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1 Department of Civil Engineering, King Fahd University of Petroleum & Minerals, Dhahran 31261, Saudi Arabia.
2 Department of Chemistry, King Fahd University of Petroleum & Minerals, Dhahran 31261, Saudi Arabia.
3 Operations & Maintenance, Riyadh Municipality, Riyadh, Saudi Arabia.
4 M&R Department, Ministry of Communications, Riyadh, Saudi Arabia.
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Abstract: Pavement weathering or stripping is a major distress in highway networks in arid regions. Using
the Saudi Arabian road network as a case study area, seventeen road test sections were selected, out of which
eight were stripped and nine were non-stripped. Aggregates from quarries used to build these sections were
also collected and subjected to detailed physical and chemical tests to evaluate the ability of these tests to
distinguish between stripped and non-stripped sections. The modified Lottman test was used to distinguish
between compacted mixes. In addition, the Swedish Rolling Bottle test, was also found to be effective in
being able to distinguish between different asphalt-aggregates for stripping potential. Eleven anti-stripping
liquid additives, lime and cement, in addition to two polymers, were evaluated for their ability to
reduce/eliminate stripping potential of stripping-prone aggregates. It was found that EE-2 Polymer, Portland
cement, and their combination were effective with all aggregate sources.
Pairs of low affinity will lose a large percentage of the Several methods have been developed to determine if
asphalt-aggregate interaction sites to the more polar and an asphalt concrete mix is sensitive to water. The main
hydrogen bonding water molecules. This leads to strip- methods can be summarized as follows (Terrel and Shute,
ping. Tests were devised (Curtis et al., 1993) to determine 1989; Curtis et al., 1991; Terrel and Al-Swailmi, 1992;
this important affinity or compatibility for different pairs AASHTO, 1995):
of asphalt-aggregates. If water is the cause of an asphalt- 1. NCHRP 246 – Indirect Tensile Test and/or
aggregate problem, these tests will allow one to evaluate Modulus Test with Lottman Conditioning.
the possibility of future pavement stripping based on this 2. NCHRP 247 – Indirect Tensile Test with
affinity. Tunnicliff and Root Conditioning.
When an aggregate absorbs water, the asphalt is 3. AASHTO T-283 – Combines feature of NCHRP
“stripped” away. This ultimately leads to pavement failure. 246 and 247.
Moisture degrades the integrity of an asphalt concrete 4. Boiling Water Tests.
matrix in three areas: loss of cohesive strength in the 5. Immersion-Compression Tests (AASHTO
asphalt film, failure of the adhesive bond between the T-165, ASTM D 1075).
aggregate and asphalt (stripping), and loss of the chemi- 6. Freeze-Thaw Pedestal Test.
cal bond (integrity) between the asphalt film and the 7. Static Immersion Test (AASHTO T-182,
aggregate. Other modes of pavement failure due to the ASTM D 1664).
presence of water are also possible. Water can remove the 8. Conditioning with Stability Test (AASHTO T-245).
soluble compounds from the asphalt causing it to fail. 9. Net Absorption/Desorption Test (developed
Failure within the aggregate can also occur. Water can by SHRP).
promote phase separation within the asphalt, where the 10. Environmental Conditioning System (ECS)
more polar molecules form a separate phase with water. (developed by SHRP).
A reduction in water induced damage can be achieved Pavement weathering or stripping is one of the major
by selecting asphalt-aggregate pairs of high affinity, mod- distresses in the highway network in the case study area,
ifying the aggregate surface through silylation, or adding the Kingdom of Saudi Arabia. Pavement stripping severi-
antistripping agents. Building roads with low air voids and ty varies from region to region in the Kingdom. The high-
good drainage reduces water-induced damage by limiting way network in Al-Qassim and Hail regions is the most
the exposure to water. affected by pavement stripping. In certain roads where
The pH of the medium can also affect the asphalt-aggre- maintenance programs are not efficient, stripping develops
gate bond. It was found (Curtis et al., 1993) that a high pH potholes that severely affect road performance. The water
(basic or alkaline environment) is detrimental to most sensitivity test used in local road departments is the typi-
asphalt-aggregate bonds. Additives such as lime or some cal water conditioning and evaluation by the Marshall sta-
liquid anti-stripping agents can improve the performance bility test. The conditioning phase includes partial satura-
of some asphalt-aggregate pairs in highly basic environ- tion of specimens with asphalt and then soaking in a water
ments. bath. The specimens are then tested for Marshall stability
Among the many factors that contribute to the degrada- and compared with the results of unconditioned speci-
tion of asphalt concrete pavements, moisture is a key ele- mens. If the ratio (condition divided by unconditioned) is
ment in the deterioration of the asphalt mix. Since the less than 75%, the mixture is considered sensitive to water.
