Run 2

A= 0.0046 C Diameter pipa (m)= 0.008 τ (s)=

Q (mL/min)= 240 Luas permukaan (m² )= 5.027E-05 Da=
Q (mL/s)= 4 u (m/s)= 7.958E-02 X PFR=
%T umpan= 97 µ (kg/m.s)= 0.0008737 X LFR=
Absorbansi umpan= 0.013228265733755 densitas (kg/m3)= 996.8 X CSTR=
C umpan = 2.87570994212069 Nre= 726.31634325
D lingkaran (m) = 0.17
V reaktor (m³) = 0.0012074272
C0 (ppm) 166.26074286

t(s) θ %T A C (ppm) C(t).dt E(t) E(θ) E(t).t f

0 0 97 0.0132 2.8757 0 7.714521E-05 0.0176301311 0 1

30 0.131272774223903 93.9 0.0273 5.9423 178.2679 0.0001594101 0.0364302624 0.0047823016 2
60 0.262545548447807 83.3 0.0794 17.2511 517.5326 0.0004627861 0.1057613337 0.0277671674 1
70 0.306303139855774 81.3 0.0899 19.5455 195.4553 0.0005243381 0.1198279123 0.0367036658 2
80 0.350060731263742 75.9 0.1198 26.0344 260.344 0.0006984115 0.1596092209 0.0558729206 2
90 0.39381832267171 84.4 0.0737 16.0125 160.1251 0.0004295595 0.0981679947 0.038660355 2
100 0.437575914079677 86 0.0655 14.2395 142.3947 0.0003819949 0.087297981 0.0381994938 2
110 0.481333505487645 85.8 0.0665 14.4593 144.5929 0.0003878919 0.0886456212 0.0426681076 2
120 0.525091096895613 80.9 0.0921 20.0112 200.1119 0.00053683 0.1226827206 0.0644196043 2
130 0.568848688303581 75.3 0.1232 26.7837 267.837 0.0007185127 0.1642029849 0.0934066526 2
140 0.612606279711548 70.5 0.1518 33.0024 330.0237 0.0008853377 0.2023277896 0.1239472745 2
150 0.656363871119516 71.7 0.1445 31.4089 314.0888 0.00084259 0.1925585919 0.1263885028 2
160 0.700121462527484 70 0.1549 33.6743 336.7434 0.0009033644 0.2064474598 0.1445382975 2
170 0.743879053935452 70.4 0.1524 33.1364 331.3638 0.0008889328 0.2031493812 0.1511185695 2
180 0.787636645343419 74.3 0.1290 28.0459 280.4591 0.0007523734 0.1719412181 0.1354272042 2
 190 0.831394236751387 11 0.9586 208.3929 2083.929 0.0055904501 1.2775954875 1.0621855252 2
200 0.875151828159355 7.8 1.1079 240.8490 2408.49 0.0064611335 1.4765743118 1.2922267084 2
210 0.918909419567323 2.1 1.6778 364.7349 3647.349 0.0097845585 2.2360825177 2.0547572884 2
220 0.96266701097529 1.2 1.9208 417.5693 4175.693 0.011201919 2.5599944152 2.4644221718 2
230 1.00642460238326 0.7 2.1549 468.4569 4684.569 0.0125670561 2.8719716379 2.8904229137 2
240 1.05018219379123 1.2 1.9208 417.5693 4175.693 0.011201919 2.5599944152 2.688460551 2
250 1.09393978519919 2.4 1.6198 352.1280 3521.28 0.0094463584 2.1587930493 2.3615896046 2
260 1.13769737660716 7.6 1.1192 243.3014 2433.014 0.0065269227 1.4916092148 1.6969998906 2
270 1.18145496801513 10.2 0.9914 215.5217 2155.217 0.005781691 1.3213001061 1.5610565746 2
280 1.2252125594231 23.2 0.6345 137.9374 1379.374 0.0037003763 0.8456535588 1.0361053611 2
290 1.26897015083106 35.7 0.4473 97.2460 972.4604 0.00260877 0.5961868428 0.7565433078 2
300 1.31272774223903 54 0.2676 58.1753 581.7527 0.0015606384 0.3566554517 0.4681915059 1
315 1.37836412935098 73 0.1367 29.7124 445.6863 0.00079708 0.1821581105 0.2510802053 2
330 1.44400051646294 72.2 0.1415 30.7528 461.2917 0.0008249893 0.1885362601 0.2722464569 2
345 1.50963690357489 89.7 0.0472 10.2625 153.9377 0.0002753072 0.0629164422 0.094980983 2
360 1.57527329068684 94.4 0.0250 5.4409 81.61306 0.0001459595 0.0333563772 0.05254541 1
390 1.70654606491074 97 0.0132 2.8757 86.2713 7.714521E-05 0.0176301311 0.0300866308 2
420 1.83781883913465 97.1 0.0128 2.7784 83.35285 7.453548E-05 0.0170337258 0.0313049023 2
450 1.96909161335855 97 0.0132 2.8757 86.2713 7.714521E-05 0.0176301311 0.0347153432 1
∫C(t) dt 37276.59 C out(ppm)
m out (mg) 149.1063
550 m out(mg)
m in (mg) 135 tm(s) =
% diff 10.4% tm(min)=
450
tm q = 914.1

