 1.20 in.
50,500 0.055 53,200 0,058
Qi = 0.93 Qi = Qcr = 0.90
a i / Q i =0.0538 In. a | / Q i = a c / Q c r =
0.055 In.
FIG. 1S--Comparison of Measured and Predicted Critical Flaw Size (External Artificial Semi-
Elliptical Flaw).

shown in Ref. (1) and in Figs. 12 through For the purpose of screening several
15 of this paper. materials for an end-product application
From the equations shown in Fig. 9, K~c data are often plotted as shown in
it can be readily seen that the critical Fig. 16(a). This is a simple and useful
flaw size is equally as dependent upon plot showing the general trends in
applied stress level as upon the material toughness with increase in strength level
fracture toughness. This is of basic in the aluminum, titanium, and steel
importance when selecting a material or a alloys. However, such a comparison can
heat-treat strength level, or both, for a be misleading. For instance, a designer
given structural application and should may reach for higher and higher ma-
be recognized when evaluating K~c data. terial strength levels by noting the minor

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262 FRACTI.rRE TOUGhNeSS TESTnnG

150

N 100
v

e,,

u
v 5 0 - - -

i , , , , I
50 100 150 200 250 3OO
ULTIMATE STRENGTH (Ftu)-KSI
(a)

i.5
I

--Z 1.G

~0.50
A
Titanium
I ;
5O 1~t0 150 200 2! 300
ULTIMATE STRENGTH (Ftu)~,KSI
(b)

i
9, 1.0

Aluminum*
0.50
. . . . . . . . . . . . . . . . . . . . . . . . . . . . .
~'itanium

50 IOO 150 200 250


EQUIVALENT ULTIMATE STRENGTH IN STEEL
(c)
FIG. 16--Material Comparisons (Base Metal, Room-TemperatureTrends).

reduction of toughness corresponding factor of safety (that is, the actual factor
with sllch strength level increases. of safety is often specified by the pro-
Recognizing that the operating stress curing agency), the data shown in Fig.
levels in structures are generally con- 16(a) might more appropriately be
trolled to a fixed percentage of the un- plotted as shown in Fig. 16(b). The
flawed tensile strength by the design ordinate of Fig. 16(b) is directly pro-

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TIFFANY AND MASTERS ON APPLIED FRACTURE MECHANICs 263

portional to the critical flaw size, thus further comparison shown in Fig. 16(c).
placing the influence of varying ma- From this figure it can be seen that the
terial strength levels into better per- titanium should provide a somewhat
spective. For example, an increase in lighter tank on the basis of equal critical
ultimate strength level from 50 to 60 flaw size.
ksi in aluminum shows a rather nominal Certainly such comparisons provide
drop in K~ from approximately 60 guidance during initial material screen-
ksi ~v/i~. to 50 ksi ~ however, in ing; however, one must not forget that
terms of critical flaw size, the use of the material anisotropy and variations in
higher strength material represents a material forms cause differences in
major decrease. The critical flaw size toughness throughout the structure, and
using the 60-ksi strength level material is likewise, the applied stress levels gener

/ / /~ 9 , / K , o Y / ?oI~176176
U
z t~)o.: ~t~/ I o.

I al .C
%%

. . . . . . . . . . . X 7 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
-r"

i
1.C ..O..~.'~ .................................... ~ J ..............................................

.<

1 FLAWSIZE a/Q CYCLICLIFE /

/
1.0

a~ MIN. From fracture-Speclmen


-
IFLAW G"OVHt
: [ POTENTIAL
'significance
O'gOeto",e,,obI,,
in terms
!
(1-!/a l) oF~176 life
FIO. 17--Significance of Proof Testing in Estimation of Minimum Tank Life.

only one half the value obtained with ally vary. Consequently, the critical
the 50-ksi material. Also, from Fig. 16(b) flaw sizes in various portions of the
the three materials can be compared structure will be different. In pressure
upon the basis of equal critical flaw size. vessels, weldments and base material
For example, pressure vessels designed loaded in the short transverse direction
from a 200-ksi steel, a 135-ksi titanium, are particularly prone to low toughness
and a 70-ksi aluminum would all have and when combined with pre-existing
approximately the same critical flaw initial defects and high applied stresses
size at a given operating pressure (that they are potentially dangerous. Weld-
is, operating stress which was a fixed ments and the short transverse parent
percentage of the material tensile metal should not be ignored during the
strength). initial material screening. Also, the
Considering the effect of structural susceptibility of the material to sub-
weight, one might wish to make the critical flaw growth in the expected

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264 FRACTURE TOUG~-ESS TESTING

service environment should not be to critical stress intensity, KIi/KI,, is


ignored. equal to 1/a. Both are independent of
While it is desirable that the material the actual proof stresses, and the actual
selected for a given structural application material toughness values. This is
have large critical flaw sizes at the significant, since the actual proof stresses
operational stress levels, low subcritical may be different because of design or
flaw-growth rates, and low probability manufactured discontinuities, and be-
of flaw occurrence (that is, good fabri- cause the toughness values will likely
cability), actual material selection will vary between base metal, weldments,
generally involve a compromise. and forgings.
The material screening program should Also, as noted in the figure, the mini-
provide sufficient insight into these items mum flaw-growth potential in the
to allow a rational compromise. tank, (a,r/Q~,- a~/Q~), is equal to

The Estimation of the Life of Pressure Probably the most predominant types
Vessels Subjected to Cyclic and Sus- of subcritical flaw growth are fatigue
tained Stresses: growth resulting from cyclic stress and
With pressure cycles and time at stress, environmentally induced sustained stress
an initial flaw or defect in a pressure growth. Also, growth may occur even in
vessel (or any other structure) will grow the absence of severe environmental
in size until it attains the critical size effects if the initial flaw size approaches
at the applied operating stress level and the critical flaw size.
failure will result. The flaw-growth The technique used for predicting the
potential (in inches) is equal to the subcritical cyclic or sustained stress flaw
critical size minus the initial size. The growth makes use of fracture specimen
life of the vessel is directly dependent testing and the stress-intensity concept.
upon this flaw-growth potential and the It has been shown (1,7) that the time or
subcritical flaw-growth characteristics of cycles to failure at a given maximum
the tankage materials. applied gross stress level depends on the
Determination of the initial flaw sizes magnitude of the initial stress intensity
generally relies upon the use of nonde- at the flaw tip, KI~, compared to the
structive inspection procedures; however, critical stress intensity, Kxo (that is,
as discussed in Ref (1), the conventional cycles or time to failure = f(KI~/KI,).
proof test can be considered to be one Also, it is seen that the ratio of initial
of the most positive inspection proce- flaw size to critical flaw size is related to
dures available. A successful proof test the stress-intensity ratio as follows:
actually defines the maximum possible
initial flaw size that exists in the vessel.
~ol = ",,IO-
This results from the functional rela-
tionship between stress level and flaw Thus, if cyclic or sustained stress frac-
size as defined by the critical stress ture specimens are used to obtain ex-
intensity (KI,) and as illustrated earlier perimentally the KIi/KI, versus cycles
in Fig. 9. This is illustrated in Fig. 17. or time curves for a material, the cycles
As seen in this figure, the ratio of maxi- or time required for any given initial
mum initial flaw size to critical flaw size, flaw to grow to critical size can be pre-
(a/Q)~/(a/Q)~r is equal to 1/o?, where a dicted. Conversely, if the required life of
is the proof-test factor. Similarly, the the structure is known in terms of stress
ratio of maximum initial stress intensity cycles or time at stress, the maximum

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TIFFANY AND MASTERS ON APPLIED FRACTURE IVIECKANICS 265

allowable initial flaw size can be de- bars, the initial stress intensities (K,;)
termined. are calculated by substituting the maxi-
The growth of through-the-thickness mum net-area cyclic stress in place of the
cracks with repeated stress cycles can net-area fracture stress, ~N. As cycling
and has been investigated (S) with rela- progresses, the notch deepens under
tively little ditficulty since this growth plane-strain conditions (in the same
can-be visually observed and measured. manner as a flaw grows in a tank under
With surface or embedded flaws (plane- cycling load) and for the specimen, by
strain condition), measurement of the virtue of the ever-increasing stress on
actual growth is restricted because of the the net area, the stress intensity in-
inability to make such visual observa- creases from the initial value, K,~, to
tions. the critical value, K,c, at which time
What normally is obtained from a failure occurs. For surface-flawed speci-
plane-strain fracture specimen cyclic mens, the initial and critical stress in-

I.C

0.8

0.4 . . . . . . . . . . - . . . .

0.~'

I0 100 1000 1 I0 100 I000


CYCLES CYCLES
(a) (b)
FIG. 18--Schematic Representation of Cyclic Flaw Growth.

test are the initial flaw size, the critical tensities are calculated, using straight-
size as measured from the fracture face, forward measurements of initial and
the cycles it took to grow from initial to critical flaw sizes, and gross stress.
critical size, and the initially applied Since flaw area is controlled to a small
cyclic stress. From these data, the initial percentage of gross area, the increase in
stress intensity, K I ; , and the critical net-area stress with cycles is negligibly
stress intensity, Kic, can be calculated. small.
In our plane-strain cyclic flaw-growth The cyclic flaw-growth data are
investigations, the round notched bar plotted in terms of stress-intensity
and the surface-flawed specimen are ratio, KI~/Kj~, versus log of cycles as
used as the primary experimental tools. shown schematically in Fig. 18(a). By
For each material investigated, several squaring the ordinate value, the plot of
specimens are statically tested to failure the ratio of initial flaw size to critical
to obtain K~, values. Additional speci- flaw size versus the log of cycles (shown
mens are then loaded to various per- in Fig. 18(/,)) can be obtained. With
centages of the critical stress intensity knowledge of the initial flaw size and the
and cycled to failure, For round notched calculated critical flaw size, the total

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266 FRACTURE TOUGHNESS TESTING

I.I

~_ 1,0
v
O 0.8
I--
.<
>_ 0.6
I--

Z
"'
I- 0.4
Z J c3 Longit. and long. transv. Kic = 54.8 Ksi iVTm-n
~ 0.2 o Weld (13-9 wlre) Kic = 31.3 Ksl iV~-n
I-.- Short transv. KIc = 23.0 Ksl iV~"n
I , , if,, , i l il,,,J , i i i,,i,J i , I ,,Jill
I0 I00 I000 I0000
CYCLES
InLOAD SPECTRUM I
9 ,, i-I (Minh J

Fro. 19--Round Notched Bar Fatigue Data for 17-7PH Steel (Plate Forging, Room Temperature).

NOTES
I. BaseMetal: 1.0-1n. Thick 2219-T87Plate
2. FractureSpecimen: SurfaceFlawed

1.0 Load Spectrum


~-I (Min)"~
%% mox
%%
0 %,
0 0.90

_u 0.80

0.7C

J I I J J ill ~ l I I IIII l I I l I Ill


1 10 100 1000

NUMBEROF CYCLESTO FAILURE


l:zo. 20--Base Metal Cyclic Flaw-Growth Data (--320 F, Longitudinal Grain).

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TIFFANY AND ~/~ASTERS ON APPLIED FRACTURE I~ECHAI~rlCS 267

i!iiiiiiiiiiiiiiiiiiiiiiiii ..... ,

9~

"6

~d
Gmax
Surface-Flawed Specimen
Q Sharply Notched Round Bar
Specimen 0
70

1 10 100 1000
CYCLES TO FAILURE

FIG. 21--Cyclic Flaw-Growth Data of 6A1-4VTitanium Plate Tested at -320 F.

. . . . . j

_..__.~ . J / - Specimen Flaw-Growth


1.0

0.9
" ~ " ' ' Actual
0.8

~... o.7
v
.' . . . . ' Predicted Fracture . . ~ ....
oF Tank V
0.~

0.5

0.4,
E) ~ Round Notch Specimen
0.3 ~ A ~ Surface Flawed Specimen
~ 17" Dia Tanks, Actual Failures
K I | v, lnltlal Stress Intensity
0.2 i KIc ~ Fracture Toughness(Plane Strain) i.e.
Critical Stress Intensity
0.1 --P" ~ Stopped Cycling - Did Not Fall
J

0 I I I I I llll [ J I I Ill I, I f I I I Ill t ~ i J iJ-~


IO ]00 1000
TANK SERVlCE LIFE (CYCLES TO FAILURE)

Fro. 22--Prediction and Verification of Tank Service Life from Specimen Flaw-Growth Data.

cycles to failure can be obtained directly example: if the initial flaw-size ratio was
from the plot. If the proof test is used, 0.40, in A cycles the flaw would have
1/a ~ can be entered on the ordinate and grown, increasing the ratio to 0.6; in B
the minimum cycles to failure read off the cycles, it would have grown to 0.8, etc.
abscissa. It should also be recognized Cyclic flaw-growth data have been
that flaw size can be determined after obtained on a number of materials using
any incremental number of cycles. For round notched bar and surface-flawed

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268 FRACTURE TOUGHNESSTESTING

FIG. 23--Over-AllView of Preflawed Tank.

FIo. 24---Tank V, Origin-of-Failure Fractograph (17-in. Diameter Ladish D6AC Steel Tank).

specimens. Some such data are shown in of this program was to verify the applica-
Figs. 19-22. It is noted that in Fig. 21, bility of fracture mechanics to the pre-
both round notched bar and surface- diction of low cycle pressure-vessel
flawed fracture specimen data are shown; failures and consisted of fatigue testing
in Fig. 22, round notched bar, uniaxial a number of fracture specimens and
surface-flawed specimen, and preflawed preflawed tanks. The initial flaws were
tank data are shown. These data have introduced in the tanks using an elec-
recently been obtained on Air Force trical discharge machine (EDM) and
Contract AF 33(657)-10251. The purpose extended a small amount by low stress

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TIF~At~Y AND MASTERS ON APPLIED FRACTURE MECHANICS 269

(a) Effect of cycling on KI~ in a room-temperature test of 17-TPH steel (longitudinal and long-
transverse plate and forging).
(b) Effect of initial overstress on subsequent cycles to failure for a 17-7PH steel (longitudinal
grain forging).
Fio. 25---Effect of Cycling and Overstreaa.

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270 FRACTURE TOUC~-ESS TESTING

and high-cycle fatigue (that is, pressure ble for computation of K~, values. The
cycling). The tanks were then subjected 0.233 coefficient in the equation decreases
to the operational cycles (0-100 per cent with decreasing d/D. The coefficient was
-0 pressure) until failure. The maximum modified in accordance with Ref (6) in the
gross-area stress during the operational computation of Ktc values where the
cycles was approximately 100 ksi. The net area at failure was sufficiently small.
material yield strength was 247 ksi. After To determine whether an initial over-
failure, both the initial and critical flaw stress (that is, the proof test) has any
sizes were measured and the initial and major influence on cyclic growth at a
critical stress intensities computed. A lower stress, a number of round notched
photograph of a failed pressure vessel specimens were given a two-cycle 10
(17 in. in diameter and approximately per cent overstress prior to cycling to

~"*~176176
....... ; .........
::....... o .......................................... .............. ....................
........... 81o* o , ,o oOTO-%*
............ ~.
v o*
9 ,. .......... .,,,,.,,,,,~ .
' o~
o ~ 9 o D~
9 "'~..
~--
0~ ......... ~ 1 7 6 1 7 6. . . . . ,...,~176 ..... ~ ........ ,.,,.,,,.,~
u Notched Bar Specimens
Plate & Forging

v o ~ Short Transverse
0,6- o ~ Longitudinal
A ~ Weld Metal
v ~ .Long Transverse
Hollow Data Points Dry
SoJid Data Points Wet
0"4 F

J [ I [ tiiii.I I | I|llliL I I I I |till I I I llliiJ


0,10. 1.0 10 100 1000
TIME AT LOAD, HOURS

FIG. 26---Sustained Stress Data for Room-TemperatureTests of 17-TPH Steel.

0.25 in. in wall thickness) is shown in failure. As expected, there was no sig-
Fig. 23. Figure 24 shows a typical fracto- nificant effect. This is shown in Fig.
graph of one of the failure origins. 25(b). It should be recognized that the
Although the question may arise as to effects of gross overloads (as in random
the possible effect of cycling stress on loadi,g profiles) might influence growth
Kxo due to metallurgical changes in the rates on subsequent cycles. It has been
material, the experimental data on noted by several investigators (8,9) in
several alloys indicate that Kic remains cyclic crack-growth tests ef center-
essentially constant. This is illustrated cracked sheet specimens that there is a
in Fig. 25(a), where the KI~ values were marked reduction in cyclic growth rate
computed from the fatigued specimens. after an initial high overstress.
As seen from the figure, the notch In the 17-7PH steel specimen tests
deepening is quite large when the applied shown previously in Fig. 19, the cyclic
initial stress intensity is low. For these speed was varied between 20 min per
cases, the round notched bar specimen cycle to 32 cycles per minute with little
equation of Ref (6) is not strictly applica- apparent effect on the cyclic growth

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TrrrA~ Ara~ MASTV-RS ON APPLIED FRACTURE Mv.CHAmCS 271

FIG. 27--Sustained Stress Flaw-Growth Data Obtained at - 3 2 0 F.

FIG. 28--Effects of Environment on Flaw-Growth Characteristics in Room-Temperature Tests.

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272 FRACTURE TOUGHNESS TESTING

rates until the initial stress intensity sustained stress flaw-growth data for
became very high with respect to the annealed 6A1-4V titanium and points out
critical value. At the high stress inten- that there appears to be a threshold
sities there was an apparent interaction stress-intensity level below which sus-
between sustained stress and cyclic tained stress growth does not occur.
growth, causing the specimens cycled at Also, these data indicated that the K~
slow speeds to fail early. This will be was not significantly altered by the sub-
discussed further in subsequent para- critical growth mechanisms.
graphs. At much higher cyclic speeds The existence of a threshold stress-

(a) 4330M steel actuator cylinder.


(b) Surface-flaw specimen test, sustained stress, 4330 steel actuator material.
FIG. 29--Analysis and Verification of Cylinder Failure.

(approximately 500 cycles per minute) intensity level is further supported by


the flaw-growth rates decreased. the data in Figs. 26 and 27 of this paper.
The application of fracture-specimen Figure 26 shows round notched bar test
testing to define the effects of sustained data for 17-7PH steel tested in both dry
load on flaw growth is essentially the and wet environments and Fig. 27 shows
same as used in defining cyclic flaw surface-flawed specimen data for 2219-
growth. A constant load is applied to T87 aluminum tested in liquid nitrogen.
either a round notched bar or surface- In neither case does it seem that the
flawed specimen such that the initial environment played an important role
stress intensity is less than the critical in the sustained stress growth. In both
value and the time to failure is recorded. cases the apparent threshold stress-
The K~/Ktc values are computed and intensity levels are quite high. As noted
the Kx~/KIc ratio plotted versus log of in Fig. 28, water had a significant effect
time to failure. Reference (1) shows such on the sustained stress flaw growth of

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T~PANY AND MASTERS ON APPLIED FRACTURE MEC~AmCS 273

welded 18 per cent nickel (250) steel. the time of fracture. From the results of
However, there are insufficient test data testing sustained stress surface-flawed
to define a threshold stress-intensity specimens in water and from the magni-
level. Likewise, for the 4330M steel tude of the initial stress intensity in the
shown in Fig. 29, water had a significant cylinder (KxdKxc = 0.305), it is ap-
effect and in this case the threshold parent that the subcritical growth and
stress-intensity level appears to be subsequent leakage experienced might
approximately 30 per cent of the critical have been expected.
value. Also shown in Fig. 29 is a fracto- Let us now consider the significance of
graph of the fracture origin of a 4330M sustained stress flaw growth and specifi-
steel hydraulic actuator (wall thickness, cally the threshold stress-intensity con-
t = 0.17 in.) used in a ground-support cept on the estimated total cyclic life of

1,0
e

Threshold_SStress. ~ ~ ~ . ~
0.8
J~--B " ~ : Cyc ic Growth
O ------ J Cycles " ~ ' Only
0.5
u I \
A Cycles '1

TOTALCYCLICLIFE
(Log Scale)
FIo. 30--Combined Cyclic and Sustained Stress Flaw-Growth Schematic Interpretation.

system. In addition to iUustrating sus- a tension-loaded structure containing an


tained-stress growth, it also illustrates initial crack or crack-like flaw. To illus-
a leak-before-failure condition. The ac- trate this, the schematic representation
tuator leaked after 32 hr at a sustained of the K-N curve is reconstructed in
stress of approximately 72.8 ksi. The Fig. 30, but superimposed on this curve
critical flaw size, based on the measured is a horizontal line at KIdKx~ = 0.80.
KI~ of the material (approximately 100 This is assumed to be the threshold
ksi ~/in.) and the applied stress of 72.8 stress intensity as determined from
ksi, is acr/O~r = 0.49 in. This exceeded sustained stress fracture tests as dis-
the wall thickness. The initial flaw size cussed in the previous paragraphs. Now
(a pre-existing crack) was measured to consider the situation where the initial
be aJQ~ = 0:046 in., and the initial stress flaw size and applied cyclic stress result
intensity was 30.5 ksi ~r Since rust in an initial stress intensity equal to 50
was apparent on the fracture surface, it per cent of the critical value. From the
appeared that moisture was present at curve, it is seen that it would take a

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274 F R A C T ~ TOUGHNESSTESTING

total of A cycles to grow this initial A cycles, depending on the time the
flaw to critical size and cause failure. maximum stress is held during each cycle.
However, in B cycles, the initial flaw The development of the exact time-cycle
would have increased in size enough to interaction curves above the threshold
cause the stress intensity to reach the value would be a complex and expensive
threshold value of K~JK~o= 0.80. With task and, as applied to most tankage
additional cycles, the stress intensity structure, may not be of great im-
would further increase and, if the stress portance. It appears more rational to
were sustained sufficiently long, it determine the basic cyclic data and the

1000 .e~ F tO0

~
Pr~f Cycles Hours

TI PD

.TIME
(a)

IT TI
__ o _ ~
I ~
,o ~
fO
/I / c

. . . . . . .

I 9
Maxax1.0 1.0 . I,~ 1000~ .~4- 100

FIG.31--StructuralLifePrediction.
appears possible that failure could occur threshold-intensity values and then
on the (B + 1) cycle. verify (through prolonged-time specimen
If, on the other hand, the cycles were cyclic tests) that time at load is not of
applied with little time at maximum major significance below the threshold
cyclic stress, it appears that the total of value. In application of the data to
A cycles could be realized. It is hypothe- fatigue21ife estimation, the maximum
sized that below the threshold K-value, allowable stress intensity would be
the time at sustained stress has little or limited to the threshold value as de-
no effect on cyclic life. Above the termined for the material in question
threshold value there will be an interac- and for the applicable service environ-
tion such that failure could occur any- ment. If the threshold value is very low,
where within the range of (B + 1) to as is the case for the wet 4330M steel

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TrFFANY AND MASl'ERS ON APPLIED F~CTUPm MEC~mCS 275

shown in Fig. 29, steps should certainly of the 100-hr sustained time (To to T.)
be taken to protect the material from can be read in Fig. 31(d). The maximum
the environment. allowable flaw size at time Te is then
shown by point C and represents the
The Determination of Nondestructive In- maximum allowable flaw size at the
spection AcceptanceLimits: start of the lO0-hr sustained stress
The information presented in the period. The effect of the cyclic loading
preceding paragraphs can now be used to is seen in Fig. 31(c), by moving 1000
discuss the problem of establishing non- cycles from Te to TB. Point B then
destructive inspection acceptance limits represents the maximum allowable size
if the service-life requirements are at time TB, or at the start of the 1000-
known. This might best be illustrated cycle period. This size is also the maxi-
by selecting a hypothetical pressure mum allowable size before the vessel is
vessel that is expected to encounter a placed into service. (Compared to the
rather complex loading history. The chosen service life, it can be shown that
problem then is to determine the maxi- the previous one-cycle proof test gener-
mum flaw size that can be allowed ally has a negligible effect on flaw
to exist before the initial pressure cycle growth.) Note that in this schematic
and still guarantee that the vessel will illustration, the maximum allowable
not fail during service operation. flaw size is less than that which could
As illustrated in Fig. 31(a), the as- have been present during a successful
sumed service requirement consists of proof test, and thus the proof test could
one proof-test cycle (at a stress level of not guarantee successful fulfillment of
a times the operating stress) followed by the service-life requirement.
1000 cycles and then 100 hr, both at a It should be noted that, in terms of
constant operating stress level of (~ = "percentage of critical," flaw size is
1.0). To define the minimum inspection completely independent of actual stress
standards required before the vessel is and toughness values. It is obvious that
placed into service, it is necessary to the determination of finite maximum
consider the critical flaw size (acr/Qc,)at allowable flaw sizes requires a detailed
the end of service and work backwards, knowledge of applied stresses in the
evaluating all portions of the loading various locations in the tankage, and of
profile that can cause flaw growth. the fracture toughness of the materials
The necessary data are shown in Figs. used.
31(b), (c), and (d). Figure 31(b) repre- Additionally, the foregoing example
sents a dimensionless presentation of the was simplified for purpose of illustration.
relationship of stress to flaw size shown Actual application would require con-
earlier. The ordinate now is plotted in sideration of the effects of service en-
terms of percentage of critical flaw size, vironment which, depending upon the
at operating stress. Figures 31(c) and (d) material, might significantly alter the
are abstracted from the type of flaw- flaw-growth rates assumed.
growth data also shown previously. When establishing an allowable initial
The approach is as follows: from flaw size for inspection purposes, the
Fig. 31(b), the critical flaw size at limitations of the inspection techniques
operating stress is represented as 100 should be recognized, and allowance
per cent of critical, and is the maximum should be made to account for lack of
allowed at time, To (or at the end of the specific knowledge of flaw geometry and
service life). The effect on flaw growth orientation. When there is this lack of

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276 F~cTtrgz T o r o a ~ s s TXS~LNO

definition, the worst possible flaw geom- stress-intensity magnification (K1/K~)


etry and orientation might be assumed. versus flaw spacing. Probably the most
For example, the length (L) of an indica- significant point is that there is very
tion seen in X-ray inspection could be little interaction between coplanar flaws
assumed to be the minor axis of an unless they are surprisingly close to-
eUiptically shaped internal flaw where gether.
the major axis is large with respect to
the minor axis (that is, L = 2a, Q CONCLUSIONS
1.0).
Also, in arriving at acceptance limits, The approach presented for applying
one must consider allowable spacing for fracture-specimen testing to practical

Fro. 32--Stress-Intenslty Magnification for Two Coplanar Elliptical Flaws.

internal or surface flaws (that is, aligned engineering problems is based upon the
flaws in weldments). An approximate premise that failures of complex tension-
analytical solution for the interaction of loaded structures generally originate at
elliptically shaped coplanar flaws has small cracks or crack-like flaws, and
been obtained by Kobayashi and Hall that the lives of these structures are
(10). The results are shown in Fig. 32 dependent upon the initial flaw sizes, the
along with experimental results on critical flaw sizes, and the flaw-growth
several Ladish D6AC steel specimens characteristics of the materials involved.
containing two coplanar semi-elliptical Primary emphasis has been placed on
surface flaws. These flaws were intro- thick-walled pressure vessels where the
duced in the specimens using an electrical critical flaw size is relatively small with
discharge machine and extended a small respect to the wall thickness (that is,
amount by low-stress fatigue. flaw depth -< approximately one half
The curves are plotted in terms of the wall thickness).

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TIFFANY AND MASTERS ON APPLIED FRACTURE MECHANICS 277

In view of the supporting experimental of fracture mechanics. Typical areas re-


data, it is concluded that critical flaw quiring further research are the deter-
sizes can be predicted with a reasonable mination of stress-intensity magnifica-
degree of accuracy and the stress-inten- tion associated with deep flaws (that is,
sity concept can be effectively used in flaw depths greater than one half the
the evaluation of subcritical flaw growth. wall thickness) and the associated
It has been shown that nondestructive effects on subcritical flaw growth, the
inspection requirements (allowable initial effects of cyclic spectrums and speeds on
flaw sizes) can be established using flaw growth, and the effects of combined
fracture-specimen test data, and in shear and tension stresses on both
addition it has been suggested that, for critical flaw size and subcritical growth.
pressure vessels, the conventional proof Additionally, the problems of environ-
test can be a powerful inspection tool. mental influence and strain-rate sen-
Presently there are limitations and sitivity are certainly deserving of more
areas of uncertainty in the application attention.

REFERENCES
(1) ASTM Special Committee on Fracture (6) G, R. Irwin, "Notes for May 1961 Meeting
Testing of High-Strength Metallic Ma- of ASTM Committee for Fracture Testing
terials, "Progress in the Measurement of of High-Strength Metallic Materials,"
Fracture Toughness and the Application of U.S. Naval Research Laboratory, Washing-
Fracture Mechanics to Engineering Prob- ton, D.C., May, 1961.
lems," Materials Research & Standards, Vol. (7) C. F. Tiffany and F. A. Pall, "An Approach
4. No. 3, March, 1964, p. 107. to the Prediction of Pressure Vessel Mini-
(2) J. E. Srawley and W. F. Brown, Jr., mum Fatigue Life Based Upon Applied
"Fracture Toughness Testing," see p. 133. Fracture Mechanics," Boeing Document
(3) Second Report of ASTM Special Committee D2-22437, March, 1963.
on Fracture Testing of High-Strength (8) R. H. Christcnsen and P. H. Denke, "Crack
Metallic Materials, "The Slow Growth and Strength & Crack Propagation Charac-
Rapid Propagation of Cracks," Materials teristics of High Strength Metals," ASD
Research & Standards, Vol. 1, No. 5, May, Document ASD-TR-61-207, January, 1962.
1961, pp. 389-393. (9) C. M. Hudson and H. F. Hardarth, "Effects
(4) G. E. Pellissier, "Some Microstructural of Changing Stress Amplitude on the Rate
Aspects of Maraging Steel in Relation to of Fatigue Crack Propagation in Two
Strength and Toughness," Technical Docu- Aluminum Alloys," NASA Technical Note
mentary Repolt RTD-TDR-63-4048, AF D-96, Nat. Aeronautics and Space Admin-
Materials Lab., Wright-Patterson Air Force istration, September, 1961.
Base, Ohio, November, 1963. (10) A. S. Kobayashi and I | R. Hall, "On the
(5) W. E. Anderson and P. Paris, "Evaluation Correction of Stress Intensity Factors for
of Aircraft Material by Fracture," Metals Two Embedded Cracks," Boeing Structural
Engineering Quarterly, Vol. 1, May, 1961, Development Research Memorandum No. 9,
pp. 33-44. The Boeing Co., 1963.

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STP381-EB/Apr. 1965

DISCUSSION
B. G. JOHNSONL-My comments per- and volume to affect correlation between
tain to the stress-intensity ratio concept test specimens and the actual part.
for predicting sustained load failure C. F. TIFFANY AND J. N. MASTERS
where the subcritical flaw growth mech- (authors)--One of the most important
anism might involve surface absorp- areas of uncertainty in the application
tion and subsequent diffusion to the of the stress-intensity concept is the
crack front. It has been postulated, for influence of environmental effects on
example, that surface-corrosion reactions subcritical flaw growth. In the case of
remote from a crack can result in a hydrogen cracking we agree that speci-
crack grown by liberation of hydrogen men volume and surface area could be
which diffuses to the crack front. For significant factors. This point is discussed
such mechanisms, one might expect in more detail in the panel discussion
geometrical effects such as surface area included in this symposium3
I Research engineer, The Boeing Co., Air-
plane Div.0 Wichita, Kans. J See p. 373.

278
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FRACTURE TOUGHNESS T E S T I N G IN ALLOY DEVELOPMENT
BY R. P. WEI1

SYNOPSIS
In the past five years, fracture mechanics has been used as a basis for the
evaluation of the fracture toughness of high-strength steels and other high-
strength alloys. Some of the considerations involved in the selection of plane-
strain fracture toughness as the most appropriate and significant parameter
for ultrahigh-strength alloy steel development are discussed in this paper.
The contribution of fracture mechanics to steel research and development
is illustrated by brief reviews of three investigations: (1) a study of the rela-
tionships between microstructure and toughness in quenched and tempered
low-alloy ultrahigh-strength steels, (2) an investigation of the effect of sulfur
level on the fracture toughness of AISI 4345 alloy steel, and (3) a study of
the influence of banding on fracture toughness anisotropy in a maraging
steel.

During the past few years, the demand basis and derived methods of fracture
for steels with increasingly higher toughness evaluation be capable of
strength and mechanical reliability has providing information that can be
accentuated the need for a sound and utilized in design considerations and in
practical basis for quantitative evalua- performance prediction.
tion and comparison of the fracture In 1959, a program was undertaken
toughness of high-strength metallic ma- by the U.S. Steel Corp. to investigate
terials. Mechanical property information the effects of chemical composition,
of a conventional and empirical nature microstructure, and processing variables
is no longer adequate as a guide in on the mechanical properties and tough-
planning and in assessing the results of ness of existing ultrahigh-strength steels
research and development programs in (>200 ksi yield strength) and to de-
the field of high-strength alloys. Unlike velop new and improved steels to meet
the situation for the lower-strength the growing demands. As part of this
steels that have been in use for many program, investigation of methods of
years, sufficient service experience in fracture toughness testing, based on the
the high-strength steels is not available Griffith-Irwin fracture mechanics analy-
to support translation of mechanical sis (1)2 was initiated. During the ensuing
property data into terms of design five years, the evaluation and utilization
requirements and expected service per- of fracture toughness testing procedures,
formance for various types of applica- as well as their improvement and ex-
tions. Thus, it is essential that the tension, has constituted an important
phase of the alloy steel development
1Senior technologist, Applied Research
Laboratory, U,S. Steel Corp., Monroeville, 2The boldface numbers in parentheses refer
Pa. to the list of references appended to this paper
279
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280 FRACTURE T o v 6 ~ s s TESTING

effort. Fracture testing procedures were (K~ or 9~ evaluations of ultrahigh-


evaluated and utilized in certain parts of strength steels in the form of sheet
this program; the prospect of extending ranging in thickness from 0.050 to 0.125
the range of application of these proce- in. Figure 1 and Table 1, which show
dures to other strength levels is now the effects of tempering treatment on
being considered. strength and toughness of a CEVR
AISI 4340 steel, illustrate the type of
-~ 35o data obtained) The 9: values correspond
3oo to different fracture modes (Fig. 2)
250 ranging from nearly plane-strain frac-
~" ~,oo ture (for 300 F tempering treatment) to
i plane-stress fracture (for 600F and
I ~'00 / above), as determined either by per-
==..-
g ~=
P- ooo
== :~_

i
o
I oc

sc
~. PERCENT SHEAR

! /
o '•"Jl'
300 400
l
500 600
I
700
I

TEMPERING T E M P E R A T U R E ( F )
/
O00
,I / II
F m 1,--Effect of Tempering Temperature "P~/ A' ~M g, "~ '| .r ' n g ~.t u. t.~.r. . m u~"~.t
ur.~
PLANE STRESS
on Strength and Fracture Toughness of 0.10- if~'ii~] TRANSITION ]1
In.-Thick C E V R AISI 4340 Steel.

TABLE 1--MECHANICAL PROPERTIES


E~c
versu~ F R A C T U R E T O U G H N E S S OF 0.10- /3c" Bo'ys
2
I N . - T H I C K C E V R AISI 4340 STEEL.
FIG. 2--Effect of Thickness and Fracture-
Telll- Mode Transition.
pering Yield Tensile Per
Tern- Strength, Strength, ~9 = ~ cent
pera-
ture, ks| ksi in-lb/in. Shear centage of shear estimates or by calcu-
deg F lation of the relative plastic-zone size
Oe (2,3) from the expression
300 211 330 75 0.47 20
400 214 296 275 1.80 50
500 223 263 730 4.40 80
600 222 256 1120 6.82 100 B ~rs t
700 212 238 > 1700 a > 21r 100
800 193 208 > 1400 ~ > 21r 100 where:
'=~, ;~ (0.38 r E = Young's modulus,
9~ = fracture toughness or critical
SELECTION OF FRACTURE TOUGHNESS
strain energy release rate,
PARAMETER AND T E S T
~r, = 0.2 per cent offset yield strength,
METHODS
and
B = specimen thickness.
For very practical reasons, fracture
t Unpublished data, R. P. Wei and F. J.
testing during the first two years was Laura, Applied Research Laboratory, U.S.
devoted mainly to fracture toughness S t e e l Corp,

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WEI ON TESTING IN ALLOY DEVELOPMENT 281

A transition in fracture mode occurs grams. The conditions under which


in the range 1 < fl, < 2~r (2,3). measurements are made are specific and
~, measurements, however, are of readily controlled. The significance of
very limited utility in general alloy gi~ has been established (1) and con-
steel development for the following firmed (4). A considerable amount of
reasons: effort, therefore, has been devoted to the
1. Because of the variation in frac- development of valid procedures for
ture mode discussed above, a uniform plane-strain fracture toughness evalua-
basis for comparison is not present. tion.
Adjustment of specimen thickness for Several procedures for plane-strain
each heat treatment so as to obtain a fracture toughness evaluation are cur-

300
u9
z _~ 2so

2 z~ 200

1so

z~ i/
~ 100 ASTEEL
B
TENSILESTRENGTH o 9
YIELD STRENGTH 9 9
_.__.L-,J ~0 V 9

0 I I, I I , I I I I I I I
400 600 800 I000 1200
TEMPERING TEMPERATURE, F

FIo. 3--Effect of Tempering Temperature on Strength and Fracture Toughness of Steels A and
B.

prescribed fracture mode or flo value rently in use at the Applied Research
is considered to be rather impractical. Laboratory:
2. g~ values are valid only for the 1. Tension testing of circumferen-
thickness tested. Translation of this tially notched round specimens,
information to other thicknesses is not 2. Tension testing of single-edge-
possible at the present time. notched (SEN) specimens (5) and
3. g~ values are not constant hut 3. Slow-bend testing of SEN speci-
depend on the size of the crack. mens.
On the other hand, plane-strain frac- The last two procedures utilize the notch
ture toughness (KIo or ~i~), which char- pop-in technique proposed by Krafft,
acterizes crack-growth resistance under et al (4). These procedures are comple-
the most severe conditions of practical mentary in that they permit 9ic evalua-
importance, appeared to be more suit- tion on steels over a wide range of thick-
able for use in alloy development pro- ness. Correlations among test results
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282 FRACTURE TOU6mCESS TESTING

obtained by the various procedures 0.3 to 0.5 per cent, have been thoroughly
have been made and will be reported investigated for possible application in
separately (6). high strength-to-weight structures. The
effects of tempering treatment on plane-
FRACTURE TESTING IN ALLOY strain fracture toughness (~ic) in this
DEVELOPMENT class of steels are similar. Figures 3 and
The contribution of fracture mechan- 4 show typical examples of this behavior.
ics to alloy development m a y be con- For each steel, fracture toughness re-

A 300 o ~

0 200

15o_
.! ~

~
// 4

STEEL
-- 100 C D

~:~ v,,,/ TENSILE STRENGTH 9 9


~ 50 _ v ~ ~ YIELD STRENGTH g 9
D- ~e 9 9

0 I I I I I I I I I t J
500 700 900 1100 1300
TEMPERING TEMPERATURE, F

FIG. 4--Effect of Tempering Temperature on Strength and Fracture Toughness of Steels C and
D.

T A B L E 2 - - C t t E M I C A L C O M P O S I T I O N OF S T E E L S I N V E S T I G A T E D ,
WEIGHT P E R CENT.

