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SUBMITTER

Business company: Výzkumný ústav anorganické chemie, a. s. (hereinafter referred to


as VÚAnCh)
Address: Revoluční 84, 400 01 Ústí nad Labem
Represented by: Ing. Milan Petrák, Board Vice-Chairman; and Ing. Lubomír Lukáč,
Board Chairman
Telephone no.: 475 309 222
CRN/VAT NO.: 62243136 / CZ62243136, VAT payer
Bank connection: Komerční banka Ústí nad Labem; account no.: 7009 – 411/0100

ORDER DOCUMENTATION

FOR OFFER PLACEMENT


FOR AN EXCESS PUBLIC CONTRACT
In compliance with Act no. 137/2006 Coll., on public contracts, as amended (hereinafter
referred to as the ‘ZVZ’).

1. Information on the type, subject, and distribution of public contract.

Public contract’s name: „Experimental units for UNICRE project”


Expected value: 67 000 000 CZK, without VAT
Public contract type: Public contract for deliveries
Tender result: Signing a contract with a selected applicant
Public contract characteristics: Excess public contract
Tender type: Open
Code of public contract's subject
In compliance with CPV classification: 38970000-5 Research, testing and scientific technical
simulators
Accepting offer varieties: NO
Dividing contract into parts: NO

2. Submitter’s contact data:


Key contact person: RNDr. Michal Ottis
E-mail: michal.ottis@vuanch.cz
Telephone no.: +420 475 309 219

Key contact person deputy: Bc. Milada Pucová


E-mail: milada.pucova@vuanch.cz
Telephone no.: +420 475 309 219

For electronic communication, the submitter recommends communicating with both contact
persons.

Postal address for the delivery of all shipments from the applicant to the submitter
throughout the entire tender:

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Výzkumný ústav anorganické chemie, a. s.
Revoluční 1521/84
400 01 Ústí nad Labem
Telephone no.: +420 475 309 219, +420 475 309 222
Fax: +420 475 212 079
E-mail:michal.ottis@vuanch.cz,
milada.pucova@vuanch.cz

3. Deadline and place for offer submission

Deadline for offer submission: Until 12:00 on 08/22/2013

Place of offer submission:


Výzkumný ústav anorganické chemie, a. s.
Revoluční 1521/84
400 01 Ústí nad Labem
The above address applies on personal deliveries: 1. floor; office 202 (Director's Secretariat)

Offer may be submitted in person, on workdays from 08:00 to 15:00; on the last day of offer
submission deadline from 08:00 to 12:00. If delivered otherwise, the submitter must receive
the offer by 12:00 on the last day of the deadline in the latest.

The moment of offer reception by the submitter is decisive for offer delivery. If delivered by
postal services, or other similar way, the moment of offer delivery to the submitter is crucial,
not the date of offer submission to the postal service, etc.

4. Requirements on Proving the Meeting of Qualification Requirements

The submitter requires for an applicant to prove he meets the qualifications within the
following scope:

- Basic qualification requirements;


- Professional qualification requirements;
- Economic and financial capability to fulfil the contract;
- Technical qualification requirements.
4.1. Basic qualification requirements
Basic qualification requirements are met by an applicant who:
4.1.a) Has not been lawfully sentenced for: a crime committed on behalf of an
organised criminal group; the crime of participating in a criminal group;
legalisation of earnings from criminal activities; criminally elicit gains;
accepting of a bribe; bribery; indirect bribery; fraud; a credit fraud; including
cases of either preparation or attempt or participation in such a crime; or if his
criminal records, regarding such a crime, were erased. In case of a legal entity,
this precondition must be met by this legal entity and by it´s statutory body or
each member of the statutory body. If is statutory body of supplier or member
of statutory body of supplier a legal entity, this assumption must fulfil statutory

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body or each member of statutory body of this legal entity. If the offer or a
request to participate submit foreign entity through its branch must this
assumption, according this paragraph, fulfil in addition to these person also
leaders of this branch. This basic qualification assumption must a supplier fulfil
both to the relationship to the territory of the Czech Republic and to the
country of its place of residence, place of business or address.

4.1.b) Has not been lawfully sentenced for: a crime, facts of which are related to the
subject of applicant's business in compliance with special legal regulations; or
his criminal records, regarding such a crime, were erased. In case of a legal
entity, this precondition must be met by this legal entity and also by it´s
statutory body or each member of the statutory body. If is statutory body of
supplier or member of statutory body of supplier a legal entity, this assumption
must fulfil statutory body or each member of statutory body of this legal entity.
If the offer or a request to participate submit foreign entity through its branch
must this assumption, according this paragraph, fulfil in addition to these
person also leaders of this branch. This basic qualification assumption must a
supplier fulfil both to the relationship to the territory of the Czech Republic and
to the country of its place of residence, place of business or address.

4.1.c) Has not, within the last 3 years, fulfilled the body of a crime of unfair
competition in the form of bribery in compliance with a special legal
regulation,

4.1.d) Has not had, within the past 3 years, his property in bankruptcy proceedings, in
which a bankruptcy decision was issued, or a bankruptcy proposal was not
rejected because the property does not cover the bankruptcy proceedings costs;
or the bankruptcy was cancelled because the property was completely
insufficient; or sequestration was applied incompliance with special legal
regulations.

4.1.e) Is not in a bankruptcy.

4.1.f) Has no tax arrears recorded in the tax registers in the Czech Republic; place of
his residence, business, or address;

4.1.g) Has no arrears of premium and penalty for public health insurance in the Czech
Republic; place of his residence, business, or address.

4.1.h) Has no arrears of premium and penalty for the social security scheme and
contributions for state employment policy in the Czech Republic; place of his
residence, business, or address.

4.1.i) Has not been, in the past 3 years, lawfully punished by disciplinary measures,
or lawfully inflicted a disciplinary punishment in compliance with special legal
regulations. If the applicant performs this activity via an authorised
representative, or another person responsible for applicant’s actions, this
precondition applies on these persons.

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4.1.j) has not listed in the register of person banned from public contracts

4.1.k) has not been fined in the past three years for allowing illegal work in
accordance to a special law regulation.

The applicant proves the fulfilment of basic qualification requirements in compliance


with points 4.1.a) and 4.1.b) with a copy of an extract from the Criminal Records;
which must not be older than 90 calendar days at the date of offer.

The applicant proves the fulfilment of basic qualification requirements in compliance


with points 4.1.c) to e), g), i), to k), and partially 4.1.f) (concerning consumer tax
declaration) with applicant’s affidavit submitted in the form of a consolidated
affidavit, binding template of which represents Annex to this order documentation.
The consolidated affidavit must not be older than 90 calendar days at the date of offer.
The consolidated affidavit must be signed by either the applicant or his authorised
representative.

The applicant proves the fulfilment of a part of the basic qualification requirement in
compliance with point 4.1.f) (concerning all tax arrears, except for consumer tax
arrears) with a copy of a confirmation by respective tax office; the confirmation must
not be older than 90 calendar days at the date of offer.

The applicant proves the fulfilment of basic qualification requirements in compliance


with point 4.1.h) by submitting a copy of a confirmation by respective body or
institution, which must not be older than 90 calendar days at the date of offer.

4.2. Professional qualification requirements

Basic qualification requirements are met by an applicant who:

- Submits an extract from Commercial Register, if he is registered there or


extract from similar register in which he is registered.

- Proof of business license according to a special law in the range corresponding


to a subject of the tender, in particular a document proving the trade licence or
another licence

The applicant proves the fulfilment of professional qualification requirements in


compliance with point 4.2. with a copy of an extract from the Companies Register or
another register in which he is registered. The extract from the Companies Register or
another register must not be older than 90 calendar days at the date of offer.
.

4.3. Economic and financial qualification requirements

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According § 50 par. 1 Czech Law on Public procurement as amended an applicant
proves it by affidavit – see Appendix No. 1

4.4. Technical qualification requirements:


Professional qualification requirements are met by an applicant who:

4.4.a) has, within the past 3 years, implemented minimum of 3 deliveries of


experimental units for testing of catalytic processes with the total amount of
over 200.000€ for each delivery or the equivalent in another currency. Amount
is calculated according to data from Czech National Bank on the date of the
tender announcement.

4.4.b) has an implementation team consisting of people authorised to provide


activities in question within range defined; while per equipment offered, the
applicant has at least 1 an engineer who:
- Has practical experience with service activities, regarding given type of
equipment, of a minimum of 3 years.
- Is adequately authorised to perform service activities on given equipment
type; if such an authorisation is required by either legal regulations or
manufacturer.
- Is able to provide a phone consultation in Czech, Slovak or English.

