You are on page 1of 20

Metals and Materials International

https://doi.org/10.1007/s12540-019-00472-3

Friction Stir Welding of Thick AA2519 Alloy: Defect Elimination,


Mechanical and Micro‑Structural Characterization
Mohammed Ubaid1 · Dhruv Bajaj1   · A. K. Mukhopadhyay2 · Arshad Noor Siddiquee1

Received: 1 August 2019 / Accepted: 16 September 2019


© The Korean Institute of Metals and Materials 2019

Abstract
Friction stir welding (FSW) of thick aluminium sections will pave way for remarkable new defence applications, provided
the accompanying challenges are successfully addressed. These challenges include elimination of tunnel defects, loss of
strength in heat-treatable aluminium alloys, tool design and excessive process forces. Accounts of defect elimination, detailed
micro-structural and mechanical characterization for thick section FSW are scarce in the published literature. Further, special
strategies such as bobbin tool, pre-drilled hole for plunging and inverted double pass are generally deployed to overcome
these challenges. This makes the process less productive and complex. In the present work, armor grade aluminum alloy
AA2519-T87 plates having a thickness of 15.4 mm have been successfully joined with a joint efficiency of greater than 75%
without supplementary strategies. The disparity in the effects of tool rotational speed and welding speed in the formation of
a sound weld has been addressed in detail to enhance the understanding of FSW of thick sections. Micro-hardness measure-
ments have been carried out throughout the transverse cross-section of the welds and correlated with different zones and
their corresponding microstructures. Scanning electron microscopy and X-ray energy dispersive spectroscopy have been
used to characterize the coarse phase particles present in the weld zones.

Keywords  Friction stir welding (FSW) · Aluminium alloy AA2519 · Thick plates · Defect elimination · Joint efficiency ·
Mechanical properties

1 Introduction alloys is unfavorable [1, 4]. A solid-state joining process


such as friction stir welding (FSW) has proved to be the key
Wrought aluminum alloys with copper as major alloying enabler towards utilizing such an aluminum alloy for the
element are of prime importance to several strategic and targeted applications [5–12].
technology intensive sectors. Classified under the 2xxx FSW studies conducted on AA2519 plates having a thick-
series, these alloys find usage in cryogenic, aerospace and ness of less than 8 mm have demonstrated the role of tool
a variety of critical defence applications [1]. AA2519 is a design in the material flow and heat balance in the welded
relatively new armor grade aluminum alloy currently being plates. Tapered as well as straight cylindrical pin profiles
utilized to develop lightweight combat structures. Charac- have exhibited defect free welds [13]. Moreover, underwater
teristics like high-strength to weight ratio, high toughness FSW (UFSW) has yielded a better joint efficiency owing to
as well as high resistance to stress corrosion cracking make suppression of precipitate dissolution and coarsening [14].
AA2519 alloy suitable for ballistic applications [2, 3]. Being Studies aimed at optimizing traverse speed have also been
an age-hardenable alloy, this alloy derives its strength from conducted. In case of UFSW, lower traverse speeds resulted
strengthening precipitates and hence fusion welding of such in sound welds [15]. Characterization of weldments from
a microstructural viewpoint, establishing a relationship of
* Dhruv Bajaj micro-hardness values corresponding to various zones has
maildhruv08@gmail.com also been performed [13–15].
Rao et al. [16] performed FSW on 10 mm and 16 mm thick
1
Department of Mechanical Engineering, Jamia Millia plates of AA7075 alloy in order to study the mechanical prop-
Islamia, New Delhi 110025, India
erties of the welds. Sound welds with a joint efficiency of 70%
2
Aeronautical Materials Division, Defence Metallurgical and 53% were observed for 10 mm and 16 mm weldments,
Research Laboratory, Hyderabad 500058, India