Steel C Mn P S Si Ni Cr Mo Y AI

A (4340 commercial) . . . . . . 0.39 0.74 0,019 0.026 0.27 1.79 0.89 0,26 ...
B (4340 CEVR) . . . . . . . . . . 0.43 0.77 0,009 0.008 0.27 1.16 0.73 0,26 ... ().'03
C (300M CEVR) . . . . . . . . . 0.42 0.74 0.005 0.006 1.60 1.87 0.83 0.37 0.10 ...
D (experimentalheat) . . . . 0.31 0.84 0.007 0.009 1.59 2.04 2.04 0.51 0.055 0.055

sidered in terms of some specific exam- mains low at low tempering tempera-
pleS. tures but abruptly increases in a critical
tempering temperature range that is
Relationships Between Microslructure and characteristic of the particular steel
Toughness in Quenched and Tempered composition. The actual level of frac-
Low-Alloy Ultra-High-Strength Ste~s: ture toughness at low tempering tem-
Quenched and tempered low-alloy peratures depends on the individual
steels, with carbon content in the range steel composition and impurity level

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WEI ON TESTING IN ALLOY DEVELOPMENT 283

o
v~
200
~~~ 9 STEEL A

0
1SO m STEEL C
u ~ --'~
~.~_ 9 STEEL D
u"7

o 100

<

I \: o
Z

0 I l J ,1 I I I
200 220 240 260 280 300 320
TENSILE STRENGTH, ksi

FIG. 5--Relationship Between Plane-Strain Fracture Toughness (glc) and Tensile Strength for
Four Steels.

350
300 o
z 250 ~~176 I

m 150 STEEL
1200 j " / T E N S I L E STRENGTH ~ C
YIELD STRENGTH V ~7
/ ~'c -a
"r IN. / PERCENT SHEAR 9 A
= SO0
O,,O
~7
W
.~176
o ~ 12

E
~. 0
I

,oo f: : .-
so

r
hi 0 I I I I 1 I I
~. ~00 400 500 600 700 800 900 I000
TEMPERING TEMPERATURE ( F )

FZG. &--Effect of Silicon on Strength and Fracture Toughness of 0.100-In.-Thick Ultrahigh-


Strength Steels.

(see Table 2). Those with lower carbon of toughness. Compared at equal tensile
(Steel D versus Steel C) and lower strength levels (Fig. 5), the abrupt
phosphorus and sulfur contents (Steel A change in fracture toughness behavior
versus Steel B) have a higher level is again apparent: above a tensile

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284 FRACTURE TOUGHNESS TESTING

1:'Io. 7--Effect of Silicon on Strength and Fracture Toughness of 0.070-In.-Thick AISI 4340
Type Ultrahigh-Strength Steels.

FIG. 8--Electron Micrograph of a Steel D FIa. 9--Electron Micrograph of ~/ Steel D


Specimen Tempered 1 Hr at 600 F (X25,000). Specimen Tempered 4 Hr at 1050 F (X25,000)

strength level of about 240 ksi, the steels B and C shows that the plane-strain
have low fracture toughness, whereas fracture toughness at a given tensile
at lower tensile strengths the toughness strength level is not improved by the
increases rapidly. Comparison of Steels addition of silicon. This had been ob-

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W E I ON TESTING IN ALLOY DEVELOPMENT 285

served previously for the fracture tough- fracture toughness at a given strength
ness of 0.100-in.-thick a and 0.070-in.- level (Fig. 5, Steels B and C), because
thick 4 ultrahigh-strength sheets (Figs. 6 the microstructural changes essential
and 7). s for improvement of toughness are in-
The systematic relationships shown hibited; although higher strengths can
in Fig. 5 created interest in the associated be retained at higher tempering tem-
microstructural changes, and conse- peratures, the balance between strength
quently a transmission-electron metal- and toughness is not improved.
lographic study was made of these steels However, attractive combinations of
after various tempering treatments, strength and fracture toughness can be
both above and below the critical tem- obtained in these quenched and tem-
pering temperature range. It was found pered low-alloy steels by tempering at
that fracture toughness is sensitively temperatures higher than conventionally
related to microstructure changes (7). used to obtain maximum yield strength.
In the region of low fracture toughness, For example, by tempering Steel B at
the martensite has a predominantly 800 F rather than in the range of 400 to
plate-like morphology. Two types of 600 F, the plane-strain fracture tough-
lattice defects are present in the marten- ness (~rc) is increased almost four times
site plates, namely, a high dislocation with an attendant sacrifice in yield
density and many microtwins. There is strength of only 15 per cent; thus ~z,
an almost continuous film of ~-carbide values of nearly 200 in-lb/in3 can be
at the martensite and twin boundaries, achieved at a yield strength level of
Fig. 8. These films appear to act as about 200 ksi.
preferred paths for crack propagation On the basis of this study, it was
through the structure either by provid- concluded that carbon strengthening
ing adjacent weak zones in the matrix alone has limited potential in the de-
or by fracturing themselves, which velopment of very-high-strength steels
would qualitatively account for the (>220 ksi yield strength) with good
low fracture toughness. Good fracture toughness. Therefore, other strengthen-
toughness develops only when certain ing mechanisms, and combinations of
important microstructural changes have mechanisms, are being actively investi-
occurred: (a) the elimination of em- gated.
brittling carbide films at the boundaries
by spheroidization, and (b) the redistri- E~ect of Sulfur on Fracture Toughness
bution and removal of lattice-defect of AISI 4345 Steels:
structure by recovery processes (Fig. 9). An adverse influence of sulfur on the
Increasing the tempering resistance of toughness of steels is generally recog-
these steels by utilizing increased nized, and the previous discussion has
amounts of certain alloyivg elements, already indicated the combined effects
such as silicon, does not lead Ln improved of sulfur and phosphorus on the fracture
toughness of the ultrahigh-strength
4Unpublished data, F. J. L a u t a ~pplied steels. However, the detailed mechanisms
Research Laboratory, U.S. Steel Corp
5 ~c results on 0.100-in.-thick material were by which sulfur affects fracture be-
obtained on 3-in.-wide centrally notched (fa- havior are not known. Therefore, an
tigue-precracked) sheet specimens. Slow crack investigation 6 has been undertaken to
extension was determined with a compliance
gage. ~c results on 0.070-in.-thiek specimens examine this problem in a more syste-
were obtained on 3-in.-wide centrally notched matic manner. A series of experimental
(p = 0.0007 in.) sheet specimens. Slow crack
extension was estimated empirically from per- 6 Unpublished data, G. E. Pellissier, Applied
centage shear (see Footnote 3 and Ref (2)). Research Laboratory, U.S. $r Corp.

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286 FRACTURE TOUGHNESS TESTING

AIS1 4345 steels, containing four differ- K~c results e (Fig. 11) clearly show an
ent levels of sulfur, was especially pre- influence of sulfur over the whole range
pared for this study. By using high- of tensile strengths.
purity starting materials, and carefully Sulfur is present in these steels in the
controlled melting procedures 7 the chem- form of isolated inclusions or grain
ical compositions and residual impurity boundary films, or both. The amount,
levels of these steels were carefully distribution, and location of the sulfur-
controlled (see Table 3). Charpy V- containing particles or films is believed
notch impact test results 6 at room tem- to be controlled primarily by the sulfur

T A B L E 3 - - C H E M I C A L COMPOSITION OF E X P E R I M E N T A L AISI 4345 STEELS,


W E I G H T P E R CENT.
Sample No. C Mn S Si Ni Cr Mo

B-1 . . . . . . . . . . . . . 0.43 0.27 0. 008 0.24 2.05 1.48 0.43


B-2 . . . . . . . . . . . . . 0.45 0.26 0,016 0.25 2.04 1.49 0.44
B-3 . . . . . . . . . . . . . 0.46 0.25 0,025 0.24 2.04 1.48 0.43
B-4 . . . . . . . . . . . . . 0.46 0.24 0.049 0.22 2.04 1.47 0.44

80]- ~ SULFUR LEVEL


"~ 30 ~ '~ ", 9 0.008 %
a- | ~\\ o o.ole~
: o | k\\ ,, o.o2s%
ta 70 a 0.049%

lop 9 o.ooe ~, ] 50
"' l o O.OIS % i
t 9 0.025 %. )
! / 'o

0200
/ I I
240 I
280 '
320 ~ " ~ 0
TENSILE STRENGTH (ksi) 30

FIG. 10--Effect of Sulfur Level on Charpy I 900 800 700 600 40


V-Notch Impact Energy of AISI 4345 Steel at I TEMPERING TEMPERATURE ( F )
Room Temperature. ~ L 2. .L J----
200 220 240 260 280 500
TENSILE STRENGTH ( k s i }
perature as a function of tensile strength
(or tempering treatment) for the four Fro. ll--lmfluence of Sulfur Level on Plane-
Strain Fracture Toughness of AISI 4345 Steel.
steels are shown in Fig. 10. It is evident
that the Charpy V-notch impact test is
not capable of delineating the influence level, but other factors, such as oxygen
of sulfur on toughness unambiguously level and solidification pattern, also
and sensitively at all stcength levels may exert important influence. Electron
for these steels. On the other hand, metallographic examination of the micro-
structures and fracture surfaces are now
Steels prepared for the U.S. Steel Corp. by being performed in the Applied Research
the Illinois Institute of Technology Research
Inst. Laboratory of the U.S. Steel Corp. and

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W E I ON TESTING IN ALLOY DEVELOPMENT 287

by various members of the Fractography of anisotropy of the material, since the


Subcommittee of the ASTM Special two types of test provide measurements
Committee on Fracture Testing of High- of fracture toughness in two different
Strength Metallic Materials. The re- principal directions in a rolled sheet or
sults of this study in conjunction with plate.
the fracture toughness test results should To test this hypothesis experimentally,
provide quantitative information that fracture toughness measurements were
will contribute to a better understanding made for the four principal planes of
of Iractvre in this type of steel. fracture in a maraging steel plate (8).
One type of specimen was used in this
Fracture Toughness Anisotropy in a study, namely, SEN tension test speci-
Maraging Steel: mens. Test specimens were cut from
Evidence that has been accumulating l~-in.-thick plate of a maraging (250)
indicates that the level of plane-strain steel (laboratory heat) which had been

TABLE 4--CHEMICAL COMPOSITION, HEAT TREATMENT, AND TENSILE


P R O P E R T I E S OF A N E X P E R I M E N T A L 18Ni-Co-Mo M A R A G I N G S T E E L .

COMPO8ITION, WEIGHT PER CENT

C Mn P S Si Ni Cr Mo Ti AI (total) N B Co Fe

--0. 013 o- oo oZ-ofooo- o s balance

HEAT TREATMENT
Solution-annealed for 1 hr at 1500 F + air cooled + aged for 3 hr a t 900 F + air cooled.

TENSILE PROPERTIES (AVERAGES OF T w o TESTS)

0.2 per cent Offset


Yield Strength, Tensile Elongation in 2 Reduction in
ksi Strength, ksi in., per cent Area, per cent

Longitudinal . . . . . . . . . . . . . . . . . 230 244 9.5 48


Transverse . . . . . . . . . . . . . . . . . . 231 244 7.0 35

fracture toughness of the 18 per cent ORIENTATION ~nc , in-'Ib/in-2


nickel - cobalt- molybdenum maraging A 245
steels calculated from surface-crack B ?.30
test results is greater (about 30 per cent) G 510
than that measured in circumferentially O 150
notched round specimen tests or in
through-thickness-crack toughness tests
(8). This rather consistent discrepancy ~_.~ ROLLING ~ 1
has raised a question as to whether the
two types of tests accurately determined
the identical toughness parameter. Ir-
wins suggested that the discrepancy is
not inherent in differences in the methods
of test and that it is rather a reflection
FIG. 12--Orientations of Fracture Toughness
s P r i v a t e communication from G. R. Irwin Specimens Cut From l~-In.-ThickPlate of Mar-
to G. E. Pellissier. aging (250) Steel.

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288 FRACTIYRE TouGnm~ss TESTING

solution-annealed for 1 hr at 1500 F merit of the fracture toughness of ultra-


and aged for 3 hr at 900 F. Chemical high-strength alloy steels. This fracture
composition and tensile properties are toughness parameter appears to be
shown in Table 4. fundamentally related to microstructure
Specimen orientation and fracture and basic mechanical behavior and may
toughness results (~,~)9 for the four differ- be utilized in structural design and per-
ent orientations are shown in Fig. 12. formance prediction. Consequently, these
The 9,~ values for the A and B orienta- methods of toughness evaluation have
tions (longitudinal and transverse) are become an integral part of the Labora-
not very different, in conformance with tory's ultra high-strength steel develop-
previous information, but the C orien- ment programs.
tation is greater by about 25 per cent. Because of practical limitations, such
~,~ for the D orientation is only about as specimen size and test-machine
60 per cent of that of the longitudinal capacity, it is very difficult to utilize
orientation. This anisotropy in fracture the present test procedures for obtaining
toughness in the maraging steel is valid fracture toughness measurements
associated with chemical segregation for steels having yield strengths below
"banding" in the material (g). This about 200 ksi. Because the fracture
anisotropy is believed to explain rea- mechanics method of assessing fracture
sonably the observed discrepancies be- toughness provides a unified basis for
tween through-thickness and surface- fracture toughness evaluation, effort is
crack test results for the maraging steels. currently being made to extend the
range of application of the method to
SIIMMARX
field strengths as low as 100 ksi. For
Fracture toughness testing, based on this purpose, a notched slow-bend test
fracture mechanics, has made some utilizing the crack pop-in technique
useful contributions to quantitative shows considerable promise.
metallurgical investigations at the Ap-
plied Research Laboratory of the U.S. Acknowledgment:
Steel Corp. The author wishes to thank F. J.
At the present time, it is believed that Lauta and G. E. Pellissier for permission
these test procedures provide the only to use their unpublished results, and A.
means for consistent and reliable assess- J. Baker for furnishing the micrographs.

REFERENCES
(1) G. R. Irwin, "Fracture Mechanics," in Naval Research Lab. Report 5486, July 27,
Structural Mechanics, Pergamon Press, 1960.
Oxford, 1960. (4) R. W. Boyle, A. M. Sullivan, and J. M.
(2) ASTM Special Committee on Fracture Krafft, "Determination of Plane-Strain
Testing of High-Strength Materials, "Frac- Fracture Toughness with Sharply Notched
ture Testing of High-Strength Sheet Ma- Sheets," Welding Researck, Vol. 27, No. 9,
terials," ASTM Bulletin, January, 1960, September, 1962, p. 428.
p. 29, and February, 1960, p. 18. (S) A. M. Sullivan, "New Specimen Design for
(3) G. R. Irwin, "Fracture Testing of High- Fracture Toughness Tests," Matoials Re-
Strength Sheet Materials Under Conditions search & Stamtards, Vol. 4, No. 1, January,
Appropriate for Stress Analysis," U.S. 1964, p. 20.
(6) R. P. Wei and F. J. Lauta, "Plane-Strain
9 ~c determinedby pop-intechnique(4,5). Fracture Toughness Evaluation Using

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WEI ON TESTING IN ALLOY DEVELOPMENT 289

Carbonitrided SEN Specimens," to be ASTM ST.P 370, Am. [oc. Testing Mats.,
pubfished in Materials Research & Standards. 1965
(7) A. J. Baker, F. J. Lauta, and R. P. Wei (8) G. E. Pellissier, "Some Microstructural
"Relationships Between Microstructure and Aspects of Maraging (250) Steel in Rela-
Toughness in Quenched and Tempered tion to Strength and Toughness," Third
Ultrahigh-Strength Steels," Structure and Maraging Steel Review Conference, WADD,
Properties of Ultrahigh-Strength Steels, Dayton, Ohio, 1963.

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F R A C T U R E T O U G H N E S S T E S T I N G AT ALCOA R E S E A R C H
LABORATORIES

BY J. G. KAUF~AN~ AND H. Y. HUNSICKER1

SYNOPSIS
At Alcoa Research Laboratories, fracture toughness determinations are
made on commercial and promising experimental alloys and tempers with
center-cracked specimens, single- and double-edge-notched specimens, and
notched round specimens. Compliance techniques are usually used to detect
the initiation of unstable crack growth. Kahn-type tear tests and sharp-
notch tension tests are used as screening tests to supplement fracture tough-
ness testing in the evaluation of the effects of composition, fabrication pro-
cedure, temper, and environment on the fracture characteristics of aluminum
alloys. Tear tests have the advantage that direct measures of the relative
amounts of energy required to propagate a crack can be obtained even for the
toughest of aluminum alloys; furthermore, the unit propagation energy from
the tear test is directly correlated with the valid values of Kc and KI,. Sharp-
notch tension tests are economical and, particularly when general yielding is
not obtained, the ratio of notch strength to yield strength provides a meaning-
ful measure of relative toughness. Specific examples are given of instances in
which these techniques have been used to: (1) determine which series of
aluminum alloys shows the most promise for the development of high-tough-
ness alloys; (2) establish optimum compositions and fabricating procedures
for specific alloys; (3) develop optimum tempers; and (4) indicate the out-
standing alloys for cryogenic applications.

The commercial a l u m i m m alloys cedures for evaluating the toughness


used in most structural applications are of these materials and, ultimately, for
so tough that low-ductility fracture, designing the toughness into critical
that is, unstable or self-propagating structures.
crack growth in elastically stressed To be able to provide reliable fracture
material, is nonexistent. However, the information, Alcoa Research Labora-
development of alloys having higher tories (ARL) have been active for m a n y
and higher strengths for aircraft and years in the fracture testing field. I t is
missile applications, where their high the purpose of this presentation to
strength must be used to the maximum relate: (1) the development of fracture-
advantage, has resulted in situations testing techniques at ARL; and (2)
where the possibility of catastrophic examples of the uses to which they have
low-ductility failure must be considered. been put in alloy-development efforts.
As a result, a need developed for pro-
' Assistant chief, Mechanical Testing Div., TEAR TESTS
and Chief, Physical Metallurgy Div., respec- After an initial survey of the problems
tively, Alcoa Research Laboratories, New
Kensington, Pa. related to evaluating the fracture char-
290
Copyright@1965 by ASTM International www.astm.org
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KAUFMAN AND HUNSICKER ON TESTING AT ALCOA LABORATORIES 291

0.001" + 0.0005" RADIUS, the test. Schematic representations of


~ x F TIP OF NOTCH +-- O.OOO5'' the curves are shown in Fig. 2, with
RO,,M CENTER LINE THROUGH HOLES
the areas considered to be associated
with initiation and with propagation of
the crack indicated. Also indicated are
the most useful parameters developed
. . . . from the test--tear strength (the maxi-
, =_. r" "~
-~ mum nominal combined direct-and-
bending stress); and unit propagation
energy.
i . | .~
This particular design of specimen was
LO.IO0" selected for several reasons. First, the
i'll; .1~:~ NO.3125'
0.3130"
O"A' specimen is small enough to be taken
2 HOLES from several orientations within almost
FiG. 1--Kahn-Type Tear Test Specimen. any aluminum alloy product, including

TEAR STRENGTH, PSI = "-P-+ MC P + ]P 4P

UNIT PROPAGATIGN ENERGY, IN "LS PER SO IN = ENERGY TO PROPAGATE A CRZ~CK


bt
I I I I [ I I J I I I

, b ~ t

i\

LOW TEAR RESISTANCE HIGH TEAR RESISTANCE

OEFORMATION, IN.

FIG. 2 - - T e a r - T e s t Load-Deformation Curves.

acteristics of aluminum alloys, ARL forgings, extrusions, and castings, as


elected to make use of a modification well as sheet and plate. Also it can con-
of the Kahn-tear test (1)* to measure veniently be tested at different tempera-
tear resistance and obtain relative tures or in various environments. A very
toughness ratings of the alloys (;.). By sharp notch is used, in place of the key-
this test procedure, the energy re- hole notch used by Kahn, because it
quired to initiate and propagate a facilitates the initiation of the crack at
crack in a specimen of the design in relatively low energy levels, increasing
Fig. 1 was determined by measuring the the ability to measure accurately the
areas under portions of the autographic energy required to propagate the crack.
load-deformation curve obtained during The large amount of energy required
= T h e boldface n u m b e r s in parentheses refer
to initiate a crack with a relatively
to the list of references appended to this paper. blunt notch overshadows and, on t h e
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292 FRACTURE TOUGHNESS TESTING

1400
LONGITUDINAL

\ TRANSVERSE
N. 1200 \
z \
\
\
_J \
'. 1000 \
_z \
\
\
\
\
800
\ r,
\ N
z \
o
-- 600
I--

\ \ \
o
0.
f-
z
m
400

200 !
, "llHn
\
\\
\
\
\\
~,1 \
,.,i \\
\1

,,! \\
\
\

,.\ ~1 \\

FIG. 3--Tear Resistance of 0.063-In. Thick Aluminum AUoy Sheet.

1600

1400 q O.OG3-IN, SHEET


(TRANSVERSE DIRECTIONI SINGLE LOT OF EACH j
k
(,.I, '%. ALLOY ANO TEMPER)
z
\
~- 1200
.J
z"
o':'~
Z
~
,,0
6061-T6 .~
~/,/ L
= .8o0 ~--o- ~ /
2
~"~o 600 I 7075-T6/

.RATE
', EVATEOTEM
ERA'OR
: /If
i -T6
200 o ~- -~:~'~--~" I "

0 I
-460"400
~
-300 -200
^ /
-I00 0 I00 200
I
300 400
TEMPERATURE, ~F

FIG. -l---Unit Propagation Energies of Some Aluminum Alloys at Various Temperatures.

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KAUFMAN AND HUNSlCKER ON TESTING AT ALCOA LABORATORIES 293

0.500" DIA.
IA.

7
60 = V NOTCH
Kt~12
NOTCH-TIP RADIt
o,ooi IN.
(o) Kt .~ 12
[b}

(c}

FIO. 5--Sharp-Notched Tension Specimens.

NOTCH-TIP RADIUS ~- 0.0005"


60"
I&" R

A---

69 "" 13/, "


J I "

14"

THEORETICAL STRESS CONCENTRATION FACTOR ~ 40


FIG. O--Sharp-Notched Tension Specimen.

autographic chart, obscures the energy values of tear strength and unit propaga-
to propagate the crack. tion energy are obtained.
The results of tear tests are greatly Unit propagation energy is used as the
dependent upon specimen size, although, primary measure of toughness from the
with specimens of the design in Fig. 1 tear test. It takes into account both
and of thicknesses in the range from the strength and the ductility of the
about 0.063 to about 0.1 in., comparable material. Tear strength is used in much

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294 FRACTtrRE TOUGHNESS TESTING

the same way as notch tensile strength --a crack--and the other dimensions
would be used, that is, on the basis of were chosen to provide the greatest
ratios of tear strength to tensile strength ability to discriminate among materials.
and to yield strength, particularly the Evaluation of the data is made through
latter. the comparison of the net strength of
The tear resistances of aluminum al- the notched specimen to the tensile
loys determined in this manner provide properties of the material. Although
a means for merit rating of alloys and many investigators use the notch-
tempers, even the most ductile combina- strength ratio as a basis for evaluation,
tions. For this purpose, comparisons the notch-yield ratio (ratio of net
may be shown in the form of bar graphs strength of notched specimen to yield
of unit propagation energy, as in Fig. 3. strength of material) provides a more
They also indicate the effects of tem- meaningful measure of the ability of a
material to deform plastically in the
2000 presence of a severe stress concentrator.
In addition, this ratio generally provides
16oo
much more consistent relative ratings
;~f 1200 when data are compared for various
notch geometries (3). The ASTM Special
g SO0 ~'
o o*
Committee on Fracture Testing of
z
u.I
High-Strength Metallic Materials has
7 600 e~Q supported this stand by citing the notch-
12)

400
yield ratio as the criterion to be used in
evaluating relative toughness in screen-
0
2O0 ing tests of sharply notched tension
9 0 LONGITUDINAL
I-- 9 TRANSVERSE specimens.3
z
o The notch tension test, like the tear
0 0,4 0,8 1.2 1.6 2.0 2.4 2,8 test, can be used for a wide range of
NOTCH-YIELD RATIO, I-IN WIDE SPECIMEN
alloys and tempers, but when general
FI6. 7--Relationship Between Notch Yield yielding takes place, the results are
Ratio and Unit Propagation Energy, 0.063-In.
Sheet. less definitive than those of the tear
tests as shown by the data in Fig. 7.
perature, as shown by the representa- When general yielding does not take
tive data in Fig. 4. place (notch-yield ratio ~1.0), there
is little scatter in the relationship be-
SHA~-NOXCH TENSION TESTS tween notch-yield ratio and unit propa-
The results of tension tests of sharply gation energy.
notched specimens have also been used
FRACTURE TOUGH~S$ TESTS
to determine the relative fracture char-
acteristics or notch toughness of alumi- Tests of wide center-slotted tension
num alloys. In most cases, notched round specimens were made at ARL almost
specimens of the design in Fig. 5(a) twenty years ago (4), but it was only
and notched sheet-type specimens of the after publication of the first report (s)
designs in Figs. 5(b) and 5(c), or, more of the ASTM Special Committee on
recently, Fig. 6 are used. Very sharp Fracture Testing of High-Strength Me-
notches (notch-tip radii <0.001 in.;
Kt > 12) are used to simulate the most ZR. H. Heyer, "Evaluation of Proposed
Tentative Method for Sharp Notch Tension
detrimental kind of stress concentrator Testing," see p. 199.

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KAUFMAN AND I-IuNsICKER ON TESTING AT ALCOA LABORATORIES 295

tallic Materials in January and Febru- where rapid crack propagation could be
ary, 1960, that ARL began to take an a potential service problem with high-
active interest in the use of fracture strength alloys.
toughness testing for the evaluation of Initial development centered on the
aluminum alloys. The test had the use of a center-notched specimen hav-
ing essentially the dimensions given in
Fig. 1 of the first report of the ASTM
Special Committee (5). The emphasis
at that time was upon the measurement
of the fracture toughness at the critical
situation, that is, at the onset of rapid
crack propagation. Early tests were made
with the ink-staining technique to meas-
ure slow crack growth. This procedure
was perfected to a rather high level by
the use of special combinations of draw-
ing and plotting inks, to provide the
proper combinations of fluidity and
stability. Later the compliance-gage
technique, in which SR-4 electrical
resistance strain gages were mounted
as clip-gages on the specimens or on
gage-length extensions as in Fig. 8,
replaced the ink-stain method of follow-
ing crack growth.
Studies were made to establish the
effect of specimen width, thickness,
and notch-tip radius on values of criti-
cal strain-energy release rate for alumi-
num alloy sheet. Concurrently with
other investigators, it was established
that uniform values of the critical frac-
ture parameters for aluminum alloys
could be established provided that: (1)
the notch-tip radius was equal to or less
t h a n - ~ of the radius of the plastic
zone (about 0.002 in. for 7075-T6);
and (2) the size of the specimen was
such that the rapid fracture took place
at nominally elastic stresses. The same
FIo. 8--Fracture Toughness Specimen in values of the critical strain-energy re-
Place for Test with SR4 Gage Units for Com- lease rate were obtained with fatigue-
pliance Measurement.
cracked and very sharply machine-
obvious advantage over any of the other notched specimens. Because of the rela-
tests available in that it provided not tive ease with which aluminum alloys
only a qualitative means for the merit could be sharply notched, it appeared
rating of materials, but also supple- unnecessary to fatigue-crack specimens.
mental design data for the situations Experiments at ARL, in agreement

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296 FRACTURE TOUGHNESS TESTING

with findings of other laboratories (S), round specimen are used, in addition
showed that the critical stress-intensity to the center-cracked specimen. The
factor, Kc, decreased with increase in single-edge-notched specimen appears
specimen thickness (Fig. 9), approaching to have the greatest versatility and has
a minimum value associated with frac- the advantage that a weU-documented
ture under wholly plane-strain condi- calibration is available (6,7). Notched
tions. It was also noted that the initia- round specimens provide an economical
tion of slow crack growth frequently way of determining Kr,, but the analy-
was associated with a short burst of sis leading to the fracture parameters
unstable crack growth (pop-in) at a is not well documented.

~Z ?o

o 60
0

6
x."
- 50
0
t.-
~J

~ 4o
I--

zW 30
Z Fo,. o 5;r.6, T6
~ 20
Ul
F-

j I0

o 0.2 0.4 0.6 0.8 1.0 1.2


THICKNESS, IN.

Fxo. 9--Fracture Toughness of 7075-T6, -T651 Sheet and Plate (Transverse).

stage where the crack driving force was Even more than in measurements of
the same as that for plane-strain frac- the critical fracture toughness, the crack-
ture. Thus if pop-in was noted in a test tip radius has been found to be a very
of a center-notched specimen, the plane- important factor in the determination
strain parameters as well as the critical of plane-strain toughness (8). Whereas
parameters could be determined from machined notches with radii in the
the test. Because of this, interest in the range of 0.0005 in. or less seem to provide
center-notched specimen continues at valid values of the critical parameters,
ARL. fatigue cracking consistently provides
Attention has been given to other lower plane-strain parameters, as shown
techniques suggested primarily for meas- by the data in Table 1. Examples of the
uring plane-strain toughness. The single- load-deformation curves obtained for
edge-notched specimen and the notched center-notched specimens with and

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T A B L E 1 - - R E S U L T S OF F R A C T U R E T O U G H N E S S T E S T S OF ~-IN. T H I C K 707~-T651
PLATE (TRANSVERSE SPECIMENS).

Type of Specimen Notch-Tip Preparation Kzr psi

Double-edge-notched ~ . . . . . . . . . . . . . . . . . . . . . . . As-machined ~ 30 400


31 400

30 900

Center-notched b . . . . . . . . . . . . . . . . . . . . . . . . . . . . As-m~ehined ~ 32 800


30 100
28 300
28 000

29 800

Fagitue-cracked' 23 000
2~ 500
26 700
24 200
23 100

24 100

Single~dge-notehed ~. . . . . . . . . . . . . . . . . . . . . . . . As-maehined a 32 600


30 800
29 700

31 000

Fatigue-cracked' 24 300
26 900

25 100

3 in. wide.
b 3 in. wide; 1-in. center slot9
3 in. wide; 1.05-in. deep slot.
Notch-tip radii _~ 0.0005 in9
9 AxiM-stress (R = 09 m a x i m u m stress ~ 20 per cent of yield strength.

~Iiiiii:~liiii:lii:~::iiiiiJJJiJiJJJJiiiiiJJJJliJJJJJI[[[i iiiiiiiiiiiiii]iiiiiiiiiil;iiiii~ ............. ;: ......

TRANSVERSE DIRECTION
[ ~ : ~ t I/4-1N.7075-T6~1 PLATE I/4- IN9 TO75-r651 PLATE
~'IN. CENTER NOTCHED SPECIMEN 3-1N..CENTER NOTCHED SPECIMEN ~

iiiiiiiiiiJiJJJiJJJiJJiiiiJJ ijijiiijjj~,iiiiijiliill~
i-[-~HIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII! 'lllllllI:l',llllllllIIIlllll[Illllllll ...... IIIII,,|,~
I-T-H-HIIIIIIIIIIIIIlIIIIIIIII[IIIlIIIIIIIIII[IIIIIIIIIIII[I
IHIIIIIIIIIIIlIIIIII[IIIIIIIIIlIIIIIIIIIIIIIIIIIIIIIII I[[
| I IH lllllllllllllIlll llIllll l llllll:Illllll IIllllllllllllll I I III f!4.,H-', I ',1 ',lllllllll-
IIIIIIIIIIIIIIIIIII~P~IIIIIIIIIIIIIII~IIIIMIIIIIIIIIIII~ ll:lllllIfIl',I 1] I I l l I ELI ~',,d[l[ IIl l ', l ltl,
H§ Ill IIIllI~'II IIIIIIIIIIIIIIII IYll
-IIIIIIIIIII~IIIIIIIIIIIIIIIIII;IIIIIIIIIIIIIIIIIIIMIIIII]
IIIIIIIIIIIIIIIII]IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII~IIIIIH
~JIIIIiIIIIIIIIIIIIIIIllIIII~IIIIIIlllIIIIIIIIII~IIIIIIII iiiiiii!~'~iiiiYi!!!!!!!!ii[i'~!!!!!!!!!!]ii~
~lilllliiiiiiiiiiiiii[iii~iiiiiiiiiiiiiiiiiU4iii!!!!!! llllllllllIlll~'lllllllllIlll~IllI]lllli-illllllllllll
z[::I~IllllI:lllIllIllllllllllllIlllllllllllllIllllIllll
ti~,illlliii[illlli~'i!!!ili!ii!!ii!iii!4iii!!iiiiiii
-iiiiiiiiiiiiii2.',,'iiiiiiilllgllilli
!Jll!!!!ilJiL~Jil!i!JJJ!iJ!!J!iJ~i!!!!ii!!Jl!!J!
?iiiiiiiiiiiiH
! ![i!:!!i ! !iiii! !i!t
: ,~" ',::: ', ~ ', ',::: ', ', ', ', ', ',: ', : ', ;~, ',: ', ', ', ', ', ~ IIl[ll',',',:',',:nu

~[iiiJiL!Tii!iJ!!!!!!iii!,'-,'i~iiilJiiiiiiiiill
..... r$................... :': i: :4 1
I~HI~-H-FrFH+H~ IIIIIIIIIII11111111111111111111111
~r~fI~:~t!!!!iiiifiiiiiiiiJlilJliiiJi.::
FIG. l O - - R e p r e s e n t s t i v e Load-Deformation Curves from Fracture T o u g h n e s s Tests.
297

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298 FRACTImE TOUOHNXSS TESTING

without fatigue cracks are shown in commercial alloys and promising experi-
Fig. 10. With the as-machined notch mental alloys, the test has not been
(Fig. 10(a)), some initial unstable extensively used for alloy development.
crack growth is indicated by a marked Cost is, of course, one factor, but there
pop-in before slow crack growth con- is a more basic problem. It is extremely
tinues. With fatigue-cracked specimens, important in all fracture toughness
the initial unstable crack growth is not testing that fracture take place at
as pronounced and comes at a lower nominally elastic stresses, that is, in
stress level, indicating a lower true value the absence of general yielding. Many
of plane-strain toughness. Thus, the aluminum alloys are too tough to de-

I I 1 I I
OPEN SYMBOLS- 16 IN, WIDE FRACTURE TOUGHNESS
~PECIMENS
" 120 - - SOLID SYMBOLS- 2 IN.WIDE FRACTURE TOUGHNESS
o SPECIMENS
o
{'~.} INDICATES TRANSVERSE DIRECTION
'<3
,5
x I00 I i
0
1.-
~ e0 t

F-
zW 60 2014-T6 0
F-
z 2020-T6 O
2020-'1"6
2024-3"86
w
6071 -T6 /I

.~ 20

0,063-1N. ALUMINUM ALLOY SHEET


I 7075-1"6
7079-'1"6
7178-T6
~7
<]
O
I---
0 t I I I
0 100 200 300 400 500 600
UNIT PROPAGATION ENERGY, I N . - L B . / I N f i

FIG. l l - - C r i t i c a l S t r e s s - I n t e n s i t y F a c t o r , K . , Versus U n i t P r o p a g a t i o n E n e r g y .

use of fatigue-cracked specimens in- velop unstable crack growth in moder-


creases the problems of detecting the ately sized specimens. Variations in
initial unstable burst of crack growth. compositions, fabrication procedures,
However, there seems little doubt that and temper frequently result in tough-
fatigue cracking is necessary in deter- nesses that fatl into this range. Further-
mining the plane-strain toughness even more, with increase in temperature, the
of aluminum alloys, and now almost all toughness of all aluminum alloys in-
K~o determinations at ARL are made creases, placing even the least ductile
with fatigue cracked specimens. of the commercial aUoys outside the
Despite the wide use of these various range where precise fracture toughness
fracture toughness tests at ARL to testing would be useful in establishing
establish the fracture parameters for toughness at elevated temperatures.

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KAUFMAN AND HUNSICKER ON TESTING AT ALCOA LABORATORIES 299

CORRELATION BETWEEN TEAR TESTS direct relation between unit propagation


AND FRACTURE TOUGHNESS TESTS energy and plane-strain toughness as
The inherent difficulties with the use shown in Fig. 12.
of the fracture toughness test for evaluat- These findings had the double effect
ing a wide range of alloys, plus the back- of: (i) increasing confidence that the
ground of information accumulated with tear test provides meaningful ratings for
the Kahn-type tear test, made it at- the alloys; and (2) providing a means for
tractive to determine whether a corre- estimating the values of fracture tough-
lation exists between data from the ness parameters from tear-test results.
two types of test. The first series of tests This added confidence, plus the prob-

70 I I I I
I FRACTURE- TOUGHNESS
n-
O o @ CENTER NOTCHED SPECIMENS
60 m n

L'
9 NOTCHED ROUND SPECIMENS
I '
>-
I- 50
N
Z
K~c2=3UPE +400
z_ 40
O3 n
m o

F-
8
-- 30
Z
v
j. '1
2O
m

Z
_.1 to [
ALUMINUM ALLOY SHEET AND PLATE
o I I I I 1
0 I00 200 300 400 500 600
UNIT PROPAGATION ENERGY,IN.-LB./IN. 2

FIG. 12--Relation Between Ki~ and Unit Propagation Energy.

to establish the extent of correlation lems in using the fracture toughness


was conducted in the time period when tests on tough materials, resulted in
center-notched specimens were being the concentration of alloy-development
tested, with the ink-stain technique to screening work on the tear test rather
measure crack growth. The results of than the fracture toughness test.
the study are shown in Fig. 11, indicat-
ing a direct correlation between critical ALLOY DEVELOPMENT
stress-intensity factor, Kc, for a given From an alloy-development viewpoint,
thickness of sheet, and unit propagation it is essential to establish a broad .under-
energy (Z). Because of the thickness standing of the effects of numerous
dependency of Kc, the correlation metallurgica] variables on strength and
would differ for each thickness. Recent toughness to serve as a guide in achiev-
testing established that there is also a ing improved combinations of these

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300 FRACTURE TOUGHNESS TESTING

mechanical properties. To do this, it is the yield strengths and unit propaga-


necessary to be able to establish a tion energy values for four commer-
reliable direct comparison of the tough- cial alloys of the AI-Mg-Mn 5000 series
nesses of a wide range of alloys and are illustrated in Fig. 13 in relation
tempers, from low-strength very high- to the magnesium contents for both
toughness materials to high-strength the annealed (-0) and cold rolled,
low-toughness materials. This has been stabilized (-H34) tempers. It is apparent
greatly facilitated by the use of tear that although the resistance to deforma-
tests, which permit evaluation of the tion, as measured by yield strength,
effects of composition, cold work, and increases continuously over this range

1600

14o6 4O
i

,,J
t~ tl
z 1200 ,,
O

-- 30 ~
n- I 0 0 0 "l-
ILl
t--
Z
bJ U.P.E.-H34 .a9 z
taJ
Z
o BOO 20
I--

~
o
er
600
! /.
or/
._I
l.U
T-
0.

i..-

z 400

200
0 I 3 4 5 6
NOMINAL Mg CONTENT, %
Fzo. 13--Yield Strengths and Unit Propagation Energy Values of Commercial 0.063-In. Sheet of
Four Aluminum-Magnesium-Manganese Alloys in Annealed (-O) and Strain Hardened, Stabi-
lized (-H34) Tempers as a Function of Nominal Magnesium Content.

heat treatment over a wide range of with increasing magnesium, the tough-
toughnesses and allow the relationships ness, as measured by unit-propagation
among these variables to he established. energy, achieves a maximum at an
These tests have been supplemented for intermediate strength level and dimin-
various purposes by other types of ishes sharply at the higher levels of
fracture tests. Some examples of the yield strength. A further reflection of
kinds of information obtained and re- decreasing toughness with increasing
lationships established are cited. strength is found in comparing the cold-
worked versus the annealed tempers.
Strain-Hardening Alloys: The effect of increasing degree of strain
As an example of the influence of hardening on the properties of the
solid solution and strain-hardening effects commercial alloy 5154 (nominally 3.5

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KAUFMAN AND HUNSICKER ON TESTING AT ALCOA LABORATORIES 301
1600 1600

N
1400 40 z 1400
z -

~ f. ,200

\
, 1200 -

w
I000 / N~ -3o ~_ s
~
~ I000
z
Z ~ w
z

_$ 8oo 20 ~ ~ soo

O 600
~-
~
~ ~oo

-- 10 1

400
~ 400

200
200 0 15 20 25 30 35 40
-0 -H32 -H34 -H36 -H38
YIELD STRENGTH, IOOOPS1
TEMPER
(INCREASING STRAIN HARDENING-a=.)
FIG. 1S--Relation Between Unit Propaga-
FIO. 14--Unit Propagation Energy of Com- tion Energy and Tensile Yield Strength of Com-
mercial 5154 Alloy 0.063-In. Sheet as a Function mercial 5154 Alloy 0.063-In. Sheet in Several
of Temper (Increasing Strain Hardening). Tempers.

2.4 I l t l l

2.0

o
,.s
,.-,,
%. A \
_J
l..,.J
_| 2o,,, - , ~ " ~':'
0 2024 -T4 0~. = ~
V 2219 - T 8 1 I~"O ~
z
ILl ~ 2219 - T 3 7 \o\ "n.,,
{:E
0.8 -0 2219-T87
e ;~024-TS6 e
n,.'
,~ i~ 2024-T81 m
I.iJ O 2014 - T 6 9 X7277-T6
I--
0.4 -o 2024-TS60 9 7079 -T6
0 2024-T86 9 7075 -T6
,~ 2020- T6 9 7178-T6
im A L C L A D
0 I I I 1 I
30 40 50 60 70 80 90~103
TENSILE YIELD S T R E N G T H - P S I

FIO. 16---Tear Strength to Yield Strength Ratio Versus Tensile Yield Strength for Commercial
lauminum Alloys.

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302 FRACTURE TOUGHNESS TESTING

per cent magnesium, 0.25 per cent of developing the highest strengths are
chromium) is demonstrated by the data of the precipitation-hardening type, and
for the various commercial tempers in those of greatest interest are the A1-Cu
Fig. 14. The unit propagation energy 2000 series and A1-Zn-Mg 7000 series.
values decrease in an approximately To obtain some guidance concerning
linear manner with increasing amounts which of these two alloy types might
of strain hardening. The relationship have greater promise for high strength
between unit propagation energy and and toughness at room temperature,
yield strength for this material as in- data from tear tests of a number of the
fluenced by extent of cold working is alloys in different tempers were plotted
illustrated in Fig. 15. as shown in Figs. 16 and 17. These data

;~ 1200
~: \<~ , ,o,,-Ts <, ~o2o-T,
tt~J t:t~ 1 7075-T6 O ~>~19"T4
\ 9 7178-T6 (~ 2014-T3 e
I000- \ 9 x7277-'r, e ~O24-T4
-~ k v 22,9-Ts,
Z~ 2219-T37
>~ ~ A 0 ~2,s-Ter
bJ 800- % % ~k O 2024-T3e"
:;P ~~ %k (D 2024 -TSI 9
to ks \ o 20,4-T~
Z ~ /% --k $ ~024-T86"
--
o r ~
~ • \ O 2024 -T86
o 2ozo-T,
~ f~ ALGLAD

400 - 8
v
0
w 200
l,,--

0 [ [ I [ I
30 40 50 60 70 80 90xlO 3
TENSILE YIELD STRENGTH - P S I

Fro. 17--Unit Propagation Energy Versus Tensile Yield Strength for Commercial Aluminum
Alloys.

These data disclose that high levels clearly indicate that at room tempera-
of toughness prevail at intermediate ture the 7000 series alloys have a dis-
contents of the solid solution-forming tinct advantage over those of the 2000
alloy dement magnesium. They are also series, and that variations in temper
indicative of little probability that for the latter merely shift the combina-
combinations of strength and toughness tion of yield strength and toughness
superior to those exhibited by the com- one direction or the other along the
mercial alloys of this type can be curves for the 2000 series alloy (9).
achieved by increasing magnesium con- Specific attention was given to the
tents only, or by introducing greater effects of variations in artificial aging
amounts of strain hardening. treatment. For 2014 for example, the
tear resistance of sheet samples w a s
Precipitation-Hardening Alloys: determined after natural aging ('1"4
The aluminum alloys that are capable temper) and after various amounts of

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KAUFMAN AND HUNSICKER ON TEST~HO AT ALCOA LABORATORIES 303

artificial aging to develop different that of the T6 temper. The results of


strength levels up to and including those these tests are summarized in Fig. 18 in
of the maximum strength T6 temper; which the unit propagation energies are
additional specimens were overaged related to the yield strengths attained
to a series of strength levels lower than during aging. The curves illustrate that

1200 I I I I g I "-
n

_J
Z IOOO
!

n~ 800
Z
uJ
Z 600
o

o. 400
0
n~
n
OVERAGED ~ ' ~ - T 6
~: 200
0
<[
n."
0
__. o I I 1 I I I
Z 2o :50 40 50 60 70 80 9 0 x I0 3
TENSILE YIELD S T R E N G T H - P S I

FIG. 18---Effects of Artificial Aging on Unit Propagation Energy 2014 Alloy.

Zn 2 I 4 516 7 8 19 IO II 12
l the strength-to-toughness relationship
Mg 1.3 2.0 2.42.6Z,83.0 3.23.33.5 3.1 differs for the underaged and overaged
I00 conditions. For a specific yield strength
o_
TENSILE lower than that of the T6 temper, under-
STRENGTH
aging provides a higher degree of tough-
g so
9
~/~ ' YIELD
STRENGTH
ness than does overaging. Information
of the type illustrated has assisted in
~
z
60
// establishing and selecting conditions of
thermal treatment for various alloys to
F-
~ 40 J/ achieve desired strength and toughness
0
combinations. Although these mechani-
Z cal property comparisons favor the
_o~: 20
naturally aged, intermediate artificially
aged, and fully aged tempers, other
o~ o characteristics such as resistance to
w 0 4 8 12 16 20
Zn + M g , % corrosion or stress corrosion, may in-
fluence the ultimate selection of temper.
FIG. 19--Tensile Properties of Experimental
Aluminum Alloy Series Containing Zinc, Mag-
nesium, 0.8 per cent Copper, 0.2 per cent Chro- High-Strength Aluminum-Zinc-Magne-
mium, 0.12 per cent Manganese in Relation to sium-Copper Alloys:
Sum of Zinc and Magnesium Content. Labora-
tory-Fabricated 0.063-In. Sheet, Heat-Treated Experimental work was undertaken
to T6 Type Temper, Tested in Longitudinal
Direction. to provide information upon which the
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304 FRACTURE TOUGHNESS TESTING
100
f throughout the series. The material was
laboratory-fabricated 0.064-in. sheet,
8o heat-treated by practices designed to
TE AR develop essentially maximum strengths.
~ RENGTH The tensile properties are plotted in
o
g 6o Fig. 19 as functions of the sum of the
l.-
zinc plus magnesium contents and in-
z~ 4o crease progressively with increasing
UA
n- YIELD alloy content. Tear tests were conducted
(nP" / STRENGTH with specimens prepared from the same
20 panels as the tension specimens. As
shown in Fig. 20, the tear strengths
increased with increasing alloy content
0
0 4. 8 12 16 20 for the first three compositions but
Zn PLUS Mg % declined progressively with further in-
Fro. 20--Tear and Yield Strength Values for crease in alloy concentration. The ratio
Experimental Alloys. of tear strength to yield strength of

2000 2,5

' 1600 2.0


~-- F-
(9 o (.9
re
LU 1200 1.5 z z
LU UJ
n," n-'
i,I I-- I-"
O3 (/)
z
o 800 1,0 0 ~ o
r -J
w LU

o
n,-
400 L ~ 0.5
fl,.
I,,-

0 0
0 4 8 12 16 20

Zn PLUS Mg,%

