JOURNAL OF EXPERIMENT

Title of Experiment : Synthesis of Tertiery Buthyl Chloride

Day/Date of /experiment : Tuesday/17th March 2020
Name/ID : Muh. Aqrim S/1913441012
Class/Group : ICP of Chemsitry Education/III
Members : 1. Andi Ria Indahsari
2. Andi Resky Handayani. HR
3. Anggraeni Febrianti
4. Eni Mendaun
5. Mawaddah WaFrahma
Assistant : Nur Rahmah Amar

A. OBJECTIVE OF EXPERIMENT
At the end of this experiment students are expected to be proficient in the
following matters.
 how to prepare and use the tools needed to make liquid organic compounds
such as reflux, solvent extraction, using separating funnels, drying, filtering,
and distillation.
 principles of aliphatic nucleophilic substitution reactions
 Typical differences between SN1 and SN2 substitution types

B. APPARATUS AND CHEMICALS

1. Apparatus
a. Destilation apparatus (1 pieces)
b. Separatory Funnel 250 mL (1 piece)
c. Funnel (1 piece)
d. Measuring Cup 25 mL (1 piece)
e. Evaporating Dish (1 piece)
f. Beaker Glass 800 mL (1 piece)
g. Enlenmeyer Flask 250 mL (1 piece)
h. Cork stoppers (1 piece)
i. Spray (1 piece)
j. Filter paper (1 piece)
k. Hot plate (1 piece)
l. Balance (1 piece)
2. Chemical
a. Tert- Butyl Alcohol ((CH3)3COH)
b. Hidrochloric Acid (HCl)
c. Sodium Hydrogen Carbonate solution 5% (NaHCO3)
d. Calcium Chloride and Calcium Sulfate (CaCl2 and CaSO4)

C. WORK PROCEDURES

12,5 gr Tert- butyl alcohol are filled 42,5 gr hydrochloric acid are added

The separating funnel is shaken

Let stand for a few minute

The lower layer is discarded NaHCO3 5% are added

The separating funnel is shaken

Let stand for a few minute

The lower layer is discarded 10 ml of H2O are added

 The separating funnel is shaken

Let stand for a few minute

The lower layer is discarded More into beaker

CaCl2

Solution was decanted

CaCl2 are Added
 6 5 6 5
7 4 7 4
8 3 8 3
9 2 9 2
10 1 11 1

The decantance result are stored in Distilled until tertiary butyl chloride
distillation flask is obtained

Makassar, 12th March 2020

Assistant Praktikan

Nur Rahma Amar Muh. Aqrim S

ID. ID. 1913441012