13
Vol.:(0123456789)
Metals and Materials International

respectively. Using a combination of computational modeling water cooling. Also, established knowledge of FSW has been
and experimentation while joining plates of 19 mm thickness, largely based upon thin plates, and there is little to guide for
Sabari et al. [14] demonstrated a lower peak temperature in the an effective tool design for thick plates. Arora et al. [21] con-
case of conventional FSW as compared to UFSW. However, cluded that, in general, peak tensile strength is obtained when
the comparison cannot be held just because the process param- shoulder diameter is thrice the thickness of base metal. This
eters were not identical. Xu et al. [17] investigated tempera- approach may not work in totality during welding of thick
ture evolution and mechanical properties of FS welded 14 mm plates; as in present case it would need shoulder diameter of
thick AA2219-O alloys. Their work showed a significant varia- 45 mm (for 15 mm thick plates) and would be anomalous.
tion of temperature and joint strength along the weld thickness. Very few researchers have successfully addressed the
Thick section FSW requires robust fixtures, tooling in order above-mentioned challenges faced in the joining of thick
to withstand massive clamping forces. The heat management plates of aluminium alloys using FSW. Currently, reports on
along the plate thickness possesses a serious challenge in the investigations on FSW of thick aluminium alloy plates
the welding of thick plates. During FSW of thick aluminium are gradually increasing in the literature, but studies based
alloys the variation of temperature from the top surface (heat upon the elimination of defects have not been widely dis-
source interface) to the bottom surface is large which requires cussed. Substantial work has been performed on the elimina-
high heat-input to keep the bottom sufficiently soft. With high tion of weld defects for thin plates [22] that has been mainly
thermal conductivity, thick section aluminum plates act like based upon the tool design. However, the elimination of
heat sink and heat flow in transverse direction is more than defects and the optimization of strength for thick aluminium
that in the axial (or thickness) direction. Heat conduction in alloy plates, solely based upon process parameters, have not
transverse directions and large temperature variation in the yet been published in the literature. Therefore, studies on the
axial direction causes vertical material movement complex. welding of 15.4 mm thick AA2519 plates were carried out in
This leads to lower cooling rate and further deterioration in the the present investigation. Tunneling defects and kissing bond
microstructure as the thickness of the base metal increases that defects were eliminated by varying the process parameters.
in turn influences the mechanical properties in and around the
stir zone (SZ) [18]. Due to the escalation of process forces, tool
design is another major challenge in the FSW of thick plates. 2 Methods
Tool pin failure is the most common cause that not only leads
to decrease in the overall life of the FSW tool, but makes the Aluminum alloy AA2519-T87 plates of dimensions 160 mm
welding a challenge at the first place. The issue of tool pin fail- (length) × 55 mm (width) were used as the base material/
ure has also been addressed in detail [19]. Increasing the pin alloy (BM). The as-received plates of thickness 16 mm were
diameter to raise the factor of safety results in tunneling defect. reduced to 15.4 mm and welded in butt configuration. The
This is because a greater amount of material has to be swept chemical composition and mechanical properties of the base
due to increased volume of the pin. Moreover, most investi- alloy are given in Tables 1 and 2, respectively. It is note-
gations on welding of AA2519 have incorporated a circular worthy (refer to Table 2) that the alloy is slightly under-
pin cross-section, which induces a lower strain rate [20]. As a aged when compared with the specified minimum tensile
result, very low advance per revolution (APR) of a tool has to strength properties in the long transverse (LT) direction in
be used to obtain defect-free FS welds [13–16]. In the current the T87 temper i.e. 0.2%PS = 400 MPa and UTS = 469 MPa
study, a tapered cylindrical cam tri-flute cross-section has been of the alloy. The alloy was processed so by the producer at
used that induces a greater strain rate and hence a higher APR the industrial scale keeping in mind a specific application.
could be created for successful FSW. Higher values of APR
lead to a decrease in total heat generation, thus improving the
mechanical properties of the FSW joints. Although UFSW Table 2  Tensile properties (LT direction) and hardness of AA2519-
reports higher joint efficiency, it is comparatively less feasible T87 plates
and reproducible as compared to its simpler version of con-
Ultimate tensile strength (MPa) 437
ventional FSW. Further, due to high rate of heat extraction, the
0.2%PS (MPa) 398
UFSW has to be performed at very high heat input in compari-
Elongation (50 mm gauge length) 12
son to conventional FSW. The especial tool design employed
Hardness (HV) 160
in this work produced better joint efficiency via FSW without

Table 1  Chemical composition Element Al Cu Si Fe Mn Mg Zn Ti V Zr


of AA2519-T87 plates (wt%)
Concentration Balance 5.4 0.08 0.12 0.28 0.18 0.018 0.1 0.06 0.14

13
Metals and Materials International

Table 3  Parameters and their levels


Process parameters Level 1 Level 2 Level 3

Shoulder diameter, D (mm) 23 26 29


Rotational speed, N (rpm) 450 560 710
Welding speed, v (mm/min) 31.5 40 50

Table 4  Experimental design
Process parameters
Experi- Shoulder Rotational Welding
ment diameter speed (rpm) speed (mm/
number (mm) min)
Fig. 1  Vertical milling machine adapted to perform FSW Taguchi ­L9 1 1 1 1
2 2 1 2
3 3 1 3
4 3 2 2
5 1 2 3
6 2 2 1
7 2 3 3
8 3 3 1
9 1 3 2
10 1 3 1

sound weld and to study the effects of the process param-


eters, rigorous trial experiments were performed. Successful
trial experiments resulted in the realisation of the tolerance
box of the FSW parameters. Three process parameters each
at three levels were selected for the final set of experiments,
as shown in Table 3. Taguchi ­L9 orthogonal array was used
to design the experiments, as shown in Table 4. It was fur-
ther utilized to find the optimum combination of process
Fig. 2  FSW tool a Schematic b HSS tool parameter yielding maximum strength and zero defect.
The metallographic samples were prepared using stand-
ard metallographic techniques and etched using Keller’s
A robust vertical milling machine adapted for performing Reagent (2 mL-HF; 4 mL-HNO3; 94 mL-H2O). Etched sam-
FSW was used to join the BM as shown in Fig. 1. An in- ples were observed under an optical microscope (OM) for
house designed and fabricated fixture [23] was used to firmly the analysis of defects and microstructural characterization.
hold the BM plates during welding as well as a especially- Scanning electron microscopy (SEM) and energy dispersive
designed tool-adapter [24] was used to hold the FSW tool. spectroscopy (EDS) were utilized to characterize the mor-
High speed steel (HSS) was used as tool material for per- phology and the chemistry of coarse second phase particles
forming the FSW process. A tapered cylindrical cam tri-flute present in weld and base alloy samples.
with left-hand threads was employed for welding. The root The test coupons were accurately machined in the trans-
and tip diameters, and the pin length were kept constant at verse direction on a CNC wire electric discharge machine
10 mm, 6.5 mm and 14.95 mm, respectively. The tool tilt and were subjected to tensile testing using a computer con-
angle was also kept constant at 2°. The FSW tool used in the trolled Tensometer of 20 kN capacity. Testing was performed
present study is shown in Fig. 2. at room temperature and a cross head speed of 2 mm/min.
Three notable process parameters viz. the shoulder diam- The micro-hardness was determined using Vickers micro-
eter, rotational speed and the welding speed were recognized hardness testing machine. Each indentation was performed
to influence the formation of a sound weld, provided effec- for a dwell of 15 s with a load of 100 g at a distance of 1 mm
tive tool geometry is used. Therefore, in order to obtain a both along the thickness of the transverse cross-section and