1930s, pavement engineers have been working to deter- Those roads experiencing stripping and weathering have
mine the moisture sensitivity of asphalt concrete mixtures. all passed the water sensitivity test. This has indicated that
Since that time, numerous tests have been developed to the water sensitivity test using Marshall stability is not
identify moisture-susceptible asphalt concrete mixtures. In reliable in determining the sensitivity of asphalt mixtures
general, there are two categories into which the water sen- to water. With the recent developments in the design and
sitivity tests can be divided. The first category includes evaluation as a result of strategic highway research pro-
tests which coat “standard” aggregates with asphalt gram (SHRP), the Ministry of Transport (MOT) in the
cement. In these tests, the loose mixture is immersed in case study area has adopted a Superpave mix design that
water, either at room temperature or at boiling tempera- utilizes a gyratory compactor. The northern part of the
ture, and a visual evaluation is made of the separation of study area is mostly affected by this phenomenon due to
asphalt from the aggregate. The second category includes the existence of water sensitive aggregates.
those tests that use compacted specimens, either laborato- The overall objective of this paper was to assess strip-
ry compacted or cores from existing pavement structures ping problems in arid regions using the highway network
(Terrel and Shute, 1989). These specimens are then water of Saudi Arabia as a case study. Secifically, current prac-
conditioned to simulate the in-service conditions of the tices by road agencies were reviewed and the tests used
pavement structure. The results of these tests are general- by these agencies were included in the test program.
ly evaluated by the ratios of conditioned to unconditioned Binder aggregate adhesion and susceptibility of that adhe-
results using a stiffness or strength test, such as the diame- sion to water damage were analyzed. Comprehensive tests
tral resilient modulus test. that predict the resistivity of asphalt-aggregate materials
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
(individually or as a mix) were adapted or modified. Task 2: Stripping test selection and evaluation: Different
Practical treatment methods were suggested to improve tests (physical and chemical) that might be used to detect
stripping resistance of local mixes. susceptibility of pavement mixes and/or materials to strip-
ping were evaluated (Table 1). Construction materials
2. Methodology (fresh aggregates, slabs, and cores) from known perform-
ance road sections were collected, in consultation with
The work was carried out in three tasks and extended government personnel. These materials were subjected to
for 30 months. different tests to evaluate their ability in predicting strip-
ping potential. A total of seventeen test sections were
Task 1: Literature review: Available literature from main selected: eight stripped and nine unstripped.
research institutions locally and abroad related to the sub- In selecting the study sections several criteria had to
ject of the research were collected, summarized, and uti-
lized to support the knowledge of the researchers in this be met Adequate drainage had to be present for the
field. pavement surface. Construction had to be according to
specifications, (i.e. percent air voids (AV%) had to be
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
NUMBER OF REPLICATES
Volumetric Properties
3 3 3 . 3 3 3 3 . 3 3 3 3 . 3 3 3 3 . 3
Environmental Conditioning
System (ECS) 2 2 2 . 2 2 2 2 . 2 2 2 2 . 2 2 2 2 . 2
within design limits, compaction temperature within second phase of the study.
allowable limits, no overheating of asphalt, aggregate gra-
dation within limits). Aggregate quarry used for supplying Task 3: Material collection, mix designs and evaluation:
aggregate in the asphaltic concrete layers had to be known In the second phase, different additives that are known
and active so that fresh aggregate could be obtained sim- from literature of being useful in preventing stripping
ilar to that used in the section. were collected and used with the collected aggregate from
The collected materials were subjected to a number of stripped sections to prepare asphalt mixes using different
chemical and physical evaluation tests to evaluate the abil- percentages of additives and combinations. The Marshall
ity of those tests to predict stripping. These tests included mix design procedure was used to determine the optimum
compacted mix evaluation methods such as environmental asphalt content for each aggregate source as shown in
conditioning system (ECS), modified Lottman test and Table 1. Different percentages of anti-stripping agents (as
Marshall durability test.; Asphalt/aggregate blend evalua- recommended by the manufacturer) were added to each
tion methods such as net adsorption in the presence of mix. Mixes were evaluated using the stripping tests.
moisture and the Swedish Rolling Bottle test and aggre-
gate tests such as methylene blue value (MBV), soundness 3. Results and Discussion
and physical properties.
Experimental design for the first phase of the project
is shown in Table 2. The response variables measured on As an initial step in the statistical analysis, the normal-
individual materials, mixtures, compacted specimens, ity assumption of the distribution of the test results was
pavement cores were used for selection of applicable checked by drawing normal probability plots of the data.
physical and/or chemical tests that are able to predict strip- The statistical data analysis was then carried out in three
ping and used for evaluation of the different mixes in the stages.
