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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST

PARUL INSTITUTE OF ENGINEERING


SHIFT
&TECHNOLOGY(DS)
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21

STUDENT
i

INFORMATION
HANDBOOK
या कुन्दे न्दत
ु ुषारहारधवला या शुभ्रवस्त्रावत
ृ ा
या वीणावरदण्डमण्ण्डतकरा या श्वेतपद्मासना ।
या ब्रह्माच्यत
ु शंकरप्रभतृ तभभदे वैः सदा पण्ू िता
सा मां पातु सरस्त्वतत भगवती तनैःशेषिाड्यापहा ॥१॥

2020-21
DEPARTMENT OF CHEMICAL
ENGINEERING

SEMESTER 5th

Div-5J

P . O . L I M D A , T A . W A G H 1O D I A , D I S T V A D O D A R A
PH. 02668-260340.
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
CLASS TIME TABLE
DEPT: CHEMICAL CLASS: 5J1 ROOM NO:
ACA YR: 2020-21 (ODD SEM) SEMESTER: FIFTH W.E.F.:
TIME MONDAY TUESDAY WEDNESDAY THURSDAY FRIDAY SATURDAY

9:30 AM to 10:30 AM MA MT-2(JP) UICP(JP) IM(JNP) MT-2(NB)

10:30 AM to
CET(YG) PRPT(PRM) PRPT(SM) CET(SM) UICP(JP)
11:30AM
11:30 TO 12:25

12:25 PM to 1:30 PM PRPT(SM) MT-2(NB) IM(JNP) CET (SM) PRPT(PRM)

CET TUT(YG)
1:30PM to 2:30PM MT-2(JP) IM (JNP) UICP(NB) UICP(NB) CDC

IM – INDUSTRIAL MANAGEMENT NBB-NITESH BARAIYA


MT-II MASS TRANSFER –II PRM-PARTH MODI
PRPT – PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY SM-SRUSTI MARFATIA
UICP - UTILITIES & INSTRUMENTATION IN CHEMICAL PLANT JP-JAMES PATEL
CET – CHEMICAL ENGINEERING THERMODYNAMICS YG-YAXITA GANDHI
JNP-JAYESH PATEL

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21

CLASS TIME TABLE


DEPT: CHEMICAL CLASS: 5J2 ROOM NO:
ACA YR: 2020-2021 (ODD SEM) SEMESTER: FIFTH W.E.F.:
TIME MONDAY TUESDAY WEDNESDAY THURSDAY FRIDAY SATURDAY

9:30 AM to 10:30 AM MT-2 (JP) MA PRPT (SM) CET (SM) UICP (JP)

10:30 AM to
IM(JNP) CET(YG) MT-2 (JP) IM (JNP) PRPT (PRM) MT-2 (NB)
11:30AM
11:30 TO 12:25

12:25 PM to 1:30 PM UICP (NB) PRPT (PRM) UICP (JP) UICP (NB) IM(JNP)

CET TUT(YG)

1:30PM to 2:30PM PRPT (SM) MT-2(NB) CET (SM) CDC

IM – INDUSTRIAL MANAGEMENT NBB-NITESH BARAIYA


MT-II MASS TRANSFER –II PRM-PARTH MODI
PRPT – PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY SM-SRUSTI MARFATIA
UIC- UTILITIES & INSTRUMENTATION IN CHEMICAL PLANT JP-JAMES PATEL
CET – CHEMICAL ENGINEERING THERMODYNAMICS YG-YAXITA GANDHI
JNP-JAYESH PATEL

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
ACADEMIC CALENDER 2020-21 (EVEN SEMESTER)

Commencement of Semester 21st June 2020

Internal Mid Semester Exams (30 marks)


Results of Internal Mid semester Exams
(30 marks)

Internal Mid Semester Exam (70 marks)

Result of Internal Mid Semester Exam


(70 marks)

Block Mid Exam

Submission of Term (1st to 4th lectures teaching)

End of Semester

Parents Meeting

Contact Details

Sr.
Name of Faculty Designation Mobile No E-mail ID
No
1 Mrs. PRABHA MODI Head 9429927893 Prabharawat.modi@gmail.com

Faculty Advisor
Sr. Name of
Designation Mobile No E-mail ID
No Faculty
MR. JAMES
1 9067824599 James.patel8831@parulunivesity.ac.in
PATEL
lecturer
MRS.SRUSTI
2 9377603367 srusti.marfatia12718@paruluniversity.ac.in
MARFATIA

Faculty List of DE CHE SEM-5

Sr Name of Alias Mobile No E-mail ID Subject


No Faculty of
1 JP James.patel8831@parulunivesity.ac.in Mt-
MR. JAMES Faculty
9067824599 2,UICP
PATEL
2 SM srusti.marfatia12718@paruluniversity.ac.in PRPT,
MRS.SRUSTI
9377603367 CET
MARFATIA