The implementation team will consist of applicant’s employees, or people working for
the applicant based on a contractual relationship. At least one member of the team
must be able to provide a telephone consultations and communicate in Czech, Slovak,
or English.

The applicant will prove the fulfilment of technical qualification requirements in


compliance with point 4.4.a) by submitting of a List of Important Deliveries, which is
part of Declaration on Technical Qualification Preconditions, binding template of
which is an Annex No 2 to this order documentation.

Annex to the above given List must consist of:

- Certificate issued by a public submitter, if services were provided to a public


submitter, or
- Certificate issued by another person, if services were provided to a person
other than a public submitter, or
- Contract with another person and proof of transaction, if it is not at the
same time possible to get certificate, according to the previous indent, from
this person.
The applicant proves the fulfilment of technical qualification requirements in
compliance with point 4.4.b) by submitting of a List of People Responsible for
Providing of Activities in Question.

Annex to the above given List and Affidavit must consist of:

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- Valid certificate authorising a specific team member to perform service
activities on a respective type of laboratory device.

4.5. Submitting Document Original Copies

Before signing a contract, applicant selected must, on submitter’s request, submit


either original copies or officially authenticated copies of documents proving the
meeting of his qualification.

4.6. Power of Attorney

If the applicant gives power of attorney to an agent to sign the offer, contract draft, or
another part of applicant’s offer, the offer must include a power of attorney, either the
original copy or an officially authenticated one, entitling the agent to perform such tasks.

4.7. Changes to Qualification

If a supplier not longer fulfil the qualification before decision about the most suitable offer
a supplier must to report this fact to submitter in writing form within seven working days.
Supplier is obligated to submit a necessary documents proving fulfilment with the full
qualification to submitter to ten working days from the notification of this fact. If the
supplier require it, the submitter can to extend the deadline or he can forgive him a missed
deadline.

This obligation is similarly applied to an applicant with whom it is possible to enter into a
contract in accordance with a submitter´s decision according § 81 ZVZ, until the moment
of signing a contract. In such a case an applicant, with whom the submitter enters into a
contract, must submit necessary documents proving fulfilment with the full qualification.
The latest date is signing of a contract.

4.8. Deadline for Qualification Proving

Applicant must prove he meets the qualification within the deadline for offer submission.

4.9. Proving the Meeting of Qualification by a Foreign Applicant

Unless otherwise resulting from a special legal regulation, a foreign applicant proves
qualification meeting by a procedure in compliance with the legal system valid in the
country of his residence, place of business, or address; within the range required by the
submitter. If, based on the legal system valid in the country of residence, place of business,
or address of a foreign applicant a certain document is not issued, the foreign applicant
must prove the meeting of such part of the qualification by an affidavit. If an obligation,
the fulfilment of which is to be proven within the qualification, is not defined in the
country of residence, place of business, or address of a foreign applicant, he makes an
affidavit on such a fact. Unless an international contract binding for the Czech Republic

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says otherwise, a foreign applicant submits the documents proving the fulfilment of
qualification in the original language, with their officially authenticated Czech translation
attached. This applies even if an applicant with residence, place of business, or place of
permanent residence within the Czech Republic proves his meeting of the qualification
with documents in language other than Czech. The obligation of attaching an officially
authenticated Czech translation to the documents does not apply on documents in Slovak.

See Anex No. 1b

4.10. Sub-suppliers

If an applicant cannot prove the full meeting of a part of qualification required by the
submitter (except for proving of the basic qualification requirements and submitting of an
extract from the Companies Register, which must always be proven by the applicant) he
has a right to prove the missing scope of qualification fulfilment via a sub-supplier. In
such a case, the applicant must present the submitter with:

- A document proving the fulfilment of the basic qualification requirement in


compliance with art. 4.1.j) by the sub-supplier and
- A document proving the fulfilment of the professional qualification requirement in
compliance with art. 4.2.a) by the sub-supplier and
- A contract signed with the sub-supplier, from which a commitment is resulting for
the sub-supplier either to provide performance intended for applicant’s fulfilment
of the public contract; or to provide things or rights, the applicant will have
available within the fulfilment of the public contract; at least in the scope in which
the applicant's qualification fulfilment was proven.

4.11. Combined Offer

Should the subject of the public contract be performed by several suppliers together;
and they either intend to submit or submit a combined offer for the purpose, each
supplier must prove their fulfilment of basic qualification requirements, and
professional qualification requirement in compliance with point 4.2.a) of this order
documentation within full extent. The meeting of other qualification requirements in
compliance with points 4.3. and 4.4. here of must be proved by all suppliers together.

Should the subject of the public contract be performed by jointly by several suppliers,
together with the documents proving the fulfilment of qualification requirements, they
must all present the submitter with a written contract containing the following
commitment: to both the submitter and third parties, incurred by any legal relations
created in connection to the public contract, all of these applicants will be committed
jointly and severally, throughout the entire period of public contract fulfilment, as well
as during the period of duration of other commitments resulting from the public
contract.

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4.12. Other Qualification Requirements
Concerning other issues, applicants’ rights and obligations as regards to proving of
qualification fulfilment are subject to respective ZVZ resolutions.

5. Brief description of the order; obligations and role of the contractor (applicant)

5.1 Technical specification of the Experimental units of the tender documentation


„Experimental units for UNICRE project“.
5.1.a) Testing units for hydrodesulfurization (HDS) and hydrocracking (HC)
The delivery has to include the following parts:
1a. 2 reactors for HDS catalyst screening
1b. 2 reactors for HDS catalyst testing
1c. 3 reactors for HC catalyst testing

General description
The units/reactors will be used to study HDS and HC catalysts, effects of reaction
conditions, feedstocks etc. on the performance of such catalysts at operating
conditions similar to industrial ones.
The reactors have to be tubular allowing placement of a catalyst fixed bed, isothermal
operation and the use of the following media: hydrogen, hydrogen sulfide, nitrogen,
air and hydrocarbons.

Reactors and Units layout


It is allowed to combine the required reactors into units but it is necessary to keep the
reactors independent with the possibility to operate them in a parallel mode. Each of
the reactors should therefore be equipped with independent feed lines as well as the
product (sampling) lines.
A big advantage of a unit is the possibility to operate reactors of the same type also in
series (it means 2-stage modes for 1a and 1b or 3-stage mode for 1c) as specified in
the following chapter.

Operating conditions
1a. “2 reactors for HDS catalyst screening”

Feedstock:
- Atmospheric gas oils, vacuum gas oils, light cycle oils, gas oil from visbreaking,
vegetable oils, etc.
- Kinematic viscosity at 40 °C ca. 2.5-5 mm2/s.
Operating conditions for each of the reactors:
The combination of max. pressure + max. temperature must be possible.

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Min Max Typical
Pressure (MPa) 15 4
Temperature (°C) 450 370
Catalyst bed volume (mL) 5 15 10
LHSV (Liquid Hourly (h-1) 0.4 8 0.5 - 3
Space Velocity )
H2/Hydrocarbons (LN/L) 100 1000 300-500

1b. “2 reactors for HDS catalyst testing”


Feedstock:
- Atmospheric gas oils, vacuum gas oils, light cycle oils, gas oil from visbreaking,
vegetable oils, etc.
- Kinematic viscosity at 40 °C about 2.5-5 mm2/s.
Operating conditions for each of the reactors:
The combination of max. pressure + max. temperature must be possible.

Min Max Typical


Pressure (MPa) 15 4-7
Temperature (°C) 450 370
Catalyst bed volume (mL) 150 350 200
LHSV (Liquid Hourly (h-1) 0.4 8 0.5 – 3
Space Velocity )
H2/Hydrocarbons (LN/L) 100 1000 300-750

1c. “3 reactors for HC catalyst testing”


Feedstock:
- Vacuum distillates: straight-run, visbreaking, vegetable oils and fats, etc.
- Kinematic viscosity at 100 °C about 5-10 mm2/s.
Operating conditions for each of the reactors:
The combination of max. pressure + max. temperature must be possible.