13
Metals and Materials International

the transverse direction, as shown in Fig. 3. The micro-hard- (voids), while Exp. No. 4 experiences minute voids (refer
ness readings were plotted on a 2D contour map. Fig. 5d) which may be attributed to insufficient mixing at
the pin-and-shoulder driven interface. Since Exp. Nos. 7 and
9 exhibit large voids which are clearly discernible in the
3 Results macrographs, the zoomed in images of their corresponding
tunnelling defects has not been shown.
3.1 Macro‑structure Macrostructures corresponding to experiments carried
out at a welding speed of 50 mm/min are shown in Fig. 6.
The macrostructures of experiment numbers (Exp. Nos.) Exp. Nos. 5, 7 and 3 correspond to Fig. 6a–c, respectively.
1–9 have been classified into three categories with respect Small and relatively large tunnel defects are experienced in
to tool traverse speed. The macrostructures of experiments Exp. Nos. 5 (refer to Fig. 6d) and 7 (refer to Fig. 6b), respec-
with traverse speeds of 31.5, 40 and 50 mm/min are shown tively, whereas a void free weld has been realised in Exp.
in Figs. 4, 5 and 6, respectively. Figure 4a–c represent the 3. The void area and tool rotational speed corresponding to
macrostructures corresponding to Exp. Nos. 1, 6 and 8, Exp. 1-9 has been shown in Table 5. The maximum void
respectively welded at a traversing speed of 31.5 mm/min. area has been observed for highest rotational speed, whereas
Exp. No. 1 is free of voids, while samples from Exp. 6 and least rotational speed yields void-free welds.
8 suffer from minute tunnel defects. At this traverse speed,
both the shoulder diameter and rotation speed increase from
Exp. No. 1 to Exp. No. 8, as shown in Fig. 4. The area of 3.2 Micro‑structure
the thermo-mechanically affected zone (TMAZ) on the
retreating side (RS) is seen to increase (refer to Fig. 4a–c) 3.2.1 Optical Micrographs
from Exp. No. 1 to Exp. No. 8 since an increase in both
the rotation speed and shoulder diameter leads to a rise in Figures 7 and 8 represent the microstructural mapping of
the net heat flux and rate of shear (due to enhanced stir- the welded samples corresponding to Exp. Nos. 1 and 10,
ring action) experienced by the material. Moreover, as the respectively. Visible difference may be observed between the
shoulder diameter increased, considerable growth in the size microstructure evolutions in the two cases. In Fig. 8, a tunnel
of the shoulder affected stirred zone (SASZ) was observed defect may be observed on the AS in Exp. No. 10, whilst, a
(Marked in Figs. 7 and 8), whereas the overall size of the reduction in rotational speed resulted in a sound weld as in
stir zone (SZ) reduced. The SZ appears bell-shaped at a rota- the case of Exp. No. 1.
tional speed of 450 rpm and shoulder diameter of 23 mm, The SZ can been distinctly categorised into three sub-
whereas with an increase in both these parameters, distortion zones, namely, shoulder affected stir zone (SASZ), transi-
in the geometry of the SZ could be noticed. tion stir zone (TSZ) and the pin affected stir zone (PASZ),
At the interface between the shoulder driven region and as shown in Figs. 7 and 8. A larger SASZ and much smaller
the pin driven region, voids could be observed, as shown TSZ are observed for Exp. No. 10 as compared to Exp. No.
in Fig. 4d, e1–e4. Figure 5a–c represent macrographs cor- 1. Also, both TSZ and PASZ can be seen to have tortuous
responding to Exp. Nos. 9, 2 and 4, respectively, welded at profiles for Exp. No. 10; whereas the transverse section pro-
a traversing speed of 40 mm/min. In the case of Exp. No. 9, files of TSZ and PASZ in Exp. No. 1 are smooth and regular.
a tunnel defect of significant magnitude could be observed The micrographs of the grain structure captured from the
(refer to Fig. 5a). Exp. No. 2 is free from tunnelling defects SASZ, TMAZ and HAZ indicate the coarsening of grains

Fig. 3  Indentation marks on the


transverse cross-section of the
welded joint

13
Metals and Materials International

Fig. 4  a Macrostructure (AS is on left and RS on right side) for Exp. No. 1, b macrostructure for Exp. No. 6, c macrostructure for Exp. No. 8, d
Void for Exp. No. 6 e-1,2,3,4) Voids for Exp. No. 8

Fig. 5  Macrostructure: a Exp.
No. 9, b Exp. No. 2, c Exp. No.
4 d Voids for Exp. No. 4

13
Metals and Materials International

Fig. 6  Macrostructure: a Exp.
No. 5, b Exp. No. 7, c Exp. No.
3 d Void for Exp. No. 5

with the increase in tool rotational speed, as observed in 20–25 at% (Cu + Fe + Mn) and 75–80 at% Al. This phase
Figs. 7a–c and 8a–c. may be described as (AlCu)6(CuFeMn). The origin of this
phase is ­Al6(CuFeMn), wherein the (Cu + Fe + Mn) con-
3.2.2 Morphology and Chemistry of Coarse Phase Particles tent is 14.28 at% and the balance being Al i.e. 85.72 at%,
as derived from the compound formula. There is a ten-
Figures 9 and 10 show the scanning electron micrographs dency for Cu atoms to replace certain amounts of Al
(SEM) and X-ray EDS analyses, respectively of the coarse atoms in this compound, and in that case, the phase will
second phase particles present in the base alloy. All the be described as (AlCu) 6(Cu + Fe + Mn) i.e. the phase
micrographs were taken using back scattered electron imag- being present in the base alloy. The coarse phase particles
ing (BSEI) mode. This enabled us to recognize (on the basis present in the base alloy are, therefore, a combination of
of atomic number contrast) the presence of two distinct vari- ­Al2Cu and (AlCu)6(Cu + Fe + Mn).
eties of coarse phase particles: one mostly having a globular Figure 11a represents a scanning electron micrograph
shape and dirty white in contrast showing only Al and Cu (in low magnification) showing various zones of the weld
peaks, and the other mostly having a plate shape and bright obtained from Exp. 1. Figure 11b, c represent scanning
white in contrast showing Al, Cu, Fe and Mn peaks (refer electron micrographs obtained from SZ and TMAZ of
to Fig. 10). the weld obtained from Exp. 1. Figure 11d, e represent
The X-ray EDS analyses obtained from the Cu-rich X-ray EDS analyses typically obtained from the coarse
globular particles showed compositions in the range of particles present in the SZ of the weld. It was revealed
30–32 at% Cu and 68–70 at% Al. This is close to the theo- that ­Al2Cu phase is not present, whilst both A
­ l6(CuFeMn)
retical composition of 33 at%Cu and 69 at%Al, as derived and (AlCu)6(CuFeMn) phases are present in this zone. On
from the compound formula of the ­Al2Cu phase. Identifi- the other hand, the X-ray EDS analyses obtained from the
cation of the coarse, globular phase as the A ­ l2Cu phase is particles present in the TMAZ revealed that such particles
justified because it is the only equilibrium phase that will were a combination of both A ­ l2Cu and (AlCu)6(CuFeMn)
have formed in the base alloy (containing as low as 0.18 wt% (Refer to Fig.  11f, g). The micrographs presented in
Mg) as well as during thermal exposure of the base alloy to Fig. 11b, c showed that the particles present in SZ are
temperatures produced during the FSW process. relatively finer and more uniformly distributed as com-
The Fe-bearing constituent phase particles present pared to the TMAZ. This is because of extensive plastic
in the base alloy showed compositions in the range of