1
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
3 NITESH NBB nitesh.baraiya270137@paruluniversity.ac.in Mt-2,
BARAIYA 8347086526 UICP

4 PARTH PRM parth.modi15167@paruluniversity.ac.in PRPT,


MODI 9265918565

6 YAXITA YG yaxita.gandhi5456@paruluniversity.ac.in CET


GANDHI

DE CHEMICAL4thSEM Detail Syllabus


COURSE TITLE: INDUSTRIAL MANAGEMENT
(COURSE CODE 3350501)

Total credit Examination scheme


Teaching Scheme
Theory Marks Practical Marks Total
Theory Tutorial Practical c ESE PA ESE PA Marks
3 0 0 3 70 30 00 00 100

Major Learning Outcomes


Unit Topics and Sub-topics
(in cognitive domain)
1.1 Definition of system
1a. Explain concepts of system
1.2 Types of systems
Unit I 1a.1 State Types of systems
1.3 System parameters
Concept of
1.4 System variable
System and
1.5 System behavior
Management
1b. Discuss management and 1.6 Fundamentals of management
Explain its functions 1.7 Functions of management
2.1 Definition, Goals, Factors considered in
2a. Describe management structure formulating structure
2b. Explain various factors for structure 2.2 Division of labor, Scalar and functional
Unit II 2c. Describe various management processes, Span of control, Delegation of
Organization processes authority, Centralization and
Structure and Decentralization
Organizational 2d. Classify the organization 2.3 Types, advantages, disadvantages,
Dynamics 2e. Apply SWOT analysis of flexibility and applications of organization
organizational structure structure
2f. Explain factors affecting 2.4 Organizational culture and factors
Organizational culture affecting organization culture

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
2.5 Moral: factors affecting moral
2g. Discuss moral and relate it 2.6 Relationship between moral and
with productivity productivity
2h. Identify factors affecting 2.7 Effect of high and low moral
job satisfaction 2.8 Job satisfaction, factors influencing job
satisfaction
3.1 Definitions, Functions, Importance of
3a. Discuss importance of material
material management, Relationship with
management
other departments
3.2 Objectives of purchase, Purchase
3b. Explain purchase procedure and systems, Purchase procedure, Terms and
system various forms used in purchase
department
3c. Classify stores 3.3 Functions of storekeeping classification
3c.1 List out various functions of stores as centralized and decentralized
of storekeeping with their advantages, disadvantages and
Unit III
3d. Compare methods of storekeeping application
Material
3.4 Functions of store keeper,
Management 3e. Describe functions of storekeeper
Types of records maintained by store,
3f. List Types of records types of storage
various types of storage equipment,
equipment
Codification of stores
3.5 Definition of inventory control,
objectives of inventory control, Derivation
3g. Discuss Objectives of inventory
of expression for EOQ, ABC analysis, other
control and derive expression for EOQ
modern methods of analysis
3h. Distinguish inventory analysis and
3.6 Inventory models such as Willson’s
inventory models
model, Replenishment model, Two bin
model
4.1 Meaning, features, objectives of
(1) PPC(Production, planning and control)
4a. Explain objectives and applications of
(2) CPM(Critical path method)
PPC and CPM , PERT
(3) PERT(Programme Evaluation and
Review Technique)
4.2 Functions of PPC with necessary forms
4b List out functions of PPC
used in it
4.3 Types of productions, Calculation of
4c Calculate critical ratio using Gantt
Unit IV Economic Batch Quantity (EBQ), Critical
charts
Management ratio scheduling and Gantt charts
Techniques 4.4 Different terms used in network
diagram by CPM/PERT
4.5 Draw network diagram for a real life
4d. Draw network diagram and project containing 10-15 activities,
determine its critical path Computation of LPO, EPO
4e. Determine floats and explain crashing 4.6 Determination of critical path on
of network network
4.7 Floats, its types and determination of
floats
4.8 Crashing of network and its application

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
4.9 Concept of value analysis, important
4f. Describe concept of value analysis
methods used in value analysis, VA flow
with its importance and various method
diagram
5.1 Factory act and its important
provisions
Unit V
5a. Describe various provisions of Factory 5.2 Workman Compensation Act its
Factory Act
act and its important provisions important provisions
and Laws
5.3 Industrial Dispute Act and its important
provisions

Reference books

Sr.
Title of Books Author Publication
No.
Factory Management & business Vora& Co. Publishers Pvt. Ltd.,
1 A.S Despande
organization Mumbai, 1962
Business organization &
2 M.C.Shukla S. Chand& Co., New Delhi, 1970
management
Industrial Engineering & DhanpatRai Publications, New Delhi,
3 O. P. Khanna
Management 1980
3rd Edition Affiliated East-West
CPM & PERT principles and
4 L.S.Srinath Press Private Limited, New Delhi,
Applications
1971