In stage I, the preliminary analysis, was to confirm that
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
ANOVA analysis was performed for the test results of tistical evaluation was performed on the test results of the
the extracted field cores as shown in Table 2. Results indi- fresh aggregate and the laboratory prepared mixes, Table
cated that at α = 0.05 (the higher the α value, the lower the 2. Table 3 shows only tests that were significant and that
significance of the difference), for all the performed tests, had a P-value (Probability to reject Ho when Ho is true)
except the ECS, the means of the stripped and non- less than 0.05 in differentiating between mixes that were
stripped sections were significantly different. This prone to stripping from sound mixes (Lapin, 1997). The
implied that the tests were capable of differentiating most significant test in predicting stripping (having the
between stripped and non-stripped sections and therefore smallest P-value) was the loss in split tensile strength
indicated a good matching between the classification of when performed on gyratory compacted samples that had
the different sections into stripped and non-stripped sec- 7 ± 1% air voids followed by vacuum saturation then soak-
tions and the test results. ing at 60°C for 24 hours (i.e. modified Lottman test). The
Stage II was to find which of the laboratory tests was other tests in a decreasing order of significance were:
capable of predicting the stripping potential of the asphalt Marshall stability test; split tensile strength of Marshall
concrete mixes. Therefore, the single factor ANOVA sta- compacted specimens soaked @ 60°C for 24 hours after
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
ITERLENE
58.40% 79.20% 100.0% 100.0% 51.20%
IN/400-S
CECABASE®
40.54% 55.80% 100.0% 47.6% 48.00%
260
POLYRAM®
44.30% 72.90% 100.0% 100.0% 53.00%
L200
ITERLENE
45.80% 76.80% 100.0% 100.0% 53.70%
IN/400
ITERLENE
32.59% 57.40% 100.0% 100.0% 44.50%
IN/400-R
ITERLENE
52.80% 86.40% 100.0% 69.0% 32.40%
IN/400-R-1
MORELIFE
21.54% 67.80% 100.0% 31.7% 36.60%
3300
EE-2
28.75% 32.30% 35.8% 41.9% 42.40%
Polymer
% loss of 100 means that conditioned samples have collapsed, resulting in ITS of zero and 100% ITS
vacuum saturation; resilient modulus of Marshall com- ulus of gyratory prepared samples having a target air void
pacted specimens soaked @ 60°C for 24 hours after vacu- between 6 and 8% after two cycles in ECS; Loss of
um saturation; split tensile strength of Marshall compact- resilient modulus of gyratory prepared samples having a
ed specimens soaked @ 60°C for 24 hours without vacu- target air void between 6 and 8% after three cycles in ECS;
um saturation; resilient modulus of gyratory prepared and Swedish Rolling Bottle value after 12 hrs. rolling.
samples having a target air void between 6 and 8% after Although all tests were statistically significant, it can
one cycle in ECS; aggregate soundness test; resilient mod- be seen that they can be divided into three groups: com-
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
pacted mix, asphalt/aggregate blend and aggregate. From adopting the Superpave mix design. This will eliminate
the first group, it can be seen from Table 3 that both the the use of the Marshall mix design. Lottman, on the other
modified Lottman test (AASHTO T-283) and the Marshall hand, is a simple test that has proven effectiveness and is
stability loss test (MOT-MRDTM 410) had the lowest dis- currently used widely in the United States. The Lottman
criminant probability P-value of 4.6E-09 as compared to a test was therefore selected as the best mix evaluation test
P-value of 9.4E-08 for Marshall stability loss. Moreover, to discriminate between compacted mixes. The Swedish
the government in the case study area is in the process of Rolling Bottle test was the only one in the second group
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
that was significant (P=.02715) in evaluating loose aggre- trol mix (no additive). It should be noted that 100% ITS
gate-asphalt blends stripping tendencies. In the third loss indicated that samples failed during the conditioning
group, aggregate soundness, which was a significant test phase ,indicating severe stripping. This resulted in a final
(P=0.0023), had the ability to distinguish between aggre- ITS of zero and therefore a 100 % ITS loss.
