Quantachrome NovaWin - Data Acquisition and Reduction

for NOVA instruments

�1994-2013, Quantachrome Instruments
version 11.03

Analysis Report
Operator: . Date:2016/11/28 Operator: quantachrome
Date:2018/05/09
Sample ID: ns_a_insitu Filename: ns_a_10insitu.qps
Sample Desc: Comment: [28]
Sample weight: 0.0473 g Sample Volume: 0.0215 cc Sample
Density:2.2 g/cc
Outgas Time: 6.0 hrs OutgasTemp: 100.0 C
Analysis gas: Nitrogen Bath Temp: 273.0 K
Press. Tolerance:0.100/0.100 (ads/des)Equil time: 60/60 sec (ads/des) Equil
timeout: 180/180 sec (ads/des)
Analysis Time: 197.4 min End of run: 2016/11/28 11:07:12 Instrument:
Nova Station A
Cell ID: 19
Data Reduction Parameters
t-Method Calc. method: de Boer

BJH/DH method Moving pt. avg.: off Ignoring P-tags below 0.35 P/Po
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid
Density: 0.806 g/cc

Diameter Pore Volume Pore Surf dV(d) dS(d) dV(logd)

dS(logd)
Area

nm cc/g m�/g cc/nm/g m�/nm/g cc/g

cc/g

3.0797 1.6104e-02 2.0916e+01 4.6858e-02 6.0860e+01

3.3195e-01 4.3113e+02
3.3367 2.7032e-02 3.4017e+01 6.4176e-02 7.6933e+01
4.9296e-01 5.9095e+02
3.7462 8.6282e-02 9.7279e+01 9.1328e-02 9.7514e+01
7.8583e-01 8.3906e+02
4.3390 9.2398e-02 1.0292e+02 1.1394e-02 1.0504e+01
1.1369e-01 1.0481e+02
4.9384 9.7340e-02 1.0692e+02 7.4657e-03 6.0471e+00
8.4766e-02 6.8659e+01
5.6800 1.0209e-01 1.1027e+02 5.7876e-03 4.0758e+00
7.5562e-02 5.3213e+01
6.6236 1.0666e-01 1.1303e+02 4.2833e-03 2.5867e+00
6.5185e-02 3.9365e+01
7.8989 1.1118e-01 1.1531e+02 3.0456e-03 1.5423e+00
5.5230e-02 2.7968e+01
9.7334 1.1560e-01 1.1713e+02 2.0221e-03 8.3099e-01
4.5128e-02 1.8546e+01
12.5424 1.2033e-01 1.1864e+02 1.3797e-03 4.4002e-01
3.9597e-02 1.2628e+01
17.2065 1.2543e-01 1.1983e+02 8.6486e-04 2.0105e-01
3.3927e-02 7.8871e+00
22.9405 1.3004e-01 1.2063e+02 8.2606e-04 1.4404e-01
4.3419e-02 7.5707e+00
93.9659 1.4659e-01 1.2133e+02 1.2127e-04 5.1622e-03
2.0696e-02 8.8101e-01

BJH desorption summary

Surface Area = 121.333 m�/g

Pore Volume = 0.147 cc/g
Pore Diameter Dv(d) = 3.746 nm