COURSE TITLE: MASS TRANSFER-II


(COURSE CODE: 3350502)

Total credit Examination scheme


Teaching Scheme Theory Practical Marks
Total
Marks
Marks
Theory Tutorial Practical c ESE PA ESE PA
4 0 4 8 70 30 40 60 200

Major Learning Outcomes


Unit Topics and Sub-topics
(in cognitive domain)
1.1 Importance of Gas-Liquid operations
1.2 Classification of equipments for Gas-Liquid
1a. Describe importance of Gas- operations
Liquid operations 1.3 Gas dispersed
1b. Classify equipments for Gas- 1.3.1 Sparged vessel
Unit – I Liquid operations 1.3.2 Mechanically Agitated Vessel
Equipment for 1c. Describe construction of 1.3.3 Tray tower
Gas Liquid equipments with diagram of 1.3 & 1.4 1.3.3.1 Types of trays
Operations 1d. Explain working principle and 1.3.3.2 Operating problems in tray tower
operation of equipments with 1.3.3.3 Tray efficiency
sketches of 1.3 & 1.4 1.4 Liquid dispersed
1.4.1 Venturi scrubber
1.4.2 Wetted wall column
1.4.3 Spray tower
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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
1.4.4 Packed tower and its operating problems
1d. Distinguish different types of
1.5 Types of packing
packing with diagram
(a) Random (b) Regular
2a Describe applications
2.1 Distillation as a versatile separation method
2b Describe the steps to Plot VLE,
2.2 Vapor Liquid Equilibria
Constant pressure, Constant
2.2.1Constant pressure equilibria
temperature equilibria
2.2.2 Constant temperature equilibria
2c Explain Relative volatility and laws -
2.3 Relative volatility
Raoult’s, Henry’s
2.4 Raoult’s law, Henry’s law, and their uses
2c.1 State their uses
2d Differenetiateazeotropes
2.5 Maximum and minimum boiling azeotropes
2.6 Flash vaporization
2e Explain
2.6.1 Material balance
-Flash vaporisation, Differential
2.6.2 Calculation of amount and composition
distillation, Continuous rectification
2.7 Differential distillation
2f Calculate amount and composition
2.7.1 Derivation of Rayleigh’s equation
for Flash vaporization
Unit – II 2.7.2 Calculation of product composition
2g Calculate product composition for
Distillation 2.8 Continuous rectification of binary solution
Differential distillation
2.8.1 The fractionation operation
2.8.2 Overall material and enthalpy balances
2.9 McCabe and Thiele method for enriching
2f. Apply McCabe-Theile method for and stripping section
multistage tray tower for enriching 2.9.1 Introduction of Feed and Location of the
and stripping section feed tray
2f.1 Calculate product rates, minimum 2.9.2 Total reflux ratio, Minimum reflux ratio,
reflux ratio and number of trays for Optimum reflux ratio
the given data 2.9.3 Calculations of product rates, minimum
reflux ratio and number of trays
2g. Compare distillation techniques viz
2.10 Important distillation techniques
(a) Steam distillation
(a) Steam distillation
(b)Vacuum and molecular distillation
(b)Vacuum and molecular distillation
(c)Azeotropic and extractive
(c)Azeotropic and extractive distillation
distillation
2h. Distinguish Reboilers 2.11 Reboilers and their use
Humidification:
3a. Analyse the VLE for a pure 3.1 Vapor-pressure curve
substance 3.2 Saturated and unsaturated vapor-gas
mixtures
3b. Explain the concepts of Absolute
Unit – III
humidity, Relative saturation, 3.3 Concept of Absolute humidity, Relative
Humidification
Percentage saturation, Dew point, Dry saturation, Percentage saturation, Dew point,
bulb temperature, Wet bulb Dry bulb temperature, Wet bulb temperature,
temperature, Adiabatic saturation Adiabatic saturation temperature, Humid
temperature, Humid volume, Humid volume, Humid heat, Enthalpy
heat, Enthalpy