13
Metals and Materials International

Fig. 7  Macrograph and Microstructure corresponding to Exp. No. 1 a TMAZ b SASZ c HAZ-1 d PASZ e TSZ f HAZ-2

deformation and very fine grains in the SZ. As compared the temperature attained in the SZ was sufficient for the
to SZ, the grains in TMAZ are coarser and elongated. dissolution of this phase. Furthermore, a larger area with
Figure 12a represents a scanning electron micrograph smaller number density of precipitates could be observed in
(in low magnification) showing various zones of the weld the SASZ region for Exp. 10 (Fig. 12a). This is because of
obtained from Exp. 10. Figure 12b–d represent scanning much higher heat input in SASZ in the case of Exp. 10 with
electron micrographs obtained from SZ, TMAZ and HAZ greater rotational speed. A large difference in the number
of the weld obtained from Exp. 10. In the SZ, a majority of density of precipitates in the SASZ and PASZ in the case of
the grains are equiaxed, whilst fewer elongated grains could Exp. 10 further confirms the significant difference in heat
also be observed. The X-ray EDS analyses obtained from the prevailing between these zones during welding. Due to this
coarse phase particles present in SZ of the weld, once again, very reason, the extent of dissolution of precipitates is much
showed the absence of the A ­ l2Cu phase whilst detected the higher in the SZ for Exp. 10 as compared to Exp. 1.
presence of both (AlCu) 6(CuFeMn) and ­A l 6(CuFeMn) Figure 13a–c represent scanning electron micrographs
phases. On the other hand, the presence of both A ­ l2Cu and obtained from SZ/TMAZ interfaces of welds obtained
­Al6(CuFeMn) phases in the TMAZ, and the presence of from Exp. 1, Exp. 3 and Exp. 10, respectively. The X-ray
­Al2Cu and (AlCu)6(CuFeMn) phases in the HAZ of the weld EDS analyses obtained from the phase particles present at
were established. such interfaces were found to be a combination of A ­ l2Cu
The absence of A ­ l2Cu phase in the SZs of the welds and (AlCu)6(CuFeMn) for Exp. 1, A ­ l2Cu and A­ l6(CuFeMn)
obtained from both Exp. 1 and Exp. 10 tends to follow that for Exp. 3 and ­Al2Cu, and (AlCu)6(CuFeMn) phases for

13
Metals and Materials International

Fig. 8  Macrograph and Microstructure corresponding to Exp. No. 10 a TMAZ b SASZ c HAZ-1 d PASZ e TSZ f HAZ-2

A list of the coarse phase particles detected in base alloy


Table 5  Defect dependency on rotational speed
and different zones of the welds (obtained from various
Experiment number Rotational speed (rpm) Void area (­ mm2) experiments) is given in Table 6 for ready comparisons.
1 450 0
2 450 0
3.3 Mechanical Characterization
3 450 0
6 560 0.047
3.3.1 Micro‑hardness
4 560 0.593
5 560 0.167
Figure 14 represents the Vickers Micro-hardness contour
8 710 0.976
map for the weld obtained in Exp. No. 1. The hardness con-
9 710 1.124
tour map has been superimposed on the macro-structural
7 710 1.593
zones characterized in Sect. 3.2 by using image processing,
as shown in Fig. 15. A maximum micro-hardness value of
154 HV was observed in the SASZ, which is comparable to
the micro-hardness of base metal (160 HV). A significant
Exp. 10. The presence of a high density of dislocations decrease in hardness could be observed in the TSZ on mov-
at such interfaces will have nucleated coarse ­Al2Cu par- ing along the weld thickness. In Fig. 14, the lowest hardness
ticles during cooling of the welds from high processing distribution region begins at the outer boundary of TMAZ.
temperatures [35]. This region has been characterized in the transverse section

