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Article history: The object of the paper is to investigate the effects of staking sequences and hybridation on the damping
Available online 9 May 2015 properties of flax–carbon twill epoxy composites. Various staking sequences of these hybrid laminates
were manufactured by platen press process. Next, dynamic properties were investigated using beam test
Keywords: specimens and an impulse technique. Damping modelling was implemented by using a finite element
Flax fibre analysis to evaluate the dissipated energies in each layer of carbon–flax laminates. The obtained results
Carbon fibre show a good agreement between the experimental damping coefficients and those deduced from
Hybrid composites
modelling. It is also shown that the position of flax layers within the hybrid composites plays a major role
Vibration testing
Damping
on their bending stiffness and damping properties.
Modelling Ó 2015 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.compstruct.2015.05.016
0263-8223/Ó 2015 Elsevier Ltd. All rights reserved.
M. Assarar et al. / Composite Structures 132 (2015) 148–154 149
testing. In particular, they showed that flax fibre reinforced com- Table 2
posites present a relatively higher damping behaviour with respect Engineering constants of the non-hybrid twill carbon and flax reinforced composite
materials.
to the other composites which could be attributed to the different
friction mechanisms intrinsic to flax fibres. Laminates EL ET GLT v LT
These studies showed that the use of natural fibres as reinforce- (GPa) (GPa) (GPa)
ment of composite materials can significantly improve their damp- Carbon fibre reinforced epoxy 54.10 54.10 3.60 0.33
ing properties and reduce unwanted vibrations of structural laminate
Flax fibre reinforced epoxy laminate 11.50 11.50 2.01 0.31
applications. For high performance applications, damping could
be, in some cases, insufficient for their safe design. In fact, it should
be combined with mechanical performances. It is within this
context that the present study of the mechanical and dynamic
properties of carbon–flax hybrid composites is proposed. This
choice is motivated by the high mechanical performance of carbon
fibre as well as the interesting dynamic properties of flax fibre. For
this purpose, non-hybrid and hybrid carbon and flax fibre rein-
forced composites were elaborated to determine, by free vibration
testing, the effects of hybridation on the dynamic properties of
hybrid composites. Next, we will show how the laminate theory
associated to a finite element analysis allows us to describe the
damping characteristics of these hybrid composites.
2. Experimental procedure
2.1. Materials
pressure of 5 bars.
Six types of twill hybrid laminates with different stacking
sequences, shown in Table 1, were elaborated to investigate the transverse vibrations. Next, the excitation and the response signals
effect of hybridation type on the composites damping. The thick- were digitalized by a dynamic analyser LMS SCADAS Mobile. This
ness and volume fraction of each plate depend on the considered analyser associated with a PC computer performs the acquisition
laminate as indicated in Table 1. of signals, controls the acquisition conditions and the analysis of
The engineering constants of flax and carbon laminates referred the acquired signals. The system allows the simultaneous acquisi-
to the material directions ð1; 2; 3Þ or ðL; T; T 0 Þ were measured in tion of four signals with a maximum sampling frequency of
static tensile tests on five specimens. The obtained mean values 102.4 kHz with a resolution of 24 bits for each channel. Impulse
are reported in Table 2. excitations of flexural vibrations were implemented at different
points of the beam, and the response was detected at the
2.2. Experimental equipment accelerometer as shown in Fig. 1. These experimental analyses
were performed on five specimens with different lengths 230,
The dynamic characteristics of the studied composite materials 250 and 270 mm in order to obtain a variation of the peak frequen-
were derived from the analysis of the free flexural vibrations of the cies values. The experimental shapes of the natural modes were
test specimens. The equipment is shown in Fig. 1. The test also estimated by the LMS PolyMAX method [29]. This method is
specimens are supported vertically by two fine rubber threads in globally divided in two steps: first, a stabilization algorithm is used
such a way to have free-free boundary conditions of the beam. to determine the natural frequencies as well as their corresponding
An impulse hammer (PCB 086C03 model) is used to induce the damping, and second, a least squares frequency domain (LSFD)
excitation of the flexural vibrations of the composite beam. method is used to calculate the mode shapes. The obtained
The specimen response was then detected by an accelerometer experimental modes were visualised in order to verify that they
(PCB 352C23 model) which measures the acceleration of the correspond to bending modes of beams with two free ends.
