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and A. Krivda
ABB Switzerland Ltd, Corporate Research, Baden-Daettwil, Switzerland
ABSTRACT
The inclined plane tracking and erosion test IEC-60587 is not specified for DC testing.
A dc test has been developed from the current ac standard and three formulations of
silicone rubber tested. These materials were tested under three voltage levels (2.3, 2.7
and 3.2 kV) for both polarities. Positive dc tests have the highest average and peak
leakage current and exhibit a higher degree of surface damage. The observed surface
degradation pattern is heavily dependant on polarity. Consistently higher levels of
erosion have been observed in the higher voltage positive cases. Erosion of the surface
always starts at the bottom electrode, and spreads toward the top electrode. Puncturing
of the 6 mm thick samples or deep erosion over more than half the distance between
electrodes has only been observed under 2.7 and 3.2 kV positive polarity tests. Results
have been analysed using a variety of leakage current analysis techniques going beyond
the criteria specified in the original ac standard. The low-frequency behaviour of the
leakage current was monitored using a 15 sample per second current recorder. The
leakage current magnitude is investigated in a case study and is shown to follow a
normal distribution. Reversing the polarity of tests shows the leakage current seen in a
test is largely independent of the surface degradation pattern present, but the surface
degradation pattern over the first three hours may dictate the morphology of ensuing
deep erosion
Index Terms — Silicone rubber, IEC 60587, dc, electrical discharge, tracking,
erosion.
There are two key processes responsible for case a test is terminated after 6 h, in accordance with test
decomposition of the SIR by rapid localised heating. method A.
Aluminium trihydrate (ATH) filler decomposes in an
endothermic reaction at around 200 C to form aluminium
oxide and water vapour. This process is said to reduce local
surface temperature and prevent damage to the base
material. At higher temperatures, the thermal
decomposition of the base material results in erosion and
leaves silica tracks, powder or char on the surface.
Meyer et al. have correlated eroded mass with
temperature using a laser ablation technique [2]. This
shows, from damage onset at approximately 300 C, there
is an exponential growth in eroded mass with temperature. Figure 1. Electrical schematic of experimental setup
Furthermore, eroded mass can be correlated directly with
the 3rd harmonic of the associated ac leakage current and
used to signify dry band arc activity [3].
Previous studies of dc tracking tests on SIR have The polarity of the supply voltage can be changed by
concluded that tracking is more severe under dc conditions reversing the orientation of the diodes. A positive voltage
than for ac [4]. Moreno et al. showed, under positive dc this test is defined as a positive potential on the top electrode
was associated with increases in magnitude and duration of and the bottom electrode at ground potential. Similarly, a
discharges [4]. There is also evidence that tracking time is negative voltage test has a negative potential on the top
less under negative dc than positive dc and the magnitude electrode and the bottom electrode remains grounded.
of current flow is higher under negative dc as compared to A detailed description of the monitoring and control
positive [5]. Investigation of wavelet transforms has shown system used in this work is given in a previous publication
that the current flow under negative dc voltage is generally [8]. As illustrated in Figure 1, the data acquisition system
less intermittent and with a higher magnitude than under captures and displays the following in real-time: supply
positive dc [6]. The work here has developed a systematic voltage, sample voltage, leakage current and a colour video
test to explore these issues further. of the test sample. A data logger, a 15 sample per second
leakage current and synchronised 3 kHz leakage current
waveform recorder, and a 15 frame per second video
2 EXPERIMENTAL recorder monitor sample activity over the test duration. The
Figure 1, shows the experimental setup, which conforms data logger records: accumulated charge, and
to IEC-60587, with the exception that a dc power source is maximum/minimum current and voltage for every minute
used. The dc is generated using a single phase full bridge period of the test. The 15 sample per second recorder
rectifier, and smoothing is provided by an 81 μF capacitor. continuously logs leakage current magnitude and sample
To ensure voltage ripple is minimised and remains below voltage for the entire six hours of a test.