350
NPe (θ=1) 103.650203108883

C (ppm)
250

150

50
 250

C (p
150
Run 3
A= 0.0046 C Diameter pipa (m)= 50 0.008
Q (mL/min)= 420 Luas permukaan (m² )= 5.027E-05
Q (mL/s)= 7 u (m/s)= 0 501.393E-01100 150 20
-50
%T umpan= 97 µ (kg/m.s)= 0.0008737
3
Absorbansi umpan= 0.0132283 densitas (kg/m )= 996.8
C umpan = 2.8757099 Nre= 1271.0536007
D lingkaran (m) = 0.17
V reaktor (m³) = 0.0012074272

t(s) θ %T A C (ppm) C(t).dt E(t) E(θ) E(t).t f

0 0 97 0.0132 2.8757 0 0.000115102 0 1

30 0.217098468669989 90.8 0.0419 9.1118 273.3532 0.0003647041 0.010941123 1
45 0.325647703004984 90 0.0458 9.9473 149.2092 0.0003981458 0.0179165621 2
60 0.434196937339978 90.1 0.0453 9.8424 147.6366 0.0003939494 0.0236369633 1
70 0.506563093563308 90 0.0458 9.9473 99.47281 0.0003981458 0.0278702077 2
80 0.578929249786637 98 0.0088 1.9074 19.07375 7.634381E-05 0.0061075051 2
90 0.651295406009967 94.7 0.0237 5.1413 51.41309 0.0002057839 0.0185205554 2
100 0.723661562233297 8.3 1.0809 234.9830 2349.83 0.0094053354 0.9405335375 2
110 0.796027718456627 0.8 2.0969 455.8500 4558.5 0.0182456677 2.0070234456 2
120 0.868393874679956 0.6 2.2218 483.0106 4830.106 0.0193327867 2.3199343998 2
130 0.940760030903286 2.2 1.6576 360.3429 3603.429 0.0144229389 1.874982053 2
140 1.01312618712662 7.9 1.1024 239.6463 2396.463 0.0095919852 1.3428779246 2
150 1.08549234334995 20 0.6990 151.9500 1519.5 0.0060818892 0.9122833844 2
160 1.15785849957328 38.7 0.4123 89.6281 896.2805 0.0035874161 0.5739865747 2
170 1.2302246557966 53 0.2757 59.9400 599.4003 0.0023991353 0.4078530029 2
180 1.30259081201993 60 0.2218 48.2280 482.2799 0.001930354 0.3474637141 2
190 1.37495696824326 63.4 0.1979 43.0241 430.2407 0.0017220642 0.3271921951 2
200 1.44732312446659 67.5 0.1707 37.1079 371.0788 0.0014852648 0.2970529605 2
210 1.51968928068992 70.9 0.1494 32.4682 324.6821 0.0012995594 0.2729074782 2
220 1.59205543691325 71 0.1487 32.3351 323.3514 0.0012942333 0.2847313233 2
230 1.66442159313658 77.8 0.1090 23.7001 237.0009 0.0009486101 0.218180326 2
240 1.73678774935991 79.1 0.1018 22.1355 221.3555 0.0008859884 0.2126372272 2
250 1.80915390558324 80.5 0.0942 20.4792 204.7916 0.0008196904 0.2049226065 2
260 1.88152006180657 85.5 0.0680 14.7900 147.8998 0.0005919776 0.1539141643 2
270 1.9538862180299 89.7 0.0472 10.2625 102.6251 0.0004107632 0.1109060549 1
285 2.0624354523649 91.3 0.0395 8.5933 128.8996 0.0003439523 0.0980264103 2
300 2.17098468669989 92.3 0.0348 7.5648 113.4727 0.0003027875 0.0908362584 2
315 2.27953392103488 94.9 0.0227 4.9421 74.13192 0.0001978116 0.0623106553 2
330 2.38808315536988 95 0.0223 4.8427 72.64042 0.0001938317 0.0639644709 1
360 2.60518162403987 97.1 0.0128 2.7784 83.35285 0.0001112082 0.0400349684 2
390 2.82228009270986 97 0.0132 2.8757 86.2713 0.000115102 0.0448897808 2
420 3.03937856137985 97 0.0132 2.8757 86.2713 0.000115102 0.0483428409 1
C out(ppm) 24984.01 C out(ppm)
m out (mg) 174.8881 m out(mg)
tm(s) =
tm(min)=
301.857 CA0 (mol/L)= 0.5
1.25774 k (L/mol.min)= 0.5
0.55708 n= 2
0.50497
0.80021
closed-open Pe
0.010 103.6502
τ 224.21
V 896.82231

f.C(t) f.E(t).t t-tm (t-tm)².E(t) f.(t-tm)².E(t) E(θ) C(t)