Table 1
Designation of the non-hybrid and hybrid laminate composites.
Laminates Ply number ratio (carbon/flax) Stacking sequence C: Carbon F: Flax Plate thickness (mm) (Carbon/Flax) Volume fraction ratio (%) (Carbon/Flax)
Carbon 8/0 CCCCCCCC 2.6/0 52/0
[C3/F]S 6/2 CCCFFCCC 1.4/1.1 40/12
[C2/F2]S 4/4 CCFFFFCC 0.6/1 25/22
[C/F3]S 2/6 CFFFFFFC 0.4/2.5 15/35
Flax 0/8 FFFFFFFF 0/3.8 0/39
[F3/C]S 2/6 FFFCCFFF 0.4/2.7 14/35
[F2/C2]S 4/4 FFCCCCFF 0.8/2.1 24/22
[F/C3]S 6/2 FCCCCCCF 1.3/1.1 41/12
150 M. Assarar et al. / Composite Structures 132 (2015) 148–154
Fig. 2. Evolution of the loss factor according to the sample number of the
and this for each element e of the structure. For each layer,
acquisition system. through-the-thickness in-plane stresses and strains are linear func-
tions of the z coordinate and are expressed as:
k;e k;e
2.3. Analysis of the experimental results rk;e
p ¼ a1p ðx; yÞz þ b1p ðx; yÞ;
k;e
p ¼ 1; 2; 6 ð2Þ
k;e
ek;e
p ¼ a2p ðx; yÞz þ b2p ðx; yÞ:
The determination of the natural frequencies and damping
coefficients of the tested specimens was done by fitting the with:
experimental responses with the LMS software using the k;e k;e
PloyMax (Polyreference Modal Analysis eXtended) method [29].
rk;e
pu rpl ek;e
pu epl
ak;e
1p ¼ k;e
; ak;e
2p ¼ k;e
;
A second identification was also done by fitting the experimental h h
Frequency Response Functions (FRF) with the analytical response
zk;e zk;e
k;e k;e k;e k;e
b1p ¼ rk;e
pu rk;e
pu rpl ; b2p ¼ ek;e
pu ek;e
pu epl : ð3Þ
of free–free beam. This fitting was obtained by a least square h
k;e
h
k;e
Fig. 3. Stresses and strains derived from the S4 finite element in the layer k.
with w11 while ET and w22 were identified in the 90° direction. At last
X X X X with the previous measured values, on identification was carried
U 11 ¼ U k;e
11 ; U 22 ¼ U k;e
22 ; U 66 out for an intermediate orientation, 45° for example, to derive
elements;e layers;k elements;e layers;k
X X GLT and w66 . The use of different lengths (230, 250 and 270 mm)
¼ U k;e
66 : ð8Þ of the beams allows us to evaluate the variation of the parameters
elements;e layers;k as a function of the frequency. The results are reported in Fig. 4 for
In the same way, the total in-plane strain energy dissipated by the engineering constants and in Fig. 5 for the specific damping
damping in the finite element assemblage is derived as: coefficients.
X X The values of the Young’s moduli increase slightly with the fre-
DU ¼ wk11 U k;e k k;e k k;e
11 þ w22 U 22 þ w66 U 66 ; ð9Þ quency (0.1% to 5%) for the carbon laminates and the flax
element;e layers;k laminates.