13
Metals and Materials International

Fig. 9  SEM images of Base alloy a 800 X b 2.25 KX

as HAZ-1. The TMAZ/HAZ-1 interface region exists clos- tensile specimen of Exp. No. 10 has been shown in Fig. 17.
est to the tensile failure location which has been shown in It can be observed that, in the TSZ, fracture path shifts from
Sect. 3.3.2. AS towards the RS on moving from SASZ to PASZ.
Rise in hardness can be observed in HAZ-2 on moving
towards the base metal. HAZ-2 extends up to a distance at
which the micro-hardness value matches that of the base 4 Discussion
metal. Also, in the HAZ-2, higher values of micro-hard-
ness could be seen in the lower half section of the weld as 4.1 Defect Elimination
compared to the upper half section. Average hardness in the
transverse direction at different heights from the weld bot- Steep temperature gradient exists along the depth during
tom reveals alternating values of 109, 111, 105 and 111 HV, welding of thick aluminium alloy plates [18, 25], and BM
as shown in Fig. 14. Further, at the bottom of the SZ, certain experiences significant variation in flow stress too. This
spots with lower hardness are also discernible. makes the material near the shoulder relatively easier to stir.
Thus, a simultaneous increase in tangential velocity of tool
3.3.2 Tensile Strength and tool diameter promotes steep reduction in flow stress
near the tool shoulder as compared to the pin driven region,
Tensile properties, fracture location and the corresponding resulting in discrepancy of material flow at the shoulder-pin
images for Exp. Nos. 1 through 10 are shown in Table 7. driven material interface. This discrepancy emerges in the
Figure 16 represents the dimensions of the machined tensile form of voids at this location.
specimen. The maximum tensile strength of 331 MPa was In all the cases represented in Figs. 4, 5 and 6, a lower
observed for Exp. No. 1 which was performed at minimum rotational speed of 450 rpm promoted void free welds, as
rotational speed, traverse speed and shoulder diameter. Ten- reported elsewhere too [26, 27]. On the other hand, defects
sile strength greater than 320 MPa was observed for travers- in the advancing side (AS) are observed because of insuf-
ing speed of 31.5 mm/min (Exp. Nos. 1, 6 and 8) irrespective ficient material movements from the RS to the AS [28].
of the variation in rotational speed and shoulder diameter. The flow of plasticized material during FSW occurs from
Optimal elongation of 32% was observed for Exp. No. 6. In the RS to AS behind the tool [29]. In addition, it is the tan-
general, higher percentage of elongations was observed for gential component of tool velocity which governs the flow
welds with less traversing speed. Moreover, all the welds in transverse direction along the periphery of the tool. This
with traversing speed greater than 31.5 mm/min failed from fact supports the strong influence of rotational speed on the
the SZ. The failure occurred at RS-TMAZ/HAZ-1 interface size of tunnel. This dependence could be confirmed from
for Exp. No. 1, whereas for Exp. Nos. 6 and 8, the tensile the defect area as shown in Table 5. In order to confirm this
specimen fractured from AS-HAZ-1. The fracture location effect, Exp. 10 has been added to this study, in which all the
across the weld cross section closely follows the path of least parameters were kept same as those of Exp. No. 1 except the
micro-hardness/resistance, being closest to the RS-TMAZ/ tool rotational speed, which was kept maximum. Notably, a
HAZ-1 interface. This can be clearly observed in the micro- significant tunnel was observed in the TSZ for Exp. No. 10
hardness contour map (Fig. 14). The image of the failed whereas, Exp. No. 1 yields void free weld with maximum

13
Metals and Materials International

Fig. 10  X-Ray EDS analysis of


Base alloy a SEM Image b Spot
1 c Spot 2 d Spot 3 e Spot 4 f
Spot 5

tensile strength (Sect. 4.3.2). The influence of the rotational shear layer material just before consolidation has its tangen-
speed on the defect formation can be explained as follows: tial velocity vector perpendicular to the traversing speed.
Figure  18 exhibits the material flow during FSW as Exp. Nos. 1 and 10 differ only in terms of tool rotational
experimentally validated by Chen and Cui [30]. The plas- speed, with the latter being higher. As mentioned in the pre-
ticized material moving beneath the shoulder and around vious section, higher rotational speeds generate higher heat
the tool pin is referred as the flow zone. In the flow zone, flux which engenders a decrease in flow stress in the flow
the material picked up from the AS is deposited behind the zone. With a decrease in flow stress, slipping of the mate-
pin in the form of discrete shear bands due to sticking and rial with the traversing tool increases and hence the ability
slipping action between the base material and tool pin. The of the tool to drag the material is curtailed [31]. As a result,

13
Metals and Materials International

Fig. 10  (continued)

13
Metals and Materials International

Fig. 11  SEM images and X-Ray EDS analysis of various zones of weld obtained from Exp. 1. a Low magnification image b SZ c TMAZ d, e
X-Ray EDS analysis of SZ f, g X-Ray EDS analysis of TMAZ

13
Metals and Materials International

Fig. 11  (continued)

13
Metals and Materials International

Fig. 12  SEM images of various zones of weld obtained from Exp. 10. a Low magnification image b SZ c TMAZ d HAZ

the softened material flowing from RS to AS in the wake of this location, as demonstrated schematically in Fig. 18. This
the weld is not able to traverse the full length of flow zone increases the probability of a tunnel near the AS at the SZ-
along the transverse direction, causing material deficiency at TMAZ interface. Consequently, at 710 rpm, a tunnel defect

13
Metals and Materials International

Enhanced material consolidation required for elimination


of such defects can be achieved by considerable reduction
in tool rotational speed, as evident from the current study.

4.2 Micro‑structural Characterization

4.2.1 Optical Micrographs

Unlike FSW of thin plates, welding of thick plates results in


large variation of flow stress along the weld thickness (axial
direction) due to wide difference in temperature between
the shoulder driven material and the root of the weld. As
a result, numerous sub-zones could be identified from the
micrographs. Owing to the fact that an appreciable thermal
gradient is observed along the thickness of the weld [18], the
SZ comprises of three distinctively identifiable sub-zones,
i.e. SASZ, TSZ and the PASZ. In the case of thin plates,
the thermal gradient is small, and, therefore, the TSZ is not
fairly distinguishable. On the contrary, a higher thermal gra-
dient in thick plates results in a distinctive transition zone.
Considering the three distinct stir zones as shown in
Figs. 7 and 8, the SASZ has a greater expanse in Exp. No.
10 which tends to suppress the TSZ. This is due to the higher
rotational speed in Exp. 10 that generates higher heat flux
and in turn reduces the flow stress in the SASZ. Hence, a
decreased flow stress leads to greater material movements by
the tool shoulder and hence conquering the TSZ. The higher
rpm and the consequent increase in heat also leads to an
abrupt variation in the radius of TSZ in Exp. No. 10, while
smooth transition occurs for Exp. No. 1, as one moves from
the SASZ to the PASZ. The PASZ of Exp. No. 1 is found be
to be bell-shaped whereas that of Exp. No. 10 is irregular in
shape. This bell-shaped PASZ arises due to a lower heat flux
which in turn promotes higher sticking action and the mate-
rial flow lines tend to create a vortex in the PASZ [32–34].
Whereas, a higher heat gradient is experienced in the case
of Exp. No. 10 and this tends to promote slipping forming
an irregular PASZ.