t2C t2C dt
2.87571 0 -228.53177 4.02904513 4.029045134 0 #DIV/0! #DIV/0!
11.8845 0.0095646032098 -198.53177 6.2831258 12.5662516 5348.0363 80220.544 9.2295E-09 0.000
17.2511 0.0277671673609 -168.53177 13.1444952 13.14449523 62103.912 1011779.2 2.1777E-06 0.000
39.0911 0.0734073315462 -158.53177 13.1778343 26.35566856 95773.114 789385.13 1.1034E-05 0.002
52.0688 0.1117458411949 -148.53177 15.4081367 30.81627348 166620.14 1311966.3 5.0628E-05 0.008
32.025 0.0773207100321 -138.53177 8.24369891 16.48739781 129701.34 1481607.4 0.0002104 0.035
28.4789 0.0763989876279 -128.53177 6.31071566 12.62143133 142394.67 1360480.1 0.0007914 0.132
28.9186 0.0853362151909 -118.53177 5.44979626 10.89959252 174957.35 1586760.1 0.0026963 0.448
40.0224 0.1288392086963 -108.53177 6.32339938 12.64679876 288161.15 2315592.5 0.0083185 1.383 3.5
3.5
53.5674 0.1868133051497 -98.531774 6.97568823 13.95137646 452644.54 3704028.5 0.023239 3.864
66.0047 0.2478945489095 -88.531774 6.93916607 13.87833214 646846.37 5497454.6 0.0587891 9.774
62.8178 0.2527770056165 -78.531774 5.1964545 10.392909 706699.78 6767730.8 0.1346731 22.391 3
3
67.3487 0.2890765949608 -68.531774 4.24274473 8.485489466 862063.08 7843814.3 0.2793631 46.447
66.2728 0.3022371390302 -58.531774 3.04545572 6.090911447 957641.34 9098522.1 0.5247616 87.247
56.0918 0.2708544084113 -48.531774 1.77208988 3.544179754 908687.49 9331644.1 0.8926056 148.405
2.5 2.5

2 2
 3 3

2.5 2.5
416.786 2.1243710503993 -38.531774 8.30012803 16.60025606 7522983.5 42158355 1.3748701 228.587
481.698 2.5844534167164 -28.531774 5.2597642 10.5195284 9633960 85784717 1.9176455 318.829
729.47 4.1095145768705 -18.531774 3.36027821 6.720556417 16084811 128593853 2.4220301 402.689
2 2
835.139 4.9288443435338 -8.5317742 0.8154008 1.630801605 20210354 181475823 2.7700991 460.559
936.914 5.7808458273633 1.4682258 0.02709064 0.054181278 24781373 224958632 2.8689016 476.986
835.139 5.3769211020369 11.468226 1.47327865 2.946557302 24051991 244166819 2.6905468 447.332
704.256 4.7231792092575 21.468226 4.35368224 8.707364475 22007999 230299954 2.2849148 379.892 1.5 1.5
486.603 3.3939997811326 31.468226 6.46328016 12.92656032 16447174 192275868 1.7571305 292.142
431.043 3.1221131492992 41.468226 9.94227537 19.88455074 15711532 160793531 1.2236089 203.438
275.875 2.0722107222603 51.468226 9.80221636 19.60443273 10814292 132629119 0.7715885 128.285 1 1
194.492 1.5130866156255 61.468226 9.8568274 19.7136548 8178392 94963418 0.4405888 73.253
58.1753 0.468191505863 71.468226 7.9712839 7.971283902 5235774.3 67070831 0.2278168 37.877
59.4248 0.5021604106815 86.468226 5.95957126 11.91914252 2948215 61379920 0.0703251 11.692 0.5 0.5
61.5056 0.5444929138769 101.46823 8.49392515 16.98785031 3348978.1 47228948 0.0173648 2.887
20.525 0.1899619660542 116.46823 3.73450018 7.469000355 1221495.5 34278552 0.0034298 0.570
5.44087 0.05254541002 131.46823 2.5227481 2.522748104 705136.86 14449743 0.0005419 0.090 0 0
5.75142 0.060173261615 161.46823 2.01132891 4.022657823 437395.48 17137985 6.9225E-06 0.001 0 0 0

5.55686 0.0626098045255 191.46823 2.73247683 5.464953656 490114.75 13912653 3.6205E-08 0.000

2.87571 0.0347153432395 221.46823 3.78383163 3.783831625 582331.26 16086690 7.7521E-11 0.000
37290.3 σ (s²)= 2567.507856 σ (s²)= 2548.2659 #DIV/0!
149.161 σ (min²)= 0.713196627
228.532
600
3.80886

500
Measured
Model 400

C (ppm)
300

200

100
 C (ppm)
300

200

100
τ (s)= 172.4895934443 CA0 (mol/L)=
Da= #REF! k (L/mol.min)=
00 150
X PFR= 200 250
#REF! 300
n= 350 400 450 500 0
0
X LFR= t (s)
#REF!
X CSTR= #REF!

E(t) vs t ; Run 3 ; Pulse

f.C(t) f.E(t).t t-tm (t-tm)².E(t) f.(t-tm)².E(t) 0.025

2.87571 0 -138.18614 2.19791993 2.197919929

0.02
9.11177 0.010941123003 -108.18614 4.26858486 4.268584864
19.8946 0.0358331242457 -93.186143 3.45736187 6.914723732
0.015
9.84244 0.0236369633361 -78.186143 2.40824135 2.408241346

E(t)
19.8946 0.0557404154934 -68.186143 1.85111932 3.702238642
0.01
3.81475 0.0122150101806 -58.186143 0.25847169 0.516943387 f(x) = 9.59474E-16 x⁶ − 1.29086E-12 x⁵ + 6.56146E-10 x⁴ − 1.53882E-07 x³ + 1.58447E-05 x²
− 0.000492897 x
10.2826 0.0370411108829 -48.186143 0.47781065 0.955621299 R²0.005
= 0.679806578485505
469.966 1.8810670749069 -38.186143 13.7146861 27.42937217
911.7 4.0140468912328 -28.186143 14.4954285 28.99085695 0
966.021 4.639868799603 -18.186143 6.39404449 12.78808898 0 50 100 150 200 250 300 350 400 450

