Certificate of analysis and (..) conformity according to PharmEthyl® European Pharmacopoeia ___ITEM ALC. PHARMETHYL 80 EP DATE (dd.mm.yyyy) 24.10.2018 PRODUCTED AND LOADED CRISTANOL BATCH NUMBER 090000046600 FROM (FACTORY NAME) +33 326 61 21 21 SATCHRMEASE DATE! 2370201 CUSTOMER ,ECNOLOGICA DE | A + Garcine ALIMENTOS S.A. VALIDATED BY) ,Czine ~HAULIER KVG 7 RETESTDATE 10.2019 TRUCK ID NUMBER RFCU8803149 | REFERENCE NUMBER aseri7es PO TASA ORDER NUMBER FO TAS! Unless mentioned otherwise the results relate to the alcohol prior to denaturing or hydration ‘Alcohol Paramotere ‘Specifications Result ‘eating procedure Eman! Content at 20°0 2095 00,0 Méthode Phamaeopée Europeenne ‘Appearance Canora? ‘Comptes | Métro Phamacopée Europeerne ‘wb Canorme" Comptes | Metode Phamacopée Europeerne test Conform” Compies | Méfode Phamacopée Europderne Boling point 70s...s700 735 __|Metoge Pharmacopée Evropeenne IDENTIFICATION specific gravity at2 0,790 S... $0,793 0.791 Méthode Pharmacopée Européenne 2.2.6 DENTIFICATION BIR Contorme Comptes Metrade Prarmecapes Européerne 2224 Anpoarane Lipide ncobre Clear, exouress | Méthode Phamacopée Euopéenne 22.162 Aciity or alkalinity (as acetic acid) pom (vv) 530 <30 | Méthode Pharmacopée Europeenne 7 UV absorption (240nm) S040 021 "Méthode Pharmacopée Européenne 2225 LV absorption (between 2801 and 260m) 030 0.09 Methode Prarmacapee Europeenne 2.2.25, UV absorption (etween 270nm and 240m) (201 Metnode Pharmacopee Ewopéeme 22.25 LU absorption (2401280-260/270-240 a) || Gompses—Metnede Prarmaconée Européeme 2.2.25 Methanol ppm(wiv) $100 < 100 ‘Méthode Pharmacopée Européenne 2.2.28 ‘Acetaldehyde + acetal (as acotaldehyde) ppm (vv) $10 <10 ‘Matnode Pharmacopde Européenne 2.2.28 Benzene | ppm (wiv) $2 <2 ‘Méthode Pharmacopée Européenne 2.2.28 im of al others impurtios | ppm iy +5900 900 Méthode Pharmacopée Européeane 22.28 Non volatile resiue bem (rw) 20 <20___ Méthode Phammaconée Euoptenne Water content (PPM) opm = 1000 172 Menode KF (EN1S429) Lead Content ppm 05 | 00 ePMS Tota higher alcohols (PPM VIN) om Ed 0 Métrode OW Boisson spiumux (PG) alysis realised on the batch by the laboratory of the loading plant. Wording of characteristics: - Appearance: Colouriese and clear liquid, impid, volatile, flammable, hygroscopic + Solubility: miscible with water and with methylene chlorid -Flame Test: bums with blue flame without smoke ~ ABSORBANCE 240/250-260/270-240nm : regular descending curve without peak ND : Not detected ‘Comments Product complies Monographie “Ethanol anhydre” 01/2015 : 1318 (pharmacopée Européenne 9éme édition) Monograph "Ethanol anhydrous" 01/2018:1318 (European Ph. Sth edition) This is a computer generated document raised upon the responsibility of the Quality manager. No signature is, required Etablished by CRISTANOL on behalf of CristalCo "Sasma CERTIFICATE OF ANALYSIS ANHYDROUS ETHYL ALCOHOL (99,9%vol.) EP GRADE FOOD GRADE Production date: 24°" Oct. 2018 Retest date: 24'" Oct. 2020 Batch nu.: Been. Container nu, RFCU 880314-9, RFCU 880218-4, FPTU 600084-0 Reference nu.: 23571752, 23571753, 23571754 Order nu.: TASA-10 Test (Unit) Specification Result Clarity of solution To Pass Test Pass Color of solution To Pass Test Pass Solubility Miscible with water Pass Identification Test A 0,790 -0,793 0,791 Identification Test B To Pass Test Pass Assay-Ethyl Alcohol at 20 8C (%vol.) 2995 100,0 Density at 20 8C (kg/liter) 0,709-0,793, 0,789 Water (%évol.) 0,4 <0,02 Nonvolatile Residue (ppm, m/v) $20 <20 Acidity and Alkalinity as Acetic acid (ppm) $30 <30 Volatile impurities (6C) Methanol (ppm, v/v) $100 <100 Acetaldehyde (ppm, v/v) 10 s10 Benzene (ppm, v/v) 82 <2 Total of All Others (ppm, v/v) <300 <300 Fusel oil (ppm, v/v) s5 o Lead (Pb) (ppm, v/v) $05 0 Product Complies with the current EP, HACCP and |S09001 principles. JECFA~ Ethyl Alcohol CAS: 64-17-5 Product Complies with the GMO declaration according to the EU regulation 1829/2003 and the EU regulation 1830/2003. Issue date: 25' Oct. 2018, The Netherlands. An ISO 9001:2015 and ISO 22000:2005 Certified Company by Lloyd's. Heliumstraat 8 « 2718 SL Zoetermeer + The Netherlands Phone: + 31.79.3633064 + Fax: 431.79.3633067 Email: sales@sasmabv.com * www,sasmabv.com