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Determining Minimum
Laboratory Soil Resistivity
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Determining Minimum
Laboratory Soil Resistivity
1. SCOPE
1.1. This test method covers the laboratory determination for the minimum resistivity of a soil.
1.2. The principal use of this test method is to determine a soil’s corrosivity and thereby identify the
conditions under which the corrosion of metals in soil may be sharply accentuated. This standard
is divided into two parts. The first part involves obtaining and preparing the sample to size for
testing, and the second part describes the test method for determining the minimum laboratory
soil resistivity.
Note 1—When less than 5 percent of a material passes the No.10 sieve, this test method may not
be indicative of the corrosion potential of the material.
2. REFERENCED DOCUMENTS
2.1. AASHTO Standards:
M 231, Weighing Devices Used in the Testing of Materials
R 76, Reducing Samples of Aggregate to Testing Size
R 90, Sampling Aggregate Products
3. SCOPE
3.1. This method covers the dry preparation of soil and soil–aggregate samples, as received from the
field, for soil resistivity determination.
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4. APPARATUS
4.1. Balance—The balance shall have sufficient capacity and be readable to 0.1 percent of the sample
mass, or better, and conform to the requirements of M 231.
4.2. Drying Apparatus—Any suitable device capable of drying samples at a temperature not exceeding
60°C (140°F).
4.3. Sieves—A series of the following sizes: 6.3 mm (1/4 in.), 4.75 mm (No. 4), 2.00 mm (No. 10), and
pan as required for preparing the sample for the minimum soil resistivity test. The sieves shall
conform to ASTM E11 (see Note 2).
4.4. Pulverizing Apparatus—Either a mortar and rubber-covered pestle or any device suitable for
breaking up the aggregations of soil particles without reducing the size of the individual grains of
soil (see Note 3).
4.5. Sample Splitter—A suitable riffle sampler or sample splitter for proportional splitting of the
sample and capable of obtaining representative portions of the sample without appreciable loss of
fines. The width of the container used to feed the riffle sampler splitter should be equal to the total
combined width of the riffle chutes. Proportional splitting of the sample on a canvas cloth is
also permitted.
Note 2—The sieve sizes that have an opening size of 6.3 mm (1/4 in.) or larger shall conform to
the requirements specified in ASTM E11, excluding column No. 7. This exclusion permits the use
of heavier screens in nonstandard frames that are larger than the 203.2 mm (8 in.) round frames.
Note 3—Other types of apparatus are satisfactory if the aggregations of soil particles are broken
up without reducing the size of the individual grains.
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5. SAMPLE SIZE
5.1. The amount of soil material required to perform the minimum soil resistivity test is as follows
(see R 90):
Sieve Size
Test Approx Mass (g) Finer Than:
Resistivity 1500 2.00 mm (No. 10)
6.2. The portion of the dried sample selected for minimum soil resistivity testing shall be separated
into fractions by one of the following methods:
6.2.1. Alternate Method Using 2.0-mm (No. 10) Sieve—The dried sample shall be separated into two
fractions using a 2.00-mm sieve. The fraction retained on the sieve shall be ground with a
pulverizing apparatus until the aggregations of the soil particles are broken into separate grains.
The ground soil shall then be separated into two fractions using the 2.00-mm sieve.
6.2.2. Alternate Method Using 4.75-mm and 2.00-mm (No. 4 and No. 10) Sieves—The dried sample shall
first be separated into two fractions using a 4.75-mm sieve. The fraction retained on this sieve
shall be ground with a pulverizing apparatus until the aggregations of soil particles are broken into
separate grains and again separated on the 4.75-mm sieve. The fraction passing the 4.75-mm sieve
shall be mixed thoroughly and, by the use of the sampler or by splitting and quartering, a
representative portion adequate for testing shall be obtained. This split-off portion shall then be
separated on the 2.00-mm sieve, and processed as in Section 6.2.1.