720.686 3.749964106004 -8.1861428 0.96652346 1.933046914 t (s)

479.293 2.6857558492469 1.8138572 0.03155838 0.063116756
303.9 1.8245667687422 11.813857 0.84883238 1.697664759
179.256 1.1479731493319 21.813857 1.70705173 3.414103461
119.88 0.8157060058162 31.813857 2.42821645 4.856432898
96.456 0.6949274281746 41.813857 3.37502827 6.750056546
86.0481 0.6543843902804 51.813857 4.62318403 9.246368069
74.2158 0.5941059210174 61.813857 5.67512691 11.35025382
64.9364 0.5458149564838 71.813857 6.70212693 13.40425387
64.6703 0.5694626466727 81.813857 8.66295986 17.32591973
47.4002 0.4363606519985 91.813857 7.9965787 15.9931574
44.2711 0.4252744543179 101.81386 9.18421073 18.36842147
40.9583 0.4098452129399 111.81386 10.2480473 20.49609459
29.58 0.3078283285004 121.81386 8.7841275 17.56825499
10.2625 0.110906054922 131.81386 7.13696604 7.13696604
17.1866 0.1960528205641 146.81386 7.4136544 14.8273088
15.1297 0.181672516769 161.81386 7.92810518 15.85621035
9.88426 0.1246213105835 176.81386 6.18421189 12.36842378
4.84269 0.0639644708524 191.81386 7.13156474 7.131564737
5.55686 0.080069936887 221.81386 5.47159996 10.94319992
5.75142 0.089779561615 251.81386 7.29864312 14.59728624
2.87571 0.0483428408696 281.81386 9.14129167 9.141291668
24953 σ (s²)= 2388.015258
C vs t ; Run 3 ; Pulse
174.671 σ (min²)= 0.663337572
138.186 600.0000

2.3031 500.0000

400.0000

C (ppm)
300.0000

200.0000 C vs t ; Pulse
600.0000
100.0000

500.0000 0.0000
0 50 100 150 200 250 300 350 400 450
t (s)
400.0000
C (ppm)

300.0000

200.0000

100.0000
 400.0000

C (ppm)
300.0000

200.0000

100.0000

0.0000
0 50 100 150 200 250 300 350 400 450 500

t (s)
 E(t) vs t ; Run 2 ; Pulse
0.014

0.012

Chart Title
0.01
Chart Title
3.5 3.5 0.008
f(x) = − 5.50623E-16 x⁶ + 7.63225E-13 x⁵ − 3.92003E-10 x⁴ + 9.05122E-08 x³
E(t)

− 8.99964E-06 x² + 0.000305644 x
0.006 R² = 0.843835063653085

3 3 0.004

0.002

0
2.5 2.5 0 50 100 150 200 250 300 350 400 450 500
t (s)

2 2
 3 3 0.004

0.002

0
2.5 2.5 0 50 100 150 200 250 300 350 400 450 500
t (s)

2 2

1.5 1.5

1 1

0.5 0.5

0 0
0 0 0.2 0.2 0.4 0.4 0.6 0.6 0.8 0.8 1 1 1.21.2 1.41.4 1.6
1.6 1.8
1.8 22

C vs t ; Run 2 ; Pulse
600

500

400
C (ppm)

300

200

100
 C (ppm)
300

200

100

0
0 50 100 150 200 250 300 350 400 450 500

t (s)

³ + 1.58447E-05 x²

400 450
0 400 450

Run 3
Run 2
 Run 3
Run 2

0 450 500
 A 0.0046 C
Q 6.83 mL/s
Q 409.80 mL/min
%T umpan 94 %
Absorbansi umpan 0.0269
C umpan 5.8418 ppm
Volume reaktor 750 mL

t (s) θ %T A C (ppm) Luas Trapesium

0 0 94 0.0269 5.8418 0
20 0.17737404854 86.4 0.0635 13.8014 138.0136
30 0.26606107281 94.9 0.0227 4.9421 161.7585
40 0.35474809708 95.6 0.0195 4.2483 45.9521
50 0.44343512135 96.2 0.0168 3.6576 39.5294
55 0.48777863349 95.1 0.0218 4.7434 21.0024
60 0.53212214563 93.2 0.0306 6.6487 28.4802
65 0.57646565776 90 0.0458 9.9473 41.4900
70 0.6208091699 94 0.0269 5.8418 39.4726
75 0.66515268203 93.9 0.0273 5.9423 29.4601
80 0.70949619417 93.4 0.0297 6.4463 30.9715
85 0.7538397063 92.4 0.0343 7.4626 34.7724
90 0.79818321844 73.1 0.1361 29.5832 92.6145
95 0.84252673057 0.1 3.0000 652.1739 1704.3927
100 0.88687024271 0.1 3.0000 652.1739 3260.8696
105 0.93121375484 0.1 3.0000 652.1739 3260.8696
110 0.97555726698 0.1 3.0000 652.1739 3260.8696
115 1.01990077912 0.1 3.0000 652.1739 3260.8696
120 1.06424429125 0.3 2.5229 548.4519 3001.5645
125 1.10858780339 2 1.6990 369.3413 2294.4830
130 1.15293131552 2.7 1.5686 341.0079 1775.8730
135 1.19727482766 13.5 0.8697 189.0579 1325.1644
140 1.24161833979 36.9 0.4330 94.1247 707.9564
145 1.28596185193 42.4 0.3726 81.0074 437.8303
150 1.33030536406 54.3 0.2652 57.6522 346.6491
155 1.3746488762 71.3 0.1469 31.9371 223.9732
160 1.41899238833 79.9 0.0975 21.1855 132.8064
165 1.46333590047 77 0.1135 24.6759 114.6535
170 1.5076794126 83.8 0.0768 16.6861 103.4050
 175 1.55202292474 84.5 0.0731 15.9007 81.4670
180 1.59636643688 92.8 0.0325 7.0548 57.3888
185 1.64070994901 91.3 0.0395 8.5933 39.1202
190 1.68505346115 95.5 0.0200 4.3471 32.3510
195 1.72939697328 88.4 0.0535 11.6408 39.9698
200 1.77374048542 97.1 0.0128 2.7784 36.0481
205 1.81808399755 98.1 0.008331 1.81108535 11.4738
210 1.86242750969 94.9 0.0227338 4.94212773 16.8830
215 1.90677102182 98.5 0.0065638 1.42690641 15.9226
Luas Kurva 26246.3713
179.26