Min Max Typical


Pressure (MPa) 20 15-20
Temperature (°C) 450 380-420
Catalyst bed volume (mL) 100 150 130
LHSV (Liquid Hourly (h-1) 0.4 8 0.5 – 3
Space Velocity )
H2/Hydrocarbons (Nl/l) 150 1500 500-1000

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Description of an experimental unit
The experimental unit consists of:

- gas line
- liquid feeding line
- reactor
- reactor heating
- separation part
- sample collection system
- gas outlet
- controlling system

Gas line
The gas sources are nitrogen and hydrogen, high pressure (20 MPa), technical grade
supplied to the testing facility. The controlling devices (mass-flow controllers and
pressure regulation) have to be independent; the feeding line could be shared.
The gas lines have to be fitted by a manual stop-valve, filter, and pressure reducing
device, pressure gauge and mass flow controller. The possibility of automatic shut-
down of gas supply is necessary.
The manufacturer’s technical solution must ensure that liquid feed cannot enter the gas
lines.
Requirements - Mass Flow Controller operating range
Hydrogen 0-50 Nl/h or 0-300 Nl/h depending on the unit dimensions
Nitrogen 0-50 Nl/h or 0-300 Nl/h depending on the unit dimensions

The specifications mentioned in chapters 1a., 1b. and 1c. must be taken into
consideration. If it is necessary for the accuracy and reliability of the measurement
more than one Flow Controller or its appropriate part must be supplied.

Flow measurement accuracy


1% of the full scale

Liquid feeding line


The feeding line consists of liquid feedstock container, stop-valve, pump, pressure
gauge, stop-valve and possibility of pumping outside the feeding line (cleaning, etc.).
For the reactors 1c the feed container and feeding lines have to be heated up to at least
80°C with the possibility of setting the temperature in the range from 50°C to max.
temperature.
The container should be outfitted by inert blanket. The pump (or pumping system) has
to ensure smooth, pulseless and accurate feed flow.

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A separate container and feed line for a sulfiding agent (for example
dimethyldisulfide) is an advantage.
Requirements - Container
Volume 10-15 L (2-5 L for sulfiding agent)

Pump
Flow rate according to the reactor volume and LHSV (0-120 or 0-2000 mL/hour).
Heated in the case of unit 1c, flow rate for unit 1c is 0-1200 mL/h).

Reactors

The reactors have to be tubular allowing placement of a catalyst fixed bed, isothermal
operation and the use of following media: hydrogen, hydrogen sulfide, nitrogen, air
and hydrocarbons.

Handling with reactor, catalyst loading and un-loading should be easy, safety
precautions are vital. These solutions are a part of the manufacturer’s technical design.
Reactor should be easily removable from the furnace, e.g. to be loaded outside the
unit.

The temperature inside of each reactor has to be monitored at least in 6 points of


catalyst bed by sensors placed in a thermowell.
Volumes, etc. are specified in the section “Operating conditions”.
Reactor heating
Preferred is electrical heating, at least 3 independent sections with minimal
temperature deviation. It has to allow isothermal profile along the reactor.
The reactor heating design is a part of the manufacturer’s technical design.
Separation part
The separation part should consist of two separators – a high-pressure separator and a
low-pressure separator.
High-pressure separator
The reaction mixture (gas and liquid) from reactor outlet is led to the high pressure
(HP) separator.
The HP separator has to be designed for efficient separation of the gas and liquid
phases while minimizing the amount of liquid fraction carried away in form of mist.
The separator should be equipped with a level control and possibility of
cooling/heating by external apparatus/source.
The gas phase is withdrawn continuously (controlled by pressure regulator) via a
scrubber containing NaOH (H2S absorption), a gas meter with thermocouple and
pressure transmitter (necessary for the mass balance). The important part of the gas

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line is a sampling valve for automatically sampling of gas by on-line gas
chromatography (GC). The GC will be connected subsequently.
The liquid phase is withdrawn automatically (continuously) to the low-pressure
separator.
Main characteristics of HP Separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-100°C

Low-pressure separator
The liquid products from the high-pressure separator are led to the low-pressure (LP)
separator.
The products are purged by nitrogen or hydrogen to remove H2S and lighter fractions.
The gaseous stream could be led to the gas phase line from high-pressure separator or
by a separate line. In the case of the separate line it has to be equipped with the same
necessary components as the gas line from HP.
The liquid products from the low-pressure separator are withdrawn by a sample
collecting system.
Main characteristics of LP Separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-100°C (temperatures below 0°C are an advantage)
Sample collecting system
The liquid products are withdrawn continuously by an automatic sampling system to
ensure unattended operation for at least 24 hours.
The automatic sampling system shall allow collecting sample for various time periods.
For the reactors 1a (catalyst screening) it shall be from 2 to 8hours, for the reactors 1b
and 1c it shall be from 2 to 8 hours too. The frequency of sampling and capacity of the
product container should be combined according to the “Typical” operating conditions
stated in the tables above.
All the parameters have to be designed according to reactor volume and unit design.

5.1.b) Testing units for sulfur-free processes


2a. “2 reactors for catalyst screening”
2b. “2 reactors for catalyst testing”

General overview
These units/reactors will be used to study catalysts, reaction conditions, feedstock etc.
for sulfur-free feedstock and processes (hydrogenation, alkylation, isomerization, etc.).
The reactors have to be tubular allowing placement of a catalyst fixed bed, isothermal
operation and the use of following media: hydrogen, nitrogen, air, water (steam) and
hydrocarbons.

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Reactors and Units layout
It is allowed to combine the required reactors into units but it is necessary to keep the
reactors independent with the possibility to operate them in a parallel mode.
A big advantage of a unit is the possibility to operate reactors of the same type also in
series (it means 2-stage modes for 2a and 2b).

Requirements and specification


The reactors and units are the same as described in chapter 1. for reactors 1a (2a) and
1b (2b) with the exception of presence of sulfur compounds, sulfiding agent tank and
H2S scrubber that are not needed for the units of type 2 (sulfur-free).
Pumps have to be utilizable also for the liquefied gas (C3 to C4) feed from pressurized
tank (up to 2 MPa – the tank is not included in the delivery). Therefore it is desirable
that the pump heads can be optionally cooled by external cooling apparatus (part of
delivery).
Liquid feeding line
The liquid feedstock container should be a closed vessel which can be optionally
pressurized by inert gas up to 1 MPa.
5.1.c) Testing unit for high-temperature processes
General overview
The unit/reactor will be used for dealkylation (catalytic or non-catalytic),
dehydrogenation and transalkylation reactions to study kinetics, catalysts, reaction
conditions, feedstock etc. at operating conditions similar to the industrial ones.
The reactors have to be tubular allowing placement of a catalyst fixed bed, isothermal
operation and the use of following media: hydrogen, nitrogen, air and hydrocarbons.

Operating conditions
Feedstock:
- Light hydrocarbon fractions to medium distillates
- Kinematic viscosity at 25 °C max. 7 mm2/s.
Operating conditions:
Min Max Typical
Pressure (MPa) 10 5
Temperature (°C) 650 600
Catalyst bed volume (mL) 100 200 180
Flow rate - feedstock (mL.h-1) 20 500 200
Flow rate - H2 (LN.h-1) 0 600 400

Description of an experimental unit


The experimental unit consists of:
- gas line

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- liquid feeding line
- reactor
- reactor heating
- separation part
- sample collection system

Gas line
The gas sources are nitrogen and hydrogen. The gas lines have to be fitted by manual
stop-valve, filter, and pressure reducing device, pressure gauge and mass flow
controller. The possibility of automatic shut-down of gas supply is necessary.
Hydrogen line has to be high pressure (20 MPa), hydrogen is technical grade supplied
to the testing facility.
Nitrogen line is necessary as a source of inert for starting up the process and catalyst
conditioning and reduction.
The manufacturer’s technical solution must ensure that liquid feed cannot enter the gas
lines.
Requirements - Mass Flow Controller flow-rate
Hydrogen 0-600 LN/h
Nitrogen 0-600 LN/h
Hydrocarbons 0-50 LN/h

The specifications mentioned in chapter “Operating conditions” must be taken into


consideration. If it is necessary for the accuracy and reliability of the measurement
more than one Flow Controller or its appropriate part must be supplied.
Flow measurement accuracy
1% of the full scale

Liquid feeding line


The feeding line consists of liquid feedstock container, balance, stop-valve, pump,
pressure gauge, stop-valve and possibility of pumping outside the reactor (cleaning,
etc.).
The container should be outfitted by inert blanket and placed on a balance connectible
to a computer. The pump (or pumping system) has to ensure smooth, pulseless and
accurate feed flow.
Requirements - Container
Volume 10-15 L
The liquid feedstock container should be a closed vessel which can be optionally
pressurized by inert gas up to 1 MPa.
Balance