4.2.2 Morphology and Chemistry of Coarse Phase Particles

For Exp. Nos. 1 and 10, the TMAZ was found to con-
sist of both ­Al2Cu and the Fe-bearing constituent phases
(refer to Table 6) whereas, the A­ l2Cu phase was not found
Fig. 13  SEM images of SZ/TMAZ Interface of weld obtained from a in the SZ. This tends to infer that the temperature attained
Exp. 1 b Exp. 3 c Exp. 10 in the SZ was sufficient for the dissolution of ­Al2Cu par-
ticles. A much more uniform distribution of second phase
is observed at the AS and not at 450 rpm in Exp. Nos. 10 particles in the SZ and their smaller size in this zone as
and 1, respectively. Importantly, the incongruity of the flow compared to the TMAZ occurs due to extensive plastic
stress occurs at the TSZ, which makes it the most favourable deformation and very fine grains in the SZ. Due to con-
location for void formation along the weld thickness. siderably higher heat input in the case of Exp. No. 10, a
The above discussion infers that during the welding broad area with substantially lesser number of precipi-
of thick section aluminium, voids form on the AS-TSZ. tates was observed in the SASZ. A large difference in the

13
Metals and Materials International

Table 6  The locations of Location Al2Cu (AlCu)6(CuFeMn) Al6(CuFeMn)


alloy phase A
­ l2Cu, and
the Fe-bearing constituent Base alloy ✓ ✓ ×
phases (AlCu)6(CuFeMn) and
SZ of weld from Expt. 1 × ✓ ✓
­Al6(CuFeMn) (✓: Present, × :
Absent) TMAZ of weld from Expt. 1 ✓ ✓ ×
SZ of weld from Expt. 10 × ✓ ✓
TMAZ of weld from Exp. 10 ✓ × ✓
HAZ of weld obtained from Exp. 10 ✓ ✓ ×
SZ/TMAZ interface from Exp. 1 ✓ ✓ ×
SZ/TMAZ interface from Exp. 3 ✓ × ✓
SZ/TMAZ interface of Exp. 10 ✓ ✓ ×

Fig. 14  Vickers Microhardness contour map for weld obtained in Exp. No. 1

Fig. 15  Hardness contour map


of Exp. No. 1 superimposed on
corresponding macrostructural
zones

density of precipitates in the SASZ and PASZ in the case The presence of a high density of dislocations at SZ/
of Exp. 10 further confirms the significant difference in TMAZ interfaces would have assisted in nucleation of
heat prevailing between these zones during welding. Due ­Al2Cu phase during cooling of the welds from high pro-
to the same reason, the extent of dissolution of precipi- cessing temperatures [35].
tates is much higher in the SZ for Exp. 10 as compared
to Exp. 1. This may be clearly observed upon comparing
Figs. 11a with 12a.

13
Metals and Materials International

Table 7  Tensile strength and Exp. no. Tensile properties Failure location Image of failed specimen
fracture location
Tensile Elonga- Joint AS RS
strength tion efficiency
(MPa) (%) (%)

1 331 32 75.7 RS-TMAZ/HAZ-1 interface

2 282 24 64.5 SZ (centre)

3 296 26 67.7 SZ (centre)

4 199 16 45.5 AS-SZ (defect)

5 305 25 69.8 AS-SZ (defect)

6 322 32 73.7 AS-HAZ-1

7 215 23 49.2 AS-SZ (defect)

8 329 26 75.3 AS-HAZ-1

9 195 23 44.6 AS-SZ (defect)

10 197 17 45.0 AS-SZ (defect)

4.3 Mechanical Characterization

4.3.1 Micro‑hardness

The decrease of hardness in TSZ ascertains the fact that


relatively high thermal gradient exists in this zone along the
Fig. 16  Dimensions of tensile specimen (in mm)

Fig. 17  Tensile sample of
experiment 10 TSZ

SASZ
AS RS

PASZ

13
Metals and Materials International

Fig. 18  Material flow during


FSW

weld thickness which leads to significant variations in local the transverse direction as observed here is similar to the
mechanical yield strength. The decrease in microhardness variation of temperature distribution on the weld cross-
values in HAZ-1 could be attributed to coarsening and disso- section measured by Mahoney et al. [36, 37]. Small locales
lution of strengthening precipitates because of the prevalent having lesser hardness have been observed in the root of the
heat flux during FSW [18]. The distortion of grains due to SZ. This is opposite to the findings of Martinez et al. [18].
plastic deformation in the TMAZ results in an increase in
dislocation density leading to higher hardness as compared 4.3.2 Tensile Strength
to HAZ. Also, due to higher dislocation density nucleation
and growth of precipitates is favoured in this zone, leading Ahead of the tool in the welding direction, the base metal
to increase in hardness. The formation of fine recrystallized enters the flow zone (refer to Fig. 18) at a constant velocity
grains in the SZ further increased micro-hardness as was equal to traversing speed. After rotation around the FSW
observed earlier in several other alloys in accordance with tool, the base material exits the flow zone behind the tool.
the Hall–Petch relationship. Assuming the FSW process as a single-phase incompressible
The hardness improves in the HAZ-2 on moving away flow, the continuity equation is represented by Eq. (1) [38]:
from the weld center due to a decrease in the heat experi-
enced by the base metal. In the HAZ-2, higher micro-hard- ∇ ⋅ u⃗ = 0 (1)
ness in the lower half section as compared to the upper half Using Eq. (1) along the weld seam, it may be pointed out
section could be due to lesser heat loss (due to convection) that the average time spent inside the flow zone by the base
from the top surface as compared to the heat dissipation metal is inversely proportional to the traversing speed during
from the bottom surface (due to conduction) [18]. The pat- welding. Evidently, high temperature and pressure prevailing
tern of alternating increase and decrease in hardness along inside the flow zone result in metallic bonding during FSW.