Estimation of PeL

(a) From the mean

PeL 97.839

(b) From the variance

(1) Gauss
PeL 62.4112726044
D/uL 0.016

(2) Open-open
PeL 65.9938183999 62.27
D/uL 0.015
σ2θ (calculated) 0.032 0.032
2
σ (exp)
θ 0.0320 0.0320
Error 0.0001 0.0000
τ 109.2470

(3) Closed-closed
PeL 61.4130166852
D/uL 0.016
σ2θ (calculated) 0.032
2
σ (exp)
θ 0.0320
Error 0.0000

(4) Closed-open
PeL 63.8039125238
D/uL 0.016
σ2θ (calculated) 0.032
σ2θ (exp) 0.0320
Error 0.0000
Gauss
D/uL 0.016
t θ
1.12756066428134
5.63780332140671
11.2756066428134
16.9134099642201
22.5512132856269
28.1890166070336
33.8268199284403
39.464623249847
45.1024265712537
50.7402298926604
56.3780332140671
62.0158365354739
67.6536398568806
73.2914431782873
78.929246499694
84.5670498211007
90.2048531425074
95.8426564639141
101.480459785321
107.118263106728
112.756066428134
118.393869749541
124.031673070948
129.669476392354
135.307279713761
140.945083035168
146.582886356575
152.220689677981
157.858492999388
163.496296320795
169.134099642201
174.771902963608
180.409706285015
186.047509606422
191.685312927828
197.323116249235
202.960919570642
closed-open
0.015
C(θ) C(t) C(θ) C(t)
0.01 5.08927E-07 0.0001221 0 0
0.05 1.70801E-06 0.0004099 1.0678E-129 2.562821037E-127
0.1 7.23253E-06 0.0017358 2.09955E-58 5.0389125067E-56
0.15 2.83276E-05 0.0067986 7.0441E-35 1.6905839318E-32
0.2 0.00010262 0.0246297 2.70113E-23 6.4827160843E-21
0.25 0.00034388 0.0825307 1.73171E-16 4.1560944135E-14
0.3 0.00106581 0.2557944 4.53949E-12 1.0894765251E-09
0.35 0.00305545 0.7333069 5.13738E-09 1.2329704674E-06
0.4 0.00810192 1.9444618 8.15601E-07 0.00019574421009
0.45 0.01987104 4.7690507 3.49581E-05 0.00838995202994
0.5 0.04507878 10.818907 0.00059917 0.14380170721611
0.55 0.0945894 22.701456 0.00527296 1.26551142190402
0.6 0.18358269 44.059846 0.02814686 6.75524638391207
0.65 0.3295641 79.095385 0.10227851 24.5468417962031
0.7 0.54722633 131.33432 0.27473138 65.9355309750612
0.75 0.84045211 201.70851 0.57949236 139.078166182465
0.8 1.19392728 286.54255 1.00435514 241.045233891629
0.85 1.56877871 376.50689 1.48074393 355.378543166017
0.9 1.90662116 457.58908 1.90780288 457.872690050462
0.95 2.14331519 514.39565 2.19427442 526.625859602625
1 2.22857158 534.85718 2.2916416 549.993983113615
1.05 2.14331519 514.39565 2.20336642 528.807940030715
1.1 1.90662116 457.58908 1.97246191 473.390858916322
1.15 1.56877871 376.50689 1.65942734 398.262560491005
1.2 1.19392728 286.54255 1.3222303 317.335270844729
1.25 0.84045211 201.70851 1.00435514 241.045233891629
1.3 0.54722633 131.33432 0.73129943 175.511862865859
1.35 0.3295641 79.095385 0.51282861 123.078867231185
1.4 0.18358269 44.059846 0.34775076 83.4601831650585
1.45 0.0945894 22.701456 0.22881851 54.9164432627995
1.5 0.04507878 10.818907 0.14653748 35.168996211876
1.55 0.01987104 4.7690507 0.09157552 21.9781252154153
1.6 0.00810192 1.9444618 0.05597311 13.4335465636238
1.65 0.00305545 0.7333069 0.03352929 8.0470298003402
1.7 0.00106581 0.2557944 0.01971908 4.73257960209746
1.75 0.00034388 0.0825307 0.01140383 2.7369184809523
1.8 0.00010262 0.0246297 0.00649418 1.55860337413468
208.598722892048 1.85 2.83276E-05 0.0067986 0.00364628 0.87510794092075
214.236526213455 1.9 7.23253E-06 0.0017358 0.00202076 0.48498158419065
219.874329534862 1.95 1.70801E-06 0.0004099 0.0011065 0.26555962683608
225.512132856269 2 3.73086E-07 8.954E-05 0.00059917 0.14380170721611
 Cao 0.8 mol/L
k 0.7 mol/min
n 0.8
τ 1.8 min 109.81 sec
Ca 0.3507060334 mol/L
m 180
m/q 26354.31918
C0 240