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Capacity according to the container and feedstock mass, accuracy 0.1 g.
Pump
Flow rate 0-500 mL/h.
Pump has to be utilizable also for the liquefied gas (C4 hydrocarbons) feed from
pressurized tank (up to 1 MPa – the tank is not included in the delivery). Therefore it
is desirable that the pumps heads can be optionally cooled by external cooling
apparatus (part of delivery).
Reactor
The reactors have to be tubular allowing placement of a catalyst fixed bed, with the
possibility to adjust isothermal axial temperature profile along the catalyst bed when
being run with inert media without chemical reaction. The use of following media is
supposed: hydrogen, nitrogen, air and hydrocarbons.
Handling with reactor, catalyst loading and un-loading should be easy, safety
precautions are vital. These solutions are part of the manufacturer’s technical design.
Reactor should be easily removable from the furnace, e.g. to be loaded outside the
unit.
The temperature inside of reactor has to be monitored at least in 6 points in the axis of
the catalyst bed by sensors placed in a thermowell.
Volumes, etc. are specified in the section “Operating conditions”.
Reactor heating
Electrical furnace, at least 3 independent sections with minimal temperature deviation.
It has to ensure isothermal axial profile along the reactor without chemical reaction.
The reactor heating design is a part of the manufacturer’s technical design.
Separation part
The separation part should consist of two separators – a high-pressure separator and a
low-pressure separator.
High-pressure separator
The reaction mixture (gas and liquid) from the reactor outlet is led to the high pressure
(HP) separator, after being cooled down to a desired temperature.
The HP separator has to be designed for efficient separation of the gas and liquid
phases while minimizing the amount of liquid fraction carried away in a form of mist.
The separator should be equipped with a level control and possibility of
cooling/heating by an external apparatus/source.
The gas phase is withdrawn continuously through a back pressure regulator and a gas
meter equipped with a thermocouple and a pressure transmitter (necessary for the mass
balance). The important part of the gas line is a sampling valve for automatically
sampling of gas by on-line gas chromatography (GC). The GC will be connected
subsequently.

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The liquid phase is withdrawn automatically (continuously) to a low-pressure
separator.
Main characteristics of HP Separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-100°C
Low-pressure separator
The liquid products from the high-pressure separator are led to the low-pressure (LP)
separator.
The products can be optionally purged by nitrogen or hydrogen to remove lighter
fractions. The gaseous stream could be led to the gas phase line from high-pressure
separator or by separate line. In the case of a separate line it has to be equipped with
the same necessary components as the gas line from HP.
The liquid products from the low-pressure separator are withdrawn by a sample
collecting system.
Main characteristics of LP Separator:
Material, pressure, capacity – according to the reactor volume and unit design
Operating temperature 25-50°C
Sample collecting system
The liquid products are withdrawn continuously by an automatic sampling system to
ensure unattended operation for at least 24 hours.
The automatic sampling system allows collecting sample for various time periods
from 2 to 6 hours.
All the parameters have to be designed according to the reactor volume and unit
design.
The separation and collecting system has to enable accurate mass balance.

5.1.d) Testing unit for catalytic combustion and reduction processes


General overview
The unit/reactor will be used for studies of selective reduction, catalytic combustion,
DeNOx, etc. reactions and to study kinetics, catalysts, reaction conditions, feedstock
etc.

Operating conditions
Feedstock:
- Liquid: hydrocarbons, oxygenates, water,
- Kinematic viscosity at 25 °C max. 7 mm2/s.
- Gas: N2, NOx, N2O, NH3, air.

Page 16 (total 40)


Operating conditions:
Min Max Typical
Pressure (MPa) 1.5 1
Temperature (°C) 650 450
Catalyst bed volume (mL) 10 20 18
Flow rate - feedstock (mL.h-1) 0 100
Flow rate - gas (LN.h-1) 0 2000

Description of an experimental unit


The experimental unit consists of:

- gas line
- liquid feeding line
- reactors
- reactors heating
- separation part
- liquid collecting vessel

Gas line
The gases are specified above (in operating conditions).
The gas line have to be fitted by manual stop-valve, filter, and pressure reducing
device, pressure gauge and mass flow controller. The possibility of automatic shut-
down of gas supply is necessary.
The selected gas will be fed from gas cylinder (max. pressure 2 MPa) or from sources
of technical grade (N2) supplied to the testing facility.
The manufacturer’s technical solution must ensure that liquid feed cannot enter the gas
lines.
Requirements
Mass Flow Controller flow-rate: 0-2000 LN/h N2
Mass Flow Controller flow-rate: 0-50 LN/h NOx
Mass Flow Controller flow-rate: 0-50 LN/h NH3
Flow measurement accuracy: 1% of the full scale

If it is necessary for the accuracy and reliability of the measurement more than one
Flow Controller or its appropriate part must be supplied.

Liquid feeding line


The feeding line shall consist of at least two parts.

Page 17 (total 40)


The first line is intended to feed water, the second one for hydrocarbons. Each line has
to be fitted by feedstock container, balance, stop-valve, pump, pressure gauge, stop-
valve and possibility of pumping outside the feeding line (cleaning, etc.).
The container for hydrocarbons should be outfitted by inert blanket and placed on a
balance. The pump (or pumping system) has to ensure smooth, pulseless and accurate
feed flow.
Requirements
Container
Volume min 1 L
Balance
Range according to the container and feedstock mass, accuracy 0.1 g.
Pump
Flow rate min. 0-100 mL/h.

Reactors
There shall be two reactors in series
The reactors have to be tubular allowing placement of an inert material or catalyst
fixed bed, isothermal operation and the use of above specified gases and feeds.
An excellent resistance to high-temperature, oxidative and corrosive environment is
expected.
The first reactor is used for vaporization of the liquid feed and proper mixing of the
gaseous phase. The second reactor is for catalytic reactions.
Handling with reactors, catalyst (or inert material) loading and un-loading should be
easy, safety precautions are vital. These solutions are a part of the manufacturer’s
technical design. Reactor should be easily removable from the furnace, e.g. to be
loaded outside the unit.
The temperature inside of the reactors has to be monitored at least in 6 points of the
catalyst bed by sensors placed in a thermowell.
Volumes, etc. are specified in the section “Operating conditions”.
Reactors heating
Electrical furnace, at least 3 independent sections with minimal temperature deviation.
It has to ensure isothermal profile along the reactor.
The reactor heating design is a part of the manufacturer’s technical design.
Separation part
The separation part should consist of two separators – a gas/liquid phase separator and
a sulfur-removing vessel. Due to possibility of presence ammonium sulfide all the
lines should be heated to 80-100°C.
Gas/liquid phase separator

Page 18 (total 40)


The reaction mixture from reactor outlet is led to the gas/liquid separator.
The separator has to be designed for efficient separation of the gas and liquid phases
while minimizing the amount of liquid fraction carried away in form of mist. The
separator should be equipped with a level control and possibility of cooling/heating by
external apparatus/source.
The gas phase is withdrawn continuously (by pressure regulator) to the sulfur-
removing vessel.
The liquid phase is withdrawn automatically (continuously) to a liquid collecting
vessel.
Main characteristics of the gas/liquid phase separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-100°C
Sulfur-removing vessel
The gas phase is recovered from gas/liquid separator to sulfur-removing vessel and
then is continuously led via a gas meter with thermocouple and pressure transmitter
(necessary for the mass balance). The important part of the gas line is a sampling valve
for automatically sampling of gas by on-line gas chromatography (GC). The GC will
be connected subsequently.
The liquid phase is withdrawn automatically (continuously) to a liquid collecting
vessel.
Main characteristics of the vessel:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-50°C
Liquid collecting vessel
The liquid products are withdrawn continuously by an automatic sampling system to
ensure unattended operation for at least 24 hours.
The automatic sampling system allows collecting sample for various time periods
from 2 to 8 hours.
All the parameters have to be designed according to reactor volume and unit design.
The separation and collecting system has to enable accurate mass balance.
5.1.e) Testing unit for adsorption and desorption processes

Page 19 (total 40)


General overview
The unit will be used for study of adsorption/desorption processes in both - gas and
liquid phase. The possibility of up-flow and down-flow testing is required including
the possibility to alternate adsorption and desorption cycles in one test.
Adsorption will be performed at various conditions (pressure, temperature, time, etc.)
and desorption will be realized by changes in temperature or pressure or displacement
by gas or liquid compounds.