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
3c.Evaluate the property of air using
DBT and WBT
3.4 Calculations of absolute humidity, relative
3e.1 Calculate –absolute humidity,
saturation, percentage saturation
relative saturation, percentage
saturation for the given process data
3d. Draw psychometric chart
3.5 Psychometric charts for Air-Water system
3d.1 List Purposes of contact of gas
3.6 Purposes of contact of gas with pure Liquid
with pure Liquid
3.7 Equipments
3e. Explain construction and working 3.7.1 Cooling towers
with diagram 3.7.2 Spray chambers
3.7.3 Spray ponds
4a. Discuss drying equilibrium and
related concepts
4.1 Drying equilibrium
4a.1 Define and calculation of
4.1.1 Insoluble solids
Moisture content, Equilibrium and
4.1.2 Hysterisis
free moisture, Bound and unbound
4.1.3 Soluble solids
moisture
4.1.4 Definitions and calculation of Moisture
4a.2 Calculate - Moisture content,
content, Equilibrium and free moisture, Bound
Equilibrium and free moisture, Bound
and unbound moisture
and unbound moisture from the given
data
4b. Classify drying & drying 4.2 Batch and continuous drying
equipments 4.3 Classification of drying equipment
4.4 Construction and working of following Drier
Unit – IV equipment
Drying Tray drier
Tunnel drier
4c. Describe construction and working
Vacuum drier
of Drier equipments
Rotary drier
Spray drier
Fluidized bed drier
Pneumatic drier
4d. Describe drying rate
characteristics for batch drying with
4.5 Drying rate curve for batch drying
sketches
4.6 Derivation of equation for drying time for
4d.1 Derive equation for drying time
constant rate period and falling rate period
for constant rate period and falling
rate period
4e. Calculate drying time 4.7 Calculation of drying time
Adsorption & Ion-Exchange:
5a. Define and state uses of
5.1 Definition and industrial application of
Adsorption
Adsorption
5b. Classify Adsorption and 5.2 Types of adsorption
Unit – V
adsorbents 5.3 Nature of adsorbents
Adsorption &
5b.1State Commonly used adsorbents 5.4 Commonly used adsorbents
Ion-Exchange
5d. Analyse Adsorption Equilibria 5.5 Adsorption Equilibria
5d.1 Describe Effect of temperature 5.5.1 Single gases and vapours
on 5.5.2 Adsorption hysteresis
adsorption and Heat of adsorption 5.2.3 Effect of temperature on adsorption
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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
and Heat of adsorption
5.6 Adsorption from liquids
5e. Apply Freudlich’s equation for 5.6.1 Adsorption from dilute solution
single stage and multi stage cross- 5.6.2 The Freundlich’s equation
current operation 5.6.3 Adsorption from concentrated solutions
5e.1Describe adsorption from dilute 5.6.4 Material balance and Freundlich’s
and concentrated solution equation for single stage and multistage cross-
current operation
5f. Describe construction and working
5.7 Higgins contactor
of Higgins contactor, Pressure swing
5.8 Pressure swing adsorber
adsorber
5.9 Ion-Exchange
5g. Appreciate concepts of Ion 5.9.1 Principles
Exchange 5.9.2 Application
5g.1 List Applicationv of Ion Exchange 5.9.3 Equilibria
5.9.4 Rate of ion exchange
6a. State Industrial applications of Crystallisation:
crystallization 6.1 Industrial applications of crystallization
6b. Explain equilibria mechanism for 6.2 Equilibria and yields
crystallisation 6.3 Super saturation and methods to get it
6b.1 State the methods to get Super 6.4 Nucleation
saturation 6.5 Crystal growth
6c. Explain working principle and
6.6 Crystallization Equipment
Unit –VI operation of Crystallization Equipment
6.6.1 Vacuum crystallizer
Crystallisation with sketch
6.6.2 Swenson walker crystallizer
6c.1Describe construction of
6.6.3 Draft tube-baffle crystallizer
Crystallization Equipment
6d. State and explain Meir’s theory 6.7 Meir’s theory
6e. Calculate the crystal yield 6.8 Crystallization with and without seeding
6.9 Calculations of crystal yield
6f. List steps to Prevent caking of
6.10 Caking of crystals and it’s prevention
crystals

S. Practical/Exercise Apprx. Hrs.


Unit No.
No. (Outcomes in psychomotor domain) Required
Demonstrate principle, construction and working of equipments for gas–
1 I 4
liquid operations with models
Prepare vapour liquid equilibria curve at atmospheric pressure for
2 I 4
Benzene-Xylene
3 II Carry out simple distillation in glass assembly 4
4 II Find out the effect of vacuum on distillation of liquid 4
5 II Carry out continuous rectification in packed column 4
6 II Find out amount of steam required in steam distillation 4
Find out the property of atmospheric air with the help of wet bulb and dry
7 III 4
bulb temperature
8 III Set desired conditions of humid air in humidity control cabin 4
9 IV Prepare drying curve of moist sand and moist limestone 4
10 IV Find out equilibrium moisture content and drying time of wet solid 4

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
11 V Characterize industrial adsorbents and observe their samples 4
12 V Remove colour impurities from water using charcoal 4
13 VI Find out the yield of crystals from saturated solution without seeding 4
14 VI Find out the yield of crystals of from saturated solution with seeding 4
Total 56

Reference Books:

S. No. Title of Books Author Publication


Mc Graw- Hill, 3rd Edition,
1 Mass Transfer Operations Robert E. Treybal
1981
McCabe, Warren L., McGraw Hill Publication,
2 Unit Operation of Chemical Engineering
Julian C. Smith New York 2004, 7th Edition
3 Unit Operations-II K. A. Gavhane NiraliPrakashan, Pune
Unit Operations of Chemical Engineering, Khanna Publishers, New
4 P. Chattopadhyay
Volume-I Delhi, 1995
Coulsion and Butterworth-Heinemann;
5 Chemical Engineering, Volume-2
Richardson 5th Edition, 2002
L.Badger, McGraw Hill Publication,
7 Introduction to Chemical Engineering
Julius T. Banchero New York, 7th Edition, 2004

COURSE TITLE: PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY


(COURSE CODE: 3350503)

Total credit Examination scheme


Teaching Scheme Theory Practical Marks
Total
Marks
Marks
Theory Tutorial Practical c ESE PA ESE PA
4 0 2 6 70 30 20 30 150

Unit Major Learning Outcomes Topics and Sub-topics


(in cognitive domain)
1a. Describe the reserves of Crude 1.1 Occurrence and history of Petroleum
Petroleum oil in India 1.2 Crude Petroleum oil reserves in India
1a.1State basics occurrence of 1.3 Composition of Petroleum
Petroleum
1.4 Classification of Petroleum
Unit – I 1a.2 Classify Petroleum
Basics of 1a.3Describe history of Petroleum
Petroleum and 1b. Explain basics of refineries and– 1.5 Refineries development in Gujarat and
Refinery products India
1b.1State types of Refineries 1.6 Types of Refineries
1b.2Describe Refinery processes- 1.7 Refinery processes
Physical and Chemical changes 1.7.1 Physical changes
1.7.2 Chemical changes
1.8 Refinery products
Unit – II Primary treatment of crude :
2a. Describe primary treatment of
Fractionation of 2.1 Dehydration and Desalting of crude oil
crude
Petroleum 2.2 Pipe still heater

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
2b. Describe distillation of crude 2.3 Atmospheric distillation of crude
and crude residue 2.4 Vacuum distillation of crude residue
2.5 Physical properties of petroleum products
and its measurements :
2.5.1 Petrol
2c. Identify Physical properties of
2.5.2 Diesel
petroleum products fractions and
2.5.3 Kerosene
measure- (Units of measure )
2.5.4 Lubricant oil
2.5.5 CNG and LPG
2.5.6 Grease
3.1 Cracking
3.1.1 Purpose of cracking
3a. Compare Cracking methods 3.1.2 Effect of temperature and pressure on
3a.1 Describe the Purpose of Cracking
cracking & Effect of temperature Cracking methods
and pressure on Cracking 3.1.3 Thermal cracking
3.1.4 catalytic cracking
Unit – III 3.1.5Fluidised bed catalytic cracking
Refinery 3b.Explain need of Reforming
3.2 Reforming
Processes 3b.1 Differentiate thermal and
3.2.1 Purpose of Reforming
catalytic reforming
3.2.2 Differentiate thermal and catalytic
3b.2 Identify effect of important
reforming
parameters on reforming
3.2.3 Platforming(Pt catalyst-Reforming)
3b.3 Explain Pt catalyst-Reforming
3.3 Other important refinery processes
3c. Explain in brief refinery
3.3.1 Hydrotreating
processes -Hydrotreating,
3.3.2 Hydrocracking
Hydrocracking, Delayed coking ,
3.3.3 Delayed coking
Visbreaking
3.3.4 Visbreaking

4a. State the purposes of sulphur


removal 4.1 Purposes and methods of sulphur removal
4a.1 Explain methods of sulphur 4.2 Doctor's sweetening
removal - Doctor's sweetening, 4.3 Catalytic desulfurization
Catalytic desulfurization , MEROX 4.4 MEROX treatment
Unit – IV
treatment
Treatment
Techniques 4b. Explain Treatment of Kerosene 4.5 Treatment of Kerosene by liquid SO2
by liquid SO2 extraction extraction
4.6 Solvent extraction processes
4c. Distinguish solvent extraction
4.6.1 Furtural extraction method
processes – Furtural, Phenol, Duo
4.6.2 Phenol extraction method
sol
4.6.3 Duo sol extraction process

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21

4.7 Purpose of dewaxing


Dewaxing Techniques
4d. Describe Purpose of dewaxing
4.8 Dewaxing without solvent
4e. Compare dewaxing Techniques
4.9 Dewaxing with solvent
4.9.1 Ketonedewaxing and propane dewaxing