E(t) E(t) E(θ) E(θ) C(t) E(t).t (s) E(t).t (s) Luas Trapesium

2.23E-04 2.22E-04 0.02 0.02 6.00 0 0.00

5.26E-04 5.24E-04 0.06 0.06 14.17 1.05E-02 0.01 1.05E-01
1.88E-04 1.88E-04 0.02 0.02 5.07 5.65E-03 0.01 8.05E-02
1.62E-04 1.61E-04 0.02 0.02 4.36 6.47E-03 0.01 6.04E-02
1.39E-04 1.39E-04 0.02 0.02 3.76 6.97E-03 0.01 6.69E-02
1.81E-04 1.80E-04 0.02 0.02 4.87 9.94E-03 0.01 4.21E-02
2.53E-04 2.52E-04 0.03 0.03 6.83 1.52E-02 0.02 6.26E-02
3.79E-04 3.77E-04 0.04 0.04 10.21 2.46E-02 0.02 9.92E-02
2.23E-04 2.22E-04 0.02 0.02 6.00 1.56E-02 0.02 1.00E-01
2.26E-04 2.25E-04 0.03 0.03 6.10 1.70E-02 0.02 8.11E-02
2.46E-04 2.45E-04 0.03 0.03 6.62 1.96E-02 0.02 9.12E-02
2.84E-04 2.83E-04 0.03 0.03 7.66 2.42E-02 0.02 1.09E-01
1.13E-03 1.12E-03 0.13 0.13 30.38 1.01E-01 0.10 3.13E-01
2.48E-02 2.47E-02 2.79 2.79 669.67 2.36E+00 2.35 6.13E+00
2.48E-02 2.47E-02 2.79 2.79 669.67 2.48E+00 2.47 1.21E+01
2.48E-02 2.47E-02 2.79 2.79 669.67 2.61E+00 2.60 1.27E+01
2.48E-02 2.47E-02 2.79 2.79 669.67 2.73E+00 2.72 1.33E+01
2.48E-02 2.47E-02 2.79 2.79 669.67 2.86E+00 2.85 1.39E+01
2.09E-02 2.08E-02 2.35 2.35 563.17 2.51E+00 2.50 1.34E+01
1.41E-02 1.40E-02 1.58 1.58 379.25 1.76E+00 1.75 1.06E+01
1.30E-02 1.29E-02 1.46 1.46 350.16 1.69E+00 1.68 8.58E+00
7.20E-03 7.17E-03 0.81 0.81 194.13 9.72E-01 0.97 6.63E+00
3.59E-03 3.57E-03 0.40 0.40 96.65 5.02E-01 0.50 3.67E+00
3.09E-03 3.07E-03 0.35 0.35 83.18 4.48E-01 0.45 2.36E+00
2.20E-03 2.19E-03 0.25 0.25 59.20 3.29E-01 0.33 1.93E+00
1.22E-03 1.21E-03 0.14 0.14 32.79 1.89E-01 0.19 1.29E+00
8.07E-04 8.04E-04 0.09 0.09 21.75 1.29E-01 0.13 7.91E-01
9.40E-04 9.36E-04 0.11 0.11 25.34 1.55E-01 0.15 7.08E-01
6.36E-04 6.33E-04 0.07 0.07 17.13 1.08E-01 0.11 6.55E-01
6.06E-04 6.03E-04 0.07 0.07 16.33 1.06E-01 0.11 5.33E-01
2.69E-04 2.68E-04 0.03 0.03 7.24 4.84E-02 0.05 3.84E-01
3.27E-04 3.26E-04 0.04 0.04 8.82 6.06E-02 0.06 2.71E-01
1.66E-04 1.65E-04 0.02 0.02 4.46 3.15E-02 0.03 2.29E-01
4.44E-04 4.42E-04 0.05 0.05 11.95 8.65E-02 0.09 2.94E-01
1.06E-04 1.05E-04 0.01 0.01 2.85 2.12E-02 0.02 2.68E-01
6.90E-05 6.87E-05 0.01 0.01 1.86 0.01414567 0.01 8.79E-02
1.88E-04 1.88E-04 0.02 0.02 5.07 0.03954249 0.04 1.34E-01
5.44E-05 5.41E-05 0.01 0.01 1.47 0.01168866 0.01 1.28E-01
0 112
mg