Operating conditions
Feedstock:
- Liquid: hydrocarbons, oxygenates, water
- Kinematic viscosity at 25 °C max. 7 mm2/s.
- Gas: light hydrocarbons, N2, ammonia, hydrogen sulfide, air, oxygenates
(alcohols).

Operating conditions:
Min Max Typical
Pressure (MPa) 0 10 7
Temperature (°C) ambient 400 150
Adsorbent volume (mL) 100 200 150
Flow rate - feedstock (mL.h-1) 50 300 100
Flow rate - N2 (LN.h-1) 50 1000 300
Testing of the real particles is supposed and it is necessary to offer reactor with
minimal internal diameter 25 mm.

Description of an experimental unit


The experimental unit consists of:

- gas lines
- liquid feeding line
- reactors
- reactors heating
- separation part
- sample collection system

Gas lines
At least 3 gas lines are required.
First line is intended for desorbant. The second line is for high-pressure nitrogen to
produce steam or evaporate the hydrocarbon adsorbant, or for ammonia or for
hydrogen sulfide. The third line is for low-pressure nitrogen to purge the unit; at the
same time it could be a source of inert gas for feedstock container.

Page 20 (total 40)


The gas lines have to be fitted by manual stop-valve, filter, and pressure reducing
device, pressure gauge and mass flow controller. The possibility of automatic shut-
down of gas supply is necessary.
Nitrogen will be from gas cylinder or technical grade from pilot plant installation.
The manufacturer’s technical solution must ensure that liquid feed cannot enter the gas
lines.
Requirements
Mass Flow Controller flow-rate
Desorbant, high-pressure, 50-500 LN/h
Nitrogen, high-pressure, 50-1000 LN/h
Ammonia, high-pressure, 50-500 LN/h
Hydrogen sulfide, high-pressure, 50-500 LN/h
Nitrogen, low-pressure, 0-1000 LN/h
Flow measurement accuracy
1% of the full scale

Liquid feeding lines


2 feeding lines have to be installed. Each line consists of liquid feedstock container,
balance, stop-valve, pump, pressure gauge, stop-valve and possibility of pumping
outside the feeding line (cleaning, etc.).
The containers should be outfitted by inert blanket and placed on a balance. The pump
(or pumping system) has to ensure smooth, pulseless and accurate feed flow.
Requirements
Container
Volume 7-10 L
Balance
Range according to the container and feedstock mass, accuracy 0.1 g.
Pump
Flow rate min. 50-500 mL/h.

Reactors
Two reactors are supposed.
The reactors have to be tubular allowing placement of an inert material or catalyst
fixed bed, isothermal operation and the use of above specified gases and feeds.

Page 21 (total 40)


In the first reactor vaporization of the liquid feed and proper mixing of the gaseous
phase have to be carried out. The second reactor is for adsorption processes. The
construction has to allow using only one reactor or both reactors in serial mode.
Handling with reactors, catalyst (or adsorbent) loading and un-loading should be easy,
safety precautions are vital. These solutions are a part of the manufacturer’s technical
design. Reactor should be easily removable from the furnace, e.g. to be loaded outside
the unit.
The reactors must be designed for the simple switching between the up-flow and
down-flow modes.
The temperature inside of the reactors has to be monitored at least in 6 points of the
catalyst (adsorbent) bed inside a thermowell.
Volumes, etc. are specified in the section “Operating conditions”.
Reactors heating
Heating by electrical furnace is supposed, at least 3 independent sections with minimal
temperature deviation. It has to ensure isothermal profile along the reactor.
The reactor heating design is a part of the manufacturer’s technical design.
Separation part
The separation part should consist of two separators – a high-pressure separator and a
low-pressure separator. For the processing gaseous products only, the direct sampling
(without passing through the separators, by-pass) must be possible.
High-pressure separator
The reaction mixture (gas and liquid) from reactor outlet is led to the high pressure
(HP) separator.
The HP separator has to be designed for efficient separation of the gas and liquid
phases while minimizing the amount of liquid fraction carried away in form of mist.
The separator should be equipped with a level control and possibility of
cooling/heating by external apparatus/source.
The gas phase is withdrawn continuously (by pressure regulator).
The liquid phase is withdrawn automatically (continuously) to the low-pressure
separator.
Main characteristics of HP Separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-100°C
Low-pressure separator
The liquid products from the high-pressure separator are led to the low-pressure (LP)
separator.

Page 22 (total 40)


The products are purged by nitrogen to remove lighter fractions.
The gaseous stream is withdrawn continuously via a gas meter with thermocouple and
pressure transmitter (necessary for the mass balance). The important part of the gas
line is a sampling valve for automatically sampling of gas by on-line gas
chromatography (GC). The GC will be connected subsequently.
The liquid products from the low-pressure separator are withdrawn by a sample
collecting system.
Main characteristics of LP Separator:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 25-50°C
Sample collecting system
The liquid products are withdrawn continuously by an automatic sampling system to
ensure unattended operation for at least 24 hours.
The automatic sampling system allows collecting sample for various time periods
from 2 to 6 hours.
All the parameters have to be designed according to reactor volume and unit design.
The separation and collecting system has to enable accurate mass balance
5.1.f) Testing unit for upgrading of crude-oil residual fractions and their
mixtures with bio-products
General overview
The unit/reactor will be used for thermal and catalytic cracking of long residues,
vacuum distillates, bio-oils, and their mixtures with the content of inhomogeneous
particles. The objective of studies will be kinetics, catalysts, reaction conditions,
feedstock etc. at various operating conditions.
The reactor has to be tubular allowing placement of a catalyst fixed bed, isothermal
operation and the use of following media: hydrogen, hydrogen sulfide, nitrogen, air
and hydrocarbons.

Operating conditions
Feedstock:
- Vacuum distillates, long residues bio-oils, and their mixtures with the content of
inhomogeneous particles.
- Kinematic viscosity at 100 °C max. 10 mm2/s.

Operating conditions:
Min Max Typical
Pressure (MPa) 20 2 or 18
Temperature (°C) 500 450

Page 23 (total 40)


Catalyst volume (mL) 50 150 100
Flow rate - feedstock (mL.h-1) 0.5 50 25
Flow rate - H2 (LN.h-1) 0 300 100

Description of an experimental unit


The experimental unit consists of:

- gas line
- liquid feeding line
- reactor
- reactor heating
- separation part
- sample collection system

Gas line
The reaction gas is hydrogen. The gas line has to be fitted by manual stop-valve, filter,
and pressure reducing device, pressure gauge and mass flow controller. The possibility
of automatic shut-down of gas supply is necessary.
To purge the unit nitrogen supply is necessary as a source of inert gas for feeding line,
the nitrogen line can be low-pressure (0.5 MPa) with safety precautions to prevent
feed or hydrogen leakage from high-pressure section.
The manufacturer’s technical solution must ensure that liquid feed cannot enter the gas
lines.
Requirements
Mass Flow Controller flow-rate
Hydrogen 0-300 LN/h
Nitrogen 0-100 LN/h
Flow measurement accuracy
1% of the full scale

Liquid feeding line


The feeding line consists of liquid feedstock container, balance, stop-valve, pump,
pressure gauge, stop-valve and possibility of pumping outside the feeding line
(cleaning, etc.).
The container has to be outfitted by inert blanket and placed on a balance. Presence of
inhomogeneous particles in feed is probable so the mixing of feed container must be
ensured. The pump (or pumping system) has to ensure smooth, pulseless and accurate
feed flow even in presence of particles in feed.
Because of the higher viscosity of the feed the container, pump and feeding line have
to be heated to min. 120 °C.

