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Abstract
Translucent MgO ceramics have been fabricated by hot-pressing using nanopowder of MgO containing 2 – 4% LiF as a fugitive additive.
Thin circular discs were pressed uniaxially with the LiF-containing nanopowders. The hot-pressing was carried out either in Ar or in vacuum,
holding at 1100 jC for 30 to 60 min at either 24 or 45 MPa. The samples were then annealed in air by either conventional or microwave
processing. The annealed samples were highly dense and optically translucent.
D 2003 Elsevier B.V. All rights reserved.
0167-577X/$ - see front matter D 2003 Elsevier B.V. All rights reserved.
doi:10.1016/S0167-577X(03)00560-3
552 Y. Fang et al. / Materials Letters 58 (2004) 551 – 554
Table 1
Hot-pressing conditions
Batch LiF% Ramping Hold Pressure
(jC/min)
A 0; 2; 4 10 1100 jC 60 min 45 MPa in Ar
B 2 3 900 jC 30 min + 45 MPa in Ar
1100 jC 30 min
C 4 3 1100 jC 60 min 24 MPa in vacuum
2.3. Hot-pressing
2.4. Annealing
2.5. Characterization
Table 2
Annealing conditions
Conventional Microwave in air Microwave in vacuuma
1000 jC 2 h 1000 jC 30 min 1000 jC 90 min
a
For samples made in hot-pressing batch C (Table 1) only. Fig. 2. Microstructure of the nano-MgO powder by (a) SEM and (b) TEM.
Y. Fang et al. / Materials Letters 58 (2004) 551 – 554 553
B ¼ 0:9k=ðtcoshÞ
References