‘Tarate the filtrate with N/10 FIC using Bromoeresol green indicator 1 Blue colour turns to yellow. Calculation % Bree Lime (CaO F) = TV x 0.373 where TV = Titrate Value RAW MEAL RESIDUE ON 90 MICRON SIEVE BY WET SIEVING Take a known quantity of sample and sieve through 90 micron Rinse the residue in the sieve with tap water unt the material stops passing through the sieve Dry the residue and weigh it Caleutation Weight of residue’ 100 Percentage Residue = Weight of sample taken SIEVE ANALYSIS OF CRUSHED LIME STONE Take a known quantity of erushed Lime Stone sample from the Vibrating Screen discharge point and Sieve through 25 mm sieve, Caleulation Weight of passing material x 100 Percentage passing = Weight of sample taken FLUORSPAR TESTING PROCEDURE, ( Ca >) ‘Take | gm of dry sample, add about 20 ml, of 25% Glacial Acetic acid and boil for approx. $ minutes Filter though No. 40 filer paper wash the residve weigh and ignite in platinum erucible at 800°C Record the weight afer ignition and calculate CaCO, by subtracting the weight difference From 100, ‘Add 10 to 15 drops of HF acid to the erucible, dry and ignite at 800° C and record the weight Determine the weight difference before and after HE acd treatment Calculate SiO, by multiplying the weight difference with 100, Ad approx. 10 ml, of 1:1 HCL into the ervcible to dissolve, transfor ittoa 500m. beaker. Dry the contents and ald 50 ml of 1:1 HaS0y ard again dyTake 100ml, ofthis solution in a 250 mil, beaker ard boil ,add approx. | gm, of NH ‘of Methyl red indicator and NHyOH drop by drop to the boiling solution tll the colour changes, Cool the solution and filter thought No-4 filter paper, wash, place the Filter pape withthe residue ina ercibe, weigh, roord the sreght and then ignite at 800°C for 30 o 40 minutes Weigh the erucible and record the weight Calculate % 0, by multiplying the weight difference with 250. Boil the filtrate, collected at Pars 3.18.cin 500ml beaker and ad approx.10m of 10% ‘ammonium oxalate solution. Filter thoush No-40 filter paper and wash il oxalate i ree Dissolve the precipitate in :1 H;S0O, and hot water. Titra the solution with standard KMnO, solution and eatetat CaP percentage, Calculation 2s %CHO = TV x 1.25 x Factor of KMnO, % Cak Purity) = %CaO x 1.393 FELDSPAR TESTING Prepare Powder pelletes and test through Lab-X. CEMENT FINENESS (BLAINE) TESTING PROCEDURE ‘This test is to be performed as per IS 4031 (part-2):1988 dealing with test for fineness of Cement by specific surface using Blaine air 4.0 TEST EQUIPMENTS 4.1 CUBE MOULD Check height of the eube mould (70.6mm “*'? _y 9 ). Check distance between opposite faces, (70,6mm *'* 9,0) 42 _VICAT APPARATUS Check following dimensions in mm Needle diameter (Initial) 1.13+-0.05 Effective length of the needle({nitial) 501.0 Diameter of plunger! 00.05 Effective length of plunger 50+-1.0 Initial diameter of Vieat mould (Split type ) 80°-1.0, Height of Vicat mould (Split type) 40+-0.2