Page 24 (total 40)


Requirements
Container
Volume 10-15 L
Balance
Range according to the container and feedstock mass, accuracy 0.1 g.
Pump
Flow rate min. 0-50 mL/h.
Reactor
The reactor/reactors have to be tubular allowing operating without or with fixed bed of
catalyst, isothermal operation and use of the following media: hydrogen, hydrogen
sulfide, nitrogen, air and hydrocarbons.
The reactions will be carried out at high temperatures and it is supposed that there will
be pre-heating reactor or section.
Handling with reactor, catalyst loading and un-loading should be easy, safety
precautions are vital. These solutions are a part of the manufacturer’s technical design.
Reactor should be easily removable from the furnace, e.g. to be loaded outside the
unit.
The temperature inside of reactor has to be monitored at least in 6 points of the
catalyst bed by sensors placed in a thermowell.
During high-temperature processing of residues and mixtures with particles the
increasing of pressure drop (coke formation) along the reactor is expected so its
measurement is necessary.
Volumes, etc. are specified in the section “Operating conditions”.
Reactor heating
Electrical furnace, at least 3 independent sections with minimal temperature deviation,
is desired. It has to ensure isothermal profile along the reactor.
The reactor heating design is a part of the manufacturer’s technical design.
Separation part
The separation part should consist of three separators – two high-pressure separators
and one low-pressure separator.
High-pressure separators
The reaction mixture (gas and liquid) from reactor outlet is led to the first high
pressure (HP) separator.
The HP separator has to be designed for efficient separation of the gas and liquid
phases at high temperatures (200-350 °C) while minimizing the amount of liquid

Page 25 (total 40)


fraction carried away in form of mist. The separator should be equipped with a level
control and possibility of cooling/heating by external apparatus/source.
The liquid phase is withdrawn automatically (continuously) to the collecting system.
The gas phase is withdrawn continuously to the second HP separator cooled to 40-70
°C. Design of the separator has to ensure efficient separation of the gas and liquid
while minimizing the amount of liquid fraction carried away in form of mist.
The gas phase is withdrawn continuously (controlled by pressure regulator) via a
scrubber containing NaOH (H2S absorption), a gas meter with thermocouple and
pressure transmitter (necessary for the mass balance). The important part of the gas
line is a sampling valve for automatically sampling of gas by on-line gas
chromatography (GC). The GC will be connected subsequently.
Main characteristics of HP Separator 1:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 200-350°C
Main characteristics of HP Separator 2:
Material, pressure, capacity – according to reactor volume and unit design
Operating temperature 40-70°C
Sample collecting system
The liquid products are withdrawn continuously by an automatic sampling system to
ensure unattended operation for at least 24 hours.
The automatic sampling system allows collecting sample for various time periods
from 2 to 6 hours.
All the parameters have to be designed according to reactor volume and unit design.
The separation and collecting system has to enable accurate mass balance.

5.2. Control system


The control system has to allow unattended operation of the each unit.
It should consist of two parts – (i) control cabinet with interface for communication and (ii)
workstation (PC) with control software. The workstation has to provide full access to all
operating parameters and programming and at the same time enable transfer of data and
communication with the Central control system. The Central control system will be
specified and connected later (communication standard OPC) but it will control the main
operating parameters and store all the data from all units. In the case of shutting down the
Central system there has to be an automatic switch to workstation and possibility of
operating the units via corresponding workstations.

Page 26 (total 40)


5.3. Workstation
Supplied software and hardware must be compatible with the supplied device.

5.4. Basic infrastructure of the pilot plant facility


Hydrogen
Purity: technical grade
Pressure: 28 MPa
Nitrogen
Purity: technical grade
Pressure: 32 MPa
Air
Purity: technical grade
Pressure: 0.4 MPa
Other Gases in cylinders
Cooling water
Temperature range: 10-25 °C
Max available flow: ca 750 L/hr
Pressure: 0.4 MPa
Electricity
230 V / 400 V
Testing reactors/units location
The units will be placed in the 3 temperated rooms with entrance doors 2.5 m height and 2 m
width. Dimensions of the rooms are (width x length x height, in meters): 13.5 x 3 x 6, 4.5 x 3
x 6, 4.5 x 3 x 6. Layout of the reactors/units must be discussed with submitter’s specialists.

5.5. Main features of the units


Units design has to be in conformity with EU directives and CE marked.
There is a non-explosion proof environment in the pilot plant facility.
Unattended operation for more than 24 hours.
Possibility of free-standing placement.

Page 27 (total 40)


Material: at least SS 316, where it is necessary (high-temperature unit) – using of material
with better resistance.
Electrical specification: 50 Hz, 400 volts, 3 phase system
The units have to be connectible to the Central control system (communication standard
OPC). The Central control system will be specified and connected later (see 5.2).

5.6 Safety
As was partly described in technical specification the units must confirm high requirements
for safety operation for long period of time. The safety precautions must include at least:
- unit producer’s alarms that disable exceeding technical manufacturing parameters
of the unit (e.g. pressure higher than 20 MPa or temperature higher than 550°C in
some units),
- software warnings (visual and acoustic) based on low-high parameters set by
operator or supervisor,

- solving serious unpredictable changes in unit run (gas leakage, feeding


interruption, sudden pressure drop, etc.) - automatic action shut down the unit to a
pre-determined safe (stand-by) mode,

- PC or software failure,

- emergency stop button,

- mechanic precautions – rupture discs, emergency valves, etc.


- two levels of alarm during the unattended period of operation: 1. Set-point not
achieved – an alarm to operator on-call to make an adjustment, 2. Serious
malfunction – automatic shutdown of the unit.
The list above cannot fully specify all the failures and situations. The safety precautions are
an inseparable part of the manufacturer’s technical design.

5.7. Apart from the usual components, the following represent an inseparable part of the
delivery, and price, of the equipment.

Documentation
Detailed instructions for use and software in either Czech or English; and basic instructions
for use in Czech.
Respective certificates authorising use within the CR, i.e. the usual certificates issued by
respective state test dept. in an EU country, etc. These documents must be translated into
Czech.
Data sheets and drawings for units and their parts (design, layouts, piping, vessels,
connections, electrical design, etc.…).
Temperature profiles of each reactor at operating conditions.

Page 28 (total 40)


Stability (diagram) of feedstock pump in the range of operating conditions.
Stability (diagram) of mass flow of gases in the range of operating conditions.

Installation
Prior to installation the layout of the units in the pilot plant facility, all the necessary
connections, interfaces and adjustments will be discussed with submitter’s responsible
persons. Supplier is responsible for:
- delivery to the place of installation including unpacking and movements,
- interconnections (ca. 10-15 meters) to the basic infrastructure of the pilot plant
facility (media, electricity, flue gas, etc., see 5.5).
START-UP procedure
The start-up operations will be started after successful installation. The main aim is to verify
that all the necessary steps for the reliable experiments were done.
The testing procedures will include at least:
- check pressure leakage with real gas (hydrogen, nitrogen, etc. with max. leakage
0.03 MPa/hour)
- testing of pumps, gas and liquid circulation,
- testing the communication between the unit devices and controlling system by the
testing of all the operating parameters.
Training
The on-site training will be performed by supplier’s qualified technical staff with real
feedstock, gases and operating parameters. Duration for each unit will be min. 5 working days
and it must include at least:
- description and demonstration of the complete documentation for unit, devices
(valves, controllers, etc.), and all the important parts
- practical demonstration and training of all common activities (reactor assembly,
catalyst bed preparation, disassembly, etc., min. 1 day/unit)
- basic and advanced maintenance
- troubleshooting and emergency shutdown procedures
- assisted run for min. 24 hours (continuously)

30 days after installation, putting in use all the units and submitter’s confirmation of the
contract fulfillment another 7 days of on-site training will carry out. The program of this
training will be according to the submitter’s requirements.

5.8 Warranty service


Warranty service for the experimental units and all the parts, software, controlling computer,
monitor, and all service, verification, and calibration activities; and both spare parts and
consumables delivered. Supplier’s warranty is set to 24 months from submitter’s acceptance.
Testing unit warranty further applies to all service, verification, and calibration activities; and
all spare parts and consumables delivered. In case of a repair within warranty period, the
warranty period is extended by the time of repair duration, i.e. by the time from defect
reporting to its removal. If a warranty repair takes more than 2 months, or the total time of

Page 29 (total 40)


repairs within one year exceeds 3 months, the submitter is authorised to demand new
equipment, its part, or defective unit, be delivered by the supplier.
Warranty service must guarantee the commencement of service action within 5 work days
from defect reporting by the submitter; spare parts delivery within 10 work days from the time
when the applicant's service engineer identifies the need for a part delivery; and defect
removal within 4 weeks from its reporting.
Supplier's guarantee of ensuring both spare parts and consumable supplies for 10 years from
fist device installation.
Remark: Service activities not included in the subject of the public order, chiefly consisting of
device adjustments on submitter’s request; and removal of defects, which the warranty does not
apply on, caused by submitter’s employees. These activities will be performed ad hoc based on
individual orders by the submitter.

5.9 More Information on the Tender

The deliveries of devices and activities related, based on the above stated, are part of the
implementation of the UniCRE Project – Unipetrol construction of a research-educational
centre, implemented within Operating Programme Research and Development for
Innovations (VaVpI), from European Regional Development Fund, via Ministry of
Education, Youth, and Sports of the CR.