gates prone to stripping. This test, however, did not have Table 6 shows the results of the combined additives. In
the capability to evaluate additives to asphalt mixes and general, it can be seen that the ITS of each mix was
therefore was eliminated. dependent on the aggregate type. The results of the second
Stage III was to find the test limits that could be set to phase indicated that for Hail aggregate, treatments
screen mixes that were prone to stripping. This was based EC9194A, Iterlene IN/400, Iterlene IN/400-R, Polyram
on the test results of the fresh aggregate and the laborato- L200, CECABASE 260, WETFIX BE, Lilamin VP 75E,
ry prepared mixes. Specification limits were calculated for Morelife 3300, EE-2 Polymer, cement, and lime were
each of the significant tests. These limits could then be effective in eliminating the stripping potential of the
used to test if the mix was prone to stripping (i.e. if the aggregate. For Al-Jouf aggregate, only EE-2 Polymer and
result of the evaluation test was higher than the set limit, cement were effective in eliminating the stripping poten-
then the mix would be prone to stripping). Assuming a tial of the aggregate. For Eastern Province aggregate, only
normal distribution of the results, the average and standard WETFIX AD-4F, EE-2 Polymer, and cement were the
deviation values for the samples Table 3, were used to find effective additives. With the Riyadh aggregate, only
the test limits. The aim was to find the limit that would Morelife 3300 and EE-2 Polymer were effective addi-
produce an equal probability of classifying the mix as not tives. The EE-2 Polymer was effective in eliminating the
being prone to stripping if the test value was lower than stripping potential of all aggregates from all sources.
the limit, to the probability of classifying the mix as being Eastman EE-2 Polymer and Portland cement and their
prone to stripping if the test value was higher than the combination proved to be effective with all studied aggre-
limit. For example, Table 3 shows that for the modified gate sources. Morelife 3300 antistripping additive com-
Lottman test (AASHTO T-283) and the Marshall stability bined with cement was the most effective with Riyadh and
loss test (MOT-MRDTM 410), the discriminating limits Hail aggregates. WETFIX AD-4F combined with cement
were 48% and 25%, respectively. was the most effective with the Eastern Province aggre-
In addition to lime and cement dust, several liquid anti- gate. Finally CECABASE 260 combined with cement
stripping agents were purchased and specifications of the was effective with the Al-Jouf aggregate.
products as provided by the companies were also obtained, For each type of aggregate, there were specific addi-
Table 4. tives that were effective in eliminating the stripping poten-
The Marshall mix design was used to arrive at the opti- tial. However, cement and EE-2 Polymer combinations
mum asphalt content for the four selected stripped loca- were effective in eliminating or effectively reducing the
tions. Eleven liquid antistripping agents were collected stripping potential of all the tested aggregates.
from the original manufacturers and administered at the
maximum recommended percentage. Moreover, cement, 4. Conclusions
lime and two polymers (Polybilt 101 and Eastman EE-2)
were used at a dosage of 4% as recommended by govern- Based on the Analysis of Variance (ANOVA) results,
ment guidelines and polymer manufacturers. Work was the modified Lottman test, the Marshall stability loss test,
carried out in two stages. The maximum recommended Environmental Conditioning System (ECS), and the
dosages of the antistripping additives were used to quanti- resilient modulus loss were effective in distinguishing
fy the effect of the additive on stripping phenomena and to between stripped and non-stripped mixes. ECS had the
screen the additives, Table 5. In the second stage , addi- lowest significance (P = .00082) among these tests while
tive combinations of promising mixes were evaluated. the modified Lottman had the highest significance (P =
Combinations included dry additives (Portland cement 4.6E–09). The Swedish Rolling Bottle was found to be
and/or lime) and liquid additives or polymers. Liquid addi- effective in screening asphalt-aggregate materials for
tives were not mixed with polymers. This was done to stripping potential. Eastman EE-2 Polymer and Portland
avoid adverse chemical reactions, Table 6. The modified cement and their combination proved to be effective with
Lottman test and the Swedish Rolling Bottle test were all studied aggregate sources. Morelife 3300 anti-stripping
used to evaluate the effectiveness of the different treat- additive combined with cement was the most effective
ments. with Riyadh and Hail aggregates. WETFIX AD-4F com-
Table 5 shows the typical stage I test results for the bined with cement was the most effective with the Eastern
Hail, Al-Jouf, Eastern Province and Riyadh region. The Province aggregate. CECABASE 260 combined with
results show the loss in the indirect tensile strength values cement was effective with Al-Jouf aggregate.
(ITS), according to the modified Lottman test procedure,
for all treatment combinations. The effectiveness of the Acknowledgements
treatments was evaluated based on the level of ITS
improvement for each aggregate as compared to the con- The authors would like to acknowledge the support
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Abdul Wahhab et al. / The Journal of Engineering Research 1 (2004) 29-38
of KACST for funded this project, KFUPM for provided Curtis, C.W., Ensley, K., and Epps, J., 1993,
the research facility, and MOT for provided the logistical “Fundamental Properties of Asphalt-Aggregate
support in selecting and sampling test sections. Interactions Including Adhesion and Absorption,”
Strategic Highway Research Program Publication,
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