5a. Describe in brief development


5.1 Development of petrochemical industry in
of petrochemical industry in Gujarat
Gujarat and in India
and in India
5.2 Manufacturing of important C1
Unit – V compounds
Petrochemicals 5b. Draw flow chart for 5.2.1 Methanol
manufacturing of 5.2.2 Formaldehyde
- C1 compounds- Methanol and 5.3 Manufacturing of important C2
Formaldehyde compounds
-C2 compounds - Ethylene 5.3.1 Ethylene dichloride
dichloride ,Vinyl chloride and 5.3.2 Vinyl chloride
Ethylene Oxide 5.3.3 Ethylene Oxide
- C3 compounds- 5.4 Manufacturing of important C3
Polypropylene.Propylene oxide compounds
-Chemicals from aromatics- 5.4.1 Polypropylene.
Linear Alkyl Benzene 5.4.2 Propylene oxide
Phenol by benzene sulfonate 5.5 Chemicals from aromatics
process 5.6 Manufacture of Linear Alkyl Benzene
5.7 Manufacture of Phenol by benzene
sulfonate process

Unit Practical/Exercise Apprx. Hrs.


S. No.
No. (outcomes in psychomotor domain) Required
1 I Prepare a detail chart of modern refinery 2
2 I Prepare a detail chart of petrochemical products 2
3 II Determine flash point by Penskey Martin method 2
4 II Determine fire point by Penskey Martin method 2
5 II Measure softening point and drop point of Grease 2
6 II Measure Aniline point of lubricating oil 2
7 II Determine penetration number of Grease 2
8 II Determine Carbon residue by Ram's bottom method 2
9 II Determine Carbon residue by conradson method 2
10 II Measure smoke point of kerosene 2
11 II Measure cloud point lubricating oil 2
12 II Measure pour point lubricating oil 2
13 II Measure initial & final boiling point of any petroleum product 2
Measure Viscosity of lube oil by Redwood
14 II 2
/Saybolt/Englerviscometer

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
Total 28

Reference Books
Sr.
Title of Books Author Publication
No.
1 Modern Petroleum Refining Processes B. K.BhaskarRao Oxford and IBH, 2007
M. GopalaRao, 3rd Edition East-West
2 Outlines of chemical Technology
Marshall Sittig press pvt. Ltd, Delhi
McGraw Hill publication
3 Shreve’s Chemical Process Industries Austin G.T.
–New Delhi, 5th edition
2nd Edition, Khanna
4 A Text on Petrochemicals B.K.BhaskarRao
Publishers, Delhi, 1998
McGraw Hill, Newyork,
5 Petroleum Refinery Engineering W.L.Nelson
1958

COURSE TITLE: UTILITIES AND INSTRUMENTATION IN CHEMICAL PLANT


(COURSE CODE: 3350504)

Total credit Examination scheme


Teaching Scheme Theory Practical Marks
Marks Total Marks
Theory Tutorial Practical c ESE PA ESE PA

4 0 4 8 70 30 40 60 200

Unit Major Learning Outcomes Topics and Sub-topics


(in cognitive domain)
1a. Explain role of Utilities in Chemical
Plant 1.1 List and use of various utilities in
1a.1 List various utilities in chemical plant chemical plant
& uses
1b. List sources of Water 1.2 Sources of water
Types of Water
1.3 Hard & Soft water
1c. Differentiate types of Water
1.4 Boiler Feed water and demineralized
water
1.5 Methods of water softening
processes
Unit – I • Lime soda process (Hot &
1d. Compare Softening processes of
Basics of Cold)
water
Petroleum and • Zeolite process
Refinery • Ion exchange process
• Phosphate process
1.6 Purification of water
1e. Explain the process of Purification of • Screening
water from raw water with sketches. • Sedimentation
• Coagulation
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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
• Filtration
• Sterilization
Utilities :
2a. Explain uses of utilities - Steam, Air &
2.1 Use of Steam, Air & Inert Gases as
Inert Gases
utilities
2.2 Properties of steam
• Enthalpy
• Wet steam
2b. Define properties of steam
• Saturated Steam
• Superheated steam
• Specific volume of steam
2c. Label the different part of steam
generator
2d. Classify steam generator 2.3 Steam Generator : Classification ,
2e. Select steam generator comparison , components
2f. compare steam generators 2.4 Factors affecting selection of Boiler
Unit – II 2g. List the Factors affecting selection of
Steam, Air & Boiler
Inert Gases 2f. Describe construction and 2.6 Construction and working of
Working of Locomotive Fire tube boiler (a) Locomotive Fire tube boiler
,Lancashire boiler (b) Lancashire boiler
2.7 Utility air
• Compressed Air
2g. Discuss utility air • Blower Air
• Fan Air
• Instrumental air
2h. Describe the working principle,
2.11 Types of Air compressors
application ofAir compressors –
• Reciprocating Air compressors
(a) Reciprocating Air
• Multistage compressors
compressors
• Rotary compressors
(b) Multistage compressors
(c) Rotary compressors
2i. Describe properties of Inert gases 2.12 Inert gas - Nitrogen, Argon
Unit – III 3a. Explain the working principle of
3.1 Concept of refrigeration
Refrigeration refrigeration
3.2 Methods of Refrigeration
• Ice Refrigeration
3b. Distinguish methods of Refrigeration
• Evaporative Refrigeration
• Vapor Refrigeration System
3c. Describe COP and TOR of refrigeration 3.3 COP and TOR of refrigeration