13
Metals and Materials International

With the decrease in traversing speed, total time spent by the Acknowledgements  One of the authors (AKM) is grateful to the
base material inside flow zone increases, resulting in better financial support of Defence Research and Development Organization
(DRDO).
metallic bonding in SZ and stronger welds, which is lucid
in the current work. It is important to note that much higher
Compliance with ethical standards 
tensile strength has been obtained for void exhibiting Exp.
Nos. 6 (322 MPa) and 8 (329 MPa) as compared to void free Conflict of interest  The authors declare that they have no conflict of
Exp. Nos. 2 (282 MPa) and 3 (296 MPa) because of least interest.
traversing speed in Exp. Nos. 6 and 8. The improvement in
the extent of metallic bonding dominates over the weaken-
ing effect of voids in Exp. Nos. 6 and 8, which failed from
HAZ-1 and not from the location of void. Loss of strength is References
another major difficulty in achieving thick section FS welds
with high joint efficiency. Although a decrease in traverse 1. X. Lei, Y. Deng, Z. Yin, G. Xu, Tungsten inert gas and friction stir
speed of the tool leads to increase in over-all heat input; welding characteristics of 4-mm-thick 2219-T87 plates at room
temperature and −196°C. J Mater Eng Perform 23(6), 2149–2158
considerable improvement in strength was observed due (2014)
to enriched bonding (too much heat input, however, may 2. D. Edwards, I. Crouch, Light alloys, in The Science of Armour
produce adverse effect due to coarsening and dissolution of Materials, ed. by I. Crouch (Elsevier, Amsterdam, 2017), pp.
strengthening precipitates). On the other hand, no visible 117–166
3. T. Børvik, L. Olovsson, S. Dey, M. Langseth, Normal and oblique
voids were observed in the case of Exp. Nos. 2 and 3, but impact of small arms bullets on AA6082-T4 aluminium protective
tensile failure occurring from the SZ center suggests the plates. Int. J. Impact Eng. 38(7), 577–589 (2011)
presence of kissing bond [22]. The displacement of fracture 4. L. Quintino, R. Miranda, U. Dilthey, D. Iordachescu, M. Banasik,
path from AS to RS occurs in the TSZ for Exp. No. 10 as S. Stano, Laser welding of structural aluminium, in Structural
Connections for Lightweight Metallic Structures, ed. by P.
shown in Fig. 17. This shift occurring in the TSZ corrobo- Moreira, L. da Silva, P. de Castro (Springer, Berlin, 2010), pp.
rates the fact that the fluctuation of flow stress occurs in this 33–57
zone. 5. M.A. Sutton, B. Yang, A.P. Reynolds, J. Yan, Banded microstruc-
ture in 2024-T351 and 2524-T351 aluminum friction stir welds:
part II. Mechanical characterization. Mater. Sci. Eng. A 364(1–2),
66–74 (2004)
6. M.A. Sutton, B. Yang, A.P. Reynolds, R. Taylor, Microstructural
5 Conclusions studies of friction stir welds in 2024-T3 aluminum. Mater. Sci.
Eng. A 323(1–2), 160–166 (2002)
7. G. Oertelt, S. Babu, S. David, E. Kenik, Effect of thermal cycling
FS welds of 15.4 mm thick plates of AA2519 alloy with a on friction stir welds of 2195 aluminum alloy. Weld. J. 80(3),
joint efficiency of more than 75% have been obtained for a 71–79 (2001)
shoulder diameter of 23 mm, rotational speed of 450 rpm 8. H.-J. Liu, H-j Zhang, Y-x Huang, Y. Lei, Mechanical properties
and welding speed of 31.5 mm/min. of underwater friction stir welded 2219 aluminum alloy. Trans.
Nonferrous Met. Soc. China 20(8), 1387–1391 (2010)
It is observed that reduced rotational speeds significantly 9. Y. Chen, H. Liu, J. Feng, Friction stir welding characteristics of
favours the elimination of tunnelling defects that typically different heat-treated-state 2219 aluminum alloy plates. Mater.
occurs at the AS-TSZ. The impact of decrease in traverse Sci. Eng. A 420(1–2), 21–25 (2006)
speed on the improvement of the weld strength is prominent 10. G. Cao, S. Kou, Friction stir welding of 2219 aluminum: behavior
of ­(Al2Cu) particles. Weld. J. 84(1), 1–8 (2005)
to such an extent that any weakening effect of voids is com- 11. K.S. Arora, S. Pandey, M. Schaper, R. Kumar, Effect of process
pensated. Significant variations in weld properties further parameters on friction stir welding of aluminum alloy 2219-T87.
takes place due to alterations in the characteristics of TSZ. Int. J. Adv. Manuf. Technol. 50(9–12), 941–952 (2010)
The incoherency between shoulder and pin driven move- 12. S. Benavides, Y. Li, L. Murr, D. Brown, J. McClure, Low-temper-
ature friction-stir welding of 2024 aluminum. Scr. Mater. 41(8),
ments of metal further suffices the formation of voids in the 809-815 (1999)
TSZ and leads to considerable variations in micro-hardness 13. S.S. Sabari, S. Malarvizhi, V. Balasubramanian, The effect of pin
values along the weld thickness. profiles on the microstructure and mechanical properties of under-
Due to the attainment of high temperature in the SZ, water friction stir welded AA2519-T87 aluminium alloy. Int. J.
Mech. Mater. Eng. 11(1), 5 (2016)
the dissolution of ­Al2Cu phase takes place. Because of the 14. S.S. Sabari, S. Malarvizhi, V. Balasubramanian, G.M. Reddy,
same reason, the SASZ experiences even further paucity Experimental and numerical investigation on under-water fric-
of strengthening phases. A large number density of coarse tion stir welding of armour grade AA2519-T87 aluminium alloy.
­Al2Cu phase particles is observed at SZ/TMAZ interfaces Defence Technol. 12(4), 324–333 (2016)
15. S.S. Sabari, S. Malarvizhi, V. Balasubramanian, Influences of tool
and this is attributed to an enhanced nucleation of the ­Al2Cu traverse speed on tensile properties of air cooled and water cooled
phase upon a high number density of dislocations existing friction stir welded AA2519-T87 aluminium alloy joints. J. Mater.
at this these locations. Process. Technol. 237, 286–300 (2016)