Throughout public contract implementation, continuous communication is expected between


the applicant and the submitter; as well as performing of individual tasks ensuring proper
delivery and services based on submitter’s instructions.

Terms of trade of implementation of this public contract are defined in a binding contract
template, which is part of this order documentation.

6. Time and Place of Performance:

Time of Performance: Performance in compliance with art. 5.1. to 5.7 herein –


Expected date of delivery: between November 2013 and
September 2014. Delivery may be divided into several parts.
Performance in compliance with art. 5.8 herein – from the date
of installation the experimental unit

Place of Performance: UniCRE premises in Chempark Záluží u Litvínova

7. Expected Tender Schedule:

Call for offer placement –


Commencement 7/25/2013
instruction release
Offer accepting Termination 8/22/2013
Envelope opening Deadline 12:00 on 8/22/2013

Page 30 (total 40)


Commencement 5/31/2013
Selecting the most suitable offer
Termination c. 6/30/2013
Negotiating contract signing with Commencement Immediately after the most suitable
selected applicant offer is selected
Contract signing Termination Expected on 7/31/2013
Commencement
Order implementation See art. 5 and 6 hereof
Termination

8. Further Tender Terms

8.1 Providing of order documentation

Order documentation, consisting of this document with all its annexes, will be
available on submitter’s web pages.

8.2. Additional Information on Order Terms

In compliance with § 49 ZVZ, an applicant is entitled to required written additional


information on the order terms; simultaneously, the submitter is entitled to provide
additional information even without prior request from an applicant.

8.3 Offer Price Processing

All prices in the offer will be given in Czech Crowns, as:

 Maximum price of experimental units described in this documentation, art.


5.1. to 5.3, including related deliveries of materials, services within the scope
specified in articles 5.4. to 5.5 and another components specified in article 5.7.
hereof. The offer price must apply to all deliveries and services within a
specific performance for the entire period of tender implementation, including
all costs and expenses incurred to the applicant in relation to the
implementation of this part performance.

Total offer price must not be exceeded and must be guaranteed as the highest
permissible price throughout all time of realization. The only regulation of offering
price can be made on the base of changing the VAT rates.

8.4 Terms of Trade and Contract Template

Terms of trade that are not specifically defined in the text hereof are defined in the
contract template attached to this order documentation.

8.5 Offer Options

Submitter accepts no offer options.

Page 31 (total 40)


8.6 Limitation to Offer Submission

Each applicant has a right to submit only one offer (either individually or as a
combined offer by several people) for each tender part.

No submitter employees may be involved in offer processing and consequent


providing of services.

If these rules are breached, the submitter rejects all offers submitted in such a way,
consequently excluding the applicant from the tender.

8.9. Tender Deadline

Tender deadline starts running at the moment the deadline for offer submission is over,
and in compliance with § 43 art. 2 ZVZ; it is set for a period of 90 days.

8.10. Security

Submitter does not require security for an advance.

8.11. Working Language

Working language of tender in question is Czech or English.

8.12. Sub-deliveries

In the offer, an applicant must declare which parts of the public contract performance
he intends to submit to sub-suppliers; and provide identification data for each sub-
supplier. A sub-supplier is not entitled to entrust another subject with implementing
the part of the public contract performance entrusted to him. The applicant submits
contracts entered into between the applicant and a sub-supplier within the proving of
qualification fulfilment in case he proves qualification fulfilment within missing range
via a sub-supplier. Other terms as regards to the sub-deliveries are defined in the
contract template.

8.13 Applicant’s Expenses

The submitter does not grant the applicant a right for compensation for expenses
related to participation in the tender even if the tender is cancelled in compliance with
The Public Procurement Act. Simultaneously, the submitter will not demand
compensation for expenses for tender implementation from an applicant; not even in
the form of settlement of actual expenses, or by tender participation fees from
applicants.

Page 32 (total 40)


9. Requirements on Offer Processing

9.1. Envelope with Applicant’s Offer

The contractor submits his offer in a non-transparent, closed, intact envelope, or other non-
transparent, closed, intact packaging, with distinctive designation: ‘Experimental units for
UniCRE project’, appeal ‘DO NOT OPEN’, applicant’s name and delivery address. The
envelope, or other package, will be adequately secured against opening (envelope seams must
be glued and stamped or otherwise designated with applicant’s identification data).
Such a secured envelope must contain 2 separate files - an original and a copy of applicant’s
offer (sheets of each file must be connected so that sheets cannot be exchanged during
handling); and a loosely enclosed CD-ROM.

9.2 Binding Contents of Applicant’s Offer


File designated as ‘Offer’ must contain:
a) Front page
(Front page stating the tender name; clear designation of tender part for which
the offer is submitted; ‘original copy/copy' designation; applicant’s
identification; applicant's name/firm; offer contents; and signature of either the
applicant of his authorised representative.)
b) Applicant’s Identification
(A document containing basic applicant information. A binding form for this
document is in Annex no. 3 herein.)
c) Powers of Attorney
(Applicant submits these only if a document within the offer contains a
signature representing the applicant, or another person, based on power of
attorney.)
d) Offer Price
(A separates sheet stating offer price for subject of performance specified in
point 8.3 hereof.)
e) Technical Specification of Machines Offered
(Separate folder meeting the specifications of a specific device.) Applicant
submits given document within structure and scope allowing the submitter to
define, without any doubts, whether the machine set offered meets submitter's
requirements stated in points 5.1 to 5.3; while given requirements are
considered the minimum, and must be met within at least the level stated.
Providing further technical specifications of the device is up to individual
applicants.
f) Description of Service Activity Assurance
(Separate offer folder within which the applicant describes the method of
organisation of both service and support activities he is prepared to ensure for
the submitter; especially regarding number of available service workers;
speed; and response to submitter’s requirement concerning the
implementation of a service task; and other possible parameters and services
related. The submitter notes that the Description Of Service Activity
Assurance must fully respect all relevant terms of fulfilment given in the

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contract template. A conflict with terms given in contract template represents
a reason for excluding applicant’s offer and his exclusion from the tender.)
g) Contract Draft
(Draft of contract on implementation of delivery and services related,
correspondent to the binding contract template hereof, completed with relevant
data at designated places. Contract draft must be signed by either the applicant
or his authorised representative).
h) Sub-delivery Information
(Submitted by the applicant only if he intends to entrust some performance parts to a sub-
supplier. Parts of public contract performance that the applicant intends to entrust to
specific sub-suppliers will be specified in the list. The document must contain
identification information of all sub-suppliers; and percentage of sub-supplier’s
performance share in the total public contract, i.e. the total offer price).
i) Submits a list of statutory bodies, or their members, who have, in the past three years,
worked for the submitted.
j) If he constitutes a joint stock company, he must submit an up-to-date list of shareholders
owning over 10% of stock.
k) Statement about prohibited agreements
An applicant´s statement that he did not and will not enter into a prohibited agreement
according a special law in connection with the award of a public contract

9.3. Binding Contents of Documents Proving Qualification


The folder must contain Documents proving the meeting of qualification requirements (see
respective regulations hereof, including possible contracts with sub-suppliers or contracts
between suppliers submitting a joint offer.)

9.4. Contents of CD - ROM


This is a data carrier containing a complete offer of an applicant, including all attachments,
in electronic form. The data carrier must be secured against rewriting. CD-ROM data must
be ordered into individual files based on “Qualification” and “Offer”

9.5. Offer Language


All of the above mentioned documents are to be in Czech (Slovak) or English language (or a
foreign language with an officially authenticated translation); Except for English expert
expressions used in a relevant field, those commonly used in the CR.

10. Reasons for Offer´s and Applicant´s Exclusion

10.1. General Reasons for Exclusion

Submitter may exclude applicant’s offer form the tender, and exclude the applicant
immediately if:

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a) In his offer, the applicant does not submit all documents required by the order
documentation within extent and form prescribed;
b) Applicant’s offer will be in conflict with terms hereof and submitter's requirements
stated herein;
c) The applicant makes such changes to the contract draft that do not correspond with
resolutions of this order documentation;
d) Applicant’s offer contains untrue or otherwise misleading data, information, and
documents;
e) Applicant’s offer contains such amendments and corrections that may mislead the
submitter;
f) In other cases resulting from ZVZ or hereof.

10.2. Insufficient Technical Level of Reactors

Within the assessment of applicants' offers in compliance with § 76 ZVZ, aside from
other things, it will be evaluated whether a reactor offered meets all specifications
within the extent given for each device in article 5.1 hereof.

