Quantachrome NovaWin - Data Acquisition and Reduction

for NOVA instruments

�1994-2013, Quantachrome Instruments
version 11.03

Analysis Report
Operator: . Date:2016/11/28 Operator: quantachrome
Date:2018/05/09
Sample ID: ns_a_insitu Filename: ns_a_10insitu.qps
Sample Desc: Comment: [28]
Sample weight: 0.0473 g Sample Volume: 0.0215 cc Sample
Density:2.2 g/cc
Outgas Time: 6.0 hrs OutgasTemp: 100.0 C
Analysis gas: Nitrogen Bath Temp: 273.0 K
Press. Tolerance:0.100/0.100 (ads/des)Equil time: 60/60 sec (ads/des) Equil
timeout: 180/180 sec (ads/des)
Analysis Time: 197.4 min End of run: 2016/11/28 11:07:12 Instrument:
Nova Station A
Cell ID: 19
Data Reduction Parameters
t-Method Calc. method: de Boer

Adsorbate Nitrogen Temperature 77.350K

Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid
Density: 0.806 g/cc

Relative Thickness Volume @

STP
Pressure
(nm) (cc/g)

1.503630e-01 4.0407e-01
92.754
1.710610e-01 4.1796e-01
96.862
2.001490e-01 4.3698e-01
102.963
2.242230e-01 4.5248e-01
108.633
2.481080e-01 4.6777e-01
116.194
2.950840e-01 4.9802e-01
145.015
3.520390e-01 5.3575e-01
167.691
4.037150e-01 5.7177e-01
173.415
4.484110e-01 6.0491e-01
176.835
4.961190e-01 6.4296e-01
180.159
5.459810e-01 6.8653e-01
183.390
5.959210e-01 7.3522e-01
186.466
6.466700e-01 7.9149e-01
189.801
6.973210e-01 8.5681e-01
193.305
 7.519750e-01 9.4159e-01
197.089

V-t method summary

Thickness method: DeBoer
Slope = 20.461
Intercept = 30.670
Correlation coefficient, r = 0.880736

Micropore volume = 0.048 cc/g

Micropore area = 182.969 m�/g
External surface area = 317.272 m�/g