Thus, for each natural mode, the damping of the structure into For the damping coefficients it is observed two different beha-
consideration is derived as: viours of the laminates. In fact, the damping coefficients increase
slightly with the frequency for carbon laminates while they are
DU found to decrease for flax laminates. Moreover, the damping coef-
w¼ : ð10Þ
U ficients w11 and w22 of flax fibre laminates are significantly higher
than carbon damping coefficients (from 200% to 283%) with
4. Results and discussion respect to the considered frequency domain. On the other hand,
the damping w66 of flax laminates is found to be 82% to 125% higher
4.1. Characteristics of the non-hybrid flax and carbon laminates than carbon composites. These differences could be related to the
flax fibre architecture which induces a high internal friction. The
The flax and carbon laminates are balanced orthotropic materi- morphology of flax fibre promotes dissipation of energy through
als. Thus, they are mainly characterised by two engineering con- friction between cellulose and hemicellulose in each cell wall
stants and two specific damping coefficients, measured in the and friction between the cell walls [26]. Friction processes are
material directions: the Young’s moduli along the warp and weft developed in the low frequency domain that could explain the
directions EL ¼ ET ; the in-plane shear modulus GLT ; and the damp- increase of damping in the low frequency domain. Also it has to
ing coefficients: w11 ¼ w22 and w66 . These parameters were derived be noted that the damping evolution is fairly the same for the coef-
by identification of the experimental responses of free-free beams ficients w11 , w22 and w66 . We verified that the values of the coeffi-
with the results obtained by the finite element analysis (Sections cients were independent of the amplitudes of the vibrations.
2.2 and 3). The identification in the 0° direction leads to EL and These values of the damping coefficients will be used in a finite
25.0
60 Flax laminates
55 22.5
Carbon laminates
50
EL= ET
20.0 ψ66
Specific damping ψ (%)
Young's modulus E (GPa)
45 17.5
ψ11= ψ22
40 15.0
35
Carbon laminates
12.5
30 Flax laminates ψ66
10.0
25
7.5 ψ11= ψ22
20
5.0
15
EL= ET 2.5
10
0.0
5 0 300 600 900 1200 1500 1800 2100
0 300 600 900 1200 1500 1800 2100 Frequency (Hz)
Frequency (Hz)
Fig. 5. Comparison between the values of the specific damping coefficients of non-
Fig. 4. Experimental results obtained for the Young’s moduli as a function of the hybrid carbon and flax laminates derived from the experimental investigation and
frequency for the non-hybrid carbon and flax laminates. the results obtained by the finite element analysis.
152 M. Assarar et al. / Composite Structures 132 (2015) 148–154
element analysis to estimate the damping evolution of hybrid flax– Fig. 7 reports the bending modulus as a function of the carbon
carbon composites as reported in the following section. fibre volume content of the different stacking sequences for a fre-
quency of 500 Hz. Usual results are obtained. The bending modulus
4.2. Properties of the hybrid carbon–flax laminates increases with the carbon content more especially when they are
placed as external layers of the hybrid laminates. As an example,
4.2.1. Finite element analysis of the hybrid laminates for about 15% of carbon fibre content, the increase of the bending
The procedure developed in Section 3 was applied to the differ- flexion is about 10% for [F3/C]S laminates compared to the flax
ent stacking sequences of the hybrid laminates (Table 1). The finite composites, while this increase is more than 148% for [C/F3]S
element analysis was implemented introducing in each layer of laminates.
each element the values of the Young’s moduli (EL, ET, GLT) and
the values of the damping coefficients w11 , w22 and w66 derived 4.2.3. Damping
from the finite analysis. This procedure gives the values of the nat- Fig. 8 reports the results deduced from the experimental inves-
ural frequencies and the global damping coefficients of the lami- tigation and from the modelling for different stacking sequences of
nates into consideration. Several lengths (230, 250 and 270 mm) the hybrid composites. The results are in good agreement.
