[76 cN 0026 ptNo: 9 Date Ig (e-]ig BATCH ADSORPTION AIM To find the constants of the Freundlich's ‘equation at room temperature for the adsorption of the acetic acid on activated carbon. APPARATUS REQUIRED Stoppered conical flask, measuring eylinder, pipette and burette. SYSTEM Acetic acid -Water - Activated carbon, CHEMICALS Acetic acid, Activated carbon, 0.1N NaQH and Phenolphthalein indicator. INTRODUCTION Adsorption is a fluid ~ solid operation and is purely a surfice phenomenon The fluid may be \ oF liquid. The solute is transferred from the fluid phase to the solid phase. The éommon’ Disord ENT levied carton, silca sol elon When an adsorbent is mixed with a solution, adsorption of solute occurs in the adsorbent surface, Due to preferential adsorption often the solute, the solute concentration in the solution falls from the initial value” @,* to the final value * C** in the liquid. The apparent adsorption of solute, neglecting any volume change in the solution, is V( Cy. C*) kg of solute adsorbed per kg of adsorbent. This is satistictory for the dilute solution where the fraction of the original solvent, which may be adsorbed. is small, Over a small concentration wats Scanned with CamScannerScanned with CamScannerAUR Ange and particularly f ‘or dilute solutions and freundlich equation may be used. It is given by KV G-C)\n Where, C*-Eaquiibrium concentration of soute, Kyi M3 Co- Initial concentration of solute, K g/m V Volume of solution / unit weight of adsorbent, m3 /kg Kin Constants ata particular temperatures, PROCEDURE, Take five Stoppered conic Scanned with CamScannerB Uline Colada 7 e Flak Y. jow Wom - 0.05 wily If pox * Hsk d,s fo x [oe 2 boyy Joke OF Plaka | Vue tees 200s thy peur hy ry Ve pe K (99 = OO wh | foexd he Pluk, oy. wy ino = 041 rly poke Giledadies for hand p: from au a om a ee Ji Bega at nag mee Inte Scanned with CamScannerUSotes i; 0 “100 Ye 100 fo too | 2c 100 | 80 | 100 1 = r “Weight of |Volumeof| | Final ) Flask | the Activated | the NaOH | Initial Cone. No. Carbon used: Cone. Cc | V(C.—C%) | In (C*) | INnVEC,-C%) C + Kg. mL kg/m’ le Ke. /m | poop lt go (26-55 |OIPS | 52h | -TST Pio 13:6 anes ato eA get [19 37 Ig M4 Ons 264 | 21S B 02. Gey 0.0% 237 3.329 Y foor2 bY (2 10-2 03 - SC poz prP| 6 Hs 0-08 v6 | ogiqg caLcuLations Normality of the acetic acid (N2) = VIN/ V2 = Final Concentrations of the Acetic Acid. = C’ = kg/m Initial Concentrations of the Acetic acid Cy = kg/m’ ‘V= Volume of the solute/Weight of the absorbent |= mkg RESULT: Report the constants of the Freundlichs equation k and n ANALYSIS OF RESULTS/CONCLUSIONS: Scanned with CamScannerScanned with CamScanner