FIG. 21--Unit Propagation Energy Values and Tear Strength-Yield Strength Ratios for Ex-
perimcntal Alloys.

development of specific alloys having these alloys decreased continuously with


improved strength and fracture-propa- increasing alloy content as shown in
gation characteristics might be based. Fig. 21. The highest unit crack-propa-
In one phase of this work, a series of gation energy was associated with the
alloy compositions was produced from lowest strength, highest dongation,
high-purity aluminum with progressively and lowest alloy content composition of
increasing amounts of the precipitation- the series. The propagation-energy val-
hardeners, zinc and magnesium (9). ues declined sharply with increasing
Supplementary alloying additions of alloy content. At a zinc plus magnesium
copper, chromium, and manganese were content of about 10 per cent and higher,
maintained at constant percentages the elastic energy in the specimens was

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KAUm~AN AND HUNSZCKER ON TESTING AT A L C O A LABORATORIES 30.5

sufficient to propagate the crack to tionship between alloys of the nonheat-


failure so that quantitative values of treatable and heat-treatable types and
energy were not obtained, but they are the broad range of toughness over which
estimated to be less than 50 in-lb/inA the tear test can provide useful infor-
Although no differences in unit-propa- mation, another series of alloys was
gation energy values could be measured prepared and tested. This alloy series
among the alloys in this range, the tear- contained 3.4 per cent magnesium
yield ratios provided some discrimina- which, from the information presented
tion. Kr values were determined for previously, may be associated with high

2400 120

m 2000
_1 100
Io
_z
f n

~ 1600

I.i.I
Z
/ 8O
O
o
O

/
t-.-
'" 1200 60 o
'Z Z
U.l
0
I-- p-

o 800
a. _J
o
nr" ~ P.E. W
>-
11_
~ 400 2O

0." 0
0 2 4 6 8
ZINC, %

FIG. 22--Effect of Zinc Content on Yield Strength and Unit Propagation Energy of Laboratory-
Fabricated 0.063-In. Sheet Containing 3.4 per cent Magnesium, 0.8 per cent Copper, 0.20 per cent
Manganese, and 0.12 per cent Chromium, Solution Heat-Treated and ArtificiailyAged (-T6 Type)
Longitudinal Direction.

several alloys of the series having yield values of crack-propagation energy in


strengths of 85,000 psi and higher. annealed or cold-worked tempers. The
The results of these tests showed a fairly alloys of this series also contained uni-
direct correlation between K~ and tear- form contents of copper, chromium, and
yield ratio. The values ranged from K~ = manganese, but zinc contents varied
54,000 psi ~r at a yield strength of from 0 to 8 per cent. The yield strengths
86,000 psi and tear-yield ratio of 0.76 and unit-crack propagation energy values
to K~" = 26,000 psi ~r at a yield of these alloys after a heat treatment
strength of 94,000 psi and tear-yield of the T6 type are plotted in Fig. 22
ratio of 0.41. in relation to the zinc content. Since the
In order to illustrate further the rela- alloys with 2 per cent zinc or lower

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306 FRACTURE TOUGHNESS TESTING

i.4
•, " I I I I I -

o K~
m 1.0

+ o-"
I-
'~ 0.6 ,.~.. ,o .,
o O0 o~
.a ,P --~ ,

~, 0.4
r
~_ BAND FOR COMMERCIAL
o 2 0 0 0 , 6 0 0 0 ANO 7000
z %
0.2 ALUMINUM A L L O Y S
A R T I F I C I A L L Y AGED

0 I I l I I
40 50 60 TO 80 90 I00
TENSILE YIELD STRENGTH, I 0 0 0 PSI, AT - 5 2 0 " F

FIc. 23~Relationship Between Notch-Yield Ratio and Tensile Yield Strength at --320 F
0.063-In. Thick Sheet; Transverse.

1,4
I I 1 I I

1.2
U.

~J
t
k-
1.0-
,/
0.8-

0
k-
rr 0.6-
/ ,.,,,o
0
J
W
)-

U
I--
0.4-
~o~
J ~o
0
Z
0.2
K t ; 17

0 I
i I I
40 50
60 70 80 90 iO0
TENSILE YIELD S T R E N G T H , I 0 0 0 PSI, A T - 4 2 5 " F

Fro. 24--Relationship Between Notch-Yield Ratio and Tensile Yield Strength at --423 F,
0.063-in. Thick Sheet; Transverse.

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KAU~MAN AND HUNSlCKER ON TESTmO AT ALCOALABORATORIES 307

showed little or no precipitation-hard- The data points for the one exception,
erring with this heat treatment, their in the two tempers tested, plotted well
properties corresponded approximately above the rest. This suggested a su-
to those of the annealed temper. periority of this particular alloy, X7106,
With increased zinc contents, however, at the lower temperatures. Confirmation
the heat treatment provided higher of this trend by other series of tests of
strengths. The unit crack propagation this alloy and of related alloys resulted
energy values decreased progressively in a new series of zirconium-bearing
with increasing zinc content. The re- aluminum alloys for cryogenic applica-
suits obtained from this alloy series as tions where high toughness is required.
well as that previously discussed iUus-
trate the merit of tear tests in com-
parative evaluation of aluminum alloys
ranging from those that are most re- The Alcoa Research Laboratories
sistant to fracture propagation to those have been active in fracture testing of
which have the highest strengths cur- aluminum alloys for many years. Frac-
rently attainable by conventional proc- ture toughness determinations are made
essing. The information from such on commercial and promising experi
tests is being used in current research mental alloys and tempers with variotL
programs having as their objective the designs of specimen, using the compli.
improvement and development of high- ance-gage technique to detect the ini-
strength alloys for minimum weight tiation of unstable crack growth. Kahn-
structures. type tear tests and sharp-notch tension
tests have been used to supplement
Alloys for CryogenicApplications: fracture toughness testing in the evalua-
Tension tests of smooth and sharply tion of the effects of composition, fabri-
notched specimens were made of a cation procedure, temper, and environ-
series of aluminum-zinc-magnesium al- ment on the fracture characteristics of
loys at room temperature, --112, --320 aluminum alloys. Tear tests have the
and -423 F (10). The notched specimens advantage that direct measures of the
were of the design shown in Fig. 5(c), relative amounts of energy required
coinciding with the recommendations to propagate a crack can be obtained
in the First Report of the ASTM Special even for the toughest of aluminum
Committee (5). Notch-yield ratios from alloys; furthermore, the unit propaga-
these tests were plotted as a function tion energy from the tear test is directly
of tensile yield strength at --320 and correlated with Kc and K~c, Sharp-
--423 F as shown in Figs. 23 and 24. notch tension tests are economical and,
At --320 F, the data points for all but in the absence of general yielding, the
one of these alloys fall into a rather ratio of notch strength to yield strength
narrow band with data for a number of provides a meaningful measure of rela-
other commercial aluminum alloys. tive toughness.

REFERENCES
(1) N. A. Kahn and E. A. Imbembo, "A (2) A. H. Knoll and J. G. Kaufman, "Kahn-
Method of Evaluating the Transition from Type Tear Tests and Crack Toughness
Shear to Cleavage-Type Failure in Ship of Aluminum Alloy Sheet," Materials
Plate," Wdding Journal, Vol. 27, 1948, Research & Standards, Vol. 4, April, 1964,
pp. 169-s-182-s. pp. 151-155.

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308 FRACTURE TOUGHNESS TESTING

(3) E. W. Johnson and J. G. Kaufman, 'The Fracture Toughness and Using Fracture
Use of Notch-YieM Ratio to Evaluate Mechanics," Materials Research & Stand-
the Notch Sensitivity of Aluminum Alloy ards, Vol. 4, No. 3, March, 1964, pp. 107-
Sheet," Proceedings, Am. Soc. Testing 118.
Mats., Vol. 62, 1962, pp. 778-793. (6) J. E. Srawley, M. H. Jones, and B. Gross,
(4) K. O. Bogardus, G. W. Stickley, and F. M. "Experimental Determination of the De-
Howell, "A Review of Information in pendence of Crack Extension Force on
the Mechanical Properties of Aluminum Crack Length for a Single-Edge-Notch Ten-
Alloys at Low Temperatures," NACA sion Specimen," NASA TN D-2396, Nat.
TN 2082, May, 1950. Aeronautics and Space Administration,
(5) Reports of Special ASTM Committee on August, 1964.
Fracture Testing of High-Strength Me- (7) B. Gross, J. E. Srawley, and W. F. Brown,
tallic Materials: Jr., "Stress Intensity Factors for a Single-
First Report--"Fracture Testing of Edge-Notch Tension Specimen by Bound-
High-Strength Sheet Materials: A Report ary Collocation of a Stress Function,"
of A Special ASTM Committee," ASTM NASA TN D-Z395, Nat. Aeronautics and
Bulletin, No. 243, January, 1960, pp. 29- Space Administration, August, 1964.
40; No. 244, February, 1960, pp 18-28. (8) M. H. Jones and W. F. Brown, Jr., "Acous-
Second Report--"The Slow Growth tic Detection of Crack Initiation in Sharply
and Rapid Propagation of Cracks," Ma- Notched Specimens," Materials Research &
terials Research & Standards, Vol. 1, No. 5, Standards, Vol. 4, No. 3, March, 1964,
May, 1961, pp. 389-393. pp. 118-128.
Third Report--"Fracture Testing of (9) J. A. Nock, Jr. and H. Y. Hunsicker,
High-Strength Sheet Materials," Materials "High-Strength Aluminum Alloys," Jour-
Research & Standards, Vol. I, No. I1, nal of Metals, Vol. 15, No. 3, March, 1963,
November, 1961, pp. 877-885.
Fourth Report--"Screening Tests for pp. 216-224.
High-Strength Alloys Using Sharply (10) W. A. Anderson, J. G. Kaufman, and J. E.
Notched Cylindrical Specimens," Materials Kane, "Notch Sensitivity of Aluminum-
Research & Standards, Vol. 2, No. 3, March, Zinc-Magnesium Alloys at Cryogenic Tem-
1962, pp. 196-204. peratures," Advances in Cryogenic Engi-
Fifth Report--"Progress in Meusuring neering, Vol. 9, 1964, pp. 104-111.

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STP381-EB/Apr. 1965

DISCUSSION
JOSEPH I. BLIIH~t1--At the U.S. J. G. KAU~'MANAND H. Y. HUNSICEER
Army Materials Research Agency we (authors)--The authors appreciate Mr.
had the occasion to make some slow Bluhm's comment and agree with him
tearing tests on wide sheets (12 in.) of that values of unit propagation energy
aluminum alloys. We found that the determined in Kahn-type tear tests
unit-propagation energy reached a stable are not absolute measures of the steady-
level only after the crack had propa- state rate at which energy is utilized.
gated some distance. Furthermore, the As stated in the text of the paper, it
unit-propagation energy varied con- is recognized that values of unit propa-
siderably from its steady-state value. gation energy are specimen-size de-
Hence, any technique of taking the pendent. However, their primary value
total area under the load-deformation is for merit rating alloys and the ex-
curve would surely include some errors cellent correlation between unit propa-
due to these boundary effects. At this gation from the tear tests and K, or
Agency, we continually determined the Kit from fracture toughness tests pro-
unload slope of the load-deformation vides adequate confidence of their
curve at various crack lengths and ability to indicate realistic ratings.
were thus able to get the instantaneous
rate of propagation energy? See discussion of paper by Klier et al, "A
Study of Certain Factors Which Modify Slow
I Chief, Applied Mechanics Research Labora- Crack Propagation ia High Strength Sheet
tory, U.S. Army Materials Research Agency, Metal," Proceedings, Am. Soc. Testing Mats.,
Watertown, Mass Vol. 64. 1964.

309
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T H E APPLICATION OF FRACTURE TOUGHNESS T E S T I N G TO T H E
D E V E L O P M E N T OF A FAMILY OF ALLOY STEELS

BY J. S. PASCOVER, 1 M . HILL, I A N D S. J. M A T A S 1

SYNOPSIS
The use of fracture toughness in the development of the 9Ni-4Co alloy sys-
tem* is described in this paper. The primary concern during this study was the
delineation of metallurgical trends rather than the generation of quantitative
data. Thus, screening tests have been employed.
The particular test chosen for any study should have four characteristics:
1. be compatible with previous data
2. be reasonable in cost
3. reflect the section size anticipated for eventual service
4. have sufficient sensitivity to define the effects of thc variables investi-
gated.
High-strength steels were screened effectively with center fatigue precracked
specimens. The thickness of the specimens was adjusted to fit a given toughness
level. The sensitivity was greatest when the ratio of the nominal notch strength
to the yield strength was between 0.4 and 0.8.
For tough materials at strength levels of 200 ksi and lower, the determination
of valid plane-strain toughness values in the early stages of alloy and process
development is impractical due to the large size of the required specimens.
Precracked and standard Charpy impact specimens appeared to define usefully
qualitative trends. However, in the final optimization programs, plane-strain
fracture toughness specimens were used to obtain absolute fracture toughness
numbers compatible with the best known state of the art.

The past few years have seen a sub- The need for materials with high
stantial increase in the need for ultra- strength and toughness has been met in
high-strength materials. However, ultra- part by the development of several
high strength per se has little practical new alloy systems. One such series of
significance since a material must also alloys, the 9 per cent nickel-4 per
show resistance to crack propagation. cent cobalt steels, was developed at the
Although such properties as fatigue Republic Steel Research Center (l-s). a
strength, stress-corrosion resistance, and This paper will describe some of the
ease of fabrication must also be con- experience gained in the use of fracture
sidered in any application, only fracture toughness testing during the alloy
toughness will be discussed herein. development phase of the 9Ni-4Co
1Research metallurgists and supervisor, alloy system research. The examples
respectively, high strength steels, Republic described in this paper were chosen for
Steel Corp., Research Center, Cleveland, Ohio. the most part to illustrate areas of use
2The 9 per cent nickel-4 per cent cobalt
steels, which are designated as HP 9-4-X steels, a The boldface numbers in parentheses refer
are proprietory steel~ of Republic Steel Corp. to the list of references appended to this paper.
310

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PASCOVER ET AL ON DEVELOPMENT OF ALLOY STEELS 311

for fracture toughness testing where Much of the literature degcribes the
the determination of the metallurgical use of fracture mechanics in its "rigor-
trends was considered more important ous" sense. The aim of this paper, how-
than adherence to the rigor of fracture ever, is not to contribute to the science
mechanics. Specifically, the use of of fracture mechanics, but rather to
fracture toughness testing in studies of describe our experiences in the use of
the effects of heat treatment, alloy fracture toughness testing in the early
composition, melting practice, and stages of alloy development.
special processing will be described.
Selection Criteria:
TEST METHODS
No single test was found which would
Selection of the specific test method be universally applicable. Therefore
was related to the anticipated use of the type of test used was tailored to our
data and to the capability of the test to needs, and selected on the basis of its
provide information on the toughness capability for delineating metallurgical
of the material easily and economically. trends.
This is discussed in the next two sections. The final selection of the testing pro-
Anticipated Use of Data: cedure followed several guide posts:
1. The data obtained should be
From our experience in alloy develop- compatible with those previously ac-
ment it became apparent that testing cumulated.
at three levels of sophistication are 2. The state of art of the testing
required. These are: method should be far enough advanced.
(a) the use of fracture toughness 3. The test chosen should be con-
testing in the initial stages of alloy and sistent with the toughness of the ma-
process development; terial.
(b) the use of fracture mechanics in 4. The cost of the testing program
the late stages of the development; and should be reasonable.
(c) the use of fracture mechanics by
the user in order to determine param- APPLICATION OF SELECTION CRITERIA
eters which are of help to design engi-
neers. Testing of Sheet Materials at Ultrahigh-
In many cases the latter type of test- Strength Levels:
ing involves "personalized" procedures When the 9Ni-4Co program was
which are tailored to specific hardware started, emphasis was given to very
applications. Although this type of high strength (250 ksi and higher).
testing is extremely useful to the manu- Two types of sheet specimens were
facturer, it is too limited in application available for testing these high-strength
for the supplier who is primarily in- materials: One, a symmetrical edge-
terested in establishing the potentials notched specimen;4 the other, a center
of an alloy or process. fatigue precracked specimen. The lat-
The use of fracture mechanics in the ter was chosen for its simplicity and
late stages of development of an alloy adaptibility to the available equipment
system or process involves determina- at the Research Center.
tion of a limited number of absolute These specimens were primarily de-
fracture toughness parameters by rigor- signed to measure plane-stress fracture
ous techniques. A direct comparison toughness parameters; although, in
can then be made with data from other 4 Presently, this specimen is invariably
sources, fatigue precraeked (11).
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t~

TABLE I~NOTCH T O U G H N E S S * O F H P 9-4-45 AS A F F E C T E D B Y T E M P E R I N G .


(H e a t 3950701)
Ratio of
T~npering Yield Net Fracture Nominal 2a, in.
Dimensions o~ Center Fatigue Tempera- Toughness Notch Kc , ksi .V/~.. Gross Stress, Shear, Notch
Frecracked Specimenb ture, c deg F Strength, ksl Strengths ksi Strength, ksl ksi per cent Strength to
Yield Strength

0 . 0 8 0 b y 2 b y 8 in. 400 245.0 260 153.2 207 d 25.67 1.25 100 0.63
2as = 0.75 in. 500 232.0 255 188.0 210 d 114.4 1.10 100 0.81
600 220.0 241.0 183.0 217 d 114.7 1.05 100 0 .8 3

0 . 1 8 0 h y 3 b y 12 in. 400 245.0 166.0 106.2 177.3 67.3 1.70 75 0 .4 3


2a0 = 1.05 in. 500 230.0 248.5 136.8 264.6 d 88.9 1.93 100 0.~9
600 22 5.0 250.0 180.0 272.0 d 117.0 1.58 100 0.80

a Values represent averages of more t h a n two specimens.


b The definition of th e fracture t ou gh ne s s p a r a m e t e r s is given below:
where: P ~ = m a x i m u m load ~
W = w id th
t ffi thickness
2ao ffi original crack length
2a original crack length plus length of slow m o v i n g crack which was de t e rmi ne d by i n k - s t a i n i n g technique.

N e t fracture toughness s t r e n g t h P,n


t(W -- 2a)

P~
Nominal notch strength
t(W - - 2a0)

P,~
Gross stress = --
tW
All specimens were normalized a t 1600 F, austenitized a t 1450 F, oil-quenched, refrigerated a t -- 120 F0 a nd t e mpe re d a t t he indicated temperatures.
" T h c ratio of n et fracture toughness s t re ng th to yield s t r e n g t h exceeded 1.0.

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PASCOVER ET AL ON DEVELOPMENT O~ ALLOY STEELS 313

some instances, plane-strain fracture 300

toughness parameters were obtainable.


The determination of Kc and K~ re- . •
3950701 VAR C-OOX
3950831 VAR C-DOX
v 250 T--L 3352127 AI-Si-DEOX
quire a knowledge of the crack length ~ , 3950855AI.$i-OEOX + VCEM
corresponding to the load at fracture
C-DEOXIDIZED
instability. Initially it was suggested ~ 200
that a useful indication of the crack
length at fracture instability could be
obtained by introducing a staining Z [] x
~ 150 AI-Si-DEOXIDIZEDo ~
substance such as India ink into the
notch or crack before starting the test
(9). At the Research Center, however, it 100
was found early in the testing program
that this method of determining crack
instability was inaccurate and nonre- I
200
I
210 220
I230
I 240
I 250
I
producible and presently, the use of YIELD STRENGTH, KSf
staining fluids is no longer recommended
Fio. 1--The Effect of Deoxidation Practice
(1o). Since other methods for detecting on the Strength-to-Toughness Relationship in
crack instability were at their infancy HP 9-4-45 Steel Sheet. Center Fatigue Pre-
at the time this particular work was cracked Specimens, Longitudinal 0.080-in.
Sheet (20).
done, the determination of Ko values
was abandoned. Furthermore, in alloy 250 - -
and process development, it was found O 395070! VAR C-OOX
0- 3950831 VAR C-DOX
that the range where Ko can be ac- 1~] 3352127 AI-$i-DEOX
,~ 395085 AI-$;-OEOX + VCEM
curately calculated was very small, as ~g 200 - -

can be seen in Table 1. It is also apparent 9


t ............f
C-DEOXlDtZEO

that it was difficult to obtain K~ for


specimens in most heat-treated condi-
tions because of the high toughness of
the alloy system. Thus, because of K / s
limited use it was decided to use other
toughness parameters which could be o L : ~
calculated from the same type of speci-
men. The use of the net-notch strength AI-Si-DEOXIDIZED /
as a parameter was not considered as it is
subject to the same objections as that
O 200
I I
210 220
I 230
I 240
I I
250
of K~. However, the use of nominal YIELD STRENGTH, KSI
notch strengths looked more promising.
This parameter indicates the load-carry- Fzo. 2--The Effect of Deoxidation Practice
on the Strength-to-Toughness Relationship in
ing capacity of the material in the pres- HP 9-4-45 Sheet. Center Fatigue Precracked
ence of a sharp notch, and does not Specimen,Longitudinal0.180-in. Sheet (20).
require the knowledge of the length of
the crack at instability. Thus, it was greater than 0.8, the accuracy of this
easily determined experimentally. Fur- parameter also diminished. To circum-
thermore, it extended the range of vent this difficulty, one simply used a
discrimination as is seen in Table 1 for thicker specimen. As can be seen in
the 0.080-in. thick specimens. At a Table 1. the ranges of sensitivity were
ratio of notch strength to yield strength extended to higher toughness levels

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314 FRACTURE TOUOHNESS TESTING

when a 0.180-in. thick specimen was is again unable to discriminate between


used instead of a 0.080-in. thick speci- variables (see Table 2). These data would
men. imply that no difference in transverse
Another example, which shows the and longitudinal toughness exists in
advantage of testing specimens with the three heats. This example suggests
two section thicknesses, is presented in that the test has a lower limit of sensi-
Fig. 1. This example involves the study tivity at which point it loses its value.
of the effect of deoxidation practice on On the basis of these and similar data,
the toughness of HP 9-4-45 steel. It is it was decided to set a lower and upper
apparent that the 0.080-in. thick speci- bound for a given symmetrical center
mens are unable to define the effects fatigue precracked specimen. The lower
limit of the ratio of nominal notch
T A B L E 2 - - T H E 1 2 I R E C T I O N A L I T Y OF strength to yield strength (NS/YS) was
N O T C H P R O P E R T I E S OF SILICON-ALU-
M I N U M D E O X I D I Z E D ~ H P 9-4-45 S T E E L .
chosen at about 0.40, with an upper
(Heat 3352127) limit at about 0.80. When the data fell
outside this range, the thickness of the
Thickness Temper- Ratio of
of Center Notch specimen was changed. Although this
Fatigue ingb Strength
Precracked Tempera- Direction to may be costly (see Appendix I for cost
Specimen, ture, Yield analysis of different fracture toughness
m. deg F Strength
specimens), this type of testing procedure
0. 080 . . . . 400 longitudinal 0.56 offered a reliable means of defining some
transverse 0.35
of the metallurgical variables in our
0.080 . . . . 600 longitudinal 0.80 alloy and process development work.
transverse 0.50

0.180 . . . . 400 longitudinal 0.25


Testing of Tough Materials:
transverse 0.24 Tough alloys, such as HP 9-4-25
0.180 . . . . 600 longitudinal 0.39
steel, were developed in anticipation of
transverse 0.38 their application in heavy sections.
Double slag, basic electric furnace practice.
For such applications, one would like
Deoxidized by addition of silicon and aluminum. to determine plane-strain fracture tough-
b All specimens were normalized at 1600 F, ness (Kz~). Unfortunately, such testing
austenitized at 1450F, oil-quenched, refriger-
ated at - - 1 2 0 F , and tempered at indicated
often requires specimens of large size
temperatures. and involves great expense. To illustrate
the specimen sizes, for example, the
of different melting practices. There required over-all diameter of the smallest
are some indications of the difference circumferentially notched round bar
at the higher strength, that is, lower of HP 9-4-25 steel heat-treated to a
toughness. On the other hand, the 0.180- 170-ksi yield strength level and having
in. thick specimens showed a significant an anticipated KI, value of the order
difference between the vacuum carbon- of 150 ksi %/~n. is of the order of 4 in. in
deoxidized product and aluminum-silicon diameter. The minimum thickness of a
deoxidized and vacuum remelted product surface-cracked specimen is on the order
(Fig. 2). The use of only one type of of 1{ to 2 in. The minimum dimensions
specimen could have been misleading of the slow bend single-edge-notched
in this instance. specimen would be on the order of 189
Under very brittle conditions, it was in. square and about 12 in. long (11).
found that the nominal notch strength Thus, in the early stages of screening
of the material is so low that the test alloys and processes, the use of these

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PASCOVER ET AL ON DEVELOPMENT OF ALLOY STEELS 315

plane-strain fracture toughness speci- tionality of small forgings and heavy


mens is a rather impractical procedure plate because of their small size.
from a material standpoint. In order to The suggested plane-strain specimens
get an idea of the response to heat treat- are of benefit in the late stages of
ment of a given new composition, one development (10,11). The next section
needs at least five different heat-treating shows the evolution of our experience
conditions. Thus, if one uses duplicates, and will elaborate on some of the under-
this will amount to ten specimens per lying reasons for our action.
heat which would involve about 100 lb
of material (assuming that one needs a SPECIFIC EXA~LES OF THE USE OF
specimen with the following minimum FRACTURE MECHANICS IN ALLOY
dimensions--189 by 189 by 12 in. equal to AND PROCESS DEVELOPMENT
about 8 lb). This would amount to The contribution of fracture mechanics
about 150 lb of raw ]naterial for this to alloy and process development may be
type of testing per heat. In the develop-
ment of a new alloy system, one usually 250 Q UNNOTCHED
~ YIfLO STRENGTH
tests close to a hundred heats.
Notwithstanding the amount of ma-
terial as such, the other problem is that ~ 1 7 6
200
one cannot make a laboratory heat of
150 lb and expect valid results on 189
thick plate. To obtain the necessary i \,,
150 -- ~ /~ NOMINALNOICH SIRINGIH
amount of hot working, one must start /
with larger ingot cross sections than are O.IlO ~ THICK 9
,.../
feasible in a laboratory. /
To suggest an idea of the cost of ~oo A I ,it I I I I
0 300 500 700
certain of the specimens required to
TEMPERING TEMPERATURE, F
obtain quantitative data, a cost analysis
was prepared and appears in Appendix FiG. 3--The Influence of Tempering Tem-
I. The cost analysis shows that the perature on the Strength and Toughness of HP
9-4-45 Steel (Heat 3950701). Nominal Notch
cheapest Ki~ specimen is at least two Strength Determined with Center Fatigue Pre-
times as expensive as the Charpy V-notch cracked Notched Specimens.
specimen.
In view of the above considerations, considered in terms of some specific
the most efficient way to screen alloys in examples. For the most part those
the early stages at the 200-ksi strength examples were selected which would
range would be to use Charpy V-notch show the usefulness of qualitative in-
specimens. This, of course, was the stead of quantitative fracture mechanics
procedure followed during the early testing. The advantage derived from
stages of the development of an ultra- such a qualitative study is the fact that
tough 200-ksi yield-strength material. it can describe metallurgical trends
However, by the introduction of a expediently and inexpensively. Only in
fatigue crack into the specimen, the the late stages of alloy and process
sensitivity of the test can be signifi- development were all the "rigors" of
cantly increased at small additional fracture mechanics applied to obtain
cost. Such specimens, referred to as accurate quantitative fracture toughness
precracked Charpy specimens (12), are parameters (or at least to the accuracy
also very useful in determining direc- of the contemporary state of art).

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316 FRACTURE TOUGHNESSTESTING

the tempering temperature is increased,


o /~ A--336 HEAl
A-335 HEAl § S[ there is a continuous decrease in
|.00 - - [ ~ A-356 HEAT f
strength and a corresponding increase
a /.
- ,~~ ~ , . _. . , ~ in toughness. This is in contrast to
-r other carbon-strengthened steels and
o in particular to chromium-molybdenum-
nickel steels, which show a discontinuous
- 4/- 5. change of toughness with tempering
temperatures (14-17).
z 0.25 -- +o9o'/.S .
This discontinuous change in tough-
Z
ness, commonly known as 500-F em-
OZ
0 400 500 600
I 700
I
800 900 1000
I I I I
brittlement, has been attributed by
TEMPERIN~ TEMPERATURE,F some to a change in carbide structure
F1o. 4--The Effect of Siliconon the Ratio of (14,15) and by others to the presence of
Notch Strength to Yield Strength at Various certain impurities (18,19). Although, at
Temperatures, for Air-Induction Melted 9Ni-
4Co-45 C Type Steels (20). first analysis, such a conspicuous absence

T A B L E 3 - - T O U G H N E S S OF B A I N I T I C A L L Y T R A N S F O R M E D H P 9-4-45 S TEEL.
(Heat 3950831)

Dimensions of Center Fatigue Transformation Yield Strength, Nominal Notch Ratio of Notch
Precracked Specimeal Temperature'a ksi Strength, ksi Strength to Yield
deg F Strength

0.180 by 3 by 12 in. 500 220 202.2 0.92


600 187 170.9 0.92
700 138 156.7 1.13

0.250 by 4 by 16 in. 500 220 200 0.91


550 210 191 0.91

a All specimens were normalized at 1600 F, austenitized a t 1450 F, transferred to salt, and held
for 8 hr at indicated temperatures.

Study of Thermal Treatments on Strength of the 500-F embrittlement range could


and Toughness of HP 9445 Steel: be attributed to lack of sensitivity of
the test, this would not explain the re-
The characteristics of the 9Ni-4Co sults shown in Fig. 4. Additions of small
steels were described in great detail in a
amounts of silicon not only caused a
variety of publications (1-8). Herein, the
drastic drop in the general toughness
use of fracture mechanics in establishing level of the steel but also showed an
the role of heat treatment in determining
introduction of this embrittlement. Thus,
the toughness of HP 9-4-45 steel will be
it is more reasonable to assume that a
described. 500-F embrittlement in HP 9-4-45 steel
Effect of Tempering on the Strength and is not pronounced and only when em-
Toughness of HP 9-4-45 Steel--The in- britfling agents such as silicon are in-
fluence of thermal treatment on the troduced into the steel does the
toughness 5 of the martensitic structure
embrittlement become apparent.
of HP 9-4-45 steel is shown in Fig. 3. As It is interesting to note that, in a
6Center fatigue precracked specimens of general study of the effect of alloy
two thickneseee were used to determine the
toughness of the material. The fracture tough-
composition on the toughness of these
hess parameter used was nominal notch strength. high-strength steels, the effect of carbide-

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PASCOVER ET AL ON DEVELOPMENT Or A~T.oy S~.~.LS 317

forming elements was related to the available on tempered martensitic struc-


toughness 6 of the steel. It was found tures.
that increasing the total amount of In a sense, we regressed when we
carbide-forming elements decreased the went back to Charpy impact test spec|-
toughness of steels having carbon mens. The results are reproduced in Fig.
contents from 0.40 to 0.45 per cent
and which were heat-treated to a '~
90 - - AVERAGE VALUESFROM
THREEPRODUCTIONHEATS
240-250-ksi yield strength level. Thus, ~1
RO i
OF HP 9-4-45 STEEL

the amount of carbide-forming elements


in HP 9-4-45 steel was kept to a mini-
@ ~o
mum (2,6,2o). Furthermore, as described >" IS
above, silicon was also shown to be ,50 -- TRANSFORMED
A~ES~HORME
D ~ =~~ . .

detrimental to toughness and is there- Z 40

fore kept to a minimum in HP 9-4-45 ~ 3o


steel. -- 20 -- TEMPERED

Effect of Isothermal Transformation of


Austenite to Bainite on Strength and t J L I L J
0 I O 160 180 200 220 3 0 260
Toughness of Sheet and Plate of HP 9-4-45
Steel~Steels heat-treated to bainific YIr"LD STRENGTH,KS1

structures were reported to have better FIG. S--The Relation between Strength and
toughness characteristics at a given Impact Toughness of J-in. Thick Plate of H P
strength level than when they were 9-4-45 Steel Heat-Treated to Bainitic and Tem-
pered Martensitic Structures (5),
heat treated to tempered martensitic
structures (~-1). To check whether a 4000
similar improvement can be realized in A O 3950831 O
HP 9-4-45 steel, 0.180-in. center fatigue 9 9 3920588.
precracked specimens were prepared. 300C
The results are given in Table 3. The
notch strength above a transformation
temperature of 500 F consistently @
decreased with increasing reaction tem- ~ BAINITE
200C
perature. The drop in notch strength
was not associated with a drop in tough-
ness but with a decrease of the yield
strength of the material. The material ~[ TEMPERED MART

was too tough and exceeded the upper I-


bound of the test. To return to the Z

range of usefulness of the test, the O 160 200 240


section thickness was increased to 88in. YIELD STRENGTN r KSl

Ag~fin the ratio of notch strength to FIG. 6--A Comparison of the Unit Energy
yield strength exceeded 0.8, indicating Absorption Characteristics of HP 9-4-45 Steel
that the material was too tough for Heat-Treated to Various Strength Levels (6).
this test. There was. little advantage in
going to 89 thick specimens, because 5. The data clearly show the superior
of cost and because no similar data were toughness of the bainitic structure as
compared to martensitic structures. To
6 Again, center fatigue precracked specimens
were used to determine the toughness of the
insure greater sensitivity, fatigue pre-
material. cracked Charpy specimens were also

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318 FahCTtraE TOUGm'rESS TESTING

4O0O - - a function of the transformation temper-


ature of bainite. A re-examination of
0.180-in. thick center fatigue precracked
~ -- 0 3920588
3000 specimens showed an even greater dis-
continuity as shown in Fig. 8. Although
r~
9 the test was of no value above the 500-F
2000 -- transformation temperature, it was of
z great value at lower transformation
temperatures because the test was within
1000 - - its sensitivity range. This re-emphasizes
~ o /x
the fallacy in using any single test to
evaluate metallurgical phenomena. For
example, if the experiment had been
0 400 500 600 700
ISOTHERMAL TRANSFORMATION TEMPERATURE, F
conducted only with Charpy impact
specimens, no such embrittlement range
FIG. 7--The Effect of Transformation Tem- would have been detected (compare
peraturc on Unit Energy Absorption of the
HP 9-4-45 Steel at Room Temperature. (Speci- Fig. 5 with Figs. 6-8). This is what
mens were Austenitized and Transformed at happened, in fact, with the earlier re-
Temperatures Indicated (6).) suits on AISI 4340 steel (21).
The use of plane-strain fracture tough-
200 ness tests was out of the question because
of the toughness of the material (Charpy
190 --
impact energy -- 70 ft-lb; W/A value =
2000 in-lb/in.2). At the high transforma-
tion temperature, 600 F, the Kx, was ex-
17o
pected to be of the order of 140 ksi ~ . ,
which would involve a specimen size of
160 GTH
at least l{-in, thickness and material
with a maximum size of 1-in. thickness
1SO was available. Slow bend single-edge-
notched specimens 0.875 in. square
140 exhibited substantial general yieldingY

130 The Effects of Anisotropy:


400 500 600
ISOTHERMAL REACTION TEMPERATURE-F Another important aspect to be con-
FIG. 8--The Effect of Duplex Structures on
sidered in the evaluation of a material or
the Notch Properties of a 9Ni-4Co-38C Steel process is the amount of variation in
(Heat 3950704). Longitudinal Center Fatigue toughness with orientation in the final
Precracked Notched Specimens of 0.180-in.
Thickness (6). product. Since failure will often occur
along planes and directions of weakness,
it is mandatory that the anisotropy oi
tested. The results are shown in Fig. 6; crack-growth resistance be explored.
in general, they show the same trends. Sheet--A typical example of such
However, the discontinuous change studies on sheet material can be made of
around the martensite transition (Ms) a study on hot-cold-worked product of
temperature was disconcerting. This can HP 9-4-45 steel. This process consists of
be seen better in Fig. 7, when the pre-
cracked Charpy data were replotted as Unpublished research, Republic Steel Corp.

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PASCOVER ET AL oN DEvELoPMENT OY ALLOY STEELS 319

350
HP 9.4-45
of grain refinement and distortion occurs

300 ~ 1 HOUR AT 400F


SILE STRENGTH
as a result of this process. The amount
of toughness variation consequent to
this grain distortion is obviously of
LONG. & TRA~ ~ . ~
2SO ~ YIELDSTRENGTH
commercial and scientific importance.
Figure 9 shows the effect of deformation
O 200 on strength and toughness (25). It is
i LONG.qL.. '~'
apparent that anisotropy does exist
1t0 ~. ~ ~ ~ ~ ~ i ~ NOMINAL NOTCH and is a function of the amount of
STRENGTH deformation.
10r
Center fatigue precracked specimens
were selected on the basis of convenience,
I 1 I I the state of art, and the then-prominent
2U 40 60 IO hope that design data could be obtained
AMOUNT OF D E F O e M A T I O N , in such a fashion.
Fzr 9--The Influence of the Amount of Plate and Forgings--The anisotropy
Hot-Cold Workingon the Anisotropyof Strength observed in heavy sections is often
and Toughnessof HP 9-4-45 Steel (25). more severe than that seen in sheet
product. Two studies of such an effect
I AC~_
O m.. ~ TRANS.
LEGENDNORMAL I
performed with different testing pro-
180 TRANS. PARALLEL cedure are reported below:
LONG. PARALLEL
v 18Ni-Co-Mo Maraging (250) Slab
z" 160
0
Material--The effects of directionality
on the toughness of an 18Ni-Co-Mo
~ |40 (250) slab of dimensions 4 by 16 by 30
-r in. were evaluated using center fatigue
~ 120 precracked specimens of varying thick-
Z
ness. s Figure 10, in which nominal
~ 100 notch strength is plotted versus specimen
0 thickness for three crack-growth direc-
Z I 1 I I I I tions, shows the results of this study.
0 0.10 0.18 0.26
From a metallurgical standpoint, it
SPECIMENTHICKNESS, INCHES appears that such anisotropy does exist,
FIo. 10--Nominal Notch Strength as a Func- a finding which has recently been con-
tion of Specimen Thickness and Orientation in a firmed by Pellisier et al (26).
Forged Slab (4 by 16 by 30 in.) of 18Ni-Co-Mo For the purposes of this paper, how-
(250) Maraging Steel. Nominal Notch Strength
was Determined on Center Fatigue Precracked ever, these data display several rather
Notched Specimens (see footnote 8). interesting characteristics. First, the abil-
ity of the test to differentiate between
the deformation of austenite prior to directions is a function of specimen
transformation and is similar in some thickness with this capability impaired
respects to the so-called ausforming at both the high and low toughness
procedure. Much has been written on extremes. Furthermore, in order to ob-
the mechanism of the property changes tain specimens of valid size, the original
resulting from this procedure and some material had to be of a size which was
controversy still exists (22-24). It is completely inconsistent with the plane-
clear, however, that when the deforma- 8 Private communication from W. F. Barclay,
tionis unidirectional, a significant amount Republic Steel Research Center.

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320 FI~CTUP.E TOUGHNESS TESTING

stress specimen used. Stated in other Republic 9-4-20 (Chromium-Molyb-


terms, the results of the tests were not denum) Plate and Billet Product--In this
applicable to hardware which might case, material from production-sized
utilize such 4 by 16 by 30-in. sections heats of this experimental alloy was
and the material used had a signifi- evaluated with respect to variation of
cantly different metallurgical history toughness with product-section size and

TABLE 4 - - T H E TOUGHNESS OF R E P U B L I C 9-4-20 (Cr, Mo) S T E E L AS I N F L U E N C E D


BY S E C T I O N SIZE, POSITION, A N D O R I E N T A T I O N .
(Heat 3930785)
Section Thickness, in, OrieutaliQ~~ Positionb W / A ~ in.4b/im~

0.550 plate . . . . . . . . . . . . . . . . . . . . . . . . . . . RW surface 3150


WR surface 1900

1.00 plate . . . . . . . . . . . . . . . . . . . . . . . . . . . . WR surface 1750

2.25 plate . . . . . . . . . . . . . . . . . . . . . . . . . . . . RW surface 3540


WT surface 2973
WR surface 2949
TR surface 3085

RW center 3233
WT center 3263
WR center 3159

2.25 by 2.25 forged square billet . . . . . . . . longitudinal surface 3636


transverse surface 2480

longitudinal center 3255


transverse center 2724

4 by 4 forged square billet . . . . . . . . . . . . . . longitudinal surface 3574


transverse surface 2338

longitudinal center 3458


transverse center 2414

Orientation symbol key:


First letter =ffi specimen axis direction
Second letter -- direction of crack propagation, where:
R •, rolling direction
W = width direction
T ffi thickness direction
Specimen notch location.
c W / A is the energy absorption per unit area of the fracturing surface (IS).
NOTE: All specimens, except 0.550-in. thick plate, were oil-quenched as quasi-infinite plates or
forgings.

than that which prevails in sheet prod- specimen orientation. The results of
uct. A more recent investigation of this study, carried out with precracked
similar 'effects was carried out on a Charpy impact specimens, are quoted
proprietory Republic alloy currently in Table 4. The strength data are not
designated "Republic 9-4-20 (Cr, Mo) ''9 yet available; however, hardness checks
(7). indicate that a completely martensitic
structure was maintained regardless oi
0 Experimental grade. The HP designation
will be used when this grade becomes com- section size (the specimens were taken
mercial. from heat-treated, quasi-infinite plates).

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PASCOVER ET AL ON DEVELOPMENT OF ALLOY STEELS 321

The results, with the exception of the heating (s). During the course of this
1-in. plate, show an insensitivity to study, some 125 experimental weld-
section size which is of obvious com- ments were prepared at various section
mercial importance. Furthermore, no thicknesses (0.50 to 2.25 in. thick) and
consistently large variation with position under varying degrees of restraint (unre-
or orientation is apparent. strained to "Navy Torture Test" condi-
The selection of the precracked tions). Because of the large number of
Charpy was again predicated on cost tests required, the toughness of the
and convenience. The material is too several metallurgical structures present
tough to be validly tested for Kr~ in in an as-welded plate, that is, base,
section thicknesses of less than at least heat-affected, and weld metal, was evalu-
0.875 in.~ The length of slow bend ated with standard Charpy and later.
single-edge-notched specimens, the most precracked Charpy specimens. When a
economical of material of the K~ speci- near optimum was reached, weldments
mens, would forbid testing in the short were prepared under conditions which
transverse direction. The precracked seemed to approximate the conditions
TABLE 5 - - P L A N E - S T R A I N F R A C T U R E T O U G H N E S S
OF H P 9-4-25 1-IN. T H I C K W E L D M E N T S . 9
Ratio of Notch
Joint Design Imposed Restraint ~ I c , k~i %/~.b Strength to Yield
Strength

Single U, flat back . . . . . . . . . . . . . . . . . . . . . . . none 119.3 1.4


Double U . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . none 116.8 1.4
Single U, V back . . . . . . . . . . . . . . . . . . . . . . . . backup clamps 118.6 1.4

~ The weldments were joined with the tungsten inert gas process (TIG). The filler-wire composi-
tion approximated that of the parent metal.
b Testing was done with slow bend single-edge-notched specimens, 0.875 by 0.~75 by 4 in., with
c r a c k depths of 0.25 in. The crack was located in the center of the weld-metal deposit.

Charpy specimens, on the other hand, encountered in the shop fabrication of a


are inexpensive, easily prepared, and large missile case. These results are
give information sufficient to suggest given in Table 5.
that the more rigorous procedures are, Since these tests were made to provide
in any case, probably unnecessary. data as nearly applicable to design as the
state of the art of testing allows, sow
Welding Studies: bend single-edge-notched Kr, specimens
In the manufacture of large structures were selected to evaluate the weld
such as missile cases, the weldability of a toughness. Since the notch strength
candidate material takes on an im- exceeded the yield strength by about