13
Metals and Materials International

16. T.S. Rao, G.M. Reddy, S.K. Rao, Microstructure and mechanical 29. A.C. Nunes, Jr. Metal flow in friction stir welding. NASA Tech-
properties of friction stir welded AA7075–T651 aluminum alloy nical Reports Server. Document ID: 20070001990. Materials
thick plates. Trans. Nonferrous Met. Soc. China 25(6), 1770–1778 Science and Technology 2006/ASM International, The Minerals,
(2015) Metals and Materials Society; October 15, 2006 - October 19,
17. W. Xu, J. Liu, G. Luan, C. Dong, Temperature evolution, micro- 2006; Cincinnati, OH; United States (2006)
structure and mechanical properties of friction stir welded thick 30. Z. Chen, S. Cui, Tool-workpiece interaction and shear layer flow
2219-O aluminum alloy joints. Mater. Des. 30(6), 1886–1893 during friction stir welding of aluminium alloys. Trans. Nonfer-
(2009) rous Met. Soc. China 17(s1A), s258–s261 (2007)
18. N. Martinez, N. Kumar, R. Mishra, K. Doherty, Microstructural 31. M. Rosales, N. Alcantara, J. Santos, R. Zettler, The backing bar
variation due to heat gradient of a thick friction stir welded alu- role in heat transfer on aluminium alloys friction stir welding.
minum 7449 alloy. J. Alloys Compd. 713, 51–63 (2017) Mater. Sci. Forum 636, 459–464 (2010)
19. A. Arora, M. Mehta, A. De, T. DebRoy, Load bearing capacity of 32. P. Su, A. Gerlich, T. North, G. Bendzsak, Material flow during
tool pin during friction stir welding. Int. J. Adv. Manuf. Technol. friction stir spot welding. Sci. Technol. Weld. Join. 11(1), 61–71
61(9–12), 911–920 (2012) (2006)
20. H. Su, C. Wu, Determination of the traverse force in friction stir 33. P. Su, A. Gerlich, T. North, G. Bendzsak, Intermixing in dissimilar
welding with different tool pin profiles. Sci. Technol. Weld. Join. friction stir spot welds. Metall. Mater. Trans. A 38(3), 584–595
24, 209–217 (2018) (2007)
21. A. Arora, A. De, T. DebRoy, Toward optimum friction stir welding 34. J. Schneider, A.C. Nunes, Jr. Influence of processing parameters
tool shoulder diameter. Scr. Mater. 64(1), 9–12 (2011) on the flow path in friction stir welding. NASA Technical Reports
22. N.Z. Khan, A.N. Siddiquee, Z.A. Khan, S.K. Shihab, Investiga- Server. Document ID: 20060026036. NASA Marshall Space
tions on tunneling and kissing bond defects in FSW joints for dis- Flight Center; Huntsville, AL, United States (2006)
similar aluminum alloys. J. Alloys Compd. 648, 360–367 (2015) 35. J.-Q. Su, T.W. Nelson, R. Mishra, M. Mahoney, Microstructural
23. Siddiquee AN, Khan NZ, Khan ZA. Universal friction stir investigation of friction stir welded 7050-T651 aluminium. Acta
welding/processing work fixture. Indian Patent Application Mater. 51(3), 713–729 (2003)
No.201611017741 A, INDIA, Publication Date: 09/09/2016 36. M. Mahoney, C. Rhodes, J. Flintoff, W. Bingel, R. Spurling, Prop-
24. Siddiquee AN, Khan NZ, Khan ZA. Universal friction stir erties of friction-stir-welded 7075 T651 aluminum. Metall. Mater.
welding/processing tool adopter. Indian Patent Application No. Trans. A 29(7), 1955–1964 (1998)
201911002618 A (19) INDIA (22) Publication Date : 22/02/2019 37. R.S. Mishra, P.S. De, N. Kumar, Friction Stir Welding and Pro-
25. C.T. Canaday, M.A. Moore, W. Tang, A.P. Reynolds, Through cessing: Science and Engineering (Springer, Berlin, 2014)
thickness property variations in a thick plate AA7050 friction stir 38. R. Nandan, G. Roy, T. Debroy, Numerical simulation of three-
welded joint. Mater. Sci. Eng. A 559, 678–682 (2013) dimensional heat transfer and plastic flow during friction stir
26. P. Colegrove, H. Shercliff, CFD modelling of friction stir welding welding. Metall. Mater. Trans. A 37(4), 1247–1259 (2006)
of thick plate 7449 aluminium alloy. Sci. Technol. Weld. Join.
11(4), 429–441 (2006) Publisher’s Note Springer Nature remains neutral with regard to
27. P. Colegrove, H. Shercliff, Experimental and numerical analysis jurisdictional claims in published maps and institutional affiliations.
of aluminium alloy 7075-T7351 friction stir welds. Sci. Technol.
Weld. Join. 8(5), 360–368 (2003)
28. Y. Zhu, G. Chen, Q. Chen, G. Zhang, Q. Shi, Simulation of mate-
rial plastic flow driven by non-uniform friction force during fric-
tion stir welding and related defect prediction. Mater. Des. 108,
400–410 (2016)

13

You might also like