IR6082A Integra Plus 2 Upgrade

Nicolet
INSTRUMENTS OF DISCOVERY
Field Service Technical Bulletin
Title: PLUS 2 Upgrade for Automatic and TBN# IR6082A

Semi-Automatic Systems
Date: May 13, 1998
Products affected: Liquid Analysis Systems
Completion time: None
Special tools and materials: N/A
CCN No. Rev 33545 Release 34105 A

Changed by Paul Karges Paul Karges
Date 12-15-97 4-27-98
Information: Replace TBN IR6082 with IR6082A
The former PLUS, originally manufactured by Spectra Tech, is no longer available. As

parts availability diminishes, PLUS defective parts must require an upgrade to the PLUS
2. Customers may also wish to upgrade to take advantage of the improved reliability and
ease of operation of the new PLUS 2(see revised Oil Analyses System and Omnic Integra
Specification Sheet for details). This bulletin describes the procedures for upgrading the
Automatic and Semi-Automatic configurations as well as upgrading from the PLUS Semi-
Automatic to the PLUS 2 Automatic configurations. For new installations refer to
Technical Bulletin IR6079.
REQUIRED PARTS:
PLUS SEMI-AUTOMATIC TO PLUS 2 SEMI-AUTOMATIC CONFIGURATION

Part Number 854-006200 includes all of the following:
Plus 2 Liquid Uptake Module .............................................. 470-083000

Plus 2 Controller Power Supply........................................... 113-727000
Plus 2 Control/Valve Module .............................................. 470-083100
Plus 2 Liquid Handling Tubing Kit....................................... 470-319800
Optional (not included)
Masterflex EZ-Loader Pump Head ...................................... 222-152800
PLUS AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

CONFIGURATION
This document contains confidential or proprietary information of Nicolet Instrument Corporation.

Neither this document nor the information therein is to be reproduced, distributed, used or disclosed,
either in whole or in part, except as specifically authorized by Nicolet Instrument Corporation.
Page 1 of 7

PLUS SEMI- AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

CONFIGURATION

CETAC Autosampler .......................................................... 222-176400
Disposable test tubes, 250, 17x100mm ................................ 470-085500

PROCEDURE:
PLUS SEMI-AUTOMATIC TO PLUS 2 SEMI- AUTOMATIC CONFIGURATION
Refer to figure 1 showing the Plus 2 components, figure 2 showing the positioning of the
Semi-Automatic configuration, figure 3 showing the Semi-Automatic plumbing diagram,
and figure 4 showing the cable connections.
After powering down the entire system, remove the following cables:
1) 9-pin interface cable from the Plus Pump to the Plus Valve Module/Power Supply.
2) 25-pin D connector on the rear panel of the Valve Module/Power Supply.
3) 9-pin D connector from the PLUS Controller rear panel to COM1 of the PC
workstation.
Disconnect he following fittings and Teflon tubing. Theses parts can be reused provided
they are in good condition:
1) Pull the 28-inch Teflon tubing out of the stainless steel tube of the PLUS unit.
2) Remove the 3 nuts and ferrules connecting the valve to the rest of the system.
Remove the Valve Module/Power Supply and the Digital Controller from the system.
Referring to figure 2, position the new Liquid Uptake System and Control/Valve Module
into the system. Referring to figure 3 restore the plumbing connections as follows:
1) Feed the beveled end of the 28-inch Teflon tube into the stainless steel tube of the
Liquid Uptake System. The other end of this tube should be connected to the flow cell
inlet port.
2) Connect the 6-inch Teflon line from the left side of the Masterflex pump head to the
top of the valve.
Page 2 of 7
3) Connect the 60-inch Teflon line from the solvent to the right port of the valve.
4) Connect the 60-inch Teflon line from the waste container to the left port of the valve.
5) Inspect the remainder of the tubing in the system and replace those pieces or fittings
that appear worn.
6) If the new Masterflex EZ loader pump head is to be installed, do so at this time
following the instructions in Technical Bulletin IR6079.
Referring to figure 4 connect the cables as follows:

1) The Control/Valve Module uses an external digital power supply. Plug the AC power
cord into this external power supply (113-727000). Then plug the external supply
output cable into the power connector on the rear left of the valve module.
2) Connect one end of the 9-pin interface cable (085-795700) into the Control/Valve
module connector labeled Pump. Connect the other end of the cable into the
Masterflex pump connector labeled Interface.
3) Connect one end of the Liquid Uptake Module(085-030800) 5-pin control cable, to
the 5-pin connector on the rear of the LUM. Connect the other end to the uptake
connector on the right rear of the Valve Module.
4) Connect one end of the 9-pin communication cable (400-030800) to the computer
connector on the rear right of the valve module. Connect the other end to COMM 1 of
the computer workstation.
This completes the upgrade of the PLUS 2 Semi-Automatic configuration. The system
should now be turned on, verified, and a flow cell calibration performed as described in
the Liquid Analysis System Installation and Service Manual.
PLUS AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

CONFIGURATION
Automatic configuration, figure 6 showing the Automatic configuration plumbing
diagram, and figure 4 showing the cable connections.
workstation.
Remove the 3 nuts and ferrules connecting the valve to the rest of the system. The nuts,
ferrules and tubing can be reused providing they are in good condition.
Referring to figure 5, position the new Control/Valve Module into the system. Referring
to figure 6 restore the plumbing connections as follows:
top of the valve.
Page 3 of 7
that appear worn.

This completes the upgrade of the PLUS 2 Automatic configuration. The system should
now be turned on, verified, and a flow cell calibration performed as described in the Liquid
Analysis System Installation and Service Manual.
PLUS SEMI- AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

CONFIGURATION
Automatic configuration, figure 6 showing the Automatic configuration plumbing
diagram, and figure 4 showing the cable connections.
workstation.
Disconnect he following fittings and Teflon tubing:

1) Pull the 28-inch Teflon tubing out of the stainless steel tube of the PLUS unit.
Disconnect the other end of the tubing from the inlet port of the flow cell. The tubing
should be discarded but the ferrules, nuts, and union can be reused if they are in good
condition.
2) Remove the 3 nuts and ferrules connecting the valve to the rest of the system. If the
tubing, nuts, and ferrules are in good condition, save for reuse.
Referring to figure 5, position the new Control/Valve Module and Autosampler into
position. Referring to figure 6 restore the plumbing connections as follows:
1) Connect a new 42 x 1/8-inch Teflon tube to the sample cell inlet line following the
recommendations in the service manual for proper tightening of this fitting. The other
end of this tube is connected to the sample probe of the Autosampler using the same
Page 4 of 7
style of nuts, ferrules and union. Do not install the sample probe in the Autosampler
yet.
top of the valve.
that appear worn.

4) Refer to the CETAC technical bulletin TBN IR6086 for cabling and setup of the
CETAC Autosampler. For the SMS autosampler, refer to the Liquid Analysis System
Installation and Service Manual.
This completes the upgrade. The system should now be turned on, verified, and a flow cell
calibration performed as described in the Liquid Analysis System Installation and Service
Manual.
FIGURE 1
Page 5 of 7
FIGURE 2
FIGURE 3
Page 6 of 7
FIGURE 4
FIGURE 5
FIGURE 6
Page 7 of 7

IR6082A Integra Plus 2 Upgrade

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IR6082A Integra Plus 2 Upgrade

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Nicolet

Title: PLUS 2 Upgrade for Automatic and TBN# IR6082A

CCN No. Rev 33545 Release 34105 A

Information: Replace TBN IR6082 with IR6082A

The former PLUS, originally manufactured by Spectra Tech, is no longer available. As

PLUS SEMI-AUTOMATIC TO PLUS 2 SEMI-AUTOMATIC CONFIGURATION

Plus 2 Liquid Uptake Module .............................................. 470-083000

Optional (not included)

Masterflex EZ-Loader Pump Head ...................................... 222-152800

PLUS AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

Plus 2 Controller Power Supply........................................... 113-727000

This document contains confidential or proprietary information of Nicolet Instrument Corporation.

Plus 2 Control/Valve Module .............................................. 470-083100

Optional (not included)

Masterflex EZ-Loader Pump Head ...................................... 222-152800

PLUS SEMI- AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

Plus 2 Controller Power Supply........................................... 113-727000

Optional (not included)

Disposable test tubes, 250, 17x100mm ................................ 470-085500

PLUS SEMI-AUTOMATIC TO PLUS 2 SEMI- AUTOMATIC CONFIGURATION

Referring to figure 4 connect the cables as follows:

PLUS AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

Referring to figure 4 connect the cables as follows:

PLUS SEMI- AUTOMATIC CONFIGURATION TO PLUS 2 AUTOMATIC

Disconnect he following fittings and Teflon tubing:

Referring to figure 4 connect the cables as follows:

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