3.00

2.50

2.00
 2.50

2.00
closed-open
0.100

1.50

E(θ)
C(θ)
3.44659E-107
0
0

1.00

0.50

0.00
0 0.5

700

600

500

400

300

200

100
200

100

0
0 50
 RUN 5 PULSE

Luas Trapesium t-tm (t-tm)².E(t) (s²) Luas Trapesium t2C

0 -112.7561 2.8298 0 0
0.1052 -92.7561 4.5242 45.2415 5520.54413227014
0.0847 -82.7561 1.2896 61.7905 4447.91495987752
0.0606 -72.7561 0.8568 10.7319 6797.25486048694
0.0672 -62.7561 0.5488 7.0282 9143.98258814511
0.0423 -57.7561 0.6029 2.8792 14348.6817965919
0.1108 -52.7561 0.7050 3.2697 23935.3729403624
0.0996 -47.7561 0.8644 3.9235 42027.2603519244
0.1005 -42.7561 0.4069 3.1781 28624.6776872775
0.0814 -37.7561 0.3227 1.8241 33425.2268485056
0.0916 -32.7561 0.2635 1.4657 41256.5200276962
0.1095 -27.7561 0.2190 1.2064 53917.3930292889
0.3140 -22.7561 0.5837 2.0068 239623.749269854
6.1550 -17.7561 7.8341 21.0444 5885869.56521739
12.1135 -12.7561 4.0432 29.6932 6521739.13043478
12.7347 -7.7561 1.4948 13.8450 7190217.39130435
13.3559 -2.7561 0.1887 4.2088 7891304.34782609
13.9771 2.2439 0.1251 0.7847 8625000
13.4127 7.2439 1.0965 3.0541 7897707.37652975
10.6664 12.2439 2.1096 8.0153 5770957.89516311
8.6201 17.2439 3.8634 14.9325 5763033.12732894
6.6537 22.2439 3.5641 18.5687 3445579.7976475
3.6862 27.2439 2.6618 15.5647 1844844.17897444
2.3740 32.2439 3.2089 14.6766 1703181.05763865
1.9425 37.2439 3.0469 15.6394 1297174.74657629
1.2952 42.2439 2.1715 13.0459 767287.835936724
0.7944 47.2439 1.8016 9.9327 542348.358600396
0.7107 52.2439 2.5661 10.9193 671802.175473735
0.6580 57.2439 2.0833 11.6234 482227.795996741
 0.5352 62.2439 2.3472 11.0760 486959.410525146
0.3860 67.2439 1.2154 8.9064 228575.124023667
0.2724 72.2439 1.7088 7.3105 294106.008454048
0.2301 77.2439 0.9882 6.7426 156930.062136252
0.2949 82.2439 3.0000 9.9706 442641.874538673
0.2691 87.2439 0.8058 9.5144 111137.13123474
0.0883 92.2439 0.5871 3.4822 76110.8619255792
0.1342 97.2439 1.7806 5.9194 217947.833033998
0.1281 102.2439 0.5683 5.8724 65958.7489669343
112.7561 s 418.8889
0.1164
0.3411
0.0329
0.5 1 1.5 2
θ
50 100 150 200
 Skala rotameter 120 KONVERSI
C tracer 60,000 ppm X segregation
X maximum mixedness
τ percobaan 112.7561 s X PFR
Da 0.8419 X LFR
X CSTR

Segregation Method Maximum Mixedness

t2C dt
X(t) X(t).E(t) Luas Trapesium F(t) 1-F(t) Xi-1
0 0 0 0 1 0.3886
55205 0.2081 1.09E-04 1.09E-03 0.0053 0.9947 0.3516
49842 0.2953 5.56E-05 8.25E-04 0.0088 0.9912 0.3297
56226 0.3729 6.04E-05 5.80E-04 0.0106 0.9894 0.3052
79706 0.4420 6.16E-05 6.10E-04 0.0121 0.9879 0.2774
58732 0.4736 8.56E-05 3.68E-04 0.0129 0.9871 0.2627
95710 0.5034 1.28E-04 5.33E-04 0.0140 0.9860 0.2471
164907 0.5316 2.01E-04 8.22E-04 0.0156 0.9844 0.2305
176630 0.5581 1.24E-04 8.14E-04 0.0171 0.9829 0.2125
155125 0.5831 1.32E-04 6.41E-04 0.0182 0.9818 0.1931
186704 0.6068 1.49E-04 7.03E-04 0.0194 0.9806 0.1722
237935 0.6290 1.79E-04 8.20E-04 0.0207 0.9793 0.1494
733853 0.6501 7.33E-04 2.28E-03 0.0242 0.9758 0.1251
15313733 0.6699 1.66E-02 4.34E-02 0.0892 0.9108 0.1149
31019022 0.6886 1.71E-02 8.44E-02 0.2134 0.7866 0.1047
34279891 0.7062 1.75E-02 8.66E-02 0.3376 0.6624 0.0948
37703804 0.7229 1.80E-02 8.88E-02 0.4619 0.5381 0.0862
41290761 0.7386 1.84E-02 9.08E-02 0.5861 0.4139 0.0818
41306768 0.7534 1.57E-02 8.52E-02 0.7005 0.2995 0.0812
34171663 0.7674 1.08E-02 6.64E-02 0.7879 0.2121 0.0777
28834978 0.7806 1.01E-02 5.24E-02 0.8556 0.1444 0.0900
23021532 0.7930 5.71E-03 3.96E-02 0.9060 0.0940 0.1021
13226060 0.8047 2.89E-03 2.15E-02 0.9330 0.0670 0.1026
8870063 0.8158 2.52E-03 1.35E-02 0.9497 0.0503 0.1101
7500890 0.8262 1.81E-03 1.08E-02 0.9629 0.0371 0.1202
5161156 0.8361 1.02E-03 7.08E-03 0.9714 0.0286 0.1205
3274090 0.8454 6.82E-04 4.25E-03 0.9765 0.0235 0.1142
3035376 0.8541 8.03E-04 3.71E-03 0.9809 0.0191 0.1174
2885075 0.8624 5.48E-04 3.38E-03 0.9848 0.0152 0.1158
2422968 0.8702 5.27E-04 2.69E-03 0.9879 0.0121 0.1206
1788836 0.8775 2.36E-04 1.91E-03 0.9901 0.0099 0.1090
1306703 0.8845 2.90E-04 1.31E-03 0.9916 0.0084 0.1018
1127590 0.8910 1.48E-04 1.09E-03 0.9928 0.0072 0.0824
1498930 0.8972 3.98E-04 1.36E-03 0.9943 0.0057 0.0893
1384448 0.9030 9.56E-05 1.23E-03 0.9957 0.0043 0.0673
468120 0.9085 6.27E-05 3.96E-04 0.9962 0.0038 0.0373
735147 0.9137 1.72E-04 5.87E-04 0.9968 0.0032 0
709766 0.9186 4.99E-05 5.55E-04 0.9974 0.0026 -
407.4242 = σ² (s²) 0.7231 0.3886
= σ² (min²)
= σ (min)
0.0320 = σ²/tm² = σ2θ
31.2 =N
2 2.5
200 250
 KONVERSI
X segregation 0.7231
X maximum mixedness 0.3886
X PFR 0.4571
Grafik
X LFR 0.4108 800 3.00E-02
X CSTR 0.5616 800
2.50E-02
closed-open Pe
0.009 114.4856257272 700
τ 110.82 2.00E-02
700
V 756.9012905 mL