portance equal to that normally at- 40 per cent, rigorous values were not
tached to strength and toughness. As obtained; however, it did appear that
the HP 9-4-25 steel alloy has been shown the value of 120 ksiv~-m, obtained may
to provide an attractive base metal with be considered as conservative estimates
K~c values of the order of 120 to 140 ksi- of the actual toughness. This has since
~/rn. (3,7,2o), work was initiated on been confirmed under testing conditions
the development of a filler metal-welding in which valid K~ values of 130 ksi~/~n.
parameter system capable of producing were obtained. 1~
high strength-high toughness welds 1~ communication from D. Lovell,
with a minimum of pre- and Post- Boeing Aircraft Co,

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322 FRhCTVR~ TOUGHNESS TESTING

This example serves again to em- strated by the development of the H P


phasize the underlying philosophy of our 9-4-X alloy steels.
research efforts. When rigor can be In general, it is suggested that for
sacrificed to cost and expediency without optimization programs in which internal
loss of effect, qualitative tests are em- comparisons are the prime objectives,
ployed. When comparison with labora- less attention need be paid to rigor if
tories other than our own is required or such a situation is desirable for purely
where data which may be used in design pragmatic reasons. On the other hand,
are desired, standard and rigorous test where the resulting data are to be used
procedures are applied. in design criteria or for comparisons
with other materials, selection of stand-
SUMMARY AND CONCLUSIONS ard and rigorous tests is mandatory.

The use of fracture toughness testing Acknowledgment:


in an alloy research program at the The authors wish to express their
Republic Steel Research Center was appreciation to W. F. Brown, Jr., of
described. I t was found that careful the National Aeronautics and Space
selection of a testing method m a y lead Administration for invaluable advice in
to valid comparisons on the basis of preparing the manuscript. The authors
toughness without the considerable cost also wish to express their appreciation to
which m a y be involved in testing with K. J. A. Kundig and S. W. Poole of the
absolute rigor using sophisticated plane- Research Center of the Republic Steel
strain fracture toughness tests. The Corp. for their cooperation and as-
validity of this approach was demon- sistance.

REFERENCES
(1) S. J. Matas, M. Hill, and H. P. Munger, Structure and Pmpertles of Ultrahigh-
"Current and Future Trends for Steels Strength Steals, ASTM STP 370, Am. Soc.
with High Strength and Toughness," ASM Testing Mats., 1965.
Metals Engineering Quarterly, Vol. 3, No. 3, (7) J. S. Pascover and S. J. Matas, "Proper-
August, 1963, p. 7. ties of HP 9-4-X Alloy Steels," Fourth
(2) T. E. Perry, S. W. Poole, and S. J. Matas, Maraging Steel Project Review Confer-
"Development and Melting of an Ultra- ence, WADC, Dayton, Ohio, 1%4.
high Strength 9%Ni-4%Co Steel," Elec- (8) G. D. Ries and S. W. Poole, "Welding of
tric Furnace Proceedings, Vol. 20, 1962, 9Ni-4Co Alloy Steels," Fourth Maraging
p. 308. Steel Project Review Conference, WADC,
t3) Aerospace Materials Handbook, Vol. 1, Dayton, Ohio, 1964.
Ferrous Alloys, Syracuse University Press, (9) ASTM Special Committee on Fracture
Syracuse, N.Y., 1964. Toughness Testing of High-Strength
(4) "Manufacturing Process Development for Metallic Materials, "Fracture Testing of
High Strength Steels", Republic Steel High-Strength Sheet Materials," ASTM
Corp., ASD Project No. 8-157, Contract Bulletin, No. 243, January, 1960, pp.
AF 33(657)-1127, Interim Progress Re- 29-40; ASTM Bulletin, No. 243, Febru-
port I, July, 1963-September, 1963. ary, 1960, pp. 18-28.
(5) "Manufacturing Process Development for (10) ASTM Special Committee on Fracture
High Strength Steels," Republic Steel Testing of High-Strength Metallic Mate-
Corp., ASD Project No. 8-157, Contract rials, "Progress in Measuring Fracture
AF 33(657)-1127, Interim Progress Re- Toughness and Using Fracture Mechan-
port ]I, September, 1963-November, ics," Materials Research & Standards,
1963. Vol. 4, No. 3, March, 1964, pp. 107-119.
(6) J. S. Pascover and S. J. Matas, "Some (11) J. E. Smwley and W. F. Brown, Jr.,
Relationships Between Structure and "Fracture Toughness Testing," see p. 133.
Properties in the 9Ni-4Co Alloy System," (12) G. M. Omer and C. E. Hartbower, "Sheet

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PASCOVER ET AL ON DEVELOPMENT OF ALLOY STEELS 323

Fracture Toughness Evaluated by Charpy (19) J. M. Capus and G. Mayer, "The Mechan-
Impact and Slow Bend," Welding Journal, ical Properties of Some Tempered Alloy
(Research Supplement), Vol. 40, Sep- Martensites," Journa~ of ate Iron and
tember, 1961, p. 4055. Steel Inst., Vol. 196, 1960, p. 149.
(13) G. M. Orner and C. E. Hartbower, "Pre- (20) S. J. Matas, "Influence of Impurities and
cracked Charpy Fracture Toughness Cor- Related Effects on Strength and Tough-
relations," presented at the symposium ness of High-Strength Steels," A S M
but not published. Metals Enginee;ing Quarterly, Vol. 4,
(14) L. J. Klingler, W. J. Barnett, R. P. Frohm- No. 2, May, 1964, p. 48.
berg, and A. R. Troiano, "The Embrittle- (21) R. F. Hehemann, V. J. Luhan, and A. R.
ment of Alloy Steel at High Strength Troiano, "Influence of Bainite on Me-
Levels," Transactions, Am. Soc. Metals, chanical Properties," Transactions, Am.
Vol. 46, 1954, p. 1557. Soc. Metals, Vol. 49, 1957, p. 409.
(15) B. J. l_ement, B. L. Averbach, and M. (22) J. C. Shyne, V. F. Zackay, and D. J.
Cohen, "Microstructural Changes on Schmatz, "The Strength of Martensite
Tempering Iron-Carbon Alloys," Trans- Formed from Cold-Worked Austenite,"
actions, Am. Soc. Metals, Vol. 46, 1954, Transactions, Am. Soc. Metals, Vol. 52,
p. 851. 1960, p. 346.
(16) G. B. Espey, M. H. Jones, and W. F. (23) R. A. Grange and J. B. Mitchell, "Strength-
Brown, Jr., "The Sharp Edge Notch ening Steels by Deforming Austenite,"
Tensile Strength of Several High Strength A S M Metals Engineering Quarterly, Vol. 1,
Steel Sheet Alloys," Proceedings, Am. Soc. 1961, p. 41.
Testing Mats., Vol. 59, 1959, p. 837. (24) C. W. Marschall, "Hot-Cold Working of
(17) S. B. Espey, M. H. Jones, and W. F. Steel to Improve Strength," DMIC Re-
Brown, Jr., "Effect of Carbon Content port 192, Batten Memorial Inst., Oct. 11,
and Melting Yractice on Room Tempera- 1963.
ture Sharp-Edge-Notch Tensile Charac- (25) S. J. Matas, M. Hill, and H. P. Munger,
teristics of H-11 Modified and 300 M "Ausforming and Hot-Cold Working--
Sheet Steels," Proceedings, Am. Soc. Methods and Properties," Mechanical
Working of Steel 1, Metallurgical Soc.
Testing Mats., Vol. 60, 1960, p. 761.
Conferences, Gordon and Breach, New
(18) A. C. Haynes and W. Stevens, "The York, N.Y., 1964, Vol. 21, p. 143.
Temperature of Formation of Martensite (26) G. E. Pellissier, "Some Microstruetural
and Bainite in I_ow-Alloy Steels; Some A~pects of Maraging (250) Steel in Rela-
Effects of Chemical Composition," Journal tion to Strength and Toughness," Third
of the Iron and Steel lnst., Vol. 183, 1956, Maraging Steel Review Conference,WADC
O. 349. Dayton, Ohio, 1963.

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APPENDIX I

COST OF VARIOUS T Y P E S OF S P E C I M E N S

During the last several years over 10,000 dollar costs. In other words, a 2-in. wide
test specimens have been prepared, tested, center-notched specimen costs approxi-
and evaluated. As a result of this program, mately twice that of a conventional Charpy.
information on the relative costs of the Accordingly, if past experience indicates
various tests was obtained and is tabulated t h a t a single Charpy test cost X X dollars,
in Table 6. D a t a are given on each aspect a 2-in. wide-center notch will cost approxi-
mately 2(XX) dollars.
of the test procedure from initial material
The figures given are subject to the fol-
and rough-blank preparation to test evalua-
lowing assumptions:
tion in terms of the appropriate parameters. 1. T h a t sufficient specimens are pre-
The costs do not include estimates of pared to permit efficient machining.
professional personnel time spent in planning 2. T h a t the test procedure, regardless of
the initial work or interpreting the results. how complex or painstaking, has become
The values given are relative rather than substantially routine.
TABLE 6--FRACTURE TOUGHNESS SPECIMENS AS EMPLOYED
AT THE REPUBLIC STEEL RESEARCH CENTER.
Total Specimen Itemized Relative Costs
Cost
Type of Specimen 1'oral Charpy Heat Test
Rough Treat- Finish Prepar- T e s t Eval- Total
SpecimenCost me.st ration uation

0.252-in. round tension . . . . 1.4 1.6 0.3 1.8 0.3 1.0 0.5 5.5
~-in. fiat tension . . . . . . . . . 2.5 2.0 0.4 2.0 0.3 1.0 0.5 9.8
Standard Charpy . . . . . . . . . 1 0.8 0.3 0.8 0.6 1.0 0.5 4.0
Precracked Charpy . . . . . . . 1.1 0.8 0.3 0.8 0.9 1.0 0.5 4.3

Center Fatigue Precracked


Specimens
2-in. wide . . . . . . . . . . . . . 2.2 0.6 0.4 1.8 4.0 1.0 1.0 8.8
3-in. wide . . . . . . . . . . . . 2.3 0.8 0.4 2.0 4.0 1.0 1.0 9.2
4 in. wide . . . . . . . . . . . . 2.5 1.0 0.4 2.4 4.0 1.0 1.0 9.8
8-in. wide . . . . . . . . . . . . 5.2 4.0 0.8 6.0 6.0 3.0 1.0 20.8
12-in. wide . . . . . . . . . . . . 7.7 6.0 0.8 10.0 8.0 5.0 1.0 30.8

Single-Edge-NotchedTen-
sion
l ~ - i n , wide . . . . . . . . . . . 1.9 0.6 0.4 0.7 4.0 1.0 1.0 7.7
3-in. wide . . . . . . . . . . . . . 2.2 0.8 0.4 1.8 4.0 1.0 1.0 9.0
4-in. wide . . . . . . . . . . . . . 2.4 1.0 0.4 2.1 4.0 1.0 1.0 9.5
0.~05-in. notched round.. 3.1 1.6 0.4 2.4 6.0 1.0 1.0 12.4
Slow Bend Single-Edge-
Notched
H-in. square . . . . . . . . . . . 1.5 0.8 0.4 0.8 2.0 1.0 1.0 6.0
7/~-in. square . . . . . . . . . . . 1.8 1.6 0.4 1.2 2.0 1.0 1.0 7.2
Surface -cracked . . . . . . . . . . 1.8 0.6 0.4 1.0 3.0 1.0 1.0 7.0
Drop-Weight Tests
3-in. A m . G a s Assn ..... 1.1 2.0 0 0.2 1.0 1.0 0.3 4.5

324

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O

TABLE 7--CHEMICAL COMPOSITIONS OF HP-9-4-X STEELS DISCUSSED IN THIS PAPER.


t~
Composition, Weight per cent
Type of Alloy Heat No. Melting Practicea Size of Heat
C Mn Si Ni Cr Mo V Co
0
Republic 9-4-20
(Cr-Mo) ........ 3930785 VAR-CDOX i0,000 lb 0.19 0.25 O.O1 6.79 1.01 1.15 0.09 4.03
H P 9-4-45 . . . . . . . . 3352127 Si-A1 E . F . 70-ton 0.41 0.22 0.26 8.25 0.26 0.13 0.10 3.60 t~
H P 9-4-45 . . . . . . . . 3950855 Si-A! + V C E M 20,000 lb 0.42 0.09 0.28 8.10 0.23 0.15 0.10 3.65
H P 9-4-45 . . . . . . . . 3950831 VAR-CDOX 20,000 Ib 0.43 0.02 0.01 8.00 0.09 0.08 0.09 3.80
H P 9-4-45 . . . . . . . . 3950701 VAR-CDOX 20,000 lb 0.40 0.I1 0.01 8.84 0.32 0.32 0.08 3,82
HP 94-45 ........ 3720588 VAR-CDOX 10,000 lb 0.41 0.21 0.03 ~.00 0.34 0.28 0.12 4.00
H P 9-4-25 . . . . . . . . . . . . . . . . . . . Typical Composition 0.27 0.20 0.10 max 8.00 0.45 0.45 0.10 4.00 ~z
H P 9-4-45 . . . . . . . . . . . . . . . . . . . Typical Composition 0.43 0.20 0.10 max 8.50 0.25 0.25 0.10 4.00
R e p u b l i c 9-4-20 O
(Cr-Mo) .................. Typical Composition 0.21 0.30 0.10 max 7.25 1.00 1.00 0.10 4.00

~ E . F . = E l e c t r i c f u r n a c e ( a i r - m e l t e d a n d silicon a l u m i n u m d e o x i d i z e d ) ; V C E M = vacuum consumable electrode-melted; VAR-CDOX = vacuum


arc re-melt and carbon deoxidized. o

Go
N
t-t

tJ
ot

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STP381-EB/Apr. 1965

DISCUSSION
J. E. CrlAlln3--When Ray Decker and tions at this stage would obviously be
I were asked to prepare a paper on the wasteful and unnecessary.
role of fracture toughness testing in In the development of PH 14-8 Mo
alloy development, we contacted a num- stainless steel, D. C. Perry of Armco
ber of individuals in various research Steel Corp. found the Allison instru-
laboratories and they were most coopera- mented bend test most useful until, as
tive in replying to a questionnaire development progressed, the steel be-
which we prepared. However, after came so tough that this test was no
putting this information together and longer definitive, at which stage a pre-
drawing some general conclusions, we cracked sheet Charpy test was employed.
felt that the resultant summary did not Fatigue-cracked center-notched speci-
justify presenting a technical paper mens for K~ determination were em-
but that the findings could be better ployed only in the later stages.
presented as a short contribution to the In the development of high-strength
discussion at the symposium. titanium alloys, E. F. Erbin of Titanium
In every case history of alloy develop- Metals Corporation of America used
ment for which we obtained details, the NASA edge-notched specimen for
there was a realization from the begin- screening and investigating variables and
ning that some form of test was required the fatigue-cracked center-notched speci-
to give an index of fracture toughness men for K, determinations.
performance to supplement the con- In the development of improved low-
ventional tension test data. However, alloy steels for heavy forgings, S. Yukawa
there appeared to be an almost universal of General Electric Co., found that the
tendency to employ some relatively Charpy V-notch fracture appearance
simple test at least during the earlier transition temperature was a useful
stages of development, the more sophisti- index of effect of metallurgical param-
cated fracture toughness tests for de- eters; at a later stage, slow bend tests
termination of K, value being employed having a fatigue-cracked or a nitrided
only in the later stages. We feel that this notch were employed and, as a final
is a very realistic approach from the stage, notched disk specimens were used
point of view of keeping the expenditure for spin-bursting tests.
in man-hours to a minimum. G. K. Bhat of Mellon Institute em-
In the initial stages of evaluating the ployed the fatigue-cracked center-
potentials of a new and promising alloy notched sheet specimen and a round
system, comparatively simple tests pro- notched tension specimen at all stages in
vide sufficient discrimination to enable the development of MX-2 (a low-alloy
the best compositions to be selected for cobalt modified 4135 ultrahigh-strength
further work. To carry out K, determina- steel), and Rocoloy 270, (a low-alloy
t Research Laboratory, International Nickel cobalt-silicon modified 4340 ultrahigh-
Co., Inc, Bayonne, N. J. strength steel). A biaxial cup test was
326
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DISCUSSION ON DEVELOPMENT OF ALLOY STEELS 327

also employed for sheet. Small 3.5-in. means of evaluation. The work of Puzak
diameter deep drawn (seamless) spin- and Pellini has established that the
closed pressure vessels, 18 in. long, were Charpy V-notch impact energy is quite
also used for study of crack growth at reliable in predicting edge drop-weight
specified stress levels, crack tolerance, tear energy and explosive tear energy.
and biaxial stress enhancement. For To sum up the situation as we see it,
investigating ~- to ~-in. thick plates, a relatively simple and inexpensive test
three-point loaded notched slow bend methods are adequate for indicating
test was found useful. The part-through- fracture toughness characteristics during
thickness surface-notched tension test the early stages of alloy development.
was also used. Fatigue-cracked notches For the final evaluation of sheet alloys,
were employed throughout. the fatigue-cracked center-notched sheet
W. F. Brown, Jr., of NASA has found specimen is well established. However,
the machined, edge-notched specimen some general agreement on the best way
very satisfactory for studies involving of measuring slow crack growth and on
the optimization of composition, and for the relative merits of compliance gages
the investigation of melting, pr6cessing, and electrical resistance methods would
and heat-treatment variables. be helpful. The situation for evaluation
At Inco, in the development of im- of heavier plate material is far less satis-
proved zerolled stainless sheet alloys by factory at the present time. Much active
trace-element control, the machined, development is proceeding on a variety
edge-notched sheet specimen was used of tests such as those utilizing notched
throughout and proved a satisfactory plate tension specimens having a single
means of evaluation. In the develop- notch on one edge only; notched slow
ment of maraging steels, a round notched bend tests; and the part-through-thick-
tension specimen (0.300 in. in major ness surface-cracked plate specimens.
diameter, 0.212 in. in minor diameter, However, there appears as yet to be no
with a root radius of 0.0006 in.) was universal acceptance of any one of these
found to be a simple and effective test. tests and some question as to the relative
There were considerable advantages in merits of acoustical and electrical meth-
time-saving and economy in working ods for following the progress of the
with round bar stock in the early stages; crack. It is believed that the present
and the ratio of notched to smooth symposium should serve a most useful
tensile strength was found to be a useful purpose in clarifying this situation.
index in evaluating the effect of com-
J. S. PASCOVER, M. HILL, AND S. J.
positional and processing variables. At a
MATAS (authors).--The authors wish to
later stage, sheet was rolled from the
thank Mr. Chard for his interesting
more promising alloys and evaluated
using the machined, edge-notched ten- discussion to our paper. It is, of course,
sion test. For the lower-strength com- gratifying to see confirmation of our
positions (below about 200-ksi yield testing philosophy by so many inde-
strength) the standard Charpy V-notch pendent organizations as was indicated
impact test appears to be a satisfactory in Mr. Chard's questionnaire.

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FRACTURE TESTING OF WELDMENTS
BY J. A. KIES,t H. L. SMITH,1 H. E. Romlvs, ~ AND H. BEP.NSTEINa

SYNOPSIS
A new and improved apparatus has been designed and built for three-point
loading of bend bars. A new formula for KI, independent of Young's modulus
has been derived which fits experimental calibrations and calculations by
B. Gross with satisfactory accuracy. A formula is provided by which the re-
quirements for specimen size and notch depth can be calculated for measuring
KIr for a given yield strength of material. A number of comparisovs are shown
for the effect of rolling direction on K~c for base plate and for several different
kinds of welding. The effect of notch position on K~, is shown. The slow bend
test has advantages of adaptability and simplicity for the purpose at hand.
It seems noteworthy that the effect of directionality on Kxc in the base
plate is in the same direction but magnified in tests of the welds in the 250-ksi
yield-strength grade. For some welding procedures the Kxc for some positions
in welds was better than for the base plate with no deficiency of hardness.
Significance tests were applied to the differences between average values of
Kic. From the KI, numbers listed one may calculate the largest tolerable
surface crack corresponding to a given stress applied. The center of the weld
presents the lowest toughness of any position.

Techniques for measuring the fracture from an expense viewpoint. The present
toughness of weldments are not unique paper contains a description of a bend-
or different from those for testing base test procedure and neglects others only
plate except for simple considerations because our immediate concern is with
of adequate sampling and for studying steels for large solid propellant booster
metallurgical variables not present in rockets in which the yield strength and
the base plate. In this investigation, use the plate thicknesses are both high
of gi, (or Kto) toughness numbers was enough to make the use of bend tests
helpful because, from current evidence, convenient. A list of the detailed reasons
these numbers do not vary significantly for choosing the three-point loading
with specimen geometry. Thus the bend test for the immediate purposes is
specimens could be efficiently planned given in the Appendix. For other appli-
cations, other tests might be preferred.
1 Head, Ballistics Branch, and head, Frac- In choosing a specimen for a given task
ture Studies Section, respectively, U.S. Naval
Research Laboratory, Washington, D. C. in measuring fracture toughness, a few
i Metallurgist, Warhead and Terminal Bal- simple rules should be observed as fol-
listics Lab., U.S. Naval Weapons Laboratory, lows:
Dahlgren, Va.
t Assistant head, Advanced Development
Plans, Special Projects Office, Bureau of Weap- (a) The plastic-zone size at critical
ors, Dept. of the Navy, Washington, D. C. load should be small compared with the
328
Copyright@1965 by ASTM International www.astm.org
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/---MACHINED SLOT, ~ WIDE WITH
[ ROUNDEDBOTTOM, WAS MADETO

Lo~,.o s T Po,.Ts ~,-~ J


' lOT ~,

4 5 ~ / _._ROOTRADIUS: 0~

a = CRACK D E P T H 7

I \ '
[
Lt. LOAOII~

I0 T
8 T
~-~,T,OUE *RACK t
POINTS r I

(a) Calibration bar for determining spring constants.


(b) Test bar for ~rc values.
FIG. 1--Bend-Test Specimens.

FIG. 2--Assembly of Bend-Test Specimen and Fixtures. The Transducers Were Adapted from a
High-Magnification Averaging Compressometer. Opening Above Upper Loading Point Was In.
tended for Deflectometer Arm Formerly Used to Measure Displacement.
329

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330 FRACTURE TOUGHNESS TESTING

crack depth and with the unbroken Tim BEND SPECIMEN AND TESTING
ligament. FIXTURES
(b) The computed nominal stress The bend specimen chosen for con-
disregarding stress-concentration factor venience in testing the plate is shown
should not exceed 1.1 times the nominal in Fig. 1. The testing fixturing was
tensile yield strength. especially designed to provide self-align-

A , D__
~yg~.,~,~0 ~
Lo. ,
@
.50 ie,

0.i0_~ ~,28 ~ 1 6 0:YCLEwEL[


C-14
16
Y5

a 12.00 ~[ ~_@_~ ,,\ 4 ~


l

'2~"
Q
Fro. 3--Details of Parts for Bend-Test Apparatus. The Loading Bars Were 4340 Steel Hardened
to 48 Rockwell C. The Other Parts Were Machined from Quenched and Tempered Alloy Steel with
a Hardness of about 26 Rockwell C (STS Armor Steel). Loading Bars Were Cemented in Place x~ith
Cyeleweld C-14 Adhesive (Chrysler Corp.) or Equivalent.

(c) The machined ne~tch should be merit and security from tilting during
terminated or extended by a real crack, load application. Figure 2 shows an
most conveniently a fatigue crack. assembly of specimen and fixture in the
(d) Testing arrangements should pro- testing machine. Further details are
vide reproducible load-deflection rela- provided by Romine. 4
tions not disturbed by variable warpage In order to satisfy testing condition
in the specimen or insecure seating of
the test fixture. 4H. E. Pmmine, "Plane Strain Fracture
Toughness Measurements of Solid Booster
(e) A closed formula for K is highly Case M~teria|s," U.S. Naval Weapons Labora-
desirable. tory Repots No. 1885, Sept. 13, 1963.

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Kiss ET AL ON TESTING OF WELDMENTS 331

4 3.000
J

ll/~--SIX BRASSSCREWSANDNUTS,
~d" NO.4"40,0..50LONG
i i W
i L 2.000
~ L250~

~l
~ ~ L ~ 0.250~
--Eoz~o
0.250~
0,250- 2.00C r I

FIc. 4--Sliding Guides for Axially Centering the Test Bar. Material, 2024-T4 Aluminum Alloy.

Plate fatigue machine adapted to introduce fatigue crack at root of machined notch in bend-test
bars. Machine is stopped at intervals to inspect progress of fatigue crack. A zoom mieroscope and
ring fluorescent light are shown in position to inspect front edge of crack. Microscope is racked in
and a small first-surface mirror is held in position to inspect crack at back of notch.
FIG. 5--Fatigue Apparatus for Introducing a Crack at the Bottom of the Notch.

(d) above, a considerable effort was ex- Special attachments were made for use
pended to provide a stable fixture easily in fatiguing the notched bars so as to
lending itself to alignment and proper introduce a real crack. Figure 5 shows
centering. Details of parts for the bend the fatigue apparatus and the test spec-
test apparatus are shown in Fig. 3 and imen. Figure 6 shows the construction
sliding guides for axially centering the of the special lever arm used for gripping
test bar are shown in Fig. 4. the specimen.
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332 FRACTURE TOUGHNESS TESTING

FORMULAS AND CALIBRATION In this case the total K or stress-intensity


In general, if we can measure loads factor is not obtained by stress analysis,
and deflections with sufficient accuracy but is given by:
we can write for P , total load, and A, E
total crack area: K~2 - (1 u 2) (~'p + 9",,) .... (2a)

t ~ dCl/M)
9 2 ~A . . . . . . . . . . . (1) for plane strain. From the experimental
point of view, the derivatives of the
where 1 / M is the compliance such that compliance with respect to crack size
the elastic deflection, $, is P / M . Here would have to be independent for Eq 2

ta.~
9 4~. .
s| ~
2 I"

9F [ ~. V/". ~ / / / j / 2 " / / y
,.....,,__/
Ib I~OUl
L-2
2~ END ~[W

| HCLE$

TOP VI[W

Fxo. 6--Extension Bar for Fatigue Machine. Material,4340Steel.

we wish to consider bend bars of width, to be correct. In case these are not
B, and depth, D. Then independent, then the total stress due
to all loads would be obtained and the
pt dO~M) resulting total, K, or stress-intensity
factor determined accordingly. There
where a is crack depth. If we choose to would be no point in determining Kp
normalize with respect to plate thick- and K~, separately. If 9p and ~ are not
hess, we can write independent, then Kp and K= would
have no usefulness as separate quantities.
9ffi ~ I(P)'d(B/M)
d~ . . . . . . .
(lb) In the present paper, 9~ - 0 for the
bend bars and there is nG ambiguity.
MasO obtained approximate' expres-
Mast 5 has postulated that for the
sions for K~ and K,~ for deep notches.
Irwin 9 factors, 9p and 9= (strain-energy
His expression for K,~ is:
release rates), acting independently on a
crack and due to tensile and bending 2Pc
loads, the total, 9, is K,,, ffi BlrUllal------~t. . . . . . . . . . . . (3)

9 = 9, + 9 . . . . . . . . . . . . . (2) ' P. Mast, private communication.

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KIES ET AL O N TESTING OF W E L D M E N T S 333

where Pe is the bending moment, m, where:


on the unbroken ligament a+2l=D
a = 2UD
2m da = - 2 d l
K~ ~
B~rllJl312
Dda = -da

and The second term within the bracket of


E q 6 assures that g = 0 for a = 0
(1 -- v 2) 4m 2 without changing the dimensions of the
~t = E B"~rP. . . . . . . . . (4) bracket. The choice of exponent 3 on l

R: -- 2.o6o - /

5
- [] ,RW,N /;
o GROSS NO. 1 / O
x GROSSNO. 2 j ~
4 -- ~ ROMINE BAR 2-6 ~ v
v ROMINE BAR 2-3 ,~,~xv

a:3
_ ~..Ap-'t~ / ~

~ I 1 I I
O.l 0.2 0.5 0.4 0.5
D
'1.0 0.9 0.8 0.7 0.6 0.5
Fro. 7 - - E q u a t i o n 10 Compared with Experimental Calibrations and Calculations.

For three-point loading as used in our was made to correspond with calibration
experiments, m --- P L / 4 and data of Romine and calculations of B.
Gross e except that for the Irwin cali-
bration the second term, [l/(D/2)4], a
first-power correction, provided a much
d(BIM) (I -- vi)Ll better fit. D is the total beam depth.
da
= - -
2Ezl'
. ....... (5) Equation 6 may be rewritten as Eq 7
with the insertion of a factor, S, needed
However, simple dimensional con- to include the 1.2 Irwin factor for sur-
siderations permit us to adapt this to face notches 7 and other effects.
shallow as well as deep notches by re-
writing E q 5 a s 6 B. Gross, private communication.
7 G. R. Irwin, " T h e Crack Extension Force
~(B/M) (1 - v,)L, [1 l~ ] for a Crack at a Free Surface B o u n d a r y , "
N R L Report 51~0, U.S. Naval Research Labora-
~--~ = --~- L~ (D72). '.(6) tory, Apr. 15, 1959.

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334 FRACTURE TOUGHNESSTESTING

1.6
1.5 O - A PANEL, LONG.
9 - A PANEL, TRANS,

/
1.4 A - B PANEL, LONG.
A - B P A N E L , TRANS.
1.3, 1:3 - A WELD
9 - B WELD
1.2
UPPER LIMIT OF VALtDLTY O'nom= I.I a'ys

~ 121

0.7~ ~// ~
0.6~ ~
0.5~

0.3 - - 5~ IFROM EQ. I0')

0.2 _ _ ~ /

0.1
o/~- I I I I .I ~ I L I I
o Io "2_0 3o r 50 r 7o so 90 Ioo ilo 120 150
KIc (~ooo F,St ~ )

l,'IG. 8--LinearityBetweenKh. and NominalStress.

d(BfM) --- 4S(1-u~)IP[~ - ~ 1 .(7) R = PLiJB 2.060 r , .(10)


da rED~
and The selection of S = 1.677 was done
B for the purpose of fitting the Romine
2S(1l ~-r ~v*)L2 [" , + -~1 -b constant..(8)
- D ~L~' and other calibration data as shown in
M
Fig. 7, This figure also shows that Eq 10
Then fits the values of R as calculated by
Gross ~ well within experimental un-
certainties in calibrations. 8 Equation 10
is the same for symmetrical four-point
Since
8Good agreement between Eq 10 and a
eorreeted version of a formula by Bueeknerof
General Ele~,,trieCo. (see footnote 11) has also
been reported in a private eot~.~munioationby
t h e n for L = 2L1 a n d S = 1.667, f]arl Hartbower. Aeroiet-General Corp.

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KIES ET AL ON TESTING OF WELDMENTS 335

FIO. 9--Effect of Crack-Propagation Direction on Fracture Appearance and KI,, Source A.

bending except that L1 then is the experimental for the Romine calibra-
distance between outer and next inner tion bars 2-3 and 2-6, the values of E --
load points. We have no experimental 27 X 106 psi, v = 0.25, D - 0.750 in.,
data at present for checking Eq 10 for and L1 = 3 in. were used. For purposes
four-point loading. In obtaining R of entering the Romine data on F!g. 7,

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336 FRACTURE TOUGHNESS TESTING

Fd(B/M)] The straight line through the origin


R = 0.824 L---ff-j xl~ x representing this equation in Fig. 8
shows good agreement with Romine's
where d(B/M)/da was experimentally results. Part of the scatter shown by the
determined. open squares may be expected on the
PLASTIC-ZONE LIMITATIONS basis of microstructural variability in
welds; however, the rest of the data
Thus far Eqs 9 and 10 for ~I and KI shows the required linearity. Variations
do not include plastic-zone corrections. in S'firrs for a given KI, value reflect
Introduction of this correction compli- variations in notch depth. Variations
cates the formula considerably and it is
larger than I0 ksi ~ . in the Kz,
suggested that this is not necessary reflect real changes in toughness. Within
provided that the nominal fiber stress a fixed type of material (base metal,
at the root of the notch is kept below for example) the K~, toughness varia-
1.1 times the yield stress. The estimated
t i o ~ are believed to be due to delamina-
plane-strain plastic-zone size, 2r~, when tions. Romine's data for plate surface-
~o~ = 1.1 ~rB is about 0.04 in. U s e d the
notched specimens range in notch depth
plasticity correction would, at the ex-
only from 0.10 to 0.14 in. Within this
treme, increase K by about 10 per cent. range, no special correlation of Kx,
DEMONSTRATION 01~ LxrmAm~ BE- with notch depth was observed.
TWEEN ~ I ~ AND NOMINAL FIBER
STRESS LIMITATIONS ON SPECIMEN SIZE
AND NOTCH D m , TH
A demonstration of the necessary
lincarity between KI. (for fixed span In forecasting the required specimen
and approximately fixed notch d~men- size and notch depth, it is necessary to
sions) and nominal fibcr stress may be know in advance how high Kr, will be.
seen in Fig. 8. These data points are for Assuming that at the root of the notch
maraging steel bars from a heat differ- the nominal fiber stress is
ent from that for the bulk of this re-
port. Only specimens containing surface r = --.
] ........... (t4)
notches are shown. ~ values were com-
puted using an equation based upon a P/.I
compliance calibration. KI~ values were BaaD1
then computed from the equation
then
KIts(I -- u s) = E~t . . . . . . . . . (11)
K t -- #nom(D)tf*O.687(a - - a T ) I l L . . ( 1 6 )
If one computes K;~ using Eq 10 for
these data points, the relationship be- If the upper limit of validity is for
tween Kx, and the load, P, is:
Gnom = 1.~ (78Y
Ku = 27.95 P . . . . . . . . . . . (12)
K~ li,. ffi 0.TS6~ys(O)Z/H~- ~rl~/J..(17)
By converting the load to maximum
fiber stress at the notch root, S', and For the limiting case, Ktc = Ku u,~,
dividing by the yield strength of the
material, the expression for Kr, becomes

K~, = 93,175 ........ (13)


or

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K I E S ET AL ON TESTING OF WELDMENTS 337

T A B L E 1 - - C O M P A R I S O N OF E D G E - N O T C H E D T E A R T E S T S W I T H B E N D TESTS.

KIr .. KIe , KIe


Bar No. from Compnance Eq 10, Single-Edg~-~lotched,
Bend Test,
k~ V ~ . k~ ~ / ~ k~i V ~ .

2 .................... 79 81.2 82~ Source B Steel


3 .................... 80 81.5 81 J

hvg ............... 79.5 81.3 81.5

KIr ,
Bend Bar No. -t- o r II Eq 10, Specimen No. .j_ KIr
EKge-Notch Tear or II ksi 3/i'-~.
ksi
Plate 1 Plate 2

1-31-2 ................... 2- 67.5 V I I BA-2 2- 73.0


1-31-3 ................... 2. 67.2 V I I BA-3 1 72.0
1-31-4 ................... 2. 66.1 V I I BA-4 .L 69.0
1-31-5 ................... 2. 68.8

Avg . . . . . . . . . . . . . . . . . . . 67.4 71.3


Plate 2 Plate 1

2-31-2 ................... 11 68.8 V I I AA-2 I1 72.0


2-31-3 ................... II 67.0 V I I AA-3 I[ 75.0
2-31-4 ................... [I 68.5
2-31-5 ................... II 68.3

Avg . . . . . . . . . . . . . . . . . . 68.1 73.5

T A B L E 2 - - C O M P A R I S O N OF E D G E - N O T C H T E A R TESTS A N D B E N D TESTS.
(U. S. Steel Corp. Tests)

KI 9 , F. KIr KIe, .
3-in. Wide Central o ,
~s~Cing'e-~'~-'Notch, Eq 10,' Bend Test by
Notch, Bueckner Formula,
ksi ~q-n. ksi %/~. ksl %/i-~. ksi %/~.

77.0 77.0 85.0 82.5


79.8 83.8 82.5

Avg 78.4 Avg 84.4 Avg 82.5

A~ == 0.101D(a -- a T) . . . . . . . (18) COMPARISON OF P ~ - S T R A I N FRAC-


lira
TURE TOUGHNESS BY THE SLOW BEND
f2(a) -- (a -- a ~) has a maximum at TEST AND BY THE SINGLE-EDGE-
aid = 0.28, or a = 0.72. Thus the most NOTCHED TEST
favorable notch-depth ratio is about
Tests were made on 18 per cent nickel
0.28. However, the term (a - aT) changes
(250,000-psi strength level) maraging
by only 0.2 per cent in going from an
steel plates from I-in. thick, air-melted
aid value of 0.25 to a value of 0.30. So stock. The bend tests were made with
within this range of notch-depth ratios,
three-point loading using ] by ~ by 7.5
one may simply use the equation
in. specimens while the single-edge-
KI = 0.540a=om(D) l/= . . . . . . . . (19) notched specimens were 3 by 12 by 0.75

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338 FRACTURE TOUGHNESS TESTING

T A B L E 3--ANALYSIS OF TEST MATERIALS.


(~-Thick P l a t e , 18 P e r C e n t Nickel M a r a g i n g Steel)

A. MATERIALS COMPOSITIONS

Composition, Plates, Weight


Element
Heat X14636 Heat X53013

C ................... 0.03 0.02


Mn ................. 0.06 0.02
P ................... O 005 0. 006
S ................... 0.010 0.009
Si . . . . . . . . . . . . . . . . . . . 0.10 0.04
Ni . . . . . . . . . . . . . . . . . . 18.37 17.59
Mo ................. 4.70 4.80
Co . . . . . . . . . . . . . . . . . . 8.49 8.06
Ti .................. 0.42 0.49
A1 . . . . . . . . . . . . . . . . . . 0.13 0.07
Cu . . . . . . . . . . . . . . . . . . . . . 0.12

B. MECHANICAL PROPERTIES OF THE PLATES

Aged Properties, 915 F for 4 hr Heat X14536 Heat X$3013

H a r d n e s s , Rc . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50 to 53 . . . . . . . . . . . . . 50 to 53
0.2 per c e n t offset yield . . . . . . . . . . . . . . . . . . . . . . . 263 ksi [I . . . . . . . . . . . . 258 ksi H
248 ksi 2. . . . . . . . . . . . 268 ksi 2.
U l t i m a t e tensile s t r e n g t h ..................... 272 ksi 1[ . . . . . . . . . . . 265 ksi []
259 ksi 2. . . . . . . . . . . . 275 ksi 2.
E l o n g a t i o n in 2 in., p e r c e n t . . . . . . . . . . . . . . . . . . . 4 . 0 1[ . . . . . . . . . . . . . . 4 . 7 [I
4 . 6 2. . . . . . . . . . . . . . . 4 . 0 2-
Reduction area, p e r cent . . . . . . . . . . . . . . . . . . . . . . 30 [[ . . . . . . . . . . . . . . . . 35 [[
33 2. . . . . . . . . . . . . . . 27 2.
A n n e a l e d , 1550 F for 1 h r :
H a r d n e s s , Rc . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32.8 32.3

C. WELD ROD COMPOSITION

C ....................... 0.02% Mo . . . . . . . . . . . . . . . . . . . . . . . 4.62%


Si . . . . . . . . . . . . . . . . . . . . . . . 0.02% Al . . . . . . . . . . . . . . . . . . . . . . . . 0.09%
Mn ....................... 0.03% Ti ........................ 0.45%
S ....................... 0. 0 0 5 % H2 . . . . . . . . . . . . . . . . . . . . . . . 1.5 ppm
p ......................... 0.004~ O~ . . . . . . . . . . . . . . . . . . . . . . . . 14. O p p m
Ni . . . . . . . . . . . . . . . . . . . . . . . . 18.24~ N2 . . . . . . . . . . . . . . . . . . . . . . . . 25.0 ppm
Co . . . . . . . . . . . . . . . . . . . . . 7.90%
N o T E - - I d e n t i c a l weld rod c o m p o s i t i o n for T I G , M I G , a n d s h o r t arc welding. Weld rod d r a w n
to different d i a m e t e r s .

D, CORRESPONDENCE BETWEEN PLATE AND HEAT NUMBERS, WELD METHOD,


AND ROLLING DIRECTION

Plate No. Heat No. Rolling Direction Orientation


NRL Plate No. Weld Method (U. S. Steel (U. S. Steel
Co.) Co.) Weld Bead Bar Length

1 .............. TIG 42298 X14636 2. [[


2 .............. TIG 42298 X14636 [[ 2.
5 .............. MIG 42298 X14636 2. [[
6 ............. MIG 156872 X53013 [[ 2.
11 . . . . . . . . . . . . . . s h o r t arc 156872 X53013 2. [[

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KIES ET AL ON TESTING OF W E L D M E N T S 339

in. in size, loaded in tension with pin- maraging steel of the 280,000-psi yield
holes at the W/2 position. Results are strength level gave the results shown in
given in Table 1.9 The material used in Table 2. The single-edge-notched speci-
this comparison was previously re- mens were loaded in tension with the
ceived from an outside source different pinholes at w/3 position. K~c - - E ~ i e /

TABLE 4--NRL PLATES 1 AND 2.


(Kxc V a l u e s f o r B a s e P l a t e , E q 10, a n d V i s u a l N o t c h D e p t h , a, U s e d . )

Plate 1, Bars _.L to Rolling Direction, Base Plate Plate 2, Bars [[ to Rolling Direction, Base Plate

Bar No. a, in. KIc, ksi ~ Bar No. a, in. KIr ksi %//~..

1-1 . . . . . . . . . . . . . . . . . 0.16 83.7 2-1 . . . . . . . . . . . . . . . 0.06 87.2


1-2 . . . . . . . . . . . . . . . . . 0.15 78.1 2-2 . . . . . . . . . . . . . . . 0.05 79.2
1-3 . . . . . . . . . . . . . . . . . 0.14 79.7 2-3 . . . . . . . . . . . . . . . calib.
1-4 . . . . . . . . . . . . . . . . . 0.12 74.1 2-4 . . . . . . . . . . . . . . . 0.07 79.5
1-5 . . . . . . . . . . . . . . . . . 0.14 93.1 2-5 . . . . . . . . . . . . . . . O. 05 9.15
1-6 . . . . . . . . . . . . . . . . . 0.15 69.5 2-6 . . . . . . . . . . . . . . . calib.
1-7 . . . . . . . . . . . . . . . . . 0.15 80.1 2-7 . . . . . . . . . . . . . . . 0.06 84.7
1-8 . . . . . . . . . . . . . . . . . 0.14 76.2 2-8 . . . . . . . . . . . . . . . 0.05 82.2
1-9 . . . . . . . . . . . . . . . . . 0.13 74.2 2-9 . . . . . . . . . . . . . . . ultrasonic test
1-10 . . . . . . . . . . . . . . . . 0.14 73.1 2-10 . . . . . . . . . . . . . . 0.05 87.3
1-11 . . . . . . . . . . . . . . . . 0.13 77.0 2-11 . . . . . . . . . . . . . . 0.07 88.0
1-12 . . . . . . . . . . . . . . . . 0.15 79.6 2-12 . . . . . . . . . . . . . . 0.05 84.9
1-13 . . . . . . . . . . . . . . . . 0.13 72.6 2-13 . . . . . . . . . . . . . . calib.
1-14 . . . . . . . . . . . . . . . 0.14 75.8 2-14 . . . . . . . . . . . . . . 0.07 81.5
1-15~ 2-15 . . . . . . . . . . . . . . 0.08 88.5
1-16J . . . . . . . . . . . . . . . calib. 2-16 . . . . . . . . . . . . . . 0.07 89.5
1-17 . . . . . . . . . . . . . . . . 0.15 75.3 2-17 . . . . . . . . . . . . . . 0.07 84.8
1-18 . . . . . . . . . . . . . . . . 0.14 75.5 2-18 . . . . . . . . . . . . . . 0.08 79.8
1-19 . . . . . . . . . . . . . . . . 0.14 82.2 edge fracture
1-20 . . . . . . . . . . . . . . . . 0.14 76.9 2-20 . . . . . . . . . . . . . . 0.20 85.0
1-21 . . . . . . . . . . . . . . . . 0.13 77.9 2-21 . . . . . . . . . . . . . . 0.16 84.9
1-22 . . . . . . . . . . . . . . . . 0.14 76.1 2-22 . . . . . . . . . . . . . . 0.17 86.3
1-23 . . . . . . . . . . . . . . . . calib. 2-23 . . . . . . . . . . . . . . 0.15 88.0
1-24 . . . . . . . . . . . . . . . . calib. 2-24 . . . . . . . . . . . . . . 0.15 82.2
1-25 . . . . . . . . . . . . . . . . 0.13 73.3 2-25 .............. 0.07 80.7
1-26 . . . . . . . . . . . . . . . 0.15 71.9 2-26 .............. calib.
1-27 . . . . . . . . . . . . . . . . 0.14 79.9 2-27 .............. 0.05 75.4
1-28 . . . . . . . . . . . . . . . . 0.13 76.2 2-28 .............. 0.14 87.2
1-29 . . . . . . . . . . . . . . . . 0.13 75.7 2-29 .............. 0.05 81.1
1-30 . . . . . . . . . . . . . . . . 0.13 73.5 2-30 .............. 0.07 84.7

Avg .............. 77.0 Avg ........... 84.3

from the one for which the bulk of the (I -- v2) where E --- 27 X 106 psi and
data are presented in this paper. v = 0.3. The bend-test values shown
Earlier work by the U.S. Steel Corp. I~ here are based on analytical results ob-
on 0.16-in. thick 18 per cent nickel tained by B. M. Wundt from work by
~ H . E. R o m i n e , " P l a n e S t r a i n F r a c t u r e
Bueckner. n
T o u g h n e s s by t h e Slow B e n d T e s t a n d T h r o u g h -
T h i c k n e s s T e n s i l e P r o p e r t i e s of U n w e l d e d 18 11 D. H . W i n n e a n d B. M . W u n d t , " A p p l i c a -
N i (250) M a r a g i n g Steel P l a t e ~,~-inch T h i c k t i o n of t h e G r i f f i t h - I r w i n T h e o r y of C r a c k
b e i n g S t u d i e d for U s e in l a r g e S o l i d - P r o p e l - P r o p a g a t i o n to t h e B u r s t i n g B e h a v i o r of D i s k s
l a n t , " N W L R e p o r t , to be p u b l i s h e d . Including Analytical and Experimental Stud-
~s U.S. Steel Corp. l e t t e r of F e b . 11, 1963, to ies," ASME P a p e r No. g~,A-24,9, p r e s e n t e d
J. M . K r a f f t . D e c e m b e r , 1957.

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340 FRACTUI~E TOUGHNESS TESTING

FIG. lO--Effect of Crack-Propagation Direction on Fracture Appearance and KI,, Source B.

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KIES ET AL ON TESTING OF WELDMENTS 341

It is tentatively concluded from Tables path. The dependence of K u on direc-


1 and 2 that K~ obtained in bend tests tion of crack propagation has been pre-
using Eq 10 gives good agreement with viously investigated by Romine. 9 Aver-
single-edged pop-in tests. Further test- age KI~ for plate surface notches was
mg is m progress. reported as 83 ksi X/'~n. versus 69
MATERIAL AND K i t TEST RESULTS FOR
ksi ~ for edge-wise propagation in
i-IN. THICK PLATE OF 18 PER CENT base bars cut in the rolling direction in
NICKEL MAKAGINGSTEEL SHOWN
the earlier tests. For bars cut transverse
IN TABLES 3 THROUGH 13
to the rolling direction, the effect was in
the same direction but less pronounced;
Compositions and heat numbers are average K~o values were 66 and 64 ksi
shown in Table 3 for materials tested X/~., respectively, for the same plate.

FiG. 12--Appearance of Crack Propagation


from an Edge Notch Propagating Across the
Rolling Direction in NRL Plate 2.
FIo. ll--Appearance of Crack Propagation
Through the Thickness and Across the Rolling
Direction in NRL Plate 2. Typical fracture appearances for bend
bars in which the notches are on the
and results shown in Tables 4 to 13, plate surface and plate edge are shown
inclusive. in Figs. 9 and 10 for plates from two
Table 4 shows Kit values obtained on different sources not represented in
base plate using bars cut perpendicular Tables 4-13. It is clear that the orienta-
to and parallel with the rolling direction. tion of the notch has an influence on the
Conditions are three-point bending. toughness of the base plates. Similar
K~ is computed from Eq 10 and visual differences according to crack-propaga-
notch depth. tion direction are illustrated for NRL
It is noteworthy that all of the tests plate 2 in Figs. 11 and 12.
in Table 4 were made with the notch
TUNGSTEN INERT GAS WELDS
on the plate surface so as to simulate
expected cracking in rocket cases. This Tungsten inert gas welding was in-
direction is conducive to crack arrest by vestigated. The typical sequence of
delamination or diversion of fracture passes is indicated by an etched cross

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FIo. 13--Etched Bars Showing TIG Lay-Up and Position of Notches in NRL Plate 6.

FIG. 14--Etched Bar Showing MIG Lay-Up FIG. 15--Etched Bar Showing Short Arc
and Position of Notch in NRL Plate 2. Weld Lay-Up and Position of Notch in NRL
Plate 11.
342

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KIE8 E T A L ON T E S T I N G OF W E L D M E N T S 343

TABLE 5--Kit NUMBERS FOR NOTCHES IN THE CENTER OF TIG WELDS.


( W e l d s a r e r u n t r a n s v e r s e to t h e bars.)

Plate 2, Bar Lengths--~ to Rolling Direction Plate 1, Bar Lengths 11to Rolling Direction

Bar No. Visual a, in. KIc, ksi ~ Bar No. Visual a, in. K t c , ksi V/i"~.

IV BA-1 . . . . . . . . . . . . 0.17 66.9 I V AA-1 . . . . . . . . . 0.15 88.8


2 ............ 0.13 57.2 2 .......... 0.13 80.1
3 ............ 0.16 70.6 3 .......... 0.16 87.5
4 ............ 0.15 61.0 4 .......... 0.15 91.2
5 ............ 0.17 68.7 5 .......... 0.16 103.1
6 ............ 0.18 57.8 6 .......... 0.14 93.3
7 ............ 0.14 60.3 7 .......... 0.20 113.8 a
8 ............ 0.15 67.6 8 .......... 0.15 90.3
9 ............ 0.14 79.5 9 .......... 0.16 69.8
10 . . . . . . . . . . . . 0.14 68.0 10 . . . . . . . . . . 0.15 74.5
11 . . . . . . . . . . . . 0.16 77.0 11 . . . . . . . . . . 0.15 60.3 ~
12 . . . . . . . . . . . . 0.15 82.4 12 . . . . . . . . . . 0.15 85.7
13 . . . . . . . . . . . . 0.18 80.2 13 . . . . . . . . . . 0.15 74.2
14 . . . . . . . . . . . . 0.14 59.4 14 . . . . . . . . . . 0.15 80.9