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
3.4 Types of Primary Refrigerants
• Ammonia
• Halo Carbons (Freon of Different
type)
3d. Use primary and secondary
• HFC (Hydro Fluorocarbon)
Refrigerants
3.5 Types of secondary Refrigerants
• Water
• Brine
3.6 Selection of Refrigerants

4.1 Importance of instrumentation in


chemical
4a. Classify instruments in chemical plant
plant
4.2 Classification of instruments
Unit – IV 4b. Describe Basic elements of
Basics of 4.3 Basic elements of instruments
instruments
Instrumentation 4c. Compare Static and Dynamic 4.4 Static and Dynamic Characteristics of
Characteristics of instruments instruments
4d. Differentiate First and second order 4.5 First order system and second order
system system
5a. Explain Temperature scale 5.1 Different Temperature scale
5b. Compare thermometers 5.2 Definition of thermometer
5b.1Explain Principle, Construction & 5.3 Principle, Construction & Working of
Working of : Mercury in glass, Bi-metallic : Mercury in glass thermometer, Bi-
, pressure spring , resistance metallic thermometer, pressure spring
thermometers thermometer, resistance thermometer,
5c. Describe Principles of 5.4 Principles of thermoelectricity
thermoelectricity and See-back effect, 5.5 See-back effect, Peltier effect and
Peltier effect and Thomson effect Thomson effect
5.6 Industrial thermocouple: their
5d. Describe principle, construction,
principle, construction, working range,
working range, lead wires of
lead wires
thermocouple and Thermowells
5.7 Thermowells in details
Unit- V
5e. Explain principle, construction, and
Measuring
working of Radiation and optical 5.8 Radiation and optical Pyrometers
Devices
Pyrometers
1. Pressure gauges
5f. Differentiate pressure gauges - diaphragm, Bourdon tube gauge, Dead
weight Gauge, Strain gauge
5g. Describe principle,
5.10 Target meter, Vortex Shredding
construction, and working of Target
meter, Turbine meter
meter, Vortex Shredding meter, Turbine
meter
5.11 Classify: Liquid level measuring
devices
5h. Classify and explain level measuring
5.12 Direct level measuring devices
devices
• Probe and tape
• Sight glass

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
• Floats
5.13 Indirect level measuring devices.
• Air trap box method
• Diaphragm box method
• Bellow system
• Differential pressure
manometer
5.14 Viscosity measurement by
5i. Compare viscosity measurement • Capillary tube method
methods • Rotating cylinder method
• Torsion viscometer
5.15 measurement of
5j. Explain principle, construction, and • Specific gravity by hydrometer
working • Humidity by hygrometer
• pH by pH meter
6a. Explain Function of relays and
6.1 Function of relays and interlocks
interlocks
6b. Explain schematic control loops for 6.2 Control loops
Unit – VI -Temperature control • Temperature control
Control Valves, -Pressure control • Pressure control
Control Loops & - Flow control • Flow control
Control System - Level control • Level control
6c. Describe process control modes with 6.6 Process control modes : P , P+I ,
sketches P+I+D, ON -OFF
6d. Explain uses of PLC and DCS System 6.7 PLC and DCS system

Practical/Exercise Apprx. Hrs.


Sr. No. Unit No.
(Major outcomes in psychomotor domain) Required
1 I Operate water treatment in water treatment plant 4
2 I Treat water using lime soda process 4
3 II Generate steam in laboratory using baby boiler 4
4 II Operate and test the working of air compressor 4
5 III Demonstrate different refrigeration cycles 4
Measure Temperature by thermometer and
6 V 4
thermocouple
7 V Measure Temperature by Bi-metallic thermometer 4
8 V Measure Pressure by mechanical pressure gauge 4
9 V Measure gas flow rate 4
10 V Measure level using direct method 4
11 V Measure viscosity by capillary tube method 4
12 V Measure specific gravity by Hydrometer 4
13 V Measure humidity by Hair hygrometer 4
14 V Measure pH by pH meter 4
15 VI Prepare a chart of components of DCS system 4
Demonstrate working of control valves and actuators
16 VI 4
using chart
Total 64