600 1.50E-02

E(t)
600

C(t), ppm
E(θ) C(t)
0 1.00E-02
1.169881423E-08 0.003 2.8077154E-06 2.8077154E-05
500
6.082523529E-07 0.000 0.00014598056 0.0007439414
2.015999072E-05 0.000 0.00483839777 0.02492189169 5.00E-03 500
0.0004259527591 0.000 0.10222866218 0.53533529977
0.0016537551367 0.000 400
0.39690123281 1.24782473748
0.00E+00
0.0057371621026 0.001 1.37691890462 4.43455034358 0 50
0.0177843984592 0.001 4.2682556302 14.1129363371
400
0.049260337579 0.001 11.8224810189 40.2268416229
0.1219190953864 0.009 300
29.2605828927 102.707659779
0.269626282531 0.059 64.7103078074 234.92722675
300
0.5328056978818 0.251 127.873367492 481.459188248
0.9407877235359 0.663 225.789053649 884.156052851
1.4843303481647 1.706 200
356.23928356 1455.07084302
2.0925971849474 0.487 502.223324387 2146.15651987 200
2.6360694673834 0.024 632.656672172 2837.1999914
2.9671821614471 0.031 712.123718747 3361.9509773
2.9843359614722 0.038
100
716.240630753 3570.91087375
2.6820530233154 0.113 643.692725596 3399.83339087 100
2.1537889825878 0.329 516.909355821 2901.50520354
1.5454504559879 0.007 370.908109437 2219.54366315
0
0.990884802034 0.033 237.812352488 1521.80115481 0 50
0.5676849648146 0.027 136.244391555 935.141860109 0
0.2906081308311 0.003 69.7459513995 514.975857387 0
0.1329303886642 0.013 31.9032932794 254.123111697
0.0543321551708 0.007 13.039717241 112.357526301
0.0198429269936 0.005 4.76230247845 44.5050492986
0.0064754608357 0.010 1.55411060056 15.7910326975
0.0018882164287 0.005 0.45317194289 5.01820635864
0.0004919817662 0.005 0.11807562388 1.42811891693
0.0001145413736 0.001 0.02748992966 0.36391388384
2.382823699E-05 0.001 0.00571877688 0.08302176634
4.429325322E-06 0.000 0.00106303808 0.01695453739
7.356976893E-07 0.002 0.00017656745 0.00309901381
1.09188613E-07 0.000 2.6205267E-05 0.00050693178
1.448009631E-08 0.000 3.4752231E-06 7.4201226E-05
1.715859393E-09 0.000 4.1180625E-07 9.7175734E-06
1.816804039E-10 0.000 4.3603297E-08 1.1385239E-06
3.835586277815 m tracer 184.830825475

1.2

0.8

0.6
F(t)

0.4

0.2

0
0 50
 Grafik E(t) vs t Run 6 Pulse
3.00E-02
800
2.50E-02

2.00E-02
700

1.50E-02
E(t)

600
1.00E-02

5.00E-03 500

0.00E+00
0 50 100 150 200 250
400
t (s)

300
Grafil C vs t Run 6 Pulse
700.0000
200 600.0000

500.0000

400.0000
C (ppm)

100 300.0000

200.0000

50 100 100.0000 150 200 250

0 0.0000
0 Time (s)50
0 50 100 100 150 200 150 250
t (s)
 Grafik F(t) vs t Run 6 Pulse

50 100 150 200 250

t (s)
 3.50

3.00

2.50

2.00
250
E(θ)

150 250 200 250

1.50

1.00

0.50
 1.00

0.50

0.00
0 0.5 1

250
1 1.5 2 2.5
θ
2.5