the specified tolerance of 5 %, one sample is tested at a This system gives the opportunity to analyse the
time. In the above circuit, the measured voltage ripple for a electrical performance of different materials, and three
single 60 mA load through a 31.5 k resistor is 28 V or 1.5 different formulations of commercially produced SIR have
% of the supply voltage. been tested. Materials B and C are currently used as HVac
Each test is performed according to Method 1, at outdoor insulation. Material A is a variation of B with an
equivalent supply voltages to 2.5 or 3.5 kV rms [7]. The increased electrical conductivity. Material A is anticipated
equivalent dc value was calculated such that the area under to gather less surface charge, increase dc electric field
the voltage waveforms is equal for ac and dc. The dc uniformity, and be more suited to HVdc applications.
voltages are thus 2.25, and 3.15 kV dc, with the addition of The dielectric sample under test is placed on a 45 degree
an intermediate voltage of 2.7 kV dc. The corresponding angle and a contaminant made from deionised water,
series resistance values for 2.25, 2.7 and 3.15 kV dc are 11, ammonium chloride and soaping agent Triton X-100
17 and 22 k respectively. These resistors are chosen to (isooctylphenoxypolyethoxyethanol) drips down the
limit the current to 205 mA and 95 mA for the lower and underside of the sample between two electrodes, as in
higher voltage cases as in the ac method. The intermediate Figure 1. The liquid emerges from a quill hole in the top
resistance gives an intermediate current limit of 123 mA. electrode and the bottom electrode has a series of teeth to
In IEC 60587 the LC based failure conditions are when permit the passage of contaminant without a damming
60 mA ± 6 mA or more has persisted in the high-voltage effect [9].The contaminant according to IEC 60587 has a
circuit for 2 to 3 seconds, and is typically implemented by conductivity of 2532 S/cm. A voltage is applied to the top
an over-current delay relay. The cut-off for this rig is electrode from which the contaminant emerges. Flow rates
software controlled, and operated when the current is of 150, 225 and 300 l/min are used for 2.25, 2.7 and 3.15
greater than 60 mA ± 0.3 mA continuously for 2 s. In any kV dc respectively, rates also taken from IEC 60587.
IEEE Transactions on Dielectrics and Electrical Insulation Vol. 17, No. 2; April 2010 523
180.0
160.0 (a)
120.0
100.0
80.0
60.0
40.0
20.0
0.0
90.0
(b)
80.0
Figure 2. Condition of material A after: top picture 40 minutes and bottom 60.0
picture 5 hours 50 minutes, where a) +2.25 b) +3.15 c) -2.25 d) -3.15
50.0
kVDC tests
40.0
because as the material is degraded the dielectric material 30.0
surface can facilitate higher surface currents. The
20.0
measurement of total accumulated charge over the test is
highest under negative test conditions, despite the fact that 10.0
positive tests, the top positive electrode is more eroded, Material: ABC ABC ABC ABC
whereas in negative tests the bottom grounded electrode is Source: +2.25 +3.15 -2.25 -3.15
more eroded. Figure 4 shows pictures of such electrode
Figure 3. Results for +2.25, +3.15, -2.25 and -3.15 kV dc tests with
erosion after 6 h of testing at 2.7 kV dc. In Figure 4b, there materials A, B and C.
is also a solid dark layer which has built up on the bottom
electrode.
IEEE Transactions on Dielectrics and Electrical Insulation Vol. 17, No. 2; April 2010 525
Figure 4. Pictures of quill hole of top electrodes (energised) and the middle-section of bottom (grounded) electrodes a) before testing b) after a 6 hour +2.7 kV dc
test and c) after a 6 hour -2.7 kV dc test; picture widths are 18 mm
The difference in electrode mass was measured before and Given that the electrodes used are allowing a current to
after testing for the tests presented in the previous section; pass through an ionic solution, it is reasonable to assume
these data are shown in Figure 5. In positive tests, electrode the erosion process is due to electrolysis. If electrolysis is
mass loss of 10 to 35 mg has been measured at the top taking place, the mass of electrode liberated should be
(energised) electrode, whereas the negative electrode shows proportional to the total charge passed. In Figure 6a, the
an increase in electrode mass and formation of a solid dark trend line shows, this is clearly the case on the top electrode
layer as can be seen in Figure 4b. This mass increase varies under positive dc.