If any of the devices offered fails to meet more than one of the specified requirement
of the above mentioned, applicant’s offer will be excluded, and the applicant will be
expelled from the tender.

11. Offer Evaluation Criteria

The most convenient offer will be selected by a five-member committee appointed by the
submitter. The committee will assess offers based on the evaluation criteria below:
A Total offer price of delivery 60 %
B Technical characteristics 35 %
D
C Service and support 5%

12. Method of Offer’s Evaluation

12.1. Criterion A - Total bid price of delivery


The lowest price is the most convenient one. The lowest price gets 100 points. Other
offers assessed will be given points values calculated as: 100 times the ratio of the
most suitable offer’s price to the price of the offer assessed.

12.2. Criterion B - Technical characteristics


For this criterion, each unit offered will be assessed individually. In this part the
committee assesses whether the units offered meet the basic specification within the
minimum requirements within point 5.1 of this order documentation.

In the first phase, the technical level for each unit offered will be assessed based on the
assessment table below. Individual units will be assessed based on the specified
parameters; points gained based on such parameters will be multiplied by the weight
of parameter given.

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Point 5.1.a) Testing units for hydrodesulfurization (HDS) and hydrocracking (HC)
1a. 2 reactors for HDS catalyst screening
1b. 2 reactors for HDS catalyst testing
1c. 3 reactors for HC catalyst testing

Para- Item Evaluation method * Parameter


meter weight
Possibility to operate reactors ofImpossible 0 points
the same type according to 1a. and1x 2-stage mode 50 points 10 %
1b. in series 2x 2-stage mode 100 points
Possibility to operate reactors ofImpossible 0 points
the same type according to 1c. in 2-stage mode 50 points 10 %
series 3-stage mode 100 points
Extra-container and feeding line No 0 points
10 %
for a sulfiding agent - HDS units Yes 100 points

Extra-container and feeding line No 0 points


10 %
for a sulfiding agent - HC unit Yes 100 points
≥ 2 °C 0 points
Temperature difference (profile)
1 – 2 °C 50 points 20 %
along the reactor
≤ 1 °C 100 points
25 to 100 °C 0 points
High-pressure separator operating
0 to 100 °C 50 points 10 %
temperatures
-20 to 100 °C 100 points
25 to 100 °C 0 points
Low-pressure separator operating
0 to 100 °C 50 points 10 %
temperatures
-20 to 100 °C 100 points
24 hours 0 points
Unattended operation 48 hours 50 points 20 %
>48 hours 100 points

Point 5.1.b) Testing units for sulphur-free processes


2a. 2 reactors for catalyst screening
2b. 2 reactors for catalyst testing

Para- Item Evaluation method * Parameter


meter weight
Possibility to operate reactors of Impossible 0 points
the same type according to 1a. and 1x 2-stage mode 50 points 20 %
1b. in series 2x 2-stage mode 100 points
≥ 2 °C 0 points
Temperature difference (profile)
1 – 2 °C 50 points 20 %
along the reactor
≤ 1 °C 100 points
High-pressure separator operating 25 to 100 °C 0 points
15 %
temperatures 0 to 100 °C 50 points

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-20 to 100 °C 100 points
25 to 100 °C 0 points
Low pressure separator operating
0 to 100 °C 50 points 15 %
temperatures
-20 to 100 °C 100 points
24 hours 0 points
Unattended operation 48 hours 50 points 30 %
>48 hours 100 points

Point 5.1.c) Testing unit for high-temperature processes

Para- Item Evaluation method * Parameter


meter weight
- 20 °C or lower 100 points
Pumps heads cooling (lowest
-10 to - 19 °C 50 points 30 %
achievable temperature)
higher then -10 0 points
Temperature difference (profile) ≥ 2 °C 0 points
along the reactor (without 1 – 2 °C 50 points 30 %
chemical reaction) ≤ 1 °C 100 points
higher then -10 0 points
Low pressure separator operating
-10 to - 19 °C 50 points 20 %
temperatures (the low limit)
20 °C or lower 100 points
24 hours 0 points
Unattended operation 48 hours 50 points 20 %
>48 hours 100 points

Point 5.1.d) Testing unit for catalytic combustion and reduction processes

Para- Item Evaluation method * Parameter


meter weight
3 0 points
Number of gas lines 15 %
>3 100 points
≥ 2 °C 0 points
Temperature difference (profile)
1 – 2 °C 50 points 30 %
along the reactor
≤ 1 °C 100 points
25 to 100 °C 0 points
Gas/liquid phase separator
0 to 100 °C 50 points 20 %
operating temperatures
-20 to 100 °C 100 points
Sulphur-removing vessel operating 25 to 50 °C 0 points
15 %
temperatures 0 to 50 °C 50 points
24 hours 0 points
Unattended operation 48 hours 50 points 20 %
>48 hours 100 points

Point 5.1.e) Testing unit for adsorption and desorption processes

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Para- Item Evaluation method * Parameter
meter weight
3 0 points
Number of gas lines 10 %
>3 100 points
≥ 2 °C 0 points
Temperature difference (profile)
1 – 2 °C 50 points 20 %
along the reactor
≤ 1 °C 100 points
25-100 °C 0 points
High-pressure separator operating
10-120 °C 50 points 20 %
temperatures
0-120 °C 100 points
25-50 °C 0 points
Low pressure separator operating
10-60 °C 50 points 25 %
temperatures
0-80 °C 100 points
24 hours 0 points
Unattended operation 48 hours 50 points 25 %
>48 hours 100 points

Point 5.1.f) Testing unit for upgrading of crude-oil residual fractions and their
mixtures with bio-products

Para- Item Evaluation method * Parameter


meter weight
120 °C 0 points
Heating the feed container, pump
120-150 °C 50 points 30 %
and feeding line
>150 °C 100 points
≥ 2 °C 0 points
Temperature difference (profile)
1 – 2 °C 50 points 20 %
along the reactor
≤ 1 °C 100 points
200-350 °C 0 points
High-pressure separator 1
150-350 °C 50 points 10 %
operating temperatures
100-350 °C 100 points
40-70 °C 0 points
High-pressure separator 2
40-100 °C 50 points 20 %
operating temperatures
40-150 °C 100 points
24 hours 0 points
Unattended operation 48 hours 50 points 20 %
>48 hours 100 points

Such calculated point evaluations of individual reactors offered by an applicant will be


made into an arithmetical mean of the total technical evaluation of reactors for an
applicant.
The offer that gains the highest evaluation of the technical parameters will be given
100 points; other offers will be given number of points proportional to the ratio of
arithmetical means of technical parameters of a specific best offer.

12.3. Criterion C - Service and support criterion

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Within the ‘service and support' criterion, overall level of service assurance and device
use based on the following criteria will be evaluated (gives both the method of
evaluation and given sub-criterion weight).

Service and support criterion

Criterion Item Significance


based on
submitter
C1 Speed of response to a reported defect 50 %
C2 Charge for the first 4 hours of service work + transport of a
50%
service worker in compliance with remark in point 5.9

Evaluation method C1 – the most convenient is the lowest value. Commitment of


service worker’s arrival within 24 hours from reporting (on workdays) gains 100
points; within 2 workdays - 70 points; within 3 workdays - 50 points; within 5
workdays - 20 points; and more than 5 workdays - 0 points.

Evaluation method C2 – the most convenient is the lowest price of expected service
action in the structure of price for the arrival of a service worker, plus 4 service hours.
The lowest price gets 100 points. Other offers assessed will be given points values
calculated as: 100 times the ratio of the most suitable offer’s price to the price of the
offer assessed.

Total evaluation will be set to that the points for offers C1 and C2 will be multiplied
by the weights based on significance, and the total weighted mean of Service Terms
criteria will be calculated. The offer that gains the most points gets 100 points for the
Service Terms criterion. Other offers assessed will be given point values calculated as:
100 times the ratio of point assessment of given offer to the point assessment of the
best offer.

12.4. Resulting Evaluation

Total point value of the offer will be calculated as: point values gained within
individual assessment criteria multiplied by the weight of respective criterion in
compliance with art. 11. The total of such point values defines the resulting point
value of an offer.

In the resulting order of offers, the most convenient offer gains the highest total
number of points.

13. Submitter’s Rights


By submitting an offer, an applicant does not gain any rights for contract signing or
order fulfilment for implementing of this public contract with the submitter.

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