Quantachrome NovaWin - Data Acquisition and Reduction

for NOVA instruments

�1994-2013, Quantachrome Instruments
version 11.03

Analysis Report
Operator: . Date:2016/11/28 Operator: quantachrome
Date:2018/05/09
Sample ID: ns_a_insitu Filename: ns_a_10insitu.qps
Sample Desc: Comment: [28]
Sample weight: 0.0473 g Sample Volume: 0.0215 cc Sample
Density:2.2 g/cc
Outgas Time: 6.0 hrs OutgasTemp: 100.0 C
Analysis gas: Nitrogen Bath Temp: 273.0 K
Press. Tolerance:0.100/0.100 (ads/des)Equil time: 60/60 sec (ads/des) Equil
timeout: 180/180 sec (ads/des)
Analysis Time: 197.4 min End of run: 2016/11/28 11:07:12 Instrument:
Nova Station A
Cell ID: 19
Data Reduction Parameters
t-Method Calc. method: de Boer

BJH/DH method Moving pt. avg.: off Ignoring P-tags below 0.35 P/Po
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid
Density: 0.806 g/cc

Diameter Pore Volume Pore Surf dV(d) dS(d) dV(logd)

dS(logd)
Area

nm cc/g m�/g cc/nm/g m�/nm/g cc/g

cc/g

3.0783 1.7115e-02 2.2240e+01 4.9075e-02 6.3768e+01

3.4748e-01 4.5151e+02
3.4239 2.6337e-02 3.3013e+01 2.6932e-02 3.1463e+01
2.1215e-01 2.4785e+02
3.8052 3.4970e-02 4.2087e+01 2.0546e-02 2.1598e+01
1.7984e-01 1.8905e+02
4.2748 4.3064e-02 4.9661e+01 1.5594e-02 1.4591e+01
1.5330e-01 1.4345e+02
4.8503 5.0502e-02 5.5795e+01 1.1771e-02 9.7071e+00
1.3127e-01 1.0826e+02
5.5690 5.8491e-02 6.1534e+01 9.9195e-03 7.1249e+00
1.2698e-01 9.1203e+01
6.4960 6.6743e-02 6.6615e+01 7.8687e-03 4.8452e+00
1.1744e-01 7.2315e+01
7.8075 7.5347e-02 7.1023e+01 5.4652e-03 2.8000e+00
9.7916e-02 5.0165e+01
9.5378 8.2115e-02 7.3861e+01 3.5884e-03 1.5049e+00
7.8550e-02 3.2943e+01
12.1082 8.8740e-02 7.6050e+01 2.0355e-03 6.7244e-01
5.6407e-02 1.8634e+01
16.9012 9.5092e-02 7.7553e+01 1.0032e-03 2.3743e-01
3.8580e-02 9.1308e+00
23.2102 9.9087e-02 7.8242e+01 6.3542e-04 1.0951e-01
3.3750e-02 5.8164e+00
32.4729 1.0375e-01 7.8817e+01 3.8141e-04 4.6982e-02
2.8178e-02 3.4709e+00
52.7966 1.0958e-01 7.9258e+01 2.0518e-04 1.5545e-02
2.4330e-02 1.8433e+00
114.6028 1.1715e-01 7.9522e+01 7.9483e-05 2.7742e-03
1.9707e-02 6.8783e-01

BJH adsorption summary

Surface Area = 79.522 m�/g

Pore Volume = 0.117 cc/g
Pore Diameter Dv(d) = 3.078 nm