between individual tests and is most likely due to oxidation In Figure 3a, the cumulative charge for -3.15 kV dc is
of the stainless steel electrodes as a result of high temperature significantly greater than -2.25 kV dc. The resultant
arcing. In the negative case, erosion occurs at the bottom electrode mass loss due to electrolysis should therefore be
electrode, yet the mass of the top electrode does not exhibit higher. However, Figure 5b shows, the recorded bottom
any change. The formation of a solid dark layer on the top electrode mass loss at -3.15 kV dc is lower than at -
electrode has not been observed in any negative tests. 2.25 kVdc. This reduction is due to electrode oxidation at
40.0
35.0
(a)
30.0
Mass Loss (mg)
25.0
20.0
15.0
10.0
5.0
0.0
-5.0
-10.0
40.0
30.0 (b)
Mass Loss (mg)
20.0
10.0
0.0
-10.0
-20.0
-30.0
Figure 5. a) mass loss from top (energised) electrode b) mass loss from Figure 6. Cumulative charge versus liberated HV electrode mass for a) top
bottom (grounded) electrode. Negative mass loss implies mass gain. electrode in positive tests and b) bottom electrode in negative tests with all
materials shown
526 G. P. Bruce and S. M. Rowland: Performance of Silicone Rubber in DC Inclined Plane Tracking Tests
As the contaminant flow rate and series resistance are the surface can also change the path in which the
increased when the test voltage is increased, the average contaminant flows, which may cause periods of non-
current increases in both polarities. This increase in average conduction as happens at 3 hour 40 minutes in the positive
leakage current would suggest a more severe test, which is test shown.
reflected in the erosion depth and mass loss. The values of
peak current, intermittency and cumulative charge however
do not follow this trend. This suggests that the process by
which discharges are stabilised or extinguished and so
cause erosion may differ.
If the percentage increase in average leakage current
from negative to positive tests is compared by dividing
positive leakage current by that of negative, for 2.7, 3.15
and 2.25 kV dc the outcome is 120%, 96% and 107%,
respectively. This similarity suggests consistency in the
polarity dependant effects at each test level. To investigate
this further, the effect of HV and LV electrode reversal are
considered in section 6.1.
The cumulative charge Qm is a measure of electrical
charge that is passed by the sample in a test. In the test
measurement system it is measured by taking an integration Figure 8. Moving average of 10 of accumulated charge per minute for
of the current signal over the 6 h of the test. It may also be material C in a positive and negative polarity 2.7 kV dc test
estimated by multiplying the average LC when the sample
is conducting by the amount of time the sample is in a
conductive state as: 5.3 INTERMITTENCY AND AVERAGE LEAKAGE
CURRENT
Q c LC (1 Intermittency ) TestTime (3) Intermittency has been quantified by finding the ratio of
The estimated cumulative charge Qc from equation (3) is times when the leakage current is below and above 1mA.
14% to 16% greater than the measured value Qm in Intermittency may be regarded as the percentage of the test
positive tests, and 13% to 15% lower for negative tests. duration that the sample surface is ‘non-conductive’. This is
This may then be a useful way of estimating aggregate distinctly different in the positive and negative cases. The
charge when full instrumentation is not available. figures from 2.7 kV dc in Table 1 show, the sample surface is
non-conductive for 29% of the time under positive
conditions, and 19% of the time for negative conditions.
5.2 CUMULATIVE CHARGE Considering that the contaminant flow rate is constant and
Figure 8 shows that the magnitude of the accumulated assuming that all contaminant is evaporated, this suggests
charge per minute is higher in the positive case over the that the rate of evaporation under positive conditions is much
duration of the test, despite intermittency being 10% greater higher. The rate of evaporation being higher is also consistent
than the negative case. This is because positive average with the average surface current being higher. Possible
current is 2 times greater, and from equation 3 this would contributing factors to this are the conductivity of the
be the expected overall effect. In the first hour of the test, contaminant being affected by electrolysis, the contaminant
accumulated charge per minute increases rapidly, as this is filament having greater/smaller cross sectional area due to the
the period when the sample surface is being conditioned by geometry of the aged surface, or polarity dependence in the
the discharges. By 1 h, the pattern of surface damage looks electro-hydrodynamic behaviour of the contaminant.
quite different for each polarity. This raises the question of As in the accumulated charge plot, Figure 9a shows a
whether it is the surface degradation which dictates the rise in average leakage current at 3 h (180 minutes) in the
leakage current, or the leakage current which controls the +2.7 kV test. After the onset of deep erosion, the
surface degradation pattern. This is investigated further in intermittency begins to vary as the sample alternates
section 8.2 where polarity is changed three hours into a test. between non conductive and highly conductive states. After
Between 1 to 3 h, the accumulated charge per minute 5 hours 20 minutes (320 minutes) there is a 2 milliamp rise
increases steadily as the surface becomes more degraded. in average current and a 20% increase in intermittency.