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
Reference books

S.
No. Title of Books Author Publication
1 Industrial instrumentation, Donald P. Eckman. JohnWilley and Sons, New York, 2004
2 Industrial Instrumentation & S. K. Singh 3rd edition
Control Tata-McGrawHil, 1987
3 Process Instrumentation and A P Kulkarni 15th Edition, April 2011,
Control NiraliPrakashan, Pune
4 Unit operation of chemical McCabe, Warren L., McGraw Hill
Engineering. Julian C. Smith Publication, New York
2004, 7th Edition
5 Plant utilities D. B. Dhone 2nd Edition, 2012
NiraliPrakashan, Pune
6 Process System Analysis & Control Donald R. Coughnour. 2nd edition, 1991, McGraw Hill
Publication, Newyork

COURSE TITLE: CHEMICAL ENGINEERING THERMODYNAMICS


(COURSE CODE: 3350505)
Total Examination scheme
Teaching Scheme credit Practical
Theory Marks Total
Marks
Marks
Theory Tutorial Practical c ESE PA ESE PA
3 2 0 5 70 30 00 00 100

Unit Major Learning Outcomes Topics and Sub-topics


(in cognitive domain)
1a. Describe scope of thermodynamics 1.1 Scope and limitations of
1.1 Define System, functions, thermodynamics
properties Process and surrounding 1.2 System, functions, properties Process
1b. Explain the System, functions, and surrounding
properties , Process and surrounding 1.2.1 System-Homogeneous and
with examples of chemical engineering heterogeneous, Closed and
field open, State of System
1c. Differentiate systems, functions, 1.2.2 Properties -Extensive and
properties and processes intensive
1d. Describe Extensive and intensive 1.2.3 Function -State and Path function
properties 1.2.4 Process -Reversible and
1e. Explain importance of Force, irreversible process
Pressure, Work and Energy physical 1.3 Force, Pressure, Work and Energy
Unit – I quantities, phase rule and zeroth law 1.4 Steady state, Equilibrium state and
Introduction and of thermodynamics Phase rule
Basic Concept 1f. Solve simple problems on -Force, 1.5 Temperature and zeroth law of
Pressure, Work and Energy physical thermodynamics
quantities, phase rule and laws of 1.6 Ideal gas temperature scale
thermodynamics 1.7 Simple examples (numerical)on Force,
Pressure, Work and Energy physical

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
quantities, phase rule and laws of
thermodynamics

2a. Explain first law and energy -


2.1 First law of thermodynamics
Internal Energy, Enthalpy and Heat
2.2 Internal Energy, Enthalpy and Heat
capacity concepts with examples of
capacity
chemical engineering
2.3 First law for non-flow processes and
Unit – II 2b. Apply first law for non-flow & flow
flow processes of chemical engineering
First Law of process of chemical engineering
2.4 Simple numerical on first law and
Thermodynamics 2c. Solve simple problems on first law
energy - Internal Energy, Enthalpy and
and energy - Internal Energy, Enthalpy
Heat capacity
and Heat capacity
3.1 PVT behavior of pure fluids
Unit – III 3.2 Ideal gas and equation of state
PVT Behavior 3.3 Ideal gas Process :
3a. Explain PVT behaviour of pure
3.3.1 Constant Volume process
fluids
3.3.2 Constant Pressure process
3b. Distinguish Ideal gas Processes
3.3.3 Constant Temperature process
3c. Compare equations of state for real
3.3.4 Adiabatic Process
gases
3.3.5 Polytropic Process
3d. Solve simple problems on Ideal gas
3.4 Equation of state for real gases
Processes, Equation of state for real
3.4.1 Vander Waals Equation
gases,
3.4.2 Virial Equation
3.4.3 Compressibility charts
3.5 Simple examples(numerical)

4.1 Heat effects accompanying chemical


reactions:
4a. Explain the heat effects of
4.1.1 The standard heat of reaction
chemical reactions
Unit – IV 4.1.2 The standard heat of combustion
4b. Apply Hess’s law of constant
Heat Effects 4.1.3 The standard heat of formation
heat summation
4.2 Hess’s Law of constant heat
4c. Calculate heat of reaction and
summation
temperature of reaction
4.3 Effects of temperature on heat of
4d. Solve simple problems on heat
reaction
Effects in chemical reactions
4.4 Temperature of reaction
4.5 Simple numerical

Unit – V 5a. Discuss limitation of first law


5.1 Limitations of first law
Second Law of 5b. Compare different statements of
5.2 Statements of Second law
Thermodynamics Second law

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
5c. Describe the concepts of Heat 5.3 Heat reservoir, Heat engine and Heat
reservoir, Heat engine and Heat pump
pump 5.4 Concept of Entropy
5d. Explain entropy 5.5 Carnot cycle and thermodynamic
5e.Explaincarnot cycle and temperature scale
thermodynamic temperature scale 5.