6.2.3. Alternate Method Using 6.3-mm and 2.00-mm ( 1/4 in.- and No. 10) Sieves—The dried sample shall
first be separated into two fractions using a 6.3-mm sieve. The fraction retained on this sieve shall
be ground with a pulverizing apparatus until the aggregations of soil particles are broken into
separate grains and again separated on the 6.3-mm sieve. The fraction passing the 6.3-mm sieve
shall be mixed thoroughly and, by the use of the sampler or by splitting and quartering, a
representative portion adequate for testing shall be obtained. This split-off portion shall then be
separated on the 2.00-mm sieve, and processed as in Section 6.2.1.
7. SCOPE
7.1. This method covers the laboratory procedure for determining the minimum resistivity of soil
samples. The values obtained from this method are relatable to the corrosion potential that a soil
may exhibit.
8.2. 100-, 200-, 500-, and 900-ohm resistors with a 1 percent tolerance.
8.4. 2.00-mm (No. 10) sieve conforming to the requirements of ASTM E11.
9.1.1. Zero the resistivity meter by clamping the two leads together, and adjusting the meter
(if necessary).
9.1.2. Connect the leads of the resistivity meter to the 100-ohm resistor and read the meter. Repeat this
process with the 200-, 500-, and 900-ohm resistors.
9.1.3. If the readings are within 10 percent of the resistance of the resistor, the meter is
functioning satisfactorily.
10.2. Add 150 mL of distilled water to the prepared soil. Mix the sample thoroughly and cover the test
sample with a damp cloth and allow the sample to stabilize until equilibrium has been reached, or
allow to cure a minimum of 12 h.
10.5. Thoroughly mix and place the sample in the soil box in layers and compact (moderate compaction
with the fingers is sufficient). Trim off the excess material with the straightedge.
10.6. Measure the resistance and calculate the resistivity of the soil in accordance with the instructions
furnished with the meter and record the test value.
10.7. Remove and retain the soil from the box, add 100 mL of distilled water to the sample, and mix
thoroughly. Clean the soil box with distilled water prior to performing the next test.
10.8. Repeat the process of placing, compacting the soil in the box, then measure the resistance and
calculate the soil resistivity (see Note 6).
10.9. Repeat the steps in Sections 10.4 to 10.8 until a minimum value can be determined.
10.10. The minimum value is used for computing the minimum soil resistivity and reporting (see Note 7).
11. REPORT
11.1. The minimum soil resistivity value determined above should be reported in units of (ohm) × (cm).
11.2. The minimum soil resistivity utilizing the typical soil box is:
minimum soil resistivity minimum reading ( ohms ) × [ 6.67 cm ]
= (1)
(See Note 8.)
Note 5—Most resistance meters without an inverting circuit allow the sample under test to
polarize during measurement causing the reading to vary (i.e., drift).
Note 6—In some soils, the minimum soil resistivity occurs when the specimen is in a slurry
condition. When this occurs, it is necessary to thoroughly mix the soil slurry and then pour the
slurry water into the soil box until full. If the soil box doesn’t reach its capacity with the addition
of the slurry water, add just enough of the mixed soil into the box until the soil box is filled; then
take the reading.
Note 7—The minimum soil resistivity can occur at any moisture content.
Note 8—Multiplying constant for each soil box is derived by:
surface area of one electrode cm 2 ( ) (2)
cm 2
measured average distance between electrodes ( cm
= ) = cm
cm
TS-1a
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T 288-6 AASHTO
Copyright American Association of State Highway and Transportation Officials
Provided by IHS Markit under license with AASHTO © 2018 by the American Association of State Highway
Licensee=WSP and Transportation
USA/5960396001, Officials.
User=Stergiopoulos, Stavros
No reproduction or networking permitted without license from IHS
All rights reserved. Duplication Not
is aforviolation of applicable law.
Resale, 07/10/2019 04:58:43 MDT
Typical soil box:
15.24 cm × 4.445 cm (3)
= 6.67 cm
10.16 cm
The soil box may be constructed of either 6.4- or 12.7-mm (1/4- or 1/2-in.) acrylic plastic. If other
size soil boxes are used, it will be necessary to determine the correct multiplier. It should also be
noted that it may be necessary to prepare extra soil for testing to fill the soil box.
13. KEYWORDS
13.1. Corrosion potential; corrosivity; resistivity; soil corrosion.
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