15 . . . . . . . . . . . . 0.16 81.0 15 . . . . . . . . . . 0.15 75.9
16 . . . . . . . . . . . . 0.15 75.3 16 . . . . . . . . . . 0.16 64.1
17 . . . . . . . . . . . . 0.16 68.2 17 . . . . . . . . . . 0.18 91.0
18 . . . . . . . . . . . . 0.16 72.3

Avg .............. 69.6 A v g. . . . . . . . . . . . . 83.8


c.v. b . . . . . . . . . . . . . 0.12 c.v. . . . . . . . . . . . . . 0.15

a T h e l a r g e difference b e t w e e n K i t for bars I V AA-7 a n d I V A A - I 1 w a s a t t r i b u t a b l e to m i c r o -


s t r u c t u r e . B a r 7 w a s fine-grained a n d B a r 11 c o a r s e - g r a i n e d a t t h e root of t h e s t a r t i n g c r a c k . T h i s
will r e c e i v e m o r e d e t a i l e d s t u d y b y m e t a l l o g r a p h y .
b Coefficient of v a r i a t i o n .

TABLE 6--KI~ FOR THE FUSION ZONE TIG WELDS.

Plate 2, Bar Lengths .a_ to Rolling Direction Plate 1, Bar Lengths [I to Rolling Direction

Bar No. Visual a, in. KIc, ksi ~ Bar No. Visual a, in. KIc, ksi %/i-~n.

IV BD-4 ............ 0.15 77.3


5 ............
6 ...........
7 ............
0.15
0.15
0.19
87.0
76.2
82.3
iv o-liiiii
23 iii t 4 ..........
calibration bars

0.19 106.7
8 ............ 0.15 89.6 5 .......... 0.16 97.3
9 ............ 0.15 81.7 6 .......... 0.17 100.8
IV BB-18 . . . . . . . . . . . 0.17 80.5 7 .......... 0.19 109.3
8 .......... 0.15 90.0
9 .......... 0.16 103.9
10 .......... 0.16 92.0

Avg .............. 82.1 Avg............. 100.0


c.v." ............. 0.06 c.v. . . . . . . . . . . . . . 0.07

6 Coefficient of variation.

section shown in Fig. 13. Kxc values the position of the notch is c o d e d as
for plates TIG welded are given in follows:
Tables 5 to 8. The orientation of the
bars perpendicular and parallel with the C.W. = center of the weld
rolling direction is i n d i c a t e d . The weld F.Z. = fusion zone where base plate
beads were transverse to the bars and is m e l t e d

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344 FRACTURE TOUGHNESS TESTING

H.A.Z. = heat-affected zone in the base verify the position of the bottom of the
plate fatigue crack below the notch. Although
D.B. = dark band just outside H.A.Z. some uncertainty remained, the position
The typical TIG weld lay-up and the code was assigned in accordance with
positions of the notches are shown in the etched appearance, not always the

TABLE 7--Kit FOR THE HEAT-AFFECTED ZONE TIG WELDS (H.A.Z.).

Plate 2, Bar Lengths _t. to Rolling Direction Plate 1, Bar Lengths ]] to Rolling Direction

Bar No. Visual a, in. K I t , ksi %/i~. Bar No. Visual a, in. KIr ksi %/i"m.

IV BB-8 ............ 0,18 87.6 IV AB-9 ........... 0.14 101.9


9 ............ 0,18 66.8 10 . . . . . . . . . . 0.14 88.6
10 ............ 0.17 71.1 11 . . . . . . . . . . 0.14 82.3
11 ............ 0.15 59.5 12 . . . . . . . . . . 0.14 82.3
12 ............ 0.19 73.2 13 . . . . . . . . . . . 0.15 104.0
13 ............ 0.14 90.0 14 . . . . . . . . . . 0.14 102.7
14 ............ 0.19 60.7 17 . . . . . . . . . . 0.16 103.1
15 ............ 0.15 76.3 18 . . . . . . . . . . 0.16 91.6
16 ............ 0.15 85.8
17 ............ 0.17 75.9

Avg .............. 74.7 Avg ............. 94.6


e.v. ~ ............ 0.14 c.v .............. 0.10

C o e f f i c i e n t of v a r i a t i o n .

TABLE 8--Kit FOR THE DARK BAND AT THE JUNCTION OF BASE PLATE AND
HEAT-AFFECTED ZONE TIG WELDS (D.B.).

Plate 2, Bar Lengths _t. to Rolling Direction Plate I, Bar Lengths [[ to Rolling Direction

Bar No. Visual a, in. E f t , ksi %/i-~. Bar No. Visual a, in. K i t , ksi ~r

IV BB-1 ............ 0.15 62.3 IV AB-1 ........... 0.15 90.3


2 ............ 0.17 62.0 2 ........... 0.13 99.8
3 ............ 0.16 59,8 3........... 0.17 117.0
4 ............ 0.16 63.5 4 .......... 0.13 82.6
5 ............ 0.15 76.5 5 .......... 0.14 97,9
6 ............ 0.13 72.1 6 .......... 0.13 106.4
7 ............ 0.16 71.8 7 .......... 0.16 83.0
8 .......... 0.15 102.2
19 . . . . . . . . . . 0.14 95.1
20 . . . . . . . . . . 0.15 91.9

Avg .............. 66.9 Avg ............ 96.6


c.v. 9 ............. 0.09 e.v .............. 0.10

" C o e f f i c i e n t of v a r i a t i o n .

Fig. 13. The weld bead lay-ups for MIG same as the original intended position.
and short arc welds are shown on etched The code letters assigned were in ac-
bendbarsinFigs. 14 and 15, respectively. cordance with Fig. 16. The notch-posi-
The K~o results for the fusion zone or tion assignments were the best that could
edge of the fusion zone in TIG welds are be done on this basis and within the
shown in Table 6. Each specimen was authors' ability' to distinguish etched
etched on the sides prior to testing to structures with the usual visual aids.

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CODE, CW -CENTER OF WELD FUSION ZONE
FZ - EDGE OF WELD FUSION ZONE
HAZ-HEAT AFFECTED ZONE
DB -DARK BAND AREA
BM - BASE METAL

HAZ FZ

BM GW

F I o . 1 6 - - C r o s s S e c t i o n of W e l d Area Showing Different Locations of S t a r t i n g Notch Tipped


~r Fatigue Crack.

TABLE 9--KI6 FOR MIG WELDS NOTCHED IN THE CENTER OF THE WELD (C.W.).

N R L Plate 6, Bar Lengths .I_ to Rolling Direction N R L Plate 5, Bar Lengths H to Rolling Direction

Bar No. Visual a, in. KIr ksi %/Tn, Bar No. Visual o, in. K I ~ , ksi

II BA-1 ............. 0.15 70.2 II AA-1 ........... 0.14 72.0


2 ............ 0.15 74.1 4 ........... 0.13 71.8
3 ............ 0.15 62.6 6 ........... 0.13 70.7
4 ............ 0.20 54.4 7 ........... O. 14 64.4
5 ............ 0.14 70.5 8 ........... 0.13 85.9
6 ............ 0.15 63.2 10 ........... 0.12 71.4
7 ............ O. 14 70.6 11 ........... 0.12 75.8
8 ............ 0.14 71.8 13 ........... 0.15 80.1
9 ............. 0.15 67.0 15 ........... 0,14 60.4
10 . . . . . . . . . . . . . 0.13 87.3 16 ........... 0.13 71.4
11 . . . . . . . . . . . . . 0.14 74.1 17 ........... 0.13 102.7
12 . . . . . . . . . . . . . 0.13 86.9 18 ........... 0.14 105.7
13 . . . . . . . . . . . . . 0.15 84.4
14 . . . . . . . . . . . . . 0.14 83.0
15 . . . . . . . . . . . . . 0.15 81.8
16 . . . . . . . . . . . . . 0.14 78.8
17 . . . . . . . . . . . . . 0.13 85.3
18 . . . . . . . . . . . . . O. 14 74.3
19 . . . . . . . . . . . . . 0.13 71.4

Avg .............. 74.3 Avg ............. 77 7


c.v. a ............. 0.12

a Coefficient of variation.

345

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346 FRACTIYRE TOUGHNESS TESTING

TABLE 10--TOUGHNESS IN THE HEAT-AFFECTED ZONE MIG WELDS (H.A.Z.).

NRL Plate 6, Bar Lengths 2_ to Rolling Direction NRL Plate 5, Bar Lengths I1 with Rolling Direction

Bar No. Visual a, in. KIc, ksi M/~n. Bar No. Visual a, in. K I c , ksi ~v/i~.

II BB-2 ............. 0.13 90.8 II AB-1 ........... 0.15 85.0


3............. 0.15 91.8 3 ........... 0.12 87.4
4............. 0.14 93.2 4 ........... 0.13 92.6
5............. 0.13 89.8 6 ........... 0.11 105.1
6............. 0.13 102.3 7 ........... 0.13 105.7
7............. 0.14 93.4 8 ........... 0.15 78.4
9 ........... 0.16 81.6
10 . . . . . . . . . . . 0.16 86.7
11 . . . . . . . . . . . 0.14 99.0

Avg .............. 93.6 Avg ............. 91.3


c.v." .............. 0.I0 c.v .............. 0.10

a C o e f f i c i e n t of v a r i a t i o n .

TABLE ll--SHORT ARC WELD TOUGHNESS DATA FOR CENTER OF THE WELD (C.W)

Plate 7, Bar Lengths 2- to Rolling Direction Plate I1, Bar Lengths ~ with Rolling Direction

Bar No. Visual a, in. K I c , ksi x / i ~ . Bar No. Visual a, in. KIr ksi x / i ~ .

V BA-1 ............. 0.150 3.5 V AA-I ............ 0.15 64.1


2 ............. 0.120 75.4 2............ 0.14 75.9
3 ............. 0.155 60.0 3 ............ 0.14 73.3
4 ............. 0.140 48.0 4............ 0.14 72.8
5 ............. 0.155 53.5 5 ............ 0.15 68.6
6 ............. 0.160 52.6 6............ 0.14 61.5
7 ............. 0.145 69.0 7............ 0.13 67.4
8 ............. 0.150 59.0 8 ............ 0.14 65.2
9 ............. 0.155 51.5 9 ............ 0,13 89.1
10 . . . . . . . . . . . . . 0.160 56.5 10 . . . . . . . . . . . . 0.14 79.3
11 . . . . . . . . . . . . 0,14 69.7
12 . . . . . . . . . . . . 0,14 74.7
13 . . . . . . . . . . . . 0.12 71.4
14 . . . . . . . . . . . . 0.15 72.4
15 . . . . . . . . . . . . 0.17 77.8
16 . . . . . . . . . . . . 0.13 75.9
17 . . . . . . . . . . . . 0.14 75.8
18 . . . . . . . . . . . . 0.12 79.1
19 . . . . . . . . . . . . 0.14 69.4

Avg .............. 56.9 Avg ............. 72.8


c.v. a . . . . . . . . . . . . . 0.16 e.v .............. 0.09

a C o e f f i c i e n t of v a r i a t i o n .

In order to get valid K~c numbers, say tion of the specimen. This corresponds
for F.Z. or H.A.Z., it is not necessary to an increment in crack depth of 0.004
for the propagation to proceed more in. The records indicate that the load at
than a very small distance in the specified pop-in is never appreciably different
structure. The load at initiation of the from that after this amount of pop-in.
fracture is hopefully the only load re- The center-of-weld toughness was
corded. The pop-in must produce an found to be less than that at any other
offset of at least ~ in. on the record position.
which corresponds to 0.0004-in. deflec- The microstructural details existing

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KIES E T AL ON T E S T I N G OF W E L D M E N T S 347

TABLE 12--Kic TES T RESULTS FOR NOTCHES TERMINATING IN THE HEAT-


AFFECTED ZONE, SHORT ARC WELDS.

Plate 7, Bar Lengths -J- to Roiling Direction Plate 11, Bar Lengths [[ with Xolling Direction

Bar No. Visual a, in. K I c , ksi %/i~. Bar No. Visual a, in. KIr ksi ~r

V BB-2 ............. 0.120 92.5 V AB-1 . . . . . . . . . . . . 0.12 113.3


4 ............ 0.130 96.5 2............ 0.13 96.4
5 ............. 0.140 89.5 3 ........... 0.11 103.2
7 ............ 0.140 85.5 4............ 0.12 111.3
8 ............. 0.130 86.5 5............ 0.14 101.1
6. . . . . . . . . . . . 0.14 101.1
7. . . . . . . . . . . . 0.14 120.4
8. . . . . . . . . . . . 0.14 116.2
9. . . . . . . . . . . . 0.14 116.9
10 . . . . . . . . . . . . 0.14 98.1
11 . . . . . . . . . . . . 0.15 109.9
12 . . . . . . . . . . . . 0.15 98.7
13 . . . . . . . . . . . . 0.14 102.4
14 . . . . . . . . . . . . 0.14 113.4
15 . . . . . . . . . . . . 0.14 106.8
16 . . . . . . . . . . . . 0.12 118.6
17 . . . . . . . . . . . . 0.13 104.5
18 . . . . . . . . . . . . 0.15 92.6

Avg .............. 90.1 Avg............. 106.8


c.v. a . . . . . . . . . . . . . . 0.04 c.v............. 0.07

Coefficient of v a r i a t i o n .

TABLE 13--SUMMARY O F Kj~ A V E R A G E VALUES AND THEIR


COEFFICIENTS O F V A R I A T I O N .
Orientation KIe
Table No. of Bar with Kind of Weld Location of Average, Coefficient
Rolling Notch ksi %/in. of Variation Heat No.
Direction

4 .............. .L base p l a t e ... 76.96 0. 060 X14636


4 ............. II base p l a t e ... 84.33 0. 041 X14636
5 ............. A_ TIG C.W. 69.63 0.116 X14636
5 ............. II TIG C.W. 83.79 0.152 X14636
6 ............. .1. TIG F.Z. 82.08 0. 057 X14636
6 .............. II TIG F.Z. 100.00 0. 068 X14636
7 .............. _[_ TIG H.A.Z. 74.69 0. 139 X14636
7 .............. II TIG H.A.Z. 94.56 0. 098 X14636
8 .............. l TIG D.B. 66.86 0.089 X14636
8 .............. I] TIG D.B. 96.62 0.104 X14636
9 ............. _k MIG C.W. 74.30 0.117 X53013
9 ............. II MIG C.W. 77.69 0. 054 X14636
10 . . . . . . . . . . . . A. MIG H.A.Z. 93.55 0.101 X53013
10 . . . . . . . . . . . . II MIG H.A.Z. 91.28 0.104 X14636
11 . . . . . . . . . . . . ]l s h o r t are C.W. 72.81 0.088 X53013
12 . . . . . . . . . . . . . I[ s h o r t arc H.A.Z. 106.77 0.074 X53013

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TABLE 14--P(t) a VALUES FOR STUDENT'S t TEST OF THE SIGNIFICANCE BETWEEN MEAN Kx, V A L U E S .

Base Plate T I G Welds MIG Welds Short Arc Welds

.s. II .s. II .s. U

__ ~ C.W. F.Z. . H.A.Z. D.B. C.W. F.Z. I-I.A.Z. D.B. C.W. I:I.A.Z. C.W. H.A.Z. C.W. H.A.Z. C.W. H.A.Z.

.. I<0.01 <0.01 0,015 >0.08 <O.Ol 0.21 >0.01 ... <0.01 <0.01 ...
H.S. H-.S. H.S. N.S. H.S. Po.S. H.S. H.S. H.S.
Base Plate
>O.0~ <0.01 <0.01 >0.01 ... >0.01 0.04 . . . . . . <0.01 <0.01
N.S. H,S. H.S. H.S. N.S. S. H.S. H.S.

<0.01 0.178 >0.3 <3.01 ...... 0.093 <0.01 . . . . . . <0.01 <0.01 ... ... C.W.
H.S. Po.S. N.S. H ~, Pr.S. H.S. H.S. H.S.
OO
0.123 <0.01 <0.01 ...... 0.05 <0.01 . . . . . . <0.01 0.014 . . . . . . F.Z.
Pr.S. H.S. H.S. S, H.S. H.S. H.S.

0.107 <0.01 ... >0.3 <0.01 . . . . . . <0.01 <0.01 ... ... H.A.Z.
Pr.S. H.S. N.S. H.S. H.S. H.S.

<0.01 ... 0.059 <0.01 . . . . . . 0.032 <0.01 ... D.B.


H.S. S. H.S. S. H.S.
TIG
Welds
<0.01 0.07 0.016 . . . . . . 0.262 0.157 <0.01 <0.01! C.W.
H.S. S. H.S. N.S. Po.S. H.S. H.S.

>0.3 >0.3 ... <0.01 0.074 <0.01 0.073 F.Z.


N.S. N.S. H.S. S. H.S. S.
II
>0.3 ........ 0.015 >0.3 <0.01 <0.Ol H.A.Z.
N.S. H.S. N.S. H.S. H.S.

<0.01 0.28 <0.01 0.026 D.B.


H.S. N.S. IcI.S. .

Co pyr igh t b y A S TM In t'l ( all r i g h t s r es er v ed ); Mo n D ec 7 1 4 : 4 2 : 5 6 E S T 2 0 1 5


D ow nlo ade d/pr inted b y
U niv ers ity of Wa sh ingto n (U n i v er si t y o f Wa sh i ng t on ) pu r su an t t o L i cen se A g r eem en t . N o f u r t h er r ep r o d u ct i o n s au t h o r i zed.
<0.01 >0.3 <0.01; <0.01 C.W~
H.S. N.S. H.S. H.S.

>0.3 <0.01 0.24 H.A.Z.


N.S. H.S. Po.S.
MIG
Welds
0,03 <0.01 C.W.
I S.
o~22
Po.S. H.S.

<0.01 <0.01 H.A.Z.


H.S. H.S.

<0.01 <0.01 C.W.

<0.01 H.A.Z.
H.S. Short
Arc
C.W. Welds

H.A.Z.

a P ( t ) is the probability of a random variation in average KI, which would equal or exceed the difference shown between two average values of Kte.
NOTE :
H.S. ~- Highly Significant, P(t) <0.024.
S. -~ Significant, P(t) 0.025 to 0.074.
Pr.S. = Probably Significant, P(t) 0.075 to 0.14.
Po.S. = Possibly Significant, P(t) 0.15 to 0.25.
N.S. -~ N o t Significant, P(t) >0.26.

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350 FRACTURE TOUGHNESS TESTING

at the tips of the cracks were not in- cedures. On this basis the bend-test
vestigated. This will be the subject of a method is not appreciably better or
future investigation aimed at offering worse than other tests such as the edge-
guidance for future materials improve- notched tear test. The significances of
ment. the differences between average K~,
The K~, test results for the heat- values are shown in Table 14. The levels
affected zone (H.A.Z.) are shown in of significance are assigned on the basis
Table 7 for T I G welds. of the probability function of t in the
The K ~ test results for d~rk band at usual t test. P(T) is the probability
the junction of the base plate and heat- that in another set of tests the average
affected zone are given ill Table 8 for values being compared would overlap
T I G welds. because of scatter in the results. Qualita-

TABLE 15--NRL CHEMICAL ANALYSES, CENTER OF WELD.

Center of Weld
Element Rod
Short Arc MIG TIG

Carbon . . . . . . . . . . . . . . . . . . . . . . . . 0.02 0.02 0.02 0.02


Manganese . . . . . . . . . . . . . . . . . . . . . 0.03 0.03 0.03 0.03
Phosphorus . . . . . . . . . . . . . . . . . . . . 0.004 0.002 0.003 0. 004
Sulfur . . . . . . . . . . . . . . . . . . . . . . . . . 0.005 0.005 0.005 0. 005
Silicon. . . . . . . . . . . . . . . . . . . . . . . . . 0.02 0.03 0.04 0.02
Nickel. . . . . . . . . . . . . . . . . . . . . . . . . 18.24 18.2 18.0 18.0
Molybdenum . . . . . . . . . . . . . . . . . . . 4.62 4.00 4.60 4.60
Cobalt . . . . . . . . . . . . . . . . . . . . . . . . . 7.90 7.79 8.28 7.67
Titanium . . . . . . . . . . . . . . . . . . . . . . 0.45 0.43 0.43 0.43
Aluminum . . . . . . . . . . . . . . . . . . . . . 0.09 0.09 0.10 0.11

METAL INERT GAS WELDS tire terms used in Table 14 are as fol-
lows for designating the differences
A photograph of the etched cross between averages:
section of a typical M I G weld is shown
as Fig. 14. Toughness numbers for such H.S. = highly significant,
welds notched in the center of the weld P(t) < 0.024
are given in Table 9. S. = significant,
K~c results for notches terminating in P(t) 0.025 to 0.074
the heat-affected zone of M I G welds Pr.S. = probably significant,
are shown in Table i0. P(t) 0.075 to 0.14
Ks, test results for notches terminating Po.S. = possibly significant,
in the center of the weld and heat- P(t) 0.15 to 0.25
affected zones for short arc welds are N.S. = not significant,
shown in Tables 11 and 12, respectively. P(0 > 0.26
SUMMARY OF THE TEST RESULTS
CONCLUSIONS
The average K ~ values and their
coefficients of variation are shown for 1. Kic values from the bend tests
the different weld methods, bar orienta- agreed well with those from edge-notched
tions, and notch positions in Table 13. tear tests.
The coefficients of variation are of about 2. A new K~, closed formula for bend
the same magnitude usually reported by tests was obtained which is independent
other authors and for other test pro- of Young's modulus of elasticity.

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KIES ET AL ON TESTING OF WELDMENTS 351

3. There were highly significant effects base plate was found, this could be ex-
of rolling direction on KI~ for both heats plained on the basis of finer grain size
of the 250 grade steel. and fewer carbide precipitates.
4. For T I G welds in bars cut parallel 9. Where wide differences in K~,
with the rolling direction, the average were found between different bars but
Kic values were higher by highly signifi- in the center of the weld at equal depths,
cant amounts than for bars cut perpen- the difference correlated with micro-
dicular to the rolling direction. This was structure. Coarse-grained weld deposits
true for all four notch positions in the with dendrites aligned mainly along the
weld. The margins of superiority were fracture path showed less toughness
magnified over that in the base plate. than fine dendrites randomly oriented.
We have no explanation. Conclusions 8 and 9 are tentative and
5. For M I G welds, no comparison was will be given additional study.
available between directions perpendicu-
Acknowledgments:
lar and parallel with the rolling direction.
6. For short arc welds, the greatest The authors are greatly indebted to
average Kic was found in the heat- the following:
affected zone. For the 250-ksi yield R. G. Hayes and A. S. Jennings of the
strength steel, the directionality effect U.S. Naval Weapons Laboratory and
in the base plate was reflected in the W. E. Anderson of the Naval Research
welds. Laboratory, for mechanical testing.
7. Where a comparison was available, F. Stonesifer and Karl McKinney
the T I G welds were more consistent of the Naval Research Laboratory, for
and generally better than for the other calculations.
types of welds investigated. W. Cohen and N. Mayer of NASA
8. Where marked superiority of Kit Headquarters, for the financial support
for shallow (versus deeper) notches in of this research and testing program.

APPENDIX

FAILURE ANALYSIS EXAMPLE--WELD FLAW


Figure 17 shows an enlarged view of a 2c = L --- prior crack length at the sur-
fracture origin in a 156-in. diameter test face = 0.500 in.
chamber made of H-11 steel. The prior
a/2c = 0.260
crack was heat-colored and presumably oc-
curred during welding. It was situated at ~rrs = uniaxial yield strength = 203,000 psi
the edge of a longitudinal weld in the cylin-
drical section. At hydrotest failure (early ~hoov/~rs = 0.378
in 1964), the hoop stress was 77,000 psi. The Q =[r _ 0.212 ( a / a r s ) 2] = 1.45
prior crack was not a very perfect semi-el-
lipse and the bottom of the prior crack was by the Tiffany chart
poorly delineated. The following data and
K~? = [3.77 (77000)3 (0.13)]/1.45
conclusions illustrate a rather typical situa-
tion. Many similar hydrotest failures were K "~ 45 ksi ~/in.
encountered in the Polaris steel motor case
development program. This is the indicated value of KIr if in-
stability or pop-in occurred at a = 0.130.
Flaw depth, a = 0.130 q- 0.020 in.
This low value is not uncommon in and
Plate thickness t = B -- 0.38 in. near welds in H-11 steel oI this thickness.

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352 FRACTURE To~c~WESS TESTING

There is no proof that instability really absolute certainty and depends on subjective
occurred at a = 0.130. It is conceivable that judgment of the fracture appearance,
some slow growth extended the crack deeper. 4. We did not have adequate data to pre-
If the slow extension had carried the crack dict the K~, or a~rit for such a crack. A con-
all the way through the thickness, the length siderable uncertainty in aerlt exists.
of the crack would have been 2ar ~ 1.0 in. 5. The important thing here is that the
as judged from the photograph. Uncertainty crack should have been detected and re-
in this number seems to be -4-15per cent and paired. Failure prevention is better than
is quite subjective. The fracture still con- failure analysis.

Fto. 17--Enlarged View of a Fracture Origin in a 156-In. Diameter Test Chamber Made of H-11
Steel.

tains almost no shear lip so that Kit is still Choice of Spedmen Type (Three-Point Bend
the determining toughness for possible ar- Test):
rest. For the through crack:
There are favorable points as well as ob-
7r~2ac jectionable points to each type of specimen
/~i ~ which one might choose to use in making
plane-strain fracture toughness measure-
ments. The application in mind will gener-
KI~ ~ 100 ksi (in.)u~ ally dictate one's choice. For the work
reported here, it was necessary to evaluate
This is higher than we have reason to believe plates with a nominal thickness of ~ in.,
is characteristic of the material. since the applieation was the 260-in. solid
booster motor case. Further, the material to
Conclusions: be evaluated was the 18 per cent nickel
1. Instability and hydrotest failure were maraging steel which has been subject to a
completely determined before the surface certain amount of banding. It was also
crack had penetrated through the thickness. desirable to study cracks propagating in the
2. The Kr for H-11 could not tolerate a thickness direction (short transverse) as the
2t or 2B crack even at 77,000 psi hoop stress more likely concern from a practical applica-
for t -- B = 0.38 in. tion standpoint.
3. The crack depth at instability seems to Because of the reasons listed here, our
have been at the initial black-walled prior choice of specimen was narrowed to either
crack border, but this is not a matter of the partially through surface crack in ten-

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KIES v.T AI, ON TESTING OF WELDm~.N'rS 353

sion or the notch bend test. I t was decided bend bars in the thickness direction. How-
that different areas of the weld could be ever. the resulting direction of crack propa-
better discriminated using the flat bottom gation might be unrealistic in relation to the
notch of a bend bar rather than the curved type of failure expected in an actual motor
perimeter of an elliptical surface notch. It case.
would require from three to four times as If one measures the compliance, C, of a
much material for a surface notch specimen bend bar as a function of notch depth, the
as that required for a bend specimen. ratio of load to deflection, at the point of
Three-point loading rather than four- interest, determines the effective notch
point loading was selected largely because depth for use in calculating g. However,
of convenience. The deflections for a given one must know E in order to relate load to
load are larger in three-point loading, re- crack size. If E is indeterminate, the rela-
quiring less magnification of strain measure- tion of load to crack size is indeterminate.
ments. Further, one bend test setup is For this reason, it was found convenient to
sufficient to test a wide range of specimen represent EC as a function of relative crack
sizes in three-point loading. depth in equation form and to use this repre-
sentation and a visual determination of crit-
Use of K Values Computedfrom an Equation: ical notch depth. The resulting K values
Difficulties not previously experienced may scatter and be somewhat altered due
were found in this investigation, such as to delaminations, but such a procedure es-
austenite segregation and carbide precipi- tablishes a K value for each test which rep-
tates which result in varying amounts of resents a relationship between load and
banding throughout each plate. These varia- notch depth independent of modulus. Such
tions result in an indeterminate modulus, E. values are believed to be more useful than
One could avoid this difficulty by notching the ~ values.

DISCUSSION
CARL E. H A R T B O W E R I AND LEOPOLD Dr. Irwin's equation ~ is:
ALBERTrNI---Results obtained from Eq
9ic = 89 d(B/M)/da ..... (21)
10 for computing the plane-strain stress-
intensity factor from slow bend tests where P / B is the bending load at frac-
have been compared with results ob- ture (or pop-in) per unit width of bar,
tained from equations derived b y H. and d(B/M)/da is the slope of the ex-
Bueckner and G. Irwin using computer perimental curve for reciprocal of the
programs at Aerojet-General Corp. spring constant at notch depth, a, as
E q u a t i o n 10 is: determined from calibration data.
Dr. Bueckner's equation s is:
K,c D 3/~ = 2.060 1 - a3J ... (20)
(1 - :)
9,, -- ' - " 7 - F.'hf(a/D) ...... (22)
where a -- 1 - a/D, D = depth of beam,
P = load, L = span/2, B -- width of where Fn = 3PL/Bh 2, ~ = Poisson's
beam, and a -- notch plus crack depth. ratio (0.32), E = Young's modulus
i Research engineering specialist and metal- (27 X 106), h = depth below the notch,
lurgical engineer, respectively, Aerojet-General andf(a/D) = 0.0126 + 1.9762 (a/D) --
Corp., Solid Rocket Operations, Sacramento,
Calif.
2 G. R. Irwin, J. A. Kies, and H. L. Smith, 8B. M. Wundt, "A Unified Interpretation
"Fracture Strengths Relative to Onset and of Room Temperature Strength of Notched
Arrest of Crack Propagation," Proceedings Specimens as Influenced by Their Size," A ~ M E
Am. Soc. Testing Mats, Vol. 58, 1958, p. 646, Paper 59 M E T 9, 1959.

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354 FRACTURE TOUGHNESS TESTING

T A B L E 1 6 - - C O M P A R I S O N OF SLOW B E N D F R A C T U R E T O U G H N E S S TES TS OF
18 P E R C E N T N I C K E L MAP, AGING S T E E L P L A T E , R E P O R T E D B Y R O M I N E , ( T A B L E
3) a U S I N G T H E S P R I N G - C O N S T A N T A N D B U E C K N E R M E T H O D S .

Measured Effective P/B Unit


Direction Fatigue Crack Load To Romhae, Bueckner,
Bar No. Notch Location Relative Crack Frac- cdI~, 9Ir ~ 2
to Rolling Depth, Depth, ture, ia.-lb/in3 in.-lb/m.
in. m. lb/im

A-1 . . . . . . parallel to plate sur- across 0.12 0.12 4514 173 157
A-3 face a t top center of weld 0.10 0.08 5247 127 162
A-7 weld 0.10 0.08 5486 138 176
A-9 0.10 0.08 5624 145 105

Av. 146 Av. 170

A-11 . . . . . parallel to plate sur- acros.o 0.10 0.02 6198 2ll 227
A-12 face at top edge of weld 0.11 0.02 7326 295 361
A-13 weld 0.12 0.11 5326 170 218
A-14 0. I0 0.02 6039 201 213

Av. 219 Av. 255

A-2 . . . . . . perpendicular to sur- across 0.14 0.13 3653 125 135


A-4 face at side center of weld 0.14 0.12 3775 123 143
A-8 w~d 0.15 0.13 3379 108 129
A-10 0.13 0.12 3508 106 109

Av. I16 Av. 129

B-1 . . . . . . parallel to plate sur- across 0.10 0.06 3533 75 98


B-3 face at top center weld 0.11 0.07 3312 77 100
B-7 of w ~ d 0.10 0.06 3396 69 90
B-9 0.10 0.06 3776 86 112

Av. 77 Av. 100

B-11 . . . . . parallel to plate sur- across 0.10 0.07 7621 (378) ~ (453)
B-12 face at top edge of weld 0.11 0.10 7320 (549) (485)
B-13 weld 0.10 0.08 7420 (440) (433)
B-14 0.11 0.09 7362 (488) (486)

Av. (464) Av. (464)

B-2 . . . . . . perpendicular to plate across 0.13 0.09 3217 104 123


B-4 surface at side ten- weld 0.12 0.08 3312 99 114
B-8 ter of weld 0.12 0.10 3270 119 I12
B-10 0.13 0.12 3073 122 110

Av. 111 Av. 115

a H. E. Romine, "Plane-Strain Fracture Toughness Measurements of Solid Booster Case Mate-


rials," Naval Weapons Lab. (Dahlgren~ Report No. 1884. Sept. 13, 1963.
b Values in parentheses are uncertain because net-section fiber stress exceeded yield strength.

2.1713 (a/D)L The equation for f(a/D) gated. Dr. Romine, in his study of
was obtained by a least-squares com- vacuum-arc remelted grade-250 18 per
puter program using corrected coordi- cent nickel maraging steel, established
nates (private communication from H. calibration curves, not only for each
Bueckner dated Mar. 2, 1964). heat but also for each v~eld, and notch and
In using Eq 21, the usual experimental specimen orientation. Unfortunately, in
procedure is to establish a calibration order to obtain reliable spring constants,
curve for each heat of material investi- calibration involves several preliminary

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DISCUSSION ON TESTING OF WELDMENTS 355

tests made under exacting conditions. heat treatment B, where the results of
Therefore, as the authors have pointed Bueckner's equation generally were more
out, there is a real advantage in equa- conservative than those obtained from
tions such as 20 and 22 which do not the spring constant. One of the advan-
require calibration experiments. tages of the spring-constant method is

T A B L E 1 7 - - C O M P A R I S O N OF SLOW B E N D F R A C T U R E T O U G I I N E S S TES TS OF 18
P E R C E N T N I C K E L M A R A G I N G S T E E L P L A T E , 200 G R A D E M A T E R I A L , I I E A T
3960524, A P P L Y I N G B U E C K N E R A N D K I E S EQUATIO N S .

Propor-
(OIc ~Ir
Measured (Kies et al), (Bueckner),
Aging Cycle
Specimen Width, Depth, tional Crack Fracture Fracture
Orientation b, in. d, in. Limit Depth, Toughness, Toughness,
deg F hrs Load, lb in. in.-Ib/in. 2 in.-lb/in.~

900 4 longitudinal 0.600 0.750 10 200 0.232 590 605


0.600 0.750 9 000 0.271 607 638
0.599 0.751 8 700 0.270 562 590
0.600 0.750 g 200 0.301 626 666

Av. 596 Av. 625

900 4 transverse 0,600 0.751 11 500 0.171 472 457


0.600 0.750 9 450 0.22S 492 502
0.600 0.750 10 400 0.270 511 513
0.600 0.752 10 600 0.207 525 526

Av. 500 Av. 499

900 16 longitudinal 0.599 0.751 10 100 0.228 560 572


0.599 0.750 8 700 0.275 586 617
0.600 0.751 l0 700 0.222 600 610
0.601 0.751 10 500 0.216 551 558

Av. 574 Av. 589

900 24 hmgitudinal 0.600 0.750 8 900 0.246 497 514


0.500 0.750 9 800 0.236 560 576
0.599 0.751 10 450 0.213 538 543
0.600 0.750 10 450 0.206 512 514

Av. 527 Av. 537

900 24 transverse 0.600 0.750 9 200 0.240 508 524


0.600 0.750 10 450 0.215 547 553
0.599 0.750 10 800 0.199 521 519
0.600 0.750 9 900 0.211 477 480

Av. 514 Av. 519

The data presented in Table 16 are that an effective crack depth is obtained
from Romine, together with recalcu- which includes the plastic zone formed
lated values of ~c using Bueckner's at the tip of the crack. Thus, the effec-
Eq 22. A comparison of the fracture tive crack should be larger than the
toughness data obtained by the two measured depth of notch plus fatigue
methods shows that Bueckner's equa- crack. Table 16 contains anomalous
tion gave approximately the same oo~c data in this regard, presumably the
values as those determined from the result of insufficient calibration data
spring constant except in the case of or inherent complications in testing

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356 FRACTUP,~ TOUGHNESSTESTING

inhomogeneons weld deposits, or both. (3-in. span), 0.6 in. wide, and 0.75 in.
Note that specimens B1-7 had measured deep. Representative computer-run frac-
crack depths of 0.10 to 0.11 in. and effec- ture toughness data are tabulated in
tive crack depths calculated from the Table 17. Note that Eqs 20 and 22
spring constant of only 0.06 to 0.07 in. provided by the authors and Bueckner
Comparisons also have been made at respectively gave approximately the
Aerojet-General Corp. between the re- same 9ic values.
sults obtained from Eqs 20 and 22 in From the data presented in Tables
forty groups of five replicate slow notch 16 and 17, it is concluded that calcula-
bend (SNB) specimens of vacuum-arc tion of plane-strain fracture toughness
remelt grade-200 18 per cent nickel from the slow bend test can be accom-
maraging steel, representing two orienta- plished using either Bueckner's or the
tions of a specimen aged at 850-950 F authors' equations, thus avoiding the
for times ranging from 4 to 24 hr. The expense (in materials and manhours)
slow notch bend specimen was 4 in. long of the calibration experiment.

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INCORPORATION OF FRACTURE INFORMATION
IN SPECIFICATIONS

BY W. F. PAYNE1

SYNOPSIS
Fracture tests for material and process specifications involving high-strength
alloys are necessary to insure adequate inspection standards for material and
hardware acceptance. Proper specimen design is necessary to produce useful
toughness information, especially a specimen size adequate to avoid general
yielding prior to fracture. Evidence of significant toughness variation in
commercial alloys is presented. The paper illustrates the use of present analyti-
cal expressions to determine inspection standards for isolated defects of various
geometry and for linear arrays of multiple defects. Specific rejection criteria
for multiple defects are suggested.

The selection of a test, including SPECIMEN SELECTION


proper specimen size and design, for a A review of specimens and appropriate
given specification and for the most stress-intensity expressions is provided
useful application of data produced for in this symposium by Paris and Sih2
nondestructive inspection limits is the and Srawley and Brown2 The relation-
final step in the engineering applica- ship of specimens to practical applica-
tion of fracture mechanics. Selection of tion of fracture mechanics is discussed
an inappropriate specimen or one of by Tiffany and Masters. 4 For specifica-
inadequate size reduces the ability to tion use, a specimen must satisfy several
apply test data in the design and quality requirements:
control aspects of the fracture-analysis 1. The configuration should be con-
cycle. Considerable attention is there- venient to use for the product involved.
fore directed toward criteria for speci- For example, a notched tension test
men selection and proper use of the specimen is convenient for bar stock.
fracture data. Specifications also re- 2. Cost must be reasonable.
quire treatment of multiple defects; 3. Test technique and interpretation
therefore, a simplified analysis is in- must be simple and insensitive to tech-
cluded to illustrate the ability of present nique variation common to a testing
fracture mechanics methods to treat laboratory.
crack-geometry variations and crack- One factor affecting convenience and
interaction effects. P. C. Paris and G. Sih, "Stress Analysis of
Cracks," see p. 30.
s j. E. Srawley and W. F. Brown, "Fracture
I Metallurgist, Solid Rocket Division Toughness Testing," see p. 133.
( R P M B ) , Air Force Rocket Propulsion Labora- 4 C. F Tiffany and J. Masters, "Applied
tory, Edwards Calif. Fracture Mechanics," see p. 249.
357
Copyright9 1965by ASTM International www.astm.org
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358 FRACTURE ToraGmr~SS TESTING

cost is the minimum specimen size that Payne (1).5 As toughness levels increase,
can properly measure the toughness in the necessary specimen size quickly
the material without encountering net- becomes very large.
section yielding prior to rapid crack Requirements for tensile load capacity
propagation. Figure 1 shows the mini- and material volume of various speci-
mum size estimates for specimens capa- mens are also of practical interest.
ble of measuring two plane-strain Comparative values of these parameters
toughness levels (expressed as the are given in Table 1. The advantage of
Kic/ars ratio) using the criteria dis- the single-edge-notched specimen is
cussed by Srawley and Brown a and evident. The bend specimen compares

FIG. 1 - - M i n i m u m Specimens for Valid Kx~ M e a s u r e m e n t .

TABLE 1--RELATIVE LOAD REQUIRE~ favorably on a load-requirement basis,


MENT OF VARIOUS SPECIMENS FOR
E Q U A L K1c/ars M E A S U R E M E N T . although the material-volume require-
ment is greater. The bend specimen is
Specimen Load
Capacity Volume convenient for tests with any notch
orientation (surface or side notch) which
Single-edge-notched ( W --- is important for plate evaluation.
fiB) . . . . . . . . . . . . . . . . . . . 1,0 1.0
C e n t e r - n o t c h e d pop-in The plane-strain fracture toughness is
( W = SB) . . . . . . . . . . . . . 2.25 1.57 calculated using the maximum load and
N o t c h e d r o u n d bar (d/D=
0.7) . . . . . . . . . . . . . . . . . . 14 9.0
initial crack dimensions for the circum-
Surface-cracked plate ferentially notched round bar and the
( W = fiB) . . . . . . . . . . . . 6.75 3.5 surface-cracked specimens. Pop-in toad
N o t c h e d three-point-loaded
bend bar ( W = 6B) . . . . 0.175 2.25 6 T h e boldface n u m b e r s in parentheses refer
to t h e list of references a p p e n d e d t o t h i s paper.

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PAYNE ON INCORPORATION INTO SPECIFICATIONS 359

values are frequently used to calculate Progress toward widespread testing


Kxc for plate specimens when the speci- ability capable of giving reproducible
men size is insufficient to produce a results seems pitifully slow. Until frac-
plane-strain fracture at maximum load. ture values and techniques are estab-
The conditions necessary for accurate lished, incorporation of fracture tests in
and reproducible pop-in load measure- material specifications on a reporting
ments have not been established. Speci- basis appears to be the only practical
fication tests cannot be effective if the approach.

T A B L E 2 - - V A R I A T I O N I N Kr T O U G H N E S S OF Ti-6A14V SHEET. a

Heat Sp~imen Pand Size, in. GrainDir~tion Kr hsl %/~n.


D5256 . . . . . . . . . . . DD22 24 X 72 L 164.7
DD23 24 X 72 L 163.6
DD26 24 X 72 L 169.2
DD27 24 X 72 L 172.0
DD29 24 X 72 L 182.1
avg. 170.3 (L)

DD24 24 X 72 T 149.4
DD30 24 X 72 T 186.8
DD38 8 X 24 T 175.2
avg. 170.4 (T)

D5257 . . . . . . . . . . . DD4 24 X 72 L 157.7


DD9 24 X 72 L 193.0
DD10 24 X 72 L 179.9
avg. 176.9 (L)

DD5 24 X 72 T 163.3
DD6 24 X 72 T 165.7
DD11 24 X 72 T 178.5
DD12 24 X 72 T 165.1
DD21 8 X 24 T 160.6
avg. 166.2 (T)

D2963 . . . . . . . . . . . 248 8 X 24 T 128.5


250 8 X 24 T 124.5
avg. 126.5 (T)

D2382 . . . . . . . . . . . 283 8 X 24 T 121.9


285 8 X 24 T 125.9
avg. 123.9 (T)

o Sheet thickness, 0.050 in., center-notched specimen; 2 a/w -- 0.25; room temperature; loading-
rate effects negligible.
b Calculated with original crack size.

results can be influenced by personal T H E USE OF SUBSIZE SPECIMENS


interpretation of the test record or
insensitive instrumentation. Sufficient The literature contains descriptions of
information to design a test specimen many extensive test programs using
of minimum size, free from interpreta- arbitrarily fixed specimen geometries.
tion problems, does not exist for most These specimens are often smaller than
materials of interest. Some prior satis- the minimum size necessary for quantita-
factory testing experience by the test- tive measurement of K~c values. The use
ing organization seems essential before of a subsized specimen produces tensile
final specimen selection. instability prior to general yielding, and

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360 FRACTURE TOUGHNESS TESTII~IC,

gives a lower limit for the crack tough- mates of crack tolerance if test data are
ness--a conservative estimate of the obtained with specimens of inadequate
true K~o value. This approach is satis- size. The influence of specimen size on
factory to eliminate material of tough- the error associated with notch-strength
ness levels inferior to the toughness analysis is shown in Appendix I. For
value the specimen is capable of meas- example, using the smallest surface-
uring; the toughness of materials exceed- cracked specimen allowed by the cri-
ing this toughness value goes essentially teria in Ref (2), a 23 per cent overesti-

T A B L E 3 - - V A R I A T I O N I N K~ T O U G H N E S S OF Ti-6AI-4V SHEET. ~

Heat Specimen No. Panel Size, in. GrainDirection Kt,b ksi %/m.

D4949 . . . . . . . . . . . DD51 24 • 72 L 335.7


avg. 335.7 (L)
DD54 8 X 24 T 137.9
avg. 137.9 (T)
M5900 . . . . . . . . . . . 203 8 X 24 T 168.3
194 8 X 24 T 186.6
205 8 • 24 T 177.2
202 8 X 24 T 170.3
avg. 175.6 (T)

D2963 . . . . . . . . . . . 225 8 • 24 T 103.4


218 8 X 24 T 120.4
239 8 X 24 T 119.8
226 8 X 24 T 117.9
avg. l l 5 , 4 (T)

252 8 X 24 L 104.4
253 8 X 24 L 102.7
254 8 X 24 L 107.5
avg. 104.7 (L)
D2133 . . . . . . . . . . . 263 8 X 24 T 112.8
264 8 X 24 T 99.7
273 8 X 24 T 110.9
259 8 X 24 T 101.9
avg. 106.3 (T)

a Sheet thickness 0.025 in.; center-notched specimen; 2 a / w ~- 0.25; room temperature; loading-
rate effects negligible.
b Calculated with original crack size.

unmeasured. The ability to relate prod- mate of crack tolerance occurs with
uct test data to proper inspection notch-strength analysis.
criteria is reduced.
TOUGHNESS VARIATIONSIN CO~RCIAL
An example of misinterpretation of
Mrr,L PRODUCTS
fracture data is the use of notch-strength
analysis for surface-crack data, as shown Do we need another evaluation test in
in Ref (I). A number of investigators material specifications? It is reasonably
have defined the critical surface-crack simple to demonstrate that the toughness
size as a crack sufficient to reduce the properties of commercial alloys are sub-
notch strength (net fracture stress) to a ject to considerable variation. It is not
value equal to the yield strength. This simple to find examples of such varia-
definition can lead to optimistic esti- tion free from the confounding influence

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PAYNE ON INCORPORATION INTO SPECIFICATIONS 361

TABLE 4--TOUGHNESS VARIATION I N 18 P E R C E N T N I C K E L - C O B A L T -


MOLYBDENUM (300) M A R A G I N G STEEL AGED 900 F FOR 3 Hr.

Heat Thickness Tensile Yield KIt,a KI~, . -- Notch Strength,


Strensth, Surface-Cracked Center-Grac~eo Center-Cracked
No. in. km Specimen, ksi ~ Specimen, ksi ~ Specimen, ksi

1 .......... 0.14 295 (3) b 125 113 (4) 193 (4)


2 .......... 0.14 294 (2) 95 73 (5) 146 ( 3 )
A ......... 0.25 284 (2) 115 . . . . . .

CHEMICAL COMPOSITION"

Heat No. Ni Co Mo Ti AI C Si P S

1 ........ 18.63 9.00 4.66 0.66 0.070 0.013 0.045 0.004 0.005
2 ........ 17.80 8.96 4.85 0.63 0. 0 6 5 0. 027 0. 0 8 4 0. 0 0 5 0. 0 1 0
A ....... 18.43 8.71 4.06 0.70 0. 0 6 5 0. 011 0.045 0. 0 0 6 0. 0 0 8

Author's best estimate from reported test data.


b N u m b e r of r e p l i c a t e tests.

TABLE 5--IMPACT TOUGHNESS VARIATION FOR AISI 4340 STEEL. ~

Average Impact Energy, ft-lb Standard Deviation, per cent


Vendor Heat Forging Forging
Billet Billet
Base Cap Base Cap

AIR MELT

A ......... 1 10.7 ... 16.5 16.7 ... 4.42


2 13.2 15.9 ... 12.9 1.12 ...
3 13.3 17.3 ... 16.6 1.54 ...

B ......... 1 14.5 20.5 23.8 13.7 8.1 24.5


2 14.9 26.0 28.6 12.2 10.6 11.9
3 16.8 25.3 29.5 5.5 13.4 12.4
4 ... 19.5 26.0 ... 12.0 18.6
5 ... 22.0 .. ... 7.8 ...
6 . . . . . . 27.'3 . . . . . . . . .

VACUUM REMELT

C ......... 1 . . . . . . 13.6 . . . . . . 12.0


2 ... 13.8 ... 0.6
3 ... ii.'5 . . . . . . 61s . . .

4 . .. 18.6 . . . . . . 7.5 . ..

D ......... 1 19.0 26.8 34.4 17.2 19.7 14.0

S p e c i m e n s n o r m a l i z e d a t 1650 F f o r 1 h r a n d a i r cooled, a u s t e n i t i z e d a t 1550 F f o r 1 h r , oil-


q u e n c h e d a n d d o u b l e - t e m p e r e d a t 9 5 0 F f o r 1 h r a n d oil q u e n c h e d . All s p e c i m e n s t r a n s v e r s e a n d
bested a t - 4 0 F.

of testing variables. Several examples toughness variation between heats.


of toughness variation are included to Tables 2 and 3 show results obtained on
show that control of strength and chem- annealed Ti-6A1-4V sheets of 0.050- and
istry is not sufficient for control of ma- 0.025-in. thickness, respectively. The
terial toughness. average Kc values vary from 125 to
Center-cracked panel tests of air- 175 ksi ~ (These values were calcu-
craft sheet materials have revealed K~ lated using initial precrack length,

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362 FRACTtrPm TO~JGHNESS TESTING

TABLE 6--CHEMICAL ANALYSIS (PERCENTAGE BY WEIGHT) AND VENDOR.


Vendor Heat C Mn Si P S Cr Ni Mo

A ..... 1 0.41 0.75 0.31 0.009 0.014 0.83 1.98 0.25


2 0.42 0.76 0.30 0.007 0.016 0.75 1.84 0.22
3 0.39 0.77 0.30 0.009 0.012 0.78 1.98 0.26

B..... 1 0.41 0.71 0.28 0.011 0.015 0.76 1.82 0.24


2 0.40 0.69 0.28 0.010 0.009 0.78 1.70 0.24
3 0.41 0.73 0.30 0.008 0.009 0.78 1.83 0.23
4 0.41 0.75 0.30 0.010 0.005 0.82 1.86 0.25
5 0.40 0.73 0.30 0.009 0.007 0.77 1.75 0.23
6 0.41 0.75 0.30 0.010 0.005 0.82 1.86 0.25

C ..... 1 0.39 0.72 0.31 0.010 0.006 0.85 1.90 0.24


2 0.38 0.70 0.31 0.012 0.005 0.85 1.90 0.24
3 0.38 0.70 0.27 0.009 0.006 0.85 1.86 0.27
4 0.39 0.71 0.27 0.009 0.005 0.87 1.88 0.26

D..... 1 0.38 0.62 0.28 0.006 0.007 0.89 1.90 0.24

RESEARCH
"TYPICAL" .'~c 9 (I RD m .L RD
{PSI IN) 800 I100

PRODUCTION
CYLINDER PLATES
60 II & .L RD

20
z
0
400 600 800 I000 1200 1400
o .,~r (PSI IN)
o
o
~) 200 F CLOSURE PLATES

=60~- el " II RD
/ 9 O.RO

~ 20

80

400 600 800 I000 1200 1400


9~/c (PSI IN)

FZG. 2--Crack Toughness (K,) Distribution Curves for AMS M-255 Low-Alloy Steel.

rather than final crack length at frac- explained with chemistry or strength
ture.) variations. The two specimens employed
Melville (3) reported fracture tough- were a 2.25- by 12-in. center-cracked
ness variations among several heats of plate and a 1 by 8-in. surface-cracked
18 per cent nickel-cobalt-molybdenum specimen. Table 4 shows the toughness
(300) maraging steel which could not be levels in three heats~ including Kxc

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PAYNE ON INCORPORATION 1NTC SPECIFICATIONS 363

values from surface-cracked specimens, lar to the rolling direction, respectively. 6


pop-in with the center-cracked specimen, Under production conditions, closure