of the free-free test specimens were investigated in such a way Moreover it is observed two different evolutions of the specific
to obtain the variation of the parameters with the frequency. The damping according to the stacking sequence. For the [C3/F]S,
results were also compared with the experimental results deduced [C2/F2]S and [C/F3]S laminates where the external layers are the car-
from the modal analysis of the experimental Fourier responses of bon layers, the damping coefficient is low and increases slightly
free-free beams (Section 2.3). with the frequency (Fig. 8). In fact, the energy is essentially dissi-
pated by the external carbon layers and consequently, the damping
4.2.2. Bending stiffness evolution is similar to the carbon laminates (Fig. 8). In contrast the
The natural angular frequencies of an orthotropic beam with damping decreases for the [F/C3]S, [F2/C2]S and [F3/C]S laminates
two free ends can be expressed [37,38] for the first three modes as: where the external layers are the flax layers. So, the energy is
m ¼ 1 x1 ¼ 22:373x0
m ¼ 2 x2 ¼ 61:673x0 ð11Þ
60 420
m ¼ 3 x3 ¼ 120:90x0 Carbon laminates
50
sffiffiffiffiffiffiffiffiffiffiffi [C2/F2]s
3 45 300
1 Efx h
x0 ¼ 2 ð12Þ
L 12qs 40 240
60
Carbon laminates
55
[C3/F]s
Bending modulus Efx (GPa)
50
[C2/F2]s
45
40 Experiment results
35 Modelling
30 [C/F3]s
25
[F/C3]s
20
[F2/C2]s
15 [F3/C]s
10 Flax laminates
0 300 600 900 1200 1500 1800 2100
Frequency (Hz)
Fig. 6. Comparison between the experimental results obtained for the bending Fig. 8. Comparison between the experimental results obtained for the damping
modulus of the hybrid flax–carbon laminates and the ones derived by the finite coefficients of the hybrid flax–carbon laminates and the ones derived by the finite
element procedure as functions of the frequency for different hybridations. element procedure as functions of the frequency for different hybridations.
M. Assarar et al. / Composite Structures 132 (2015) 148–154 153
20
Composite
Carbon layers Flax
18
Flax layers
16
14
12
ΔU/Utotal
10 [C/F3]s Fig. 11. Evolution of the damping and specific bending modulus according to
different stacking sequences at 500 Hz.
8
[C2/F2]s
6 Carbon [C3/F]s dissipated in the [C3/F]S and [C2/F2]S laminates are essentially
due to carbon layers: 66% to 94%. For [F/C3]S and [F2/C2]S laminates,
4
the dissipation is clearly governed by the flax layers: 90% to
2 97%.
The evolution of the damping as a function of the flax fibre vol-
0
ume content for the different stacking sequences is reported in
(a)
Fig. 10 for a frequency of 500 Hz. A significant increase in specific
20 damping is observed when the flax fibres are placed outside the
Composite
Carbon layers [F3/C]s Flax hybrid laminates. For example, the damping increases by about
18 [F2/C2]s
Flax layers 6% for the [C3/F]S laminate and 196% for the [F/C3]S compared to
16 the carbon laminates. This difference is attributed principally to
[F/C3]s the damping in carbon and flax fibres as shown in Fig. 8 and
14
already reported in the case of other traditional composites
12 [34,35].
ΔU/Utotal
10
4.2.4. Parametric study
8 The study implemented previously on the different hybrid lam-
6 inates showed that the finite element procedure allows us to
Carbon derive correctly the dynamic properties of hybrid carbon–flax lam-
4 inates. Also, this analysis demonstrated that structural damping of
2 these materials is strongly related to their bending stiffness and
dissipated energy in carbon and flax fibres.
0 Thus, a short parametric study is implemented to show how it is
(b) possible to combine both mechanical performances of carbon fibre
and interesting damping properties of flax fibres. In this
Fig. 9. Comparison between energies dissipated in carbon and flax layers of the
studied laminates at 500 Hz: (a) flax layers placed inside the carbon fibre laminates context three stacking sequences ([F/C/C/C/C/F], [C/C/F/F/C/C] and
and (b) flax layers placed outside the carbon fibre laminates. [C/F/C/C/F/C]) are analysed by the finite element procedure
(Section 2.2). For each of these stacking sequences, the total
thickness of the carbon and flax layers are 5 and 1 mm,
respectively.
Fig. 11 presents the evolution of the damping and specific bend-
ing modulus according to the different stacking sequences for a fre-
quency of 500 Hz. It is clearly observed that the addition of two flax
fibre layers to the carbon laminate increases significantly its damp-
ing by 15% to 30%. We also note that the [C/F/C/C/F/C] laminate is
very interesting in terms of rigidity and damping compared to the
[C/C/F/F/C/C] laminate. In fact, for practically the same specific
modulus as the carbon laminate, the stacking sequence
[C/F/C/C/F/C] increases its damping by about 15% vs. 2% for
[C/C/F/F/C/C].
5. Conclusion
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