From 3-6 h under negative conditions there is no significant Observed video images at this time, does not show if this
change in the rate of accumulated charge, however, in the particular condition gave any increased rate of damage.
positive case, there is a transition at the three hour point Because the increase in current was met by an increase in
where the rate increases by 0.1 C/minute. This occurs at the intermittency, the accumulated charge for this period
onset of deep erosion in the test, where the formation of remains fairly constant. In the -2.7 kV dc test, the average
char on the surface allows a larger volume of contaminant current is smaller in magnitude, but is also remarkably
to be retained at any one time. The result is often higher stable over the course of the test. The intermittency is also
peak currents and more damaging discharges. The char on lower than the positive case, and there are a number of
528 G. P. Bruce and S. M. Rowland: Performance of Silicone Rubber in DC Inclined Plane Tracking Tests
periods when the intermittency reduces to zero. It shows that the maximum and average leakage current in
Synchronised current and video images at 3 and 5 hours each hour of the test are greater under positive conditions,
into the test, show stable arcs, and these are perhaps the yet the ratio of maximum to mean current is much lower in
most damaging periods in the test. the positive case. This ratio is a further behavioural
difference between positive and negative conditions. The
5.4 LEAKAGE CURRENT DISTRIBUTION same result is also observed in the 2.25 and 3.15 kV dc
The leakage current distribution has been analysed by tests.
sampling the current magnitude at a rate of 15 samples per
second and plotting the information in a histogram with a
6 IMPACT OF POLARITY REVERSAL
bin range of 1mA. In
Figure 10, the first column (<1mA) shows the percentage In order to investigate some of the phenomena which
of recorded discharges where the sample surface was non- have been observed during the standardised test, two
conducting; this is the measure of intermittency. When the further types of tests were introduced: reversal of electrode
sample is conducting, the distribution of leakage current potential, and reversing polarity mid-way through a test.
magnitude follows a normal distribution. It is envisaged 6.1 REVERSED POTENTIAL TESTS
that the current follows a normal distribution because there
In the following ‘reversed potential’ tests, the bottom
are a large number of factors which contribute to its overall
electrode is energised and the top electrode is grounded as
nature.
depicted in Figure 12. The effect of this is that the potential
5.5 BOX AND WHISKER PLOTS across the sample is opposite polarity and equivalent to the
In Figure 11, the distribution of the leakage current standard opposite polarity test, however, the potential with
magnitude has been calculated in each hour of the test. This respect to external objects is changed. Results are presented
is shown as a box and whisker plot, which identifies the: from single 2.7 kV dc tests on material A.
1. Minimum current in that hour
2. Mean minus the standard deviation
3. Average current for that hour
4. Mean plus the standard deviation
5. Maximum current in that hour
Figure 10. Histogram of leakage current magnitude for (a) +2.7 kV, and
Figure 9. Intermittency (%) and average current (mA) in 10 minute (b) -2.7 kV on material C. Best fit normal distributions are shown and
intervals for (a) +2.7kVDC (b) -2.7kV dc on material C. mean (μ) and standard deviation given (σ)
IEEE Transactions on Dielectrics and Electrical Insulation Vol. 17, No. 2; April 2010 529
Figure 13. Box and whisker plots (a) +2.7kV dc normal test and (b) -2.7
kV dc reversed potential test on material A.
loss was caused in the negative to positive test. This test Neg to
Pos
10.1 45.8 27 149 159 2.4 1.2 0.02 0.004
also had higher average and peak currents than the other Pos 12.1 35 29 162 185 4.6 1.2 0.04 0.000
reversed polarity test. Similarly, electrode mass loss and Pos to 8.5 33.2 23 145 142 1.5 0.4 0.02 0.003
cumulative charge were very similar in each reversed Neg