and notch strength for the center- plates (135 plates from 28 heats) gave
cracked specimen (reflecting plane-stress an average toughness (~c) of 1000
toughness behavior). in-lb/in3 with no directionality. Cyl-
Table 5 is a summary of impact tough- inder plates (29 plates from 13 heats)
ness data on AISI 4340 low-alloy steel were also checked and gave an average
obtained in a forging procurement ~c value of 500 in-lb/in. ~ with no direc-
program by Watertown Arsenal. Tough- tionality. The actual toughness distribu-

.J
/

.. A

i l i I
SPEC. AXIS FRACTURE
NO. - DIRECTION
I W R
J
2 W T
3 R W
4 R T
5 T W
6 T R

FIG. 3--Crack-Propagation Directions in Plate.

ness variation from vendor to vendor is tion curves are shown in Fig. 2. These
most significant, followed by heat varia- pronounced toughness differences be-
tion and location in the forging. The tween the closure and cylinder plates
chemical analysis is given in Table 6 could not be correlated with chemistry
and is very uniform except for sulfur or strength level.
content of the first four heats. The possible directionality of tough-
In the Polaris program, research
e Measured with center-cracked specimens
studies by Aerojet on AMS M-255 low- 2.5 in. wide with 30 per c e n t notch and notch
alloy steel plate (hardened to a minimum radius less t h a n 0 001 in. formed by elox m a -
yield strength of 190 ksi) indicated chining. The notch was n~t fatigue-cracked,
b u t t h e radius was about ~ of the plastic-zone
~ values of 800 and 1100 in-lb/in. ~ for radius and m a y have been satisfactory for
the direction parallel to and perpendicu- valid Kc values.

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364 FRACTtTRW T o u G ~ s s TESTING

ness in the mill products must be con- steel. The values were 310, 245, 230, and
sidered, for various specimens often 150 in-lb/in. ~ corresponding to orienta-
measure the toughness of different tions RT, RW, WR, and TW, respec-
directions. In a three-dimensional body, tively. This toughness variation arises
there are six potentially different fracturefrom chemical banding and preferential
directions as shown in Fig. 3, although orientation of impurities by the rolling
there are only three different axes. For operation. If toughness tests are used to
sheet products, a center-notched or control the laminar banding, specimens
single-edge-notched specimen would with orientation WR or RW should be
measure crack toughness in the WR used. Use of specimens with a W T or
and RW orientation (Nos. 1 and 3 of RT orientation would be misleading
Fig. 3). A surface-cracked specimen because the indicated toughness would
would measure the toughness of the improve as the banding became more
W T and RT directions (Nos. 2 and 4 of severe. For sheet and thin plate, surface-
cracked specimens would be misleading

~ RW
FRACTURE
DIRECTION
and single-edge-notched, center-notched,
or possibly notched bend tests would be
necessary. Occurrence of any splitting
RT
in a fracture surface with W T or RT
orientation should suggest additional
tests in the WR or W T orientation.
The precracked round bar tension
specimen can propagate in any direction
in the plane of the notch. Tiffany and
Lorenz (5) measured the propagation
direction in notched bars of D6AC low-
0 ~S ,5o 4.5 (o0 75 90
AN6LE
e(DE6REE~ alloy steel by careful fracture-surface
analysis. The distribution curve for
FIo. 4--Frequency D~tdbution of Propaga- propagation direction relative to grain
tionAnglein Notched Round Bar Tests on
D6AC Low-AlloySteel. direction is shown in Fig. 4. In this
example, the toughness value did not
Fig. 3). A precracked round tensile bar vary significantly for the different propa-
would measure the lowest toughness gation angles involved.
orientation for a given axis direction. Sufficient data have been included to
With tl~ick plate, single-edge-notched or show the toughness variation that can be
surface-cracked specimens can be sliced encountered in conuuercial mill products,
through the thickness, which allows including variation among heats, among
evaluation of any orientation of the W grain directions, and among propagation
and R directions. A bend specimen can directions for a specific grain direction.
usually be used to measure any orienta- Proper attention to the source of tough-
tion of the W and R direction. Testing ness variation is necessary in a fracture
in the short-transverse (T) direction is evaluation program. In previous at-
usually difficult or impassible on finished tempts to compare toughness "values
mill products. from different specimens, the difference
Pellisier (4) has reported 9,~ values in measured values has often been asso-
for 1-in. plate of 18 per cent nickel- ciated with material orientation variables
cobalt-molybdenum (250) maraging rather than specimen variables.

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PAYNE ON INCORPORATION INTO SPECIFICATIONS 365

-- ~ -- ~ ' ~ - "6 J ~ ~A ~,

(a) SURFACE FLAWS

Cb) INTERNAL FLAWS


Fro. 5--Equivalent Flaw Geometryfor SingleCracks.

(•) ( SPACING (S)

a) S=2D
D=5.2

(a) S=D D=3.5

O0 (b) S=O
D=4.4 (~ FAILURE LIKELYt CRITICALSIZE FOR
_
S-O.5D D -. 2 . B
INTERNAL SPLIT
~ CRITICAL SIZE FOR ~NGLE ELLIP~7
0:0:0:0:0<3
"--_"<r _~S-"
(c) CRACKARREST LIKELY
S= 0.3D D=I.6
(c) FAILURELIKELY (.d) CRACKARREST Fro. 7--Equivalent Flaw Geometry for an
S=0.5D D=3.2 LIKELY Array of Cracks.
S= 0.3D D=2.4
FzG. 6--Equivalent Flaw Geometryfor Two
Cracks.

EFFECT OF FLAW GEOMETRY AND elastic fracture prior to general yielding


MULTIPLE FLAW INTERACTIONS but small compared with structural
thickness. (Most real problems are non-
Specifications must establish allowable
ideal and should be handled individ-
defect levels for many possible combina-
tions of flaw shape, location, and fre- ually.) Crack orientation is taken as
quency of occurrence (multiple defects). perpendicular to the principal load. This
Fracture mechanics can help establish simple model is used to illustrate that
these defect limits. The simplified model present knowledge can be employed
used consists of a structural member con- usefully in specifications.
raining cracks sufficiently large to induce Available stress-intensity expressions

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366 FRACTURE TOUGHNESS TESTING

were used to determine various arrange- 7(c). The interaction of two coplanar
ments of flaw size, shape, location, and elliptical surface flaws was discussed by
interactions which should produce an Tiffany and Masters# Very little inter-
equivalent "effective crack size" and action was found unless the separation
therefore equal fracture strength. A became less than the flaw depth. Espe-
plane-strain fracture mode is assumed, cially noteworthy is the confirmation of
and size units given are relative to a long predicted behavior by experimental
surface crack with assumed depth of one results, as evident in Fig. 32 of their
unit. The calculations made are included paper.
in Appendix II. The effect of crack shape The results of these crack-interaction
for surface cracks and internal cracks is predictions may be summarized as
shown in Fig. 5. The effect of crack size follows:
and separation for two flaws and a linear 1. Cracks separated by more than
array of flaws are shown in Figs. 6 and 7, three crack lengths may be considered
respectively. Careful interpretation of as independent flaws.
the flaw-interaction effect is required, 2. For two adjacent flaws, diameters
because the analysis is based on stress- less than 40 per cent of critical single-flaw
intensity magnification between the diameter may be neglected.
cracks rather than around the entire 3. For a linear array of flaws, diam-
crack surface. The magnification effect eters less than 30 per cent of the critical
between cracks tends to initiate fracture single-flaw diameter may be neglected.
of the ligament between the cracks. As 4. For a two-dimensional array (esti-
the crack edges get close together, the mated only), diameters less than 20 per
magnification effect becomes unlimited cent of the critical single-flaw diameter
and the joining of these flaws would be may be neglected.
certain. However, general propagation 5. For two coplanar surface flaws,
to total fracture would be questionable interaction may be neglected if the
if the crack size after joining were signifi- separation distance exceeds two crack
cantly smaller than the critical single- depths.
flaw size of appropriate geometry. For These relative crack-geometry effects
example, the two flaws of Fig. 6(c) could should be generally valid for any homo-
join together and form an ellipse of geneous material. The actual crack sizes
nearly critical size which would probably will be dictated by specific values of crack
propagate to complete fracture, as indi- toughness, applied stress, and secondary
cated in the figure. However, the two influences such as plastic-zone correc.
flaws in Fig. 6(d) could join together and tions.
still require considerable crack growth
before critical size and general fracture QUANTITATIVE INSPECTION LIMITS
occurred. Propagation of these defects to Establishing sound engineering in-
failure seems unlikely and crack arrest spection criteria requires more than
would be expected. Similarly, the connec- accurate toughness measurements on
tion of cracks in a linear array would be raw material and analytical expressions
expected to induce total fracture only if relating flaw size and crack toughness
the resulting crack width approached to fracture strength. To establish initial
the critical crack width for a long internal inspection limits that would insure a
crack as shown in Fig. 7(a). Smaller successful service life requires several
cracks would join to form stable sub- additional steps:
critical cracks as shown in Fig. 7(b) and 1. Evaluation of toughness and

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PAYNE ON INCORPORATION INTO SPECn~ICATIONS 367

strength changes during manufacturing sen ted during this symposium. For ex-
operations such as forming, welding, and ample, the critical diameter, D, for an
heat treatments. internal circular flaw (Q of 2.2) under
2. Evaluation of subcritical crack plane-strain conditions, with an applied
growth during service. stress, ~, can, by neglecting plastic-zone
3. Establishing an inspection safety corrections, be written as D = 1.4
factor to protect against inspection (Kit/errs) 2. We can define a general
limitations and unknowns or changes in factor, f, as the "inspection safety fac-
service conditions. tor," having a value between 0 and 1.
The f factor reflects both subcritical
The pronounced effects of operations crack-growth allowance and safety mar-
such as heat treatment and welding are gin selected to account for uncertainties
well known. The influence of forming in service conditions and inspection
operations should also be considered. operations. This would produce the form
For example, Sernka (6) has reported D = 1.4f(Ki~/ars) 2. Such representation
that direct aging after shear spinning would help separate and communicate
of 18 per cent nickel-cobalt-molybdenum the analytical estimates and engineering
(300) maraging steel reduced the Kc design judgments used to produce final
toughness from 150 to 80 ksi ~ The inspection limits from initial crack-
proper crack toughness value for estab. toughness and strength-level informa-
fishing hardware acceptance limits may tion.
be different from the values charac-
teristic of the as-received mill product. CONCLUSIONS
Preliminary attempts to evaluate
subcritical crack growth for pressure- Fracture tests as part of material
vessel applications are discussed by specifications are necessary and should
Tiffany and Masters. 4 Even for this be used even though testing problems
simple application, uncertainties exist in still exist. The principal problems are
crack-growth predictions and additional specimen selection, test interpretation,
safety margins must be employed until lack of assured reproducibility between
growth kinetics is better understood. specimens, and uncertain toughness
Uncertainties also exist with any in- variation with orientation. A period of
spection method. Most nondestructive joint user and supplier trial testing effort
inspection methods can fail to detect on a report-only basis is suggested to
cracks or defects that are tight or in an minimize these problems.
inconvenient orientation. Human error Present fracture mechanics methods
must also be expected. Additional un- can aid in establishing rejection stand
certainties, such as residual stresses and ards for various crack geometries and
local material heterogeneities, make interaction of multiple cracks. This type
precise analysis of growth kinetics and of analysis is essential for nondestructive
fracture behavior difficult. It is clear inspection limits and material review
that final hardware acceptance criteria, board actions on specific material and
based on nondestructive inspection, hardware discrepancies.
must contain an engineering judgment The inherent ability of fracture me-
on the proper safety margin to accom- chanics analysis effectively to integrate
modate these unknowns. the frequently divergent disciplines of
It is possible to include this judgment materials, manufacturing, .and quality
factor in the analytical expressions pre- control operations should be recognized.

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368 FRACrUa~ T o u g m , mss T~STr.NO

A cknowledgment: provided by H. Bernstein of the Special


Project Office, Department of the Navy.
The impact-toughness information The assistance of C. F. Tiffany and
in Table 5 was taken from information P. C. Paris in many discussions on the
supplied by D. E. DriscoU of Watertown application problem is gratefully ac-
Arsenal. The Polaris M-255 data were knowledged.

RE~'ERENCES
(1) W. F. Payne, "Analysis of Surface Crock (4) G. E. Pellisier, "Some Mierostructural
Fracture Toughness Information," F~mrd* Aspects of Maraging Steel in Relation of
Maraging Steel Project Review, Volume 1, Strength and Toughness," Third Mamging
ML-TDR-64-225, USAF, Wright-Patterson Steal Project Raq~,'w, RTD-TDR-63.d048,
Air Force Base, Ohio, July, 1964, pp. 307- USAF, Wright-Patterson Air Force Base,
367.
(2) "Progress in Measuring Fracture Tough- Ohio, November, 1963, pp. 407--428.
ness and Using Fracture Mechanics," Ma- (5) C. F. Tiffany and P. M. Lorenz, "An In-
tmials Research & Standards, Am. Soe. vestigation of Low-cycle Fatigue Failures
Testing Mats., Vol. 4, No. 3, March, 1964, Using Applied Fracture Mechanics," ML-
pp. 107-119. TDR-64-53, USAF, Wright-Patterson Air
(3) A. Melville, "Metallurgical Evaluation of Force Base, Ohio, May, 1964, p. 26.
18% Nickel Maraging Steel (300 ksi (6) R. F. Sernka, "Some Considerations in
Strength Level)," Third Maraging Steal Shear Spin Processing," ASM Technical
Project Reriew, RTD-TDR-63-4048, USAF, Report No. W4-1.1, Am. SOc. Metals,
Wright-Patterson Air Force Base, Ohio,
November, 1963, pp. 327-368. March, 1964.

APPENDIX I

COMPARISON OF CRITICAL CRACK-SIZE DETERMINATION WITH GROSS-


AND NET-STRESS CRITERIA FOR SURFACE-CRACKED SPECIMEN

Use of net stress, rather than gross stress, crack-size relationship predicted by the
has unfortunately been adopted by many Irwin analysis. The fracture curve termi-
investigators. The use of net stress to deter- nates at the yield strength (point A) and
mine crack tolerance can lead to incorrect the a/Q~, value for a fracture stress equal
(optimistic) estimates of crack tolerance. to the yield strength is given by:
The following analysis was performed to
indicate when such estimates would be sig-
,, = 1.21r era t . . . . . . . . . (1)
nificantly in error.
The critical crack size, a,r is defined as The apparent critical crack size determined
the minimum surface-crack size sufficient to with the net stress equal to yield-strength
initiate rapid fracture in a surface-cracked criterion (point B) is larger by the amount,
flat tension specimen subjected to a given e. The (a/Q)~t at B can he calculated by
tensile load or gross stress. For this study, determination of the identical value of
the specific critical crack size of interest is (a/Q)~t at point C. If ~roe, *ffi ~rrs, then
the a~r value for a gross strength equal to the gross stress at C for a ratio, x, of crack
the 0.2 per cent offset yield strength, usually area to specimen area, where x = A d A o ,
the highest conceivable design strength for must be
material. Crack size will be represented in
crg(r ---- r -- x) = ~rs(1 -- x)...(2)
the "normalized" form, a]Q, which is equiva-
lent to crack-depth or crack-length repre- The ratio of ~net to ~o as a function of crack
sentation when the a/Q ratio is constant. area A,/Ao, is shown in Fig. 9. Hence,
Figure 8 shows the fracture-stress versus (a/Q)n,t can be found from

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PAYNE ON INCORPORATION INTO SPECIFICATIONS 369

o'.T s

O'ys

] (Kic= CONSTANT)
I
I
(CI,/Q)cR (CL/Q)NET
FL,~W SIZE {Q/Q)
FIG. 8--Fracture-Strength Curve for Surface Cracks.

1.30
/
o
1.20
/
~ ASTM (TENTATIVE)LIMIT

i.iO
/
I.O0 /
O O.IO 0.20 Q.30
Ac/A o RATIO
FIO. 9--Effect of Crack Area on Ratio of Net Stress to Gross Stress for a Surface-Cracked
Specimen.
TABLE 7 - - E F F E C T OF GEOMETRY ON
NET STRESS AND (a/Q)orUSING NET-
~a 1.21~8s( 1 - x) = ..... (3)
STRESS ANALYSIS.
Error in Subtracting E q 1 from E q 3, the error in
x = AetAo 1 -- x Cnet/ag (a/Q)or, critical crack-size determinations, using the
per cent
net-stress criteria, is given b y
0 1.00 1.00 0.0
0.01 0.99 1.010 2.0
0.02 0.98 1. 020 4.1
0.03 0.97 1.031 6.3
0.04 0.96 1. 042 8.6
0.05 0.95 1.053 10.8 1 . 2 1 ~ r s ~ (1 -- x) 2 1 . . . . (4)
0.07 0.93 1.07,5 15.6
0.10 0.90 1.111 23.4
0.13 0.87 1.149 32.0 e(%) ffi 100 (1 -- x)' 1 ..... (.5)
0.15 0.85 1.176 38.4
0.20 0.80 1. 250 56.2
0.25 0.75 1. 333 77.7 Although the actual error in (a/Q),, varies
0.30 0.70 1.428 104.1
with the (Kz#o'rs) ratio, the relative o r

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370 FRACTURE TOUGHNESS TESTING

/
40

lu

-~ 3O

~ 20
STM {TENTATIVE') LIMIT

0 0.05 0.10 0.15

A c / A o RATIO

FIG. 10---Error (Overestimate) in Crack-Tolerance Estimates Caused by Notch-Strength


Criteria as a Function of Surface-Crack Area.

percentage of error is only a function of the example, a 10 per cent error (overestimate)
crack and specimen geometry. Calculations would be expected for a crack area of about
using Eq 5 are given in Table 7 and shown 5 per cent, a common value for small surface-
in Fig. 10. cracked specimens. The ASTM limit of
The use of (a/Q)~r, or act or let, based gnet ----< 1.1 gg (established for Kic calcula-
on net-stress criteria can introduce signifi- tions with ga only) could acllow a 23 per
cant errors (overestimates), especially for cent overestimate of (a/Q)r if analyzed
small cracked specimen geometries. For using net-stress criteria.
APPENDIX II

CALCULATION OF EQUIVALENT CRACK SIZE FOR VARIOUS CRACK


GEOMETRIES AND INTERACTION OF MULTIPLE CRACKS

The effect of crack geometry (single crack size). All size units are based on a long
cracks) can be calculated with the expres- surface crack of a depth of one unit.
sions found in the Fifth Report of the ASTM For surface cracks, all geometries must

TABLE 8. TABLE 9.
Geometry Q Depth, a Length, 2c Minor
Geometry Q Axis ffi c
2(1.21a)
Long crack ..... 1.0 1.0 very long
2c = 4 a . . . . . . . . 1.61 1.6 6.4
Long internal
2c = 2 a . . . . . . . . 2.42 2.4 4.8
split ........ 1.0 2.42 very long
c = 2b . . . . . . . . 1.61 3.90 7.8
c = b (circular). 2.42 5.85 5.85
Special Committees on Fracture Testing of
High-Strength Metallic Materials (2) for
the plane-strain fracture mode. The calcula- have identical (a/Q) values. For cracks of
tions are made without any plastic-zone length 2c and depth a, see Table 8.
correction (which does not affect relative For internal cracks, the surface equation

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PAYNE ON INCORPORATION INTO SPECIFICATIONS 371

TABLE 10--EFFECT OF MULTIPLE FLAW 2 (1.21a), the sizes equivalent to the surface
GEOMETRY ON ALLOWABLE DEFECT
SIZE. cracks given in Table 8 are given in Table 9.
The effect of multiple cracks was esti-
Numberof ssum~l mated from the analysis for stress-intensity
Cracks
~epara- Mk ~meter Separa-
tion
tion magnification between colinear through-
thickness cracks, assuming the effects would
1 (circular).9 9 i.85 be similar for internal cracks under plane-
2 ........... 4D t .02 5.6 22.4 strain conditions. A more accurate analytical
2D t.06 5.2 10.4 treatment may appear in the future, but no
D t.16 4.4 4.4 serious changes in the conclusions drawn
0.5D t.34 3.2 1.6
0.3D t .56 2.4 0.7 from this engineering estimate are expected.
The size for multiple cracks equivalent to
3 ........... 4D t.06 5.2 20.8 an internal circular crack of 5.8 units varies
2D t.12 4.6 9.3
D [.30 3.5 3.5 inversely with the square of the magnifica-
0.5D t.58 2.3 1.2 tion factor, M , . As noted in the paper, the
0.3D t.9 1.6 0.5 magnification effect only occurs between the
particles. Crack propagation between mul-
is altered by elimination for the 1.21 co- tiple circular cracks of size considerably less
efficient which means the effective crack than the critical size for a long internal
size for internal defects is 1.21 larger than split would presumably be arrested as a
the size of surface cracks. For internal de- subcritical crack. The values obtained with
fects of major axis, 2c, and minor axis, 2b ffi these calculations are given in Table 10.

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STP381-EB/Apr. 1965
372 FRACTURE TOUGHNESS TESTING

DISCUSSION
j. STEPHEN PASCOVERX---Mr.Payne is 2. excessive net section yielding
to be congratulated on a fine paper and 3. the properties of the weld metal
on his "user-oriented" approach to
fracture toughness testing. The present All three of these qualifications were
discussion is concerned, however, with pointed out in the original report.
the data reported in Table 7, item 7, on While the integrity of the data was not
the 9Ni-4Co(200) alloy. This value for essential in the context of the subject
paper, the tendency to quote values from
K~c of 70 ksi V/i~. ( K , c / Y S = 0.35) is such compilations out of context makes
not representative of those normally
it mandatory that more representative
obtained in this steel. Referring to the
values be pointed out. Such data appear
author's source, * the value reported in Table 11.
represents:
1. a nontypical composition S First Quarterly Progress Report on AF
Contract AF33(657)-11229, Development of
Welding Procedures and Filler Materials for
a Research metallurgist, Republic Steel Joining High Strength Low Alloy Steels E R
Corp., Cleveland, Ohio. 5554, October, 1953 (unpublished).

TABLE l l - - P R O P E R T I E S OF 9 P E R C E N T NICKEL-4 P E R C E N T
COBALT (200) MATERIALS.

Tempering Yield U l t i m a t e KIr Notch


Strpn~th,
Form Temperature, Strength, Tensile kai ~/imn. Ref Remarks
deg F kai Strength,ksi

1-in. plate . . . . . 400 193 259.4 111 142 ~ surface-flawed speci"


men 3 ill. wide
and 1 in. thick.
a = 0.27in.,l-
0.88 in.

1 in. plate . . . . . . 800 189 205.5 138 182 a same specimen, a ~-


0.30 in., l -~ 0.90
in.

1-m. plate . . . . . . 1000 185 195 ... 195 a a = 0.34, l = 1.1 in.

1-in. plate . . . . . . 1000 193 202.5 139.4 300 b slow bend specimen.
0.875 by 0.875 by
4 in.

Side center weld


metal 1-in.
plate. . . . . . . . . as T I G 173.0 203.0 118.3 253 b slow bend specimen
welded as above, avg. of
three weldments

a Aerospace Structure Metals Handbook, Syracuse University Press, Syracuse, N. Y., 1964 edi-
tion, Section FeUH, Code 1221.
b E. A. Steigerwald, TAPCO group of Thompson-Ramo Wooldridge, private communication
to J. G. Hill, United Technology Center, Oct. 25, 1963.

Copyright9 1965 by ASTM International www.astm.org

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Panel Discussion

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INTRODUCTION TO THE PANEL DISCUSSION
BY W. F. BROWN, JR.
During the planning for this Sym- A. A. Wells, Queens University, Belfast
posium it became quite evident that Ireland
amp!e opportunity should be provided
for those interested in fracture testing The panel gave first attention to
to ask questions of the authors and to written questions submitted in advance
make comments on their papers. Such of the meeting. An appropriate notice to
opportunity is normally provided by a this effect appeared as part of an article
discussion period after each presentation, summarizing the activities of the ASTM
but this is almost always too short to be Special Committee on Fracture Testing
effective. It was therefore decided to de- published in the March, 1964 issue of
vote an entire session to a panel discus- Materials Research & Standards. The
sion, the panel being made up of a group response to this notice was gratifying;
of people who have been closely con- many pertinent and often penetrating
nected with the ASTM Special Com- questions were received in advance of
mittee for Fracture Testing of High the meeting both from persons in this
Strength Materials, and most of whom country and from abroad. Questions and
also wrote papers for the symposium. comments from the floor formed the
The panel discussion was based on ques- basis for discussion in the last half of the
tions submitted to the members. These session. These encompassed a broad
related not only to information presented range of experience in fracture testing,
in the symposium papers but also in- from high strength alloys to plastics.
cluded questions of general interest in Unfortunately, time did not permit
fracture mechanics. covering all of the written questions,
The panel was composed of the follow- nor was the panel able to resolve satis-
ing persons: factorily, in the time available, some of
W. F. Brown, Jr., chairman: NASA-Lewis, the points raised in the discussion from
Cleveland, Ohio the floor.
T. J. Dolan, University of Illinois, Urbana, The entire panel discussion was satis-
Ill. factorily tape-recorded, and the following
G. I. Irwin, U. S. Naval Research Labora- account is based on a transcription made
tory, Washington, D. C.
Paul C. Paris, Lehigh University and Na- from the tapes. The record is complete
tional Science Foundation, Washington, with the exception of those parts of the
D.C. discussion from the floor which dealt
W. F. Payne, Air Force Flight Test Center, with data not presented to the panel
Boron, Calif. either before or during the meeting.
J. E. Srawley, NASA-Lewis, Cleveland, The panel members wish to express
Ohio their appreciation to Mrs. M. A. Bishop
C. F. Tiffany, Boeing-Aerospace Div.,
Seattle, Wash. of the Strength of Materials Branch,
Volker Weiss, Syracuse University, Syra- NASA-Lewis, for her efforts in reducing
cuse, N. Y. the tapes to typescript,
375
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376 FI~.ACTURETOUGHNESS TESTING

PANEL DISCUSSION

W. F. BROWN (author)--One of the are equally good; but in some cases (dif-
authors has compared different analytical ficult problems) the things which can
solutions for the symmetrically notched be done give results only within 10 per
plate on the basis of solutions obtained cent. So, in summary, it is a matter of
by complex-variable techniques (con- judgment on these problems, which is
formal mapping procedures) which are mainly a matter of understanding the
stated to give very high accuracy. Mr. details of mathematical analysis.
Paris, is there a basis for considering the MR. BROWN--I would like to ask
accuracy of the solutions obtained by Mr. Paris another question. Does the
complex variable techniques to be higher mathematician have formal methods for
than those available by other methods? predicting the accuracy of these solu-
P. C. PARIS (author)--In my inter- tions?
pretation, this is strictly an elasticity MR. PARIs--The best method is ex-
problem to be solved. The accuracy of the perience, as it is in many other situations.
solution of an elasticity problem can be However, if you look at convergence, that
"exact" if one satisfies the differential is, how rapidly terms or results converge
equations involved (that is, equilibrium, in a series, it is one means of judging the
compatibility) and all of the boundary accuracy of solutions. For example,
conditions of the problem with the Isida has used methods in which ex-
mathematical solution. The solutions tremely high convergence is present.
which are referred to in the question are Therefore, the confidence in the methods
approximate solutions, so it is a matter that he has used should be very high.
of judgment as to how well these approxi- Very often it is mainly a matter of con-
mate solutions suit each of the equations. vergence upon which the accuracy of ap-
There are some principles of theory of proximate solutions are judged by the
elasticity which help one to make these mathematician.
judgments. For example, if an error is J. E. SRAWLEY (author)--May I ask
made in a boundary condition which is Mr. Paris a related question? How
well away from the crack tip and the error accurate is the basis of comparison
is of the nature of adding an equilibrium between the results of experimental
system of forces which has small dimen- compliance measurements of ~ and
sions, St. Venant's principle states that analytical calculations of K?
far away from that system of forces no MR. PARIS---In theory, the compliance
appreciable change in stresses will be method is exact. But there is a question
caused. Then there would be no error in which is not quite resolved in my mind
stresses near the crack tip. The complex- as to whether the compliance measure-
variable methods to which the question ment should be interpreted as plane-
refers are probably those used by Oscar stress or plane-strain. And, though com-
Bowie." He uses methods of mapping of pliance measurements should be exact, in
problems and he does this to a very high practice they are difficult to perform. I
degree of accuracy, using very sophistica- think the compliance measurements
ted mathematical techniques; probably which have been made, for example, at
his answers are well within 1 per cent. the Lewis Research Center of the Na-
Similarly, other approximate methods, tional Aeronautics and Space Adminis-
such as collocation techniques and en- tration (NASA) have been done with
ergy methods, often give results which extreme care, and from what I can gather
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PAI'V~:L Discussion 377

should be very accurate. But let us point ing conditions for the two approaches are
out one thing on this, that if the compli- different. Bowie's analysis relates to a
ance measurements are plane-strain specimen with uniform distribution of
measurements, instead of plane-stress, stress, whereas compliance measurements
then both Bowie's and Gross's solutions are based almost without exception on
to the edge-notched plate (which we are pin loading. Compliance specimens gen-
really referring to here) are in disagree- erally are not long enough to permit the
ment with the compliance measurements. concentrated pin load to approach a uni-
MR. BRowN--Mr. Paris, I gather form stress distribution at some section
from what you are saying, that if we between the pin and the crack; since this
have competent mathematicians work- would be a necessary condition for equiv-
ing on these problems and if their re- alence between the two approaches, the
sults agree, we probably have the right results should not be exactly comparable.
answer. Additional confidence is gained MR. BROWN--I disagree with that and
ii we have experimental methods which would like to get Mr. Srawley's comment.
check the mathematical techniques. He was the one responsible for these com-
MR. PARIS--Well, yes. I would like to pliance measurements, and great pains
make one further comment. After going were taken to avoid interaction between
through all the papers and looking at all the stress fields of the notch and of the
of the methods myself, I would be much pins.
more pleased if we could have two differ- MR. SRAWLEY--In our compliance
ent analytical approaches to each prob- measurements we did establish by experi-
lem and have them agree to within 1 per ment what was a sufficient specimen
cent before we say "this is it." length to avoid interference between the
MR. BRowN--That certainly would be stress-field disturbance around the crack
desirable. Mr. Srawley and I have been and those around the loading pin holes3
accused of being overly concerned with However, some specimen bending occurs
the stress-analysis accuracy, considering in compliance measurement, just as in an
that the reproducibility of material be- actual crack toughness test, and this is
havior is sometimes rather poor. Our not considered in the analytical pro-
concern stems in part from a lack of cedures of either Bowie or Gross. The
familiarity with all the mathematical results show an increasing discrepancy
solutions. However, a knowledge of this with increasing crack depth between the
accuracy is necessary if we are properly experimental and analytical values of K.
to evaluate our fracture data. We do not I attribute this primarily to the speci-
demand an accuracy of 1 or 2 per cent, men bending effect. I would like to add
but we do want to know what the ac- that I think we have a more accurate
curacy may be within reasonable limits. knowledge of the dependence of ~ or K
Very little attention seems to have been on crack length for single-edge-notched
given to this question in the past. specimens, either in tension or bending,
J. I. BLtmML---The apparent dis- than for any other type of specimen, be-
crepancy between Bowie's results and cause we have accurate compliance data
those derived from compliance tech- for these specimens which are in good
niques is believed to stem from the fact agreement with the analytical results.
that the specimen configuration and load- 2 j. E. Srawley, M. H. Jones and B. Gross,
"Experimental Determination of the Depend-
ence of Crack Extension Force on Crack Length
1 Chief, Applied Mechanics Research Labora- for a Single-Edge-Notch Specimen," N A S A T N
tory, U.S. Army Materials Research Agency, D-~398, National Aeronautics and Space Ad-
Watertown Arsenal, Watertown, Mass. mini-qtration, August, 1964.

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378 FRACTURE TOUGHNESSTESTING

MR. BROWN--I will direct the next same question to Mr. Srawley who has
question to George Irwin. What is meant been engaged in the problem of trying to
by the onset of rapid crack extension and measure the onset of rapid crack exten-
why does the committee equate this with sion.
the maximum load in a fracture test? MR. SRAWLEY--In general, I agree
G. R. IRWIN (author)--The onset of with what Mr. Irwin has said. The onset
gross plastic yielding of a tensile bar is of rapid crack extension is not always
usually abrupt, in a relative sense. It is sharply defined, but the load at which it
natural, therefore, to use this as a meas- occurs is very little different from the
urement point to indicate the strength of maximum load recorded in the test. By
the material relative to plastic yielding. taking it as occurring at maximum load,
In the case of fracture, the onset of rapid we remove any ambiguity about what
crack extension is abrupt to about the load to use in calculating K~ or 9~. The
same degree and use of this as a measure- practical testing problem is not to de-
ment point for crack toughness is an fine the load, but to define the crack
equally natural choice. We cannot ex- length at onset of rapid crack extension,
pect every material and test situation to because the crack length may increase
provide a perfectly sharp measurement considerably in the last stage of the test
point for crack toughness. The problem while the load is almost constant. Even
here is not unfamiliar because lack of when a record of crack length versus
sharpness in the yield-point indication time is obtained during a test, there is no
is often encountered. It is considered apparent objective basis for choosing the
best to adopt such rules as are necessary point of onset of rapid crack extension--
so that a property characteristic of re- different investigators will choose signifi-
sistance to plastic yielding can be meas- cantly different values. The other thing
ured and recorded, and we must do the I would say about the choice of the max-
same thing for fracture. In case of meas- imum load as the point of onset of rapid
urement-point ambiguity in a crack crack extension is that it is appropriate
toughness test due to lack of any abrupt for use in connection with the concept of
starting point for onset of fast fracture, the crack-extension resistance curve.
one can usually resolve the problem by I consider this a very promising basis
selecting the place in the behavior pat- for further exploration into the question
tern where the relationship of crack ex- of fracture toughness. For research pur-
tension to load provides a nearest ap- poses at least, it would be desirable to
proach to abruptness. conduct tests to determine R-curves
The crack speed necessary to cause a rather than simply ~,, as elaborated in
maximum load point is roughly the speci- the symposium paper by Mr. Brown and
men width divided by the load-rise tin~e, me.
which is a very small velocity. In addi- MR. BROwN--The next is a very prac-
tion, in the absence of crack extension, tical question. Consider two materials of
the load must increase until fully plastic roughly the same yield strength and hav-
yielding has developed. Thus, when on- ing the same fracture toughness (K,)
set of rapid crack propagation is abrupt value, these values to be determined
and occurs prior to general yielding, a from the same type and size of speci-
maximum load point occurs in coinci- men. In one case, the K, responds to a
dence with the initial acceleration of the relatively low gross-area stress combined
crack speed. with substantial slow crack extension,
MR. BROWN--I would like to refer the and in the other case with a higher gross-

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PARCEL DISCUSSION 379

area stress but with less slow crack ex- the larger plastic zone surrounding the
tension, so balanced that we get the same tip of the crack. It is actually working in
value in Kc. Which material is to be service at a stress which is a much lower
preferred for pressure-vessel applica- fraction of the critical stress than was
tion? used to determine the Kc value; the
MR. IRwiN--The answer to that ques- short crack might be preferable from this
tion depends upon the application. If the viewpoint. I think perhaps the most im-
slow crack extension under consideration portant factor is whether or not the
was due to an environment effect not nature of the environment will stimulate
present in service, then of course this par- slow crack growth to critical size.
ticular amount of slow crack extension is MR. B R O W N - - W e certainly should
not important. On the other hand, one hear from Mr. Tiffany, because he gave
can well recognize that there might be the lead paper on practical application.
cases in service where the slow crack ex- C. F. T ~ F A ~ (author)--If the speci-
tension was quite possibly due to an en- mens contained different initial crack
vironmental effect, in these cases one sizes, one might expect that the specimen
should consider the environmental effects with the smaller crack would fail at a
when selecting materials for the service high gross-stress level with only a small
application. amount of slow growth, and the speci-
MR. BROWN--I wonder if Mr. Dolan men with the larger crack would fail at a
would care to comment on that? It is a lower gross stress with a much larger
practical application question. amount of slow crack extension. In such
T. J. DOLAN3--It seems to me that the a case, there would be no choice between
answer depends on the individual circum- the materials since one might expect
stances involved. I could well visualize them to behave in an identical fashion
that if you are talking about a thin- had the same crack size been used in
wall pressure vessel where you were pri- both specimens.
marily concerned with getting something If, on the other hand, it is specified
that would resist brittle rupture (and that the initial crack sizes were the same
where it might be preferable to have a in the two specimens, the same Kc values
"leak before rupture" condition), the were obtained, and yet one material dis-
material with the slow crack growth played a large amount of slow growth
would allow development of a crack and low failure stress and the other dis-
through the wall and an obvious leak played a small amount of slow growth
before a complete rupture of the vessel. and high failure stress, I would concur
However, if you're working with a thick- in Mr. Irwin's suspicion of an environ-
wall vessel where the wall thickness is mental effect. In that it is known that
such that the critical crack size would be some high-strength materials are very
reached before penetration through the susceptible to environmentally induced
wall, then you might draw the opposite slow growth, I would be tempted to se-
conclusion. If design of the pressure lect the material which did not display
vessel is based on a working stress as a the large amount of slow growth. Also,
fraction of the yield point, you would one might justify this selection me.rely on
find that the steel which had the short the fact that a higher failure stress is ob-
crack at the critical stress condition has tained with the material which did not
have a large amount of slow growth.
3 Professor and Head, Department of The-
oretical and Applied Mechanics, University of MR. BRowN--Apparently the answer
Illinois, Urbana, Ill. to this question cannot be given in any

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380 FRACTURE TOUGHNESS TESTING

simple terms, but the discussion does in- care to comment on the stress-intensity
dicate that we must always consider our factor associated with wing cracks pro-
fracture-test results in terms of the serv- duced by bending with the moments per-
ice conditions. pendicular to the sheet plane. As you
The next question is as follows: The know, these cracks intersect at the mid-
stress analysis used for a through-crack thickness and produce a V-type crack
plate specimen assumes a crack to have a front.
straight front. However, in real situa- MR. PARIS--In that case, at the tip of
tions, a crack front is usually curved. the V the stress-intensity factor would
Depending on the crack length, the be infinite, if it is a sharp tip. Slow crack
curved front can constitute an apprecia- extension would begin there immediately
ble part of the total crack extension. At upon loading and produce a curved
what point will this curvature introduce crack front. However, usually one should
significant errors into the analysis? look at the gross-stress environment and
M~. PARis--There is a little discussion not details at this fine a level. The aver-
in m y paper which bears somewhat on age value of K along the crack front,
this question. If one has a straight crack which is the one given by the usual for-
front through a sheet, the stress-intensity mulas, is ordinarily sufficient.
value along that crack front will vary W. F. PAYNE (author)--Does not this
somewhat, since the sheet will have a curvature insure that the actual applied
local stress field which is plane-stress on K at mid-thickness will be closer to the
the surface and plane-strain in the cen- value calculated from surface-crack
ter. The displacements for plane strain length? From a practical standpoint,
would have to be smaller for the same K this slight curvature would have a
value. Consequently, displacement con- beneficial, rather than a detrimental, ef-
tinuity implies that at the center there fect.
will be a tendency to have a higher stress- MR. PARis--The curvature which
intensity factor than at the surface. The forms is partially based on the tendency
difference can be as much as about 5 per of the crack to equalize the stress-in-
cent from the inside to the surface. Now tensity factor along the crack front. But
that is partially the cause of the growth there is another complicating factor, since
of the crack from the center at first, in- the surface material will be associated
stead of from the outside. The plasticity with plane stress and the center material
involved also bears on this. The crack with plane strain. The amounts of plas-
front then will become curved and a ticity associated with each of these states,
tongue will form, and when the tongue as well as the tendency for fracture, are
forms there will be two effects. First, the different. Therefore, a higher apparent
material which has not been fractured in toughness at the surface leads to a
advancing the center of the crack will higher stress-intensity factor at the sur-
tend to hold the crack closed and, by face than at the center, prior to sudden
holding it closed, it will reduce the stress- failure. Hence the curvature which oc-
intensity factor on the tip of the tongue- curs may overequalize and lead again to
crack front. How much it will be reduced variation in K along the crack front
is a very difficult question to answer. which is difficult to estimate.
Second, the curvature of the tip of the MR. IRWIN--I have two comments on
tongue also reduces the stress-intensity the matter of crack-front curvature.
factor there. First, one can consider the laboratory
MR. BRowN--Mr. Paris, would you test in terms of how accurately it models

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PANEL DISCUSSION 381

some typical service situation. If the search Laboratory (NRL) introduced a


crack-front curvatures are similar in the fracture toughness requirement in the
laboratory test and the expected service military specification on Plexiglas wind-
situation, then the shape of the crack in shield material for aircraft. The efforts of
the laboratory test should not introduce W. S. Pellini and P. P. Puzak at NRL
error. have resulted in certain toughness re-
The second comment concerns an in- quirements for ship-plate materials, in
teresting aspect of crack-front curvature terms of Charpy impact energy require-
which we noticed from examination of ments supported by explosion tests and
crack-arrest lines on adhesive-joint drop-weight tear-test studies. I believe
test specimens. In the testing arrange- the Army has also employed Charpy im-
ment used by Ripling and Mostovoy pact requirements in material specifica-
(Materials Research Laboratory), two tions for armor-plate applications.
long adherend bars, joined by the ad- The Air Force has traditionally ex-
hesive, are separated by forces acting on pected contractors to establish their own
the bars at one end. It is essentially a toughness requirements and standards.
stiff-adherend type of a peel test. The Divided thought and confusion prevail
separating forces are quickly relaxed by among contractors on this technical
crack extension. Thus a succession of problem, and no industry-wide standards
onsets and arrests of crack propagation apply to Air Force procurement activi-
was observed as the test progressed. We ties. The completion of standardization
noted the curvature of the arrest lines work by organizations such as the Ameri-
and thought this indicated an undesirable can Society for Testing and Materials
degree of plane-stress yielding influence will be necessary before a uniform tough-
at the side borders of the crack plane. ness requirement is reflected by Air Force
However, when we doubled the thick- contractors. Even then, the specifications
ness of the specimens, the curvature of will be individual contractor specifica-
the arrest lines was not significantly re- tions and will presumably vary in ap-
duced. The reason for this can be under- proach among contractors.
stood if one reflects upon the anticlastic I can think of one example where an
curvature of the upper and lower sur- Air Force contractor has put in a surface-
faces of a beam in simple bending. 4 Be- crack test in a steel-plate procurement.
cause of the anticlastic curvature tend- The specification requires three different
dency, a straight crack front, extending specimen sizes and three different surface-
across from one free surface face of a crack lengths (sizes) per specimen size.
plate specimen to the opposite face, is not Unfortunately, the specimen sizes rela-
expected even in a material of extreme tive to strength and toughness levels are
brittleness. such that even with the largest surface
MR. BROWN--Moving on to the next crack, one encounters general yielding.
question, I would like to ask Mr. Payne The result is a plasticity test, not an elas-
whether fracture toughness tests are now tic fracture test. In that particular pro-
being incorporated into government curement, over 200 fracture tests have
specifications? been conducted by the supplier and all
MR. PAy~rE--Some ten years ago, J. tests have gone into general yielding.
A. Kies and others at the Naval Re- This does indicate that the toughness is
somewhat more than the specimen is
4A. E. H. Love, Mathematical Theory of
Elasticity, 4th edition, Dover Publications, N. Y.,
capable of measuring, but quantitative,
N. Y., 1944, p. 131. elastic fracture-strength values were im-

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382 FRAcrm~E TOUGHNESS TES'HNC_,

possible. The end result is information of Mr. Brown and me, in the section en-
limited usefulness. Because the actual titled "Variation of gc with Crack Length
specifications are individually by the Air and Specimen Width."
Force contractors, no consistent Air MR. BROwN--The study of plane-
Force pattern to toughness in specifica- strain crack toughness becomes more
tions can be found. In the Army and the difficult as the ratio of toughness to yield
the Navy, however, the situation is con- strength increases. For materials of low
siderably different, although they use yield strength and very high toughness,
more conventional tests. very large specimens are required in
MR. BROWN--Mr. Heyer, in his sym- order to provide crack sizes sufficiently
posium paper, has described a screening large to cause fracture before yielding.
test procedure that seems straightforward It would seem from a practical viewpoint
and practical. Mr. Srawley, under what that there is some upper limit of crack
circumstances would it be necessary for size beyond which we need not be con-
the alloy developer to go beyond this and cerned with fracture toughness tests. Mr.
to determine actual Kc values? Srawley, would you please give us your
MR. S~wL~Y--For screening pur- thoughts on this?
poses the procedure which has been de- MR. Sl~AWLEY--Frankly, I have not
veloped by the ASTM Special Committee completely resolved this question to my
on Fracture Testing of High-Strength own satisfaction, but it does seem to me
Metallic Materials and evaluated by that there is a point beyond which you
round-robin program, as discussed in do not need to go in most cases. If your
Mr. Heyer's contribution to this sym- material is such that you need a plane-
posium, seems to me to be entirely ade- strain crack toughness specimen that
quate. By screening, I mean selecting the contains a crack several inches long,
more promising from a variety of com- then the contemplated structure will be
binations of such variables as composi- able to tolerate cracks that are at least
tion and heat treatment which a given the same size. If this is not sufficient for
organization might wish to investigate. assurance of safety, then I would suggest
I see no point in subjecting every con- that consideration be given to redesign
ceivable variation to an elaborate frac- of the structure or to other measures
ture toughness testing program which which would guarantee that such large
would be much more expensive. How- cracks did not occur.
ever, when the screening program turns MR. BROwN--Mr. Wells, would you
up what appears to be a promising ma- care to comment on this matter? Your
terial or treatment, then this should bc experience is primarily with lower-
subjected to a very thorough study of strength materials.
plane-strain crack toughness, covering A. A. W~LLSS--I beg to disagree with
the variables that may be important in Mr. Srawley, and to suggest that thick
potential applications, such as tempera- plate structures of mild steel may need
ture, strain rate, and orientation of to tolerate defects inches long without
cracks with respect to fibering. As far as fracture. They may be buried and unde-
so-called plane-stress fracture toughness tected within the thickness.
testing is concerned, 9r or K~ measure-
ment, I do not believe that this should 5 Professor, Department of Civil Engineering,
be done as a matter of course, but only in Queens University, Belfast, Ireland; formerly
deputy director, British Welding Research
connection with specific applications. Assn., Research Station, Abington Hall, Cam-
This point is discussed in the paper by bridge, England.

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PANEL DISCUSSION 383

MR. BRow~--Mr. Wells, what do you edge that there are cases where very
people do in the way of inspection? Some large cracks occur, for instance, Pellini
of these large defects you must be able and Puzak 6 cite the case of a hydraulic
to find by even rather crude inspection press cylinder which failed from a fatigue
techniques. Are the vessels of such con- crack which was about 16 in. long by 8
struction and put in such environments in. deep. I would like to ask Mr. Wells
that they cannot be inspected regularly? what he considers is a reasonable toler-
Is that why your defects of critical size able crack size.
are so large? MR. WETxs--For these situations I
MR. WELLS--High-temperature" and believe in Irwin's "leak-before-break"
irradiated vessels cannot easily be in- concept. In fact, if one can tolerate a
spected in service. Defects may also be twice-thickness crack in all parts then
pessimistically assumed to grow during the structure is indeed a viable one.
service and between inspections. One con- MR. BROWN--Mr. Wells, do you really
siders particularly the possibility of frac- believe in leak-before-break calculations
ture during cooling down after a period of when applied to the low-strength heavy
service, due to the presence of one of these sections of interest to you? How do you
enlarged defects. make these calculations?
One can also consider the possibility of MR. WELLS--It so happens that we do
embrittled weld-heat-affected zones pres- not have to do the calculations. We have
ent in as-welded structures. Here the thick-plate testing facilities that permit
parent material may be capable of toler- us to gain experience on different types
ating a long crack, but the embrittled of steel at full scale. To quote some fig-
region may not. Nondestructive testing ures: a good quality 3-in. thick silicon
can be of added importance in such cases. killed steel that we use extensively
Fracture toughness testing on the em- (40,000 psi yield point) fractures at
brittled material should also be worth the --10 C with a 6-in. long crack and at
performance. - 4 0 C with a 3-in. long crack.
MR. PnYNE--Since you are concerned, V. WEISS (author)--The difficulty in
there is one aerospace application I can the discussion of this problem stems from
think of that needed a large critical the difference in viewpoints. One party
crack-size capability. A low-toughness may claim the absence of any danger or
aluminum alloy was used in a very large need to resort to sharp-crack fracture
integral wing-tank structure. In n;y mechanics because extensive plastic
opinion, you could not effectively inspect flow must have occurred if the yield
the structure in any way except to en- strength is required to fracture a part
counter a fuel leak. This would then re- containing a 6-in. crack. Another party
quire a considerable critical crack length may insist on a solution within the sharp-
to insure leakage prior to failure. crack fracture mechanics framework.
MR. S~wLEy--Returning to Mr. This, then, requires the availability of a
Wells's remarks, I did say that I had not plasticity solution for a crack, such as
completely resolved the question to my McClintock and Irwin have indicated in
own satisfaction, and I recognize that his their symposium paper. Such a solution
views and mine are colored by experi-
ences of different kinds. He is more aware W. S. Pellini and P. P. Puzak, "Fracture
of large structures and large defects, Analysis Diagram Procedures for the Fracture-
Safe Engineering Design of Steel Structures,"
while I am more conscious of small de- NRL Report 69~0, Naval Researcl~ Laboratory,
fects at high stress levels. I do acknowl- March, 1963.

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384 FRACTURE TOUGHNESS T~STmO

would also considerably improve the discussed. I had in mind the use of screen-
plasticity-correction procedures now uti- ing tests in alloy-development labora-
lized for ultra-high-strength materials tories. For aircraft skin applications, I
where sharp-crack fracture mechanics would agree that fracture toughness tests
does apply reasonably well. utilizing appropriately long cracks are
MR. WELLS--May I add a postscript, required. However, these would only be
in view of Mr. Weiss's contribution? My applied to materials which had already
quoted figures related to failure at yield- survived the screening stage.
point stress, without substantial yield Mg. PnY•v.--One application where
strain. For vessels subject to the first the plane-strain fracture strength may
hydrostatic test, we are more interested have to be measured and analyzed em-
in failure at 89 per cent over-all strain pirically, rather than predicted from
with much smaller defects than 6 or 3 in., legitimate Kxc data, is a small-diameter,
because modern design allows this thin-wall solid-propellant motor case
amount of plastic strain at pressure- containing surface cracks. The surface-
vessel nozzles and the like. Much of our crack expressions (as reviewed in Paris's
effort on general yielding fracture me- paper) may predict too high a fracture
chanics has been to try to equate these stress for crack depths exceeding, say,
two situations, of large defects with small half the thickness. For very deep cracks,
applied strains, and small defects with the plastic zone extends through a sig-
large strains. nificant portion of the uncracked thick-
MR. PARIs--On to the same subject, I ness, if not entirely through the wall.
would like to cite the case of the skin of The stress field is disturbed and no longer
commercial transport airplanes, the cur- described by the linear elastic field equa-
rent airplanes on which most of you tions.
flew here. In the long lives which are On the other hand, crack sizes too small
expected of these airplanes, sizable to propagate prior to net-section yielding
fatigue cracks may grow. They have to are similarly outside the legitimate realm
be discovered before they cause a dis- of elastic fracture mechanics. The small-
aster, and, as a consequence, it is current est semicircular crack depth of interest
practice to design skins of the pressure would be about 0.6 (Kido'ys) 2. Hence,
cabins and wings for commercial trans- for thicknesses tess than 1.2 (Kxders) 2,
ports so that they may sustain a very a semicircular crack depth sufficiently
long crack; often cracks of 20 in. or more large to fail without general yielding will
are required before a critical crack length exceed half the thickness. The crack tip
is reached at the working stress level in will be surrounded by a plastic-zone
these aircraft. Tests which do not simu- width of at least an additional 0.1
late these conditions are not very good (KiJr 2. This suggests that surface-
tests for choosing materials for this ap- crack tests on thicknesses less than about
plication. Though screening tests may be 1.0 (Kxc/~rs) ~ would have to be entirely
of initial help, programs which actually empirical.
test the material at the nominal stress In 18 per cent nickel 300 maraging
level involved in the airframe are most steel, with assumed KI~ of about 100
appropriate for this type of application. ksi ~r and yield strength of 300 ksi, a
Mm SltAWL~Y--I would like to make minimum wall thickness of 0.1 in. is re-
it clear that my previous comments on quired for meaningful surface-crack tests
screening tests were not intended to ap- from the linear elastic analysis stand-
ply to the case that Mr. Paris has just point. The Air Force has sponsored

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PANEL DISCUSSION 385

fabrication of several 40-in. diameter minum alloy. Most of the specimens had
cases (of the 300 maraging steel) with a fatigue cracks extending from the slot
design wall thickness of 0.045 in., well or notch, and at the right-hand side of
under the minimum 1.0 (Kz,/~rrs) ~ thick- Fig. 1 we show a plot of the apparent
ness. Empirical fracture-test work would KIr value versus the length of fatigue-
be required to establish flaw-size frac- crack extension. When the fatigue cracks
ture strength relationships for surface are absent or very short, the apparent
cracks in this example. However, the K~, is lower for the V-notch specimens
framework of fracture analysis--es- than for the slotted specimens, but with
peciaUy the emphasis of gross applied sufficient fatigue-crack extension the re-
stress at fracture-is useful as a guide sults converge to a common value of
for empirical analysis. K ~ . Thus the effect of notch angle is
MR. BaOWN--I have to stop discussion negligible, provided the notch is ex-
on that question and move on. The next tended by a fatigue crack of adequate

I I l I I I 40, l I I ~'-
12 SHARP "V"
tO ~. OO
3O
v
~6
o
..J
t
~. 20 6~Ao~ ~t'~176
4 0 MILS 13 250 - ,3
"" I0 -

2
OSHARP'V= O JEWELER SAW
0 I I I
POTENTIAL 0 I0 20 30 f~50
FATIGUE CRACK LENGTH
(Aoo), MILS
Fzo. 1--Pop-in Behavior as Influencedby Fatigue-CrackLength for Single-Edge-NotchedSpeci-
mens of 88 Thick 7075-T6 AluminumAHoyPlate.

question is: Has the influence of notch length, in this case at least 0.02 in. The
shape as well as depth and notch acuity ASTM Special Committee recommends
been fully investigated? Mr. Srawley, that specimens should always be fatigue-
will you comment briefly on this? cracked if they are to be used for valid
MR. SRAWL~Y--The influence of KI~ measurement. These results give
notch shape is one of several details of some guidance about the necessary length
fracture toughness testing which, in my of the fatigue crack, but ought to be sup-
opinion, have not been sufficiently ex- plemented by additional data for other
plored. However, we do have some in- materials and specimen thicknesses.
formation about it which is summarized There is another effect of the lerigth
in Fig. 1. The data were obtained with of fatigue-crack extension, shown on the
single-edge-notched tension specimens of left-hand side of Fig. 1. With no fatigue
two kinds, one having a 60-deg angle crack, there is a very pronounced step in
notch and the other a 0.012-in. wide the record of load versus electrical
saw-cut sl0t. The specimens were ~ in. potential change, indicating the sudden
thick and 3 in. wide, of 7075-T6 alu- extension of a relatively large tongue of

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386 FRACTURE TOUGHNESS TESTING

square fracture. With increasing length shows something about the effect of
of fatigue crack, the magnitude of this fatigue stress level. This shows the re-
initial pop-in indication diminishes, and sults of tests of surface-cracked speci-
the load at which it occurs decreases, mens of ~t~-in. thick H-11 steel sheet.
corresponding to decreasing values of K. The yield strength was 213,000 psi, and
MR. B~OWN--I would like to ask Mr. the specimens were fatigue-cracked in
Srawley another question which bears on bending at three levels of the maximum
this one. What is the influence of fatigue- nominal fiber stress, as indicated. The
50,000 I I I

48,000 A (9-
A

46,000 - A 9 0 91490 _

44,000 -

~ 42,000 A A
Y
0

40,000 -
A C)
O FATIGUE STRESS
60,500 psi 9
38,000 -
83,500 psi 0
130,000 psi /k

36,000 I I I
140,000 150,000 160,000 170,000 18G ooo
GROSS FRACTURE STRESS,psi
FIG. 2--Plot of K Versus Gross-Fracture Stress for Three Groups of Specimens.

cracking conditions such as maximum K value plotted in each case corresponds


stress and resulting crack shape on the to the maximum load and the measured
measured values of plane-strain tough- dimensions of the fatigue crack, that is,
ness? it is a K~, value if we assume that no
MR. SRAWLEY--Again, our informa- slow crack extension occurred. There are
tion on this point is inadequate, but Fig. ten points for each of the three fatigue-
2, taken from a previous paper of mine/ stressing levels, and there is no signifi-
cant difference among the three average
7 j. Srawley, "Small Fatigue Cracks as Frac- K values. However, the dispersion of the
ture Origins in Tests of High Strength Steel
Sheet," Proceedi~s, Am. Soc. Testing Mats., results is greater for the higher fatigue-
Vol. 02, 1962, pp. 734-741. stressing levels than for the lowest level.
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PANEL DISCUSSION 387

In general, we recommend that fatigue tion will be met for most tests. Paul
cracking should be conducted at the Kuhn and his associates at NASA have,
lowest practical nominal stress level, in over the past few years, been analyzing
no case greater than half the yield crack-propagation data by means of a
strength of the material. It should take "notch analysis" based on a modified
something like 15 or 20 min to complete Neuber stress-concentration factor. Mr.
the fatigue cracking of a specimen at 1500 Kuhn has prepared a written discussion
cpm. If the number of cycles is much which comments both on his approach
less than 20,000, the fatigue-stressing and on fracture mechanics as we have
level is too high. The crack shape is been discussing it here.
another guide as to whether the fatigue- P. KtmNS--Fracture mechanics has
cracking conditions were satisfactory. been and is an invaluable tool for dealing
The broken surface of a specimen should with a subject of vital importance in
always be examined after a test, and if structural engineering. However, an in-
the fatigue crack deviates markedly from creasing amount of dissatisfaction has
being flat and square to the specimen been expressed on two main scores:
surface, or if the fatigue-crack front in a (a) unsatisfactory agreement between
single-edge-cracked or center-cracked notch-toughness values obtained with
specimen is markedly curved, then the different specimen configurations, and
result of the test should be regarded with (b) inaccuracy of predictions of
some suspicion. strength of cracked structures (such as
MR. DOLAN--There is a tendency, pressurized cylinders).
when people aIe anxious to get specimens Most of the dissatisfaction has been
prepared rapidly, to fatigue-crack these expressed by engineers dealing with
at rather high stresses and for very short sheet material, and the entire following
periods of time. I was surprised that, in discussion is strictly confined to sheet
the Hartbower and Orner paper, they material with through-cracks.
indicate that it takes only 2 min to pro- A critical examination of fracture
duce fatigue cracks in their Charpy mechanics and comparison with other
specimens. This to me seems to be ab- approaches in the area indicated show
normally short time; even if you run that most of the trouble can be charged
them at 1500 cpm, you have only about to the fundamental formulation of frac-
3000 cycles to initiate and to develop ture mechanics, specifically, the use of
the crack. To produce a sizable fatigue the quantity, S(a11~), to describe the
crack in this period of time requires a notch toughness of a material. The fol-
cyclic strain of at least 1 per cent, which lowing discussion will give the reasoning
means that the zone in advance of the that leads to this conclusion.
tip of the crack has large plastic de- Fracture mechanics in its present form
formations developed which are abnor- is essentially a stress-concentration
mal as compared with what you would approach? Of basic importance in the
get by cracking with a low-amplitude following discussion is the range of
cyclic stress. I recommend in general stress-concentration factors of practical
that fatigue cracking be done at nominal interest. Two types of application may
stresses much below the critical fracture serve as examples.
stress you are expecting to reach in the *Assistant Chief, Structures Div., National
subsequent test. Aeronautics and Space Administration, Langley
MR. BROWN--I think that is a good Research Center, Hampton, Va.
9 "Fracture Testing of High Strength Sheet
point. However, if we follow the com- Materials," A S T M Bulletin, No. 243, January,
mittee's recommendation, this condi- 1960, p. 30.
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388 FRACTURE TOUGHNESS TESTING

In most types of pressure vessels, it is the stress-concentration factor can be


desired that the vessel be able to develop written as
a hoop stress equal to the yield stress in
S C F = 1 + Cl(a) in . . . . . . . . (2a)
the presence of cracks. The associated
stress-concentration factor, therefore, where C~ is a materials constant but de-
must be less than the ratio of ultimate pendent on temperature. The method
strength to yield strength (roughly); this presented by Kuhn and FiggO~ shows
ratio is usually less than 1.2 and seldom how C~ can be calculated from known
exceeds 1.5. materials' properties and shows numerous
In the screening program for supersonic applications to aluminum alloys; other
transport skin materials, the 1-in. wide papers ua2 show applications to ti-
ASTM V-notch specimen was used. On tanium alloys.
the basis of service experience with alu- Griffith, interested in developing a
minum alloys, the rule of thumb was theory for the fracture of glass, simpli-
formulated that materials would prob- fied, Eq 2a, to the form
ably be not acceptable if they had a
S C F ~ G(a)U2 . . . . . . . . . . (2b)
notch-strength ratio less than 0.7, cor-
responding to a stress-concentration Substitution of Eq 2b into Eq 1 gives
factor of 1/0.7, or 1.4.
These two examples demonstrate that F,u
S= ~
G(a)~/~ . . . . . . . . . . . .
.(3)
many practical applications involve
stress-concentration factors less than 1.5;
and transferring a m to the left side gives
factors substantially greater than this
occur only in special applications (pres- Ftu
S ( a ) ~n = - - . ........... (4)
sure cabins of airplanes). This writer is G
not aware of any practical application on
metal structures involving a stress-con- The quantity on the left is the notch-
centration factor as large as 10 (failure at toughness parameter used in fracture
one tenth of the ultimate strength). mechanics in its earlier form. Since the
Consider now a wide sheet containing two quantities on the right (F t~ and Cx)
a transverse crack and subjected to ten- are materials constants (at least in good
sile stress. The tensile stress causing fail- approximation) it might be expected
ure may be defined by the formula that S ( a u~) is also a materials constant.
Unfortunately, this expectation is not
F:u fulfilled because the simplified expression,
s = ~cF .............. (i)
Eq 2b, for the stress-concentration factor
which leads to Eq 4 is not accurate
provided that the SCF (stress-concen- enough except in extreme cases.
tration factor) is suitably calculated. For The use of Eq 2b in place of Eq 2a
the purpose of mathematical analysis, 10 p. Kuhn and I. E. Figge, "Unified Notch-
the crack can be represented by an elon- Strength Analysis for Wrought Aluminum
gated ellipse; the theoretical stress-con- Alloys," NA~gA TAr D-1~59, National Aero-
nautics and Space Administration, 1962.
centration factor for such a hole is u p. Kuhn, "Notch Effects on Fatigue and
Static Strength," I C A F - A G A R D Sltrapo~um
Kr = 1 + 2 ( a l p ) lz2 . . . . . . . . . (2) on Aeronautical Fatioue, Rome, Italy, April,
1963.
where a is the major semi-axis and p the P. Kuhn, "The Prediction of Notch and
Crack Strength Under Static or Fatigue Load-
tip radius. For cracks in actual materials ing," SAE-ASME Air Transport and Space
(with an arbitrary amount of ductility), Meeting, New York, N. Y., April, 1964.

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PANEL DISCUSSmN 389

means that 1 has been omitted (or sub- cracks, the formula no longer predicts
tracted) from the stress-concentration infinite strength. However, in some typi-
factor. In Griffith's problem, this was cal cases, the predicted strength is still
permissible because he was dealing with about 50 per cent higher than the tensile
a stress-concentration factor of about 100 strength, an error which can hardly be
(ratio of theoretical to actual tensile considered tolerable. Moreover, since
strength of glass). However, as noted the correction is tied to a physical char-
earlier, the stress-concentration factors acteristic (plasticity) of the material,
of interest in structural engineering are while the main trouble is the algebraic
usually less than 1.5. Clearly, an intoler- one of using an unduly simplified stress-
able error is introduced if 1 is subtracted concentration factor, the correction can
from a factor of 1.5. The error introduced hardly be expected to be very successful
by subtracting 1 might be considered over a wide range of widths and ma-
acceptable if the stress-concentration terials.
factor were greater than 10, but as MR. BRowN--Thank you, Mr. Kuhn,
pointed out earlier, there appear to be for your comments. Before going further
no cases of practical interest in this I would like to ask you whether or not
range. stable crack-extension measurements
The maximum error is introduced in were made on the wide-plate tests you
the limiting case of vanishingly small referred to. Such measurements would
cracks. If Eq 4 is used in reverse to pre- be necessary properly to calculate K~
dict the failing stress of such a specimen according to the fracture mechanics equa-
from a given value of S (aV~), an in- tions as presented in the reports of the
finite stress is predicted, while the answer ASTM Special Committee on Fracture
should, of course, be F t , . This implies, Testing of High-Strength Metallic Ma-
furthermore, that the prediction is terials. Also these measurements would
seriously in error for any short crack. permit calculation of the net stress at
The method used by my associates fracture instability. If this were above
and me :~ employs the complete Eq the yield strength, then the results would
2a instead of Eq 2b and correlates very not be suitable for analysis by fracture
successfully for one material, tests on mechanics.
center-cracked specimens ranging from MR. KtmN--In the tests that we have
35 to 9 in. wide, edge-notched specimens made and those made by many others
2.25 in. wide, and V-notch specimens in the airframe industry, no attempt has
0.64 in. wide. By c o n t r a s t , / ~ = 60 for been made to measure stable crack ex-
w = 2.25 in.,/s = 90 f o r w = 12 in., tension or determine when unstable ex-
a n d / ~ = 105 for w = 35 in. These tension starts. The point that I make,
observations (and others) indicate that and I know other people agree, is that
most of the width-correlation troubles what matters is the fracture load. It
experienced in fracture mechanics can makes no difference whether at that time
be attributed to the same source--use the crack propagates at 300 or 3000 f t /
of the simplified Eq 2b. sec. As long as it fails, it fails.
The unsatisfactory ability of fracture MR. BROWN--Mr. Irwin wishes to
mechanics to correlate tests on different reply to Mr. Kuhn.
widths has led to the introduction of MR. IRWIN--Mr. Kuhn suggests that
plastic-zone correction. This correction the fracture mechanics approach is handi-
does improve the results. For instance, capped by neglect of the additive factor
for specimens with vanishingly small of 1 in his Eq 2a as compared to his Eq

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390 FRACrVRE TOUOHNESS Tv.sTmo

2b. A large degree of equivalence exists axial rather than biaxial tension. When
between the stress-concentration factor he draws a fictitious ellipse through the
approach and the fracture mechanics ap- plastic zone to represent the influence of
proach, as has been pointed out in frac- plastic-flow stress relaxation, he prefers
ture mechanics papers. However, the to regard this ellipse as subject to free-
degree of equivalence is somewhat less surface stress conditions. This preference
than one might infer from Mr. Kuhn's and the specialization of the stress state
discussion, He assumes we should first to uniaxial tension are responsible for the
replace the influence of the plastic zone difference between Eqs 5 and 6 for ~,.
by an elliptical rounding of the crack The stress- concentration factor ap-
shape. Next, we should derive the maxi- proach used by Mr. Kuhn and the frac-
mum stress at the fictitious notch root ture mechanics approach are (or should
by linear elastic analysis and use this be) mathematically equivalent in the
maximum stress as the fracture criterion. representation of stresses in the elastic
Mr. Kuhn's Eq 2 is valid for a round stress field at distances of, say, 5p or
hole in a plate (p = a). The resulting more from the focal points of Mr. Kuhn's
value of K r = 3 is the familiar stress- ellipse. Mr. Kuhn's comment should be
elevation factor for a round hole in uni- interpreted merely as a statement that
axial tension. For biaxial tension, the he thinks the proper fracture criterion is
added term of 1, to which Kuhn directs a maximum stress derived in the special
attention, does not apply and (for the way indicated above, and he thinks frac-
round hole in biaxial tension) K r = 2. ture data are better represented when
Equations 2a and 2b from his discussion such a criterion is used. These opinions
are not suitable for comparison with are based upon some experience and are
linear elastic fracture mechanics. Let us deserving of respect. However, his refer-
consider a two-dimensional crack of ence to "intolerable error" in basic
length 2a in an infinite plate with axial mathematical aspects of fracture me-
tension ~ normal to the crack. If an el- chanics injects an unnecessary aspect of
liptical boundary is constructed around controversy and is inappropriate. For
but close to the crack with the ends of example, it is impossible to predict a
the crack at the focal points, the stress strength greater than that for general
~, where the ellipse intersects the x-axis yielding, as claimed by Mr. Kuhn, unless
is given by the fracture mechanics is improperly
used. We can recognize that many spe-
~ = ~(a/p)'~' . . . . . . . . . . . . (5)
cialized ideas about the proper criterion
where p is the radius of curvature at the for fracture exist, including Mr. Kuhn's,
end region of the ellipse. From Mr. and these deserve trial in future research.
Kuhn's Eq 2, if this ellipse is regarded as However, the basic mathematical treat-
a free surface, the stress, ~v, at the same ment of linear elastic fracture mechanics
point is given by is quite straightforward and does not
contain "intolerable" mathematical er-
gv -- ~[1 + 2(alp) ll*] . . . . . . . . (6)
rors.
From comparison of Eqs 5 and 6, one Mr. Kuhn's representation of the crack
sees that the factor of 2 multiplying as an ellipse through the plastic zone
( a l p ) '12 corresponds to the KT = 2 rela- with free surface boundaries is intended
tionship for a round hole with biaxial to adjust for the effect of plastic strains
tension. The added factor of 1 in Eq 2a near the crack. The fracture mechanics
is due to Mr. Kuhn's assumption of uni- adjustment for plasticity attempts to

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PARCEL DISCUSSION 391

maintain both a greater degree of sim- straightforward, neat, one-parameter


plicity and a better situation for linkage approach of elastic fracture mechanics.
to methods of elastic-plastic analysis. It involves knowledge of the stress-con-
As was pointed out in the McClintock centration factor, the stress gradient, and
and Irwin paper given in this symposium, also the stress state at the root of the
the elementary plasticity correction thus notch. It is affected by the relative notch
suggested consists in adding to the crack depth, by the material ductility or plas-
length an amount ticity and it has inherent in it a dimen-
sional material constant, the equivalent
particle size, r or 7. All these quantities
must be related to the deformation char-
acteristics of the material because what
This procedure, where ~, is th, uniaxial determines fracture is not the original
yield strength, preserves the analysis specimen geometry but the geometry at
simplicity of linear elastic fracture me- a point in the specimen's deformation
chanics and the one-parameter nature of history just prior to fracture. For exam-
the fracture criterion. More sophisticated ple, two identical specimens, one with a
corrections for plasticity are possible large plastic zone, the other one with no
which would permit a closer representa- plastic zone, will certainly have a dif-
tion of data in the high stress level range. ferent fracture behavior.
However, the necessity of this for prac- Now, while Sachs was considerably
tical applications is not yet clear. concerned with mild notches for the solu-
The disadvantages of the stress-con- tion of design problems, he was also very
centration factor approach are primarily insistent about requiring the testing of
in terms of complexity and overspecial- sharper and sharper notches in order to
ization. The fact that the stress-concen- arrive at a comparative evaluation of
tration factor is dimensionless tends to materials. We did not consider fatigue
distract attention from the central im- cracks at the time, but we used the sharp-
portance of the crack-size length factor. est notches that could be machined. Mr.
Also the stress-concentration factor view- Irwin's statement is certainly correct
point is rather biased toward a maximum that in some alloys it does not make too
stress type of fracture criterion. In con- much difference whether the root radius
trast, the fracture mechanics approach is is 0.003, 0.001, or less than 0.001 in. We
sufficiently simple and unspecialized so have, however, tested alloys which are
that it is relatively easy to supplement quite sensitive to reduction in root radius
the analysis so as to introduce criteria in this range down to fatigue cracks.
such as critical stress, critical strain, or H-11 and 300M steels heat-treated to
critical displacement at the crack border high strengths and tested at low temper-
when circumstances appropriate for atures are cases in point. Such a situa-
these ideas seem to be present. tion represents an actual engineering
MR. WEiss--The stress-concentration problem and it has its root in the so-
factor approach that Mr. Kuhn has pre- called plasticity dilemma. If the material
sented is indeed a very satisfactory ap- and the notch or crack geometry just
proach for cases where one deals with prior to the onset of fracture is repre-
mild notches. We at Syracuse, and es- sented by a low stress-concentration
pecially George Sachs, devoted a great factor, a high ratio of notch strength to
deal of energy to this type of work. It is tensile strength, or a high ratio of crack
a more complicated approach than the strength to yield strength, then plas-

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392 FRACTUP~ TOUGHNESS Tr~sTmG

ticity effects must have modified the considerably farther than using an elastic
original shape considerably to produce linear theory.
the observed effects. The development of As a result of using notch analysis, we
an analytical treatment of these proc- not only get a much better correlation
esses, most likely in terms of properties over the full range of specimen widths
available from careful tension tests, is (from 89to 35 in.), but we also avoid the
one of our ambitious goals. complete breakdown of the formula for
The data that Mr. Kuhn reported zero crack length and for 100 per cent
here show the lowest K, value for the crack length which is characteristic of the
smallest specimen and an increase with Kc formula. Notch analysis says that for
increasing size. I wonder if this is not one either zero crack length or 100 per cent
of the virtues of the plasticity correction crack length the net-section stress is
as proposed by Mr. Irwin: it gives a con- equal to the ultimate tensile strength in
servative estimate for small specimens the case of a crack; consequently, it
where the plastic-zone size and the speci- does not need the artificial cut-off line
men dimensions are comparable. In us- which says that above the yield strength
ing such data, one must however, guard or 0.8 of the yield strength the theory
against a transition from plane stress to becomes invalid. Notch analysis is valid
plane strain beyond the point where up to some indefinite point well above
curve of the Kc versus size or width has the yield--possibly up to the ultimate
levelled off. for cracks. I would also like to make a
MR. Tir'rAwY--I would like to com- comment with respect to Mr. Tiffany's
ment on Mr. Kuhn's statement that I remark that he is not interested in the
should only be interested in the failing strength. This also bears on the remarks
strength of a structure with a pre-exist- which Mr. Weiss made. The test of a
ing crack. I take exception to this. I am fuselage costs on the order of a million
not so much interested in the failing dollars, and that test has to be made
strength as I am in knowing what the with a crack length specified by the
critical crack size is at the maximum Federal Aviation Administration (FAA).
operating or limit stress levels in the The designer would like to be sure that
structure. Further, I am interested in the fuselage does not blow up prema-
knowing what initial crack size I might turely when FAA witnesses are standing
expect in the structure and how many around. Need for a second miUion-dollar
load cycles and how much time at load test, damage to company prestige, and
can be encountered before this initial possible loss of sales are potent reasons
crack grows to critical size and failure for being interested in a good estimate
results. of the strength of the cracked fuselage
Mm KUHN--I would like to point out before the test is made.
that calling our notch analysis a linear I. Fmor~3--Several methods have
elastic analysis is incorrect. Although I been proposed to predict the residual
passed over that point, I did mention static strength of structural parts con-
that we applied two successive correla- taining cracks and notches. Other meth-
tions, one for size effect and one for ods have been proposed which provide a
plasticity; we have, therefore, in effect, useful tool for comparing materials on a
an engineering approximation to a non- notch-toughness basis. Each of the
linear theory which involves plasticity.
ts Structures Div., National Aeronautics and
It is an engineering method and it does Space Administration, Langley Research Cen-
not go all the way, but it does carry ter, Hampton, Va.

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PAN'EL DISCUSSIOn 393

methods has its limitations; in their pres- cussion that presents interesting and ap-
ent form, some are valid only for sheet parently divergent points of view. My
specimens with through-cracks; others understanding is that Mr. Kuhn will
become invalid when the crack is short; present his approach to the fracture
and all appear to be questionable when problem at a forthcoming meeting of the
the net-section stress is in the plastic ASTM Special Committee on Fracture
range. Consequently, there is consider- Testing of High-Strength Metallic Ma-
able difficulty in deciding which method terials. We certainly look forward to
is best to use for a specific problem. I these further discussions.
believe it would be timely to consider HERSCH~.T. SMITH~--I would like to
defining the range of applicability of the ask Mr. Tiffany whether it is feasible to
various methods. This would probably lower the operating stress of a service
mean a comprehensive study of such structure with time in service in order to
factors as the geometrical, mathematical, stay within the safe fatigue or static
and loading limitations and also might stress levels set by the particular frac-
include the probable percentage of error ture toughness of the material and the
that might be expected. Such an effort length to which cracks may have grown?
would not only aid the designer in se- MR. TiFFaNY--There is an actual serv-
lecting the most appropriate method for ice example for which we have done
his particular problem but would also exactly that. The missile helium tank
give direction to future studies of frac- which I mentioned in my paper for this
ture toughness. symposium is an example. This particu-
MR. Bl~OWN--Mr. Figge is correct lar tank was designed so that the applied
when he suggests that systematic pro- stress at maximum operating pressure
grams be established with the objective was 25 per cent below the uniaxial tensile
of defining the range of applicability of ultimate strength of the material and it
the various fracture test methods now in was proof-tested to 1.1 times the maxi-
use. This procedure is quite obviously the mum expected operating pressure. The
most efficient and logical one to follow. missiles are stored with these tanks pres-
However, it would require a concentrated surized continuously except for an oc-
effort lasting several years. Unfortu- casional depressurization when person-
nately, the persons and organizations nel are in the vicinity of the missile.
best qualified for such a program are so When these tanks were initially put
busily engaged in trying to apply the into service, one helium tank failed after
concepts now in vogue that they are 21 br at operating pressure. The failure
allowed insufficient time to plan and origin was found to be a forging inclu-
carry out long-range research programs sion which had an initial size approxi-
of this type. Under these circumstances, mately 80 per cent of the critical size.
our test specimens sometime become full- During the 21 hr at stress, the flaw grew
scale structures and such specimens are to critical size and failure resulted. As a
both difficult to analyze and rather ex- result of this failure, an extensive investi-
pensive. gation was performed to determine
The remedy, I think, lies with the rec- fracture toughness and subcritical cyclic
ognition by management that fracture and sustained stress flow growth char-
testing research per sr descrves continu- acteristics of the tankage materials.
ous support which is completely di-
vorced from specific hardware programs. 14Mechanics Div., Naval Research Labora-
I am sorry to have to close this dis- tory. Washington.D. C.

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394 FRACTURE TOUGHNESS TESTING

Quite a bit of the data are given in the sidering. In the case of Charpy testing,
paper. the transition temperature for many
Probably the most significant out- materials is not well defined and covers a
come of this investigation was that sus- rather broad range. I t is not one pre-
tained fracture specimen tests indicated cise, single temperature. V(ithin this
that an initial flaw which was approxi- transition-temperature range we fre-
mately 70 per cent of the critical size or quently observe a good deal of scatter.
greater could grow to critical size with With this thought in mind, can we use a
sustained stress and that a successful Charpy test (or, for that matter, any
proof test to 1.1 times operating could other test) as a screening test when it is
not guarantee that such a flow would not possible that transition-temperature
be present in the vessel when it was put ranges may overlap or be in close proxim-
into service. The successful proof test ity so that we may be comparing a speci-
indicated that the maximum possible men on the tail of one transition-tem-
initial flaw size was (1/1.15) 100, or 83 per perature curve with that on the plateau
cent of the critical size. Any tanks which of another? Is it possible that in all
actually contained flaws between about types of fracture tests we should look at
70 and 83 per cent of critical size might the properties over a temperature range?
then be expected to fail under sustained C. E. HnRTBOWER--It was learned
stress loading. Those greater than 83 per many years ago that one must test over
cent should fail the tank during the a range of temperature encompassing
proof test. anticipated service conditions. If one
I t was apparent that either a higher were to test at room temperature ex-
proof pressure should be used so as to clusively and compare materials A and
guarantee a smaller maximum possible B, material A might be found to be
initial flaw size, or the operating stress much better than material B at room
should be lowered, which would increase temperature; whereas, on testing at some
the critical flaw size and thus lower the lower temperature (sometimes as little
maximum possible initial flaw size in as 10 F) both materials may be lacking
terms of percentage of critical size. Since in toughness. This points up one of the
the proof stress using the 1.1 factor was advantages in precracked Charpy impact
already approaching both the material's testing. One can run tests at tempera-
tensile yield and ultimate strength, it tures down to liquid-nitrogen tempera-
was not felt that the proof stress could be ture and up to -[-400 F almost as easily
increased. Consequently, it was decided as at room temperature. For example, in
to lower the storage pressure in the mis- screening 6A1-4V titanium for use in
sile tanks and bring them up to full pres- rocket-motor cases, precracked Charpy
sure immediately upon firing. This was tests are made at the expected operating
accomplished by incorporating ground temperature, an intermediate tempera-
supply tanks in the missile shelters. ture, and room temperature. In some
Z. P. SnPERSTEIx~s--Perhaps this heats of 6A1-V4 titanium, all bought to
question should be addressed to Mr. the same specification and all heat-
Hartbower, who is interested in pre- treated to the same strength, the pre-
cracked Charpy tests, but it applies cracked Charpy test shows the tough-
equally to other tests that we are con- hess to be increased by a factor of 2 on
raising the test temperature from room
55 Douglas Missile and Space Systems Div.,
Douglas Aircraft Company, Sant~ Moniea, temperature to ~-300F; whereas other
Calif. heats show little or no change. Testing

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PANEL DISCUSSION 395

over a range of loading rates is equally as performed with a specimen encompassing


important as testing over a range of the full thickness of the material, inso-
temperature in some materials. When far as possible. The limiting thicknesses
tested in slow bend and in impact, the in precracked Charpy testing encompass
precracked Charpy test sometimes shows a reasonably broad range from approxi-
unexpected trends, as Mr. Krafft pointed mately 0.06 to 0.80 in.; that is, material
out in his symposium paper. Mr. Saper- in this range can and should be tested in
stein's comment suggests that scatter the full thickness. Returning to the ques-
may invalidate the Charpy test for pur- tion raised by Mr. Saperstein regarding
poses of screening; this is not clear. I scatter in testing over a range of temper-
agree that when the scatter is great in a ature, it is important to recognize that
given material condition, it is difficult to scatter in the Charpy test varies con-
interpret the results. siderably from material to material and
Mr. W~LLS--I am very interested in from heat to heat. I recall one dramatic
the Charpy test. We have tried to em- difference in scatter from end to end of a
brace the Charpy specimen within our single 289 thick plate. One end of the
treatment of cracking under fully plastic plate had an ASTM grain size of about
conditions, using the crack-opening dis- 3 and the other end about 8. The ma-
placement fracture criterion, and find on terial from the two ends of the plate
this basis that there should be propor- differed widely in that the transition
tionality between 9 and W/A. One re- curve of the coarse-grain end involved a
gards Mr. Hartbower's correlation be- scatter band approximately 100 F wide
tween these two quantities as satisfying and that of the fine-grain end was less
because he sticks to the same thickness in than 20 F wide. 18 Such variation in scat-
his Charpy testing as in the material be- ter in a single plate is a special case; how-
ing examined. I think that this is im- ever, variable scatter from heat to heat
portant and that the transition observed is common in some materials. However,
in testing in this way has its counterpart in some materials or material conditions,
in ASTM fracture toughness testing in scatter in the precracked Charpy test is
the sense of distinguishing between practically nonexistent. One such ma-
plane-strain and plane-stress conditions. terial was supplied by Mr. Srawley while
The scatter observed in Charpy testing, at the Naval Research Laboratory. 1~
sometimes called "bimodality," is evi- MR. BRowN--Regarding the thickness
dence of hovering on the brink of the effect generally observed in fracture tests,
one or the other. to what extent is the variation of K,
However, if one performs a Charpy test with thickness thought to be a geometry
with a standard thickness specimen for effect and to what extent is it a result of
the purpose of assessing a thick material, metallurgical variation?
the thickness of the material will also
need to be taken into account, because ~s C. E. Hartbower a n d W. S. Pellini, "Me-
the transitional onset of plane-strain chanical a n d Material Variables Affecting Cor-
relation," Welding Journal, Vol. 29, No. 7,
fracture will occur at a larger W/A or July, 1950, p. 356-s.
fracture toughness value for the full 1~G. M. Orner a n d C. E. Hartbower,."Sheet
thickness of plate. The small-specimen Fracture Toughness Evaluated by C h a r p y I m -
pact and Slow Bend," Welding Journal Supple-
test under these circumstances is non- ment, Vol. 40, No. 9, September, 1961, p. 411-s.
conservative. Figure 12 shows a shift in the precracked Charpy
transition curves both with thickness a n d melt-
MR. HARTBOWER--I agree with Mr. ing practice, together with remarkably little
Wells that the Charpy test should be s c a t t e r in the test data.

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396 FRACTURE TOUGHNESS TESTING

MR. BLUH~t--It has been suggested quite small as compared to the hardware,
that the thickness effect on fracture consequently, the environmental effect
toughness, ~, (or K~), which is generally may be less severe in the specimen than
observed at a fixed temperature, can be in the hardware. For example, in the case
explained upon the basis of simple ge- of hydrogen-induced crack growth the
ometric considerations,ls'19 Furthermore, hydrogen content in the material may be
many data are available which tend to dependent upon the total surface area
support this geometrically derived criti- exposed to the environment and in turn
cal shear-lip concept. However, if tem- the rate of crack growth is dependent
perature-transition effects are considered, upon the hydrogen content. Also, I sup-
then it must be emphasized that the pose it may be possible that surface
model upon which this concept was based area may play some role in stress-corro-
assumed that no metallurgical trans- sion cracking.
formation occurred in the temperature All I can say to this is that I agree
ranges considered; and, further, that the that specimen size may affect the results
crystallographic modes of shear or flat of sustained-stress fracture specimen
fracture, or both, did not change over tests. However, as I pointed out in my
these temperature ranges. It is quite con- paper for this symposium, if such tests
ceivable (and this is suggested in the show a severe effect (that is, low apparent
reference papers) that a flat fracture threshold stress-intensity level) when
mode may change from one type to performed in the expected service en-
another (each being flat), but with sig- vironment, one should either do some-
nificantly different energy-absorbing thing to protect the material from the
capacities. This would lead to a temper- environment or possibly even change the
ature-transition behavior which would material in the hardware. On the other
be superposed on the geometry effect hand, if the specimen tests show no ap-
described in the basic reference. parent susceptibility to environmentally
B. G. JOHNSON2~ comments per- induced crack growth one might expect,
tain to the stress-intensity ratio concept but not necessarily guarantee, there will
for predicting sustained load failure not be such crack growth in the hard-
where the subcritical flaw-growth mecha- ware.
nism might involve surface absorption E. J. RIPLING~L---Iwould like to de-
and subsequent diffusion to the crack scribe a plane-stress fracture testing
front. For such mechanisms, one might procedure on which our laboratory is cur-
expect geometric effects such as surface rently working so that the panel mem-
area and volume to affect correlation bers, particularly Messrs. Srawley and
between test specimens and the actual Brown, might give us their comments.
part. The technique was initially developed for
MR. TII~rANY--I think Mr. Johnson is adhesive joints, but because it has some
referring to the fact that in a specimen advantageous characteristics we have
test the sample being tested is generally recently been using it on homogeneous
t8 j. I. Bluhm, "A Model for the Effect of systems, including metals and ceramics.
T h i c k n e s s on Fracture Toughness," Proceedinos, Both the testing procedure and method
Am. Soc. Testing Mats., VoL 61, p. 1324, 1961. of analysis, as applied to adhesives have
19 j. I. Bluhm, "Geometry Effect on Shear
Lip and Fracture Toughness Transition Tem- been described.22 Their application to
perature for Bimodal Fracture," Proceedinqs, solid members as opposed to joints is
Am. Scc. Testing Mats., Vol. 62, p. 914, 1962.
~0 Research engineer, The Boeing Co., Wich- 2t Materials Research Laboratory, Inc.,
ita, Kans. Riehton Park, Ill.

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PANEL DIscussmN 397

quite new and has not been formally made some distance into the sample to
disclosed as yet. serve as a crack starter. (We have most
The unique characteristic of the sam- recently been making this cut from the
pie is that it uses crack-line loading two sides with a slitting cutter or abra-
rather than a remotely applied load. sive wheel so that it has a winged front.)
Irwin and Kies have pointed out that The crack starter is then extended to
for such loading the crack-extension form a natural crack by pulling on rods
force, ~, decreases rather than in- that fit into loading holes, E. The crack
creases with crack length, a; conse- initially jumps a considerable distance on
quently, crack extension is stable. Since this first pull, and we hope to minimize
a crack will propagate when ~ equals this distance by the use of the winged
~,~ (ignoring strain rate), stability results slot. After forming the natural crack, the
from the moving crack running into a sample is reloaded until the crack ex-
region of decreasing 9, while ~ is con- tends, it is then unloaded, and the proc-
stant for the material. It is this relation- ess is repeated until the crack finally
ship between ~ and ~c that causes the runs the full length of the sample. Each
crack to become self-arresting. For a loading, of course, gives a value for 9~ 9
remotely applied load, on the other hand, Edge grooves are added to the sides
increases with a so that once the crack of the sample to guide the crack. Other

]|
I|
FIo. 3--Design of Fracture Toughness Specimen Using Crack-Line Loading.

begins to extend, it continues into a re- than this, the experimental details and
gion of increasing 9, making crack exten- analysis for homogeneous materials are
sion unstable. identical with those described in the
The sample shape that Sheldon Mosto- reference given in footnote 22 for ad-
voy and I have been using for adhesives hesive joints.
is 2 in. tall, of variable thickness, and This procedure for measuring ~,~ ap-
about 1 ft long. With this test specimen, pears to have a number of advantages
we collect about 20 to 30 data points over those previously proposed:
along its length so that we get a good 1. The use of fatigue to form a sharp
average value of 9i~. crack is not necessary.
For homogeneous materials, the sam- 2. The required loads for measuring
ple shapes have been more variable, rang- plane-strain toughness are small.
ing from I by 1 by 4 in. up to about the 3. The displacements for obtaining
same size as used for the adhesives. A compliance are large.
typical sample shape might be as shown 4. Small samples can be used. For ex..
in Fig. 3. ample, we used this test to measure the
To conduct a test, a saw cut, F, is fracture toughness in the short trans-
verse direction of 1-in. thick steel armor
E. J. Ripling, S. Mostovoy, and R. L. plate.
Patrick, "Measuring Fracture Toughness of
Adhesive Joints," Materials ReSearch & ,Stand- MR. SRAWrEY--The specimen pro-
ards, Vol. 4, No. 3, March, 1964, pp. 129-134. posed by Mr. Ripling is indeed most in

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398 FRACTURE TOUGHNESS TESTING

teresting. While this specimen is men- make a crack about 2 in. long. If the end
tioned in the symposium paper by Mr. of the crack is blunt, then it takes an
Brown and me, we regarded it as a special appreciable amount of energy to get it
case, appropriate for testing adhesive to make the first jump. If you want the
joints. We were not aware that it had crack to jump only a small distance, you
been used successfully for homogeneous can put a C-clamp downstream on the
materials. However, I recollect now that sample and the crack then cannot run
there is a treatment of the cleavage of past it. I do not see how a crack formed
crystals by Gilman 23 that concerns a in this way can differ from a running
very similar sort of specimen. I am in- crack that we encounter in real circum-

DIMENSIONS IN INCHES ~ t r/re =_


I lAB ;.-,
2 "i I |
[ ] :':o?=.l i,,'.l!, t
-;
1"~-'1/2"~ / "~ I/2:- 20 CL. 2 THE).
NOTCH ~ _
~ ~x~7/////////////~.
0:025-~ I~ ~NITIAL NOTCH
9 -~ ~ / ' ~ DIMENSIONS ~ _
SPECIMEN PREPARATION: " ~ ' * ~
.... rn 0.003 MAX.-~-~ :~ 40 ~
I. MACHINE NU/(.;H ~ :
2. COMPRESS NOTCH CLOSED ~--~r//~Y///////~//////////%~/////~
3. STRESSRELIEVE II50"F/IHOUR r/--.~~
4. FINISH MACHINE
FIG. 4---Small Fracture Specimen Suitable for Use in Reactor Studies.

terested in the claim that there is no stances. On the adhesive work, we use
need for fatigue cracking of Mr. Rip- samples about 1 ft long and 2 in. deep
ling's specimen. Is this true for homoge- and we get 20 to 30 data points along the
neous materials or only for adhesive length of the sample so that we get a good
joints? average on ~c.
MR. Rn, LINC,---We have not done a MR. SRnW~EY--Do you use side
great deal of alloy testing, but from the notches to prevent the crack from devi-
little we have done there seems to be no ating from its initial plane?
problem. We use a 15-rail slitting saw to MR. RIyLINC.--Yes, we do. And this is
a modification that Mast of N R L sug-
t~j. Gilman, "Cleavage and Ductility in gested. These force the crack to remain
Crystals," Fracture, edited by B. L. Averbaeh
e t al, Technology Press and John Wiley &
within the plane along which you want
Sons, Inc., New York, N. Y., 1959, p. 193. it to run and also suppress shear lips.

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PANEL DISCUSSION 399

R. E. JOHNSON~-A specimen similar MR. WEISS---I wouldI like to make a


to Mr. Ripling's was designed by Man- comment on the type of specimen pro-
joine.25 Because of its small size (see posed by Mr. Ripling, using side notches.
Fig. 4), it can be irradiated in a reactor This specimen limits the plastic zone
core without excessive heat generation associated with the edge notch. If the
from gamma radiation. We may specu- specimen represents a design application,
late that fracture data obtained under this is fine; however, it is not clear how
such loadings will, when properly ana- one would calculate a representative Kc
lyzed, yield information as useful as value or any other value which would
that from conventional specimens. In- agree with that obtained from another
deed, these specimens provide flat, brit- specimen design. We have recently ob-
tle fractures with much less expenditure tained a few results from sheet speci-
of material than is required under simple mens having the same crack geometry
tensile loading. but different lengths. One might specu-
Such a specimen may be most appli. late that the shorter specimens would
cable to the testing of tough metals. have less stored energy and, therefore,
Along these lines, previous comments cast higher strength than the longer speci-
doubt on the sanity of those trying to mens. However, we found that the
measure the toughness of materials strength decreased substantially with a
when critical crack sizes range in inches. decrease in specimen length. The only
In defense of this minority group, at- explanation we have is one that might be
tention should be directed toward, for associated with end effects. By means of
example, the fracture behavior of low- compliance gages we were able to deter-
alloy steels in nuclear reactor pressure mine that the energy-release rate in-
vessels. Given sufficient exposure to neu- creases for the shorter specimen. There.
trons, the initially high toughness may fore, I think that Mr. Ripling's specimen
be drastically reduced. In order to meas- is a conservative specimen but, since we
ure that change, one must have an initial do not know how conservative it is, a
value in which confidence can be placed penalty may be imposed on the material
and I submit this as a subject worthy of that is being evaluated.
the panel's consideration. MR. IRwin--The stress analysis of a
MR. BRowN--Perhaps you refer to specimen such as that described by Mr.
some of my previous remarks to Mr. Ripling would appear to be rather for-
Wells. They were not designed to test midable since it contains side notches.
anyone's sanity, but rather to get the However, one can use a compliance
problem clearly fixed in the minds of calibration to obtain an average ~ value
those who have worried about very small which would represent the average acros;
cracks in high-strength alloys. I think the thickness between the side notches.
your arguments are quite sound and, If the observed crack front has only
combined with those of Mr. Wells, give moderate curvature, then there is some
proper emphasis to the highly complex assurance of only a moderate variation
problem of assessing the fracture be- of 9 throughout the thickness.
havior of low-strength alloys. MR. BRowN--Messrs. Wells and
Burdekin have offered to present their
24Engineer, Westinghouse Electric Corp., concepts regarding crack-opening dis-
Pittsburgh, Penna. placement measurements. These ideas
~ M. J. Man]oine, "Biaxial Brittle Fracture
Tests," A S - ~ E Preprint 6$-Met-3 American are directly related to the problems we
Society of Mechanical Engineers, 1964. have just been discussing concerning the

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400 FRACTURE TOUOHNESS TESTING

evaluation of the fracture characteristics tip without increase in length of the


of low-strength alloys. crack. The magnitude of this separation
F. M. BtrgDr.X.L~e--The use of frac- at the crack tip has been termed the
ture mechanics concepts to predict the crack-opening displacement. The ASTM
conditions for failure of certain materials treatment can be extended by means of a
has now become widel~ accepted, but the tensile dislocation analysis to take into
range of materials to which the straight- account this widespread plastic deforma-
forward ASTM treatment is strictly ap- tion;7. ~8
plicable is, of necessity, limited to truly The model for such a tensile disloca-
brittle materials and those, such as high- tion analysis is shown in Fig. 5. This
strength steels, which fracture with only model is based on a real crack of length

I" Uniform applied stress o" lot infinillfl


e'b " % = rv = coast '

01
a

~x

: cos / W-~T)"
901

6 ~wE Iogsec rr(~)


"

Fro. 5--Representation of Local Crack-Tip Plasticity by Tensile Dislocation.

small amounts of plastic deformation 2a in an infinite plate. Under a uniform


localized at the tips of defects. For mild stress, a, applied in the y direction, a
steel, however, quite widespread plastic plastic zone is produced at the tip of the
flow may take place before the initiation real crack extending to x = :eat. This
of fracture even when the actual propa- situation is represented for the purposes
gation is of a brittle nature (that is, ex- of analysis by a crack of length 2at,
hibiting a crystalline appearance and low which is surrounded by an entirely dastic
surface deformation). The presence of a
plastic zone at the tip of a crack enables A. A. Wells, "Notched Bar Tests, Fracture
the two faces to move apart at the crack Mechanics and Strenoth o$ Welded Structures,"
Houdremont Lecture, International Institute of
leWritten discussion prepared jointly by A. Welding, British Welding Journal, Vol. 12, No. 1,
A. Welh, Queens University, Belfast, Ireland, San. 1965.
and by F. M. Burdekin and D. E. W. Stone of u F. M. Burdekin and D. E. W. Stone, "Frac-
The British Welding Research Assn., Reeeareh ture Mechanlca Proor~s Report CI$0/I, 196~,"
Station, Abington Hall, C~mbridge, England. British Welding Research Assn., 1965.

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PANEL DISCUSSION 401

stress field when under load, but which assuming plane-stress conditions. The
is stressed not only by the externally stress function for a crack in an infinite
applied stress, r but also by a series of plate under biaxial tension is well known
internal tensile stresses in the y-direction and it is only necessary to superpose a
of magnitude, gb, at x = b in the region, uniform stress, - a , in the x-direction to
-4-a __< 4-b __< -+-al. The stresses applied satisfy boundary conditions for an in-
within the crack of length 2al represent finite plate under uniaxial tension. The
the stresses in the plastic zone at the tip internal stress was considered to consist
of the real crack and, for the purposes of of a series of internal forces of magnitude,
this analysis, will be taken as constant ab rib. The existing stress function for a
and equal to the uniaxial tensile yield pair of splitting forces, taken negative to
_ 0.20

Stobte crocking---.--m.o
.-- 0.16

,,
R,Tm CRACKLENGTH . .9_ ,, .1.
,u GAUGELENGTH y 12 9 9 /

~ 0.12
.2"
O.OG Theoretico[ retetionship
from tension distocotion ~ "
ey
5
~ o.o~
.~" ~ Pop-in"?

t I ! I t I I I I I
0.1 0-2 0-3 O.t, 0-'; O'S
NON-DIHENSIONALSTRAIN [~y}
Fzo. 6--Comparison of Theory and Experiment for Rehtionship between Crack-Opening Dis-
placement and Over-all Strain for 7075-T6Aluminum Alloy.

stress of the material, % . While the as- represent tension, can now be integrated
sumption that plastic deformation is con- over the range from b = 4-a to b = q-a1
fined to the plane of the crack is not a to give a stress function for the internal
rigorous plastic solution, experimentally stress system. The two stress functions
determined plastic-strain patterns show for the external and internal stress sys-
that, for thin sheets of mild steel at tems can then be combined in any re-
least, such deformations are confined to quired proportion to form the final stress
a narrow band along the plane of the function. This proportion is determined
crack until the incidence of 45-deg slip by the requirement that no stresses exist
lines and a general yield mechanism. in excess of the yield stress of the ma-
The stresses and displacements around terial, or in terms of the ASTM treat-
the elastically stressed crack of length ment, this may be regarded as equating
2al can then be analyzed using the Wes- the stress-intensity factors of the two
tergaard stress-function technique and individual applied stress systems. It cab

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402 FRAC"rVRE TOUGHNESS TESTING

be shown that for the stresses at the It is possible to relate the crack open-
point x = a~ to remain finite, the rela- ing displacement 6 to the more familiar
tionship between the real crack length, quantity ~, the crack-extension force,
a, and the extent of the plastic zone, a~, to compare the analysis with the ASTM
is: treatment for small plastic zones. This
o
analysis makes use of the relationship,
- - ~ COS = ~ , derived by local energy argu-
ments similar to those used to relate K
Thus a total combined stress function and 9, to effect this comparison. By ex-
may be formulated from which the open- panding the expression for 6 as a series
ing displacement at the tip of the real and considering the effect of the in-
crack can be calculated as fluence of successive terms, it can be

5 = " ~ log, scc { seen that good agreement is obtained


both with the basic ASTM expression,
9 = (~ra/E, and with the suggested cor-
The variation of 6 with the ratio of ap- rection for small plastic zones.
plied stressto yield stress, a/~y, becomes
very sensitive to small changes in this -= - ~ - log, sec
ratio as it approaches unity, and it is
therefore preferred to relate the crack- Thus, if ~ = %6
opening displaccmcnt, 6, to the over-all
strain, e, over a gage length, 2y. A some-
what more complex expression may be
derived from the analysis for over-all
strain, and Fig. 6 shows a comparison of +~ +~ + ...
theory and experiment for the relation-
ship between crack-opening displacement Taking only the first term in the expan-
and over-all strain for a particular ratio sion,
of crack Icngth to gage length plotted
~ro-~a ~o~a
on a nondimensional basis. The experi- 9= E r ASTM:9 =
mental results werc obtained on an
aluminum alloy of low work-hardening Taking the first and second terms,
capacity to give a true comparison with
the theory which is of course based on a
non-work-hardening material. The open- ~=-~- ~+~
ing displacement at the crack tip was
measured optically using a microscope c.~. ASTM: ~ = T 1+
fitted with calibrated shutters. The dis-
continuity in the experimental results Taking the first three terms,
was accompanied by a noise indicating a
possible pop-in, and thus perhaps a
change from plane-strain to plane-stress ~=-~- I+~ +~-~
conditions. It must be pointed out, how-
cvcr, that in similar experiments on mild The concept of a critical ~ for initiation
stecl the agreement between thcory and of fracture of high-strength materials
experiment was not so good, and this is has proved so successful that it was logi-
bclieved to be largely due to strain hard- cal to extend the implied critical dis-
cning. placement for fracture with localized

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PANEL DISCUSSION 403

plasticity to situations where the plas- physical measurement of crack-opening


ticity was more substantial. It was this displacement was made with a small
background which led Mr. Wells to probe placed in the root of the notches
propose the hypothesis of a critical crack- throughout the tests. The results shown
opening displacement for fracture ini- give the values of opening displacement
tiation, dependent only on material tem- at fracture measured on 3-in. thick,
perature, strain rate, and triaxiality of 3-ft wide edge-notched plates in tension,
stress, but applicable even with extensive and on 3- and ~-in. square notched slow
yielding. The critical displacement cri- bend tests. A variety of notch depths

lOOx['lO: "~" "I ~ ~ .... I ) | I | l I

• 3in, thick 3It squore notch tensite specimens


3in. squore notch bend specimens
80 o 3/6in. sqgof:e notch bend specimens

~ S0

I
.5'
,Ic

~-' 20
OF "

]
I I. [
-120 -100 -80 -60 -/,0 -20 0
TEHPERATURE.[~ }
FIO. 7--Effect of Ratio of Crack Length to Plate Width on Relationship between Applied Stress
and the Opening Displacement as Taken from the Tensile Dis]ocationAnalysis.

terion is compatible with those concepts were employed, but in all cases the tip of
of fracture by the opening mode, which the notch was formed by a fine saw cut
operate by the creation of a series of 0.006 in. thick9 The first immediate im-
microcracks ahead of the crack, followed pression is that the results are closely
by a drawing out of the bridges between similar for the immensely different sizes
them to complete the fracture process. of specimen employed, despite the fact
This criterion has been examined ex- that the tension tests failed around or
perimentally in a series of tests on mild even below general yield, and the bend
steel specimens of different sizes and specimens well afteryield. Different trends
geometrical configurations, and the re- are observable, however, in that there is
sults to date are shown in Fig. 7. The an apparent transition indicated for each

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404 FRACTURE TOUGHNESS TESTING

type of specimen where there is a drop in is shown in Fig. 8 for three different
the opening displacement at fracture ratios of net applied stress (*'n) to yield
with decreasing temperature. stress (ay). It may be seen that failure
In addition, those specimens marked below general yieM is most likely with a
with arrows showed fibrous thumbnails at ratio of crack length to plate width of
the notch root. This effectively changes about 0.3, which agrees with the sug-
the depth and geometry of notch and gested ratio for the occurrence of a maxi-
gives a deceptively high reading for mum of 9. Also shown are the ratios of
opening displacement at initiation of un- net stress to yield stress at fracture in

0'9 [ I I ! I I | I I

i 1.'1/, ii1.12
O.S

ol-212
0.7 II -10"C
9 -I,O C
0"6 • -53"C

0.5 "-'

[ .~

0.3

0.2

(1-1

0
O 0.1 0.2 0"3 0'4 0'5 0:6 0'? 0.9 0.9 1.0

FIG. 8--ExperimentallyObserved Variation of Crack Opening with Temperature.

stable fracture. Triaxiality effects are some of the wide-plate tension tests
suspected and current work is aimed at previously described, and it can be seen
explaining these effects more satisfac- that good agreement is obtained.
torily. The work reviewed has been an at-
From the tensile dislocation analysis tempt at the extension of linear fracture
described previously, it is possible to ap- mechanics to materials such as mild steel
proximate the effects of finite plate width having the property of substantial yield-
by considering finite widths within an ing. It is seen that this approach, em-
infinite plate. The relationship between ploying the crack-opening displacement
the opening displacement, 8, and the concept, is contiguous with the ASTM
crack length, 2a, in a plate of width 2B, treatment of high-strength materials,

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PANEL DISCUSSION 405

and shows great promise of extending the no impediment to measurement of crack-


range of applicability of fracture me- opening displacement under the same
chanics to yielding materials. circumstances. Fracture experiments con-
MR. BROWN--I would like to ask Mr. ducted at given temperatures on tensile
Burdekin what use he makes of these wide plates with edge notches of a wide
crack-opening displacements in rating range of depths, leading to fracture both
materials in regard to their toughness? below and above general yield, have
Do you standardize on a specimen and shown the same crack-opening displace-
then measure the opening displacement? ment at fracture in both cases.
MR. BURDEKIN--We are at a very The intervention of triaxial stress ef-
early stage in this approach, but eventu- fects on fracture is shown in these tests,
ally we hope to be able to correlate re- as in established fracture toughness test-
sults from different sizes of specimen so ing, by the exhibition of plane-strain and
that the answers for full-scale behavior plane-stress fractures in different thick-
can be predicted from small-scale tests. nesses of materials. In addition, with
Using small specimens, we would then be the additional boundary effects that
able to rate the toughness of the rela- arise in thick plate testing, the effects be-
tively low-strength materials we are come more complex. The maximum tri-
working with. The first problem facing axiality (lowest fracture toughness at
us is to sort out the effects of triaxiality given temperature) observed in an edge-
on critical crack-opening displacements. notched tensile plate of mild steel, is
MR. BRowN--What attention are you higher than that seen in an equal thick-
drawing to the role of triaxiality in your hess bend specimen with three-point
test, and what is affecting the magnitude loading. The triaxiality appears to rise
of triaxiality? with edge notch depth, in a plate of
MR. BURDEKIN~I am suggesting that given thickness, to a maximum when the
even under plane-strain conditions, varia- notch depth equals the thickness, and
tions in the relative magnitudes of three declines with deeper notches. These
principal stresses may occur. With a effects assume added importance when
plastic zone at the tip of a physical crack it is realized that they move the ductility
of finite root radius, the stresses at the transition temperature over an observed
crack tip in the x- and y-directions of the range of about 40 C.
classical analyses are no longer equal, and It is considered that the ASTM frac-
the stress in the thickness direction will ture toughness testing methods for high-
consequently be different from that of strength steels, now under discussion,
the linear elastic case, so that the ratios should be re-examined for further evi-
of the principal stresses may be different. dence of these effects.
M~. WELLS--A particular property of MR. IRwiN--When we employ linear
the crack-opening displacement approach elastic fracture mechanics analysis, in-
to fracture is that it is fully contiguous ferentiaUy this means that the terms of
with the alternative treatment in terms reference are significant and helpful to
of 9 or K. That is to say, a material in us in visualizing the physical phenomena.
possession of a characteristic fracture In the high-stress level or general yield-
toughness, 9, has a corresponding crack- ing range, we need other viewpoints in
opening displacement at fracture, equal to order to provide terms of reference which
~c divided by the material yield stress. are meaningful. For this purpose, the
Whereas 9~ cannot be measured in speci- crack-opening displacement idea pro-
mens which yield before fracture, there is posed by Mr. Wells is certainly worth a

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406 FRACTURE TOUGHNESS TESTING

good try. I would also recommend the that a relatively small inhomogeneity
analysis in the McClintock and Irwin may nucleate a strain-controlled failure.
paper as worth a good try, a critical P. N. RANDALLS~ would like to
fracture strain combined with a struc- refer back to the first report of the com-
tural-size factor. mittee and ask: how do you rationalize
B. M. WUNDT29--I would like to ask
Mr. Wells to comment on the following
in light of his description of crack-open-
ing displacement measurements. It is
possible to calculate, using advanced
methods of elastic-plastic analysis, the
strain at burst in the bore of a rotating
disk. For heterogeneous materials, these
strains have been found to be from 0.75
per cent to a few per cent and the stress
at about the yield strength. In these :: ~ ~
cases the fracture appears to be controlled
by a critical strain. 1-
MR. WELLS--It is the object of our
studies to evaluate such situations as
described by Mr. Wundt, but we have
not ourselves worked on the spinning
disk configuration. I am of the opinion
that the crack-opening displacement ap-
~ s~ ~1~~
proach would be helpful in dealing with
the problem of correlation in the plastic
range between the disk results and those I
from smaller-notched bend and tension I
tests. I
MR. WEiss--Fracture in ductile ma- I
terials may certainly originate from a
region of heterogeneity by some strain-
1
controlled process. The paper by McClin- I
CRACK SIZE
tock and Irwin shows that one needs
FIG. 9--Notch-Strength Versus Crack-Size
about 20 times the elastic strain for this Curves for Two Materials, Tested UsingSurface-
to happen. Neuber's relationship be- Cracked Specimens showing Intersection at
tween true stress concentration factor, Stresses below the Yield Strength of Either
Material.
true strain concentration factor, and
elastic stress concentration factor
slow crack growth in terms of linear
((K,K,) u2 = Kel,,,tic) elastic fracture mechanics? How can you
do this wouthout consideration of plas-
suggests that such a heterogeneity would ticity? I raise this question because I feel
have to be equivalent to a stress concen- there is a tendency among the uniniti-
tration with a stress concentration factor ated to oversell linear elastic fracture
between 4 and 5. Thus, it is conceivable mechanics for engineering use, whereas it

~gGeneral Electric Co., Large Steam Gen- a0 T R W Space Technology Laboratories,


erator Dept., Schenectady, N . Y . Redonda Beach, Calif.

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PANEL DISCUSSION 407

seems that one must go beyond that to has the steeper slope contrary to the
explain even the common observation experimental findings. There is the addi-
that crack growth can be stable. tional question: if K~o values are to be
MR. IRWIN--I had a long discussion of obtained from tests at only one crack
these matters at the November, 1963, size, how shall that size be chosen? The
ASME meeting.8~ Obviously, to explain rating of the two materials depends on
any behavior aspect in the region of large this choice.
nonlinear strains at the crack tip, one MR. SRAWLEY--In general, a higher-
must have ideas beyond linear elastic strength material will have a shorter
fracture mechanics. Consider a length of critical crack size than a lower-strength
plane-strain crack border along which the material. The curves usually intersect at
stress condition is one of plane strain. a crack length less than that at which the
Small openings must be developing near lower-strength material could sustain
the real border of the crack and the crack loading to the yield strength before frac-
can scarcely spread forward unless these turing. The corresponding stress is
advance openings are joining laterally in slightly higher than the yield strength of
the direction parallel to the crack border. the weaker material.
A priori, the simultaneous forward and MR. PAYNE--When using surface-
lateral joining of advance openings is a crack specimens, tests of several crack
process in which the final stages through sizes are always desirable. The question
any given set of advance openings should of whether material ratings will change
be quite rapid. With this behavior oc- with crack size must be examined in light
curring in nearly equal degree in each of whether or not all conditions for a
segment of the crack border, an abrupt valid fracture toughness test are met. It
forward-motion instability is expected. is not clear whether the curve crossing
Why, then, do we sometimes observe mentioned by Mr. Randall was obtained
slow crack extension in plane strain? In using specimens of sufficient size to avoid
the absence of a time-dependent influ- net-section yielding and having crack
ence such as stress corrosion, slow growth depths less than one half the thickness. I
occurs primarily as a crack-arrest be- believe Mr. Randall's remarks are based
havior due to load transfer from the on the data for Ti-6A1-4V alloy which he
plane-strain region to adjacent unbroken published early this year, 3. and not all
shear lips. of these data met the conditions for a
MR. RANDALL--I would also like to valid toughness test.
question the use of expressions from MR. RANDALL--My remarks were
fracture mechanics that relate the stress based on data in the ASME paper plus a
at failure to crack size by a single con- great deal more that were obtained by
stant, K~,. Figure 9, giving typical other organizations participating in the
graphs for a steel or titanium alloy heat- Minuteman program. Crack depths of 65
treated to two strength levels, shows that per cent of the thickness were considered
the curves cross, often at stresses below permissible since the plastic zone did not
the yield strength. Plots of expressions appear to reach to the back face of the
from fracture mechanics have slopes pro- specimen, as evidenced by the absence
portional to K~,--the tougher material of a dimple there prior to fracture.
al O. R. Irwin, "Crack Toughness Testing of
Strain Rate Sensitive Materials," Transactions, P. N. Randall and R. P. Felgar, " P a r t
A S M E Series A, Vol. 86, p. 444, Oct., 1964. Through Crack Test-Relation to Solid Propel-
See also the present paper by J. M. Krafft and lant Rocket Cases," A S M E Paper No. 63-WA
G. R. Irwin, p. 114. 187, A m . Sac. Mechanical Engineers, 1964.

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408 FRACTUIU~-TOUGHNESSTESTING

MI~. PAYNE--I recently published u In hardware, net- and gross-fracture


a re-analysis of Ti-6A1-4V alloy data pre- strengths are identical for practical pur-
sented in Mr. Randall's ASME paper. poses due to the large area involved. Use
If those data points are eliminated which of net stress for laboratory surface-crack
did not have stresses above the yield specimens simply produces artificially
strength or had crack depths greater elevated strength values which are sensi-
than one half the thickness, the remain- tive to actual specimen dimensions.
ing data yielded a constant value of The use of crack area for surface cracks
Kro and the crossovers were not observed. seems highly unrealistic. Surface-crack
I would suggest that when unexpected fractures begin at the maximum depth
behavior is observed, such as that just point, rather than randomly around the
B~O00

TENSILE STRENOTH
74000 . . . . . . . . . . " ---
EXPERIMENTAL
~ ------ PREDrCTED
a. I YIELD
6~000 ~TRESS

z 5~000
o
V-
,?,
Ul
40000
0

30,000

2o,ooo
0.02 0.04 0.06 0.00 0.10 0.12 0.14 0.16 0.18

CRACK DEPTH (IN)

FIG. 10---Experimental and Predicted Gross-Section Stress for Semi-Elliptical Surface-Cracked


Panels of 2014-T6 Alloy. (Ratio of Crack Depth to One Half the Crack Length Is 0.50.)

illustrated by Mr. Randall, larger speci- crack tip. Description of the stress dis-
mens be tested to find out whether or not tribution at fracture should apply to the
the behavior persists. region where fracture occurs. The stresses
I would also like to make a comment on at the maximum crack depth are in-
the methods used to represent surface- fluenced far more by depth than by crack
crack specimen data. In my opinion, a length, and the crack area parameter
curve of gross strength versus crack size does not reflect this.
(expressed as a/Q or crack depth with a C. M. CARMXNtt---I believe that our
constant ratio of crack depth to length, argument concerns the consistency of
rather than area) would be appropriate Kr, values as measured by different tech-
for a designer. niques. For example, at Frankford Ar-
" W. F. Payne, "Analysis of Surface Crack senal we measured the Kz~ values of 2014-
Fracture Toughness Information," A F Report
No. ML TDR-#~-s Vol. I, Fourth Maraging t4Metallurgist, Metallurgy Research Lab-
~Jteel Project Review, 1964, pp. 307-367. oratory, Franldord Arsenal, Philadelphia, Pa.

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PANZL DISCUSSmN 409

T6 aluminum using a circumferentially appears to be some question concerning


notched round specimen. Using this the suitability of the data for a fracture
K~c value, we calculated the failure mechanics analysis. Of course, to make a
stress of ~-in. thick panels of thismaterial fair judgment on this point we would
having part-through cracks. These cracks have to examine all pertinent information
were machined and fatigued so that they and we cannot do that here. However,
would all have the same geometry. The this controversy again emphasizes the
data developed are shown in Fig. 10. fact that judgments concerning the valid-
The agreement between the calculated ity of fracture mechanics analysis require
and experimental breaking stresses shows very carefully designed experiments in
good consistency in K~c values using which all pertinent variables are sys-
widely different specimen geometries. tematically controlled. Perhaps this
MR. B~owN--I do not think we are would be a suitable note on which to
going to come to any definite conclusions conclude what has been a most interest-
about Mr. Randall's observations. There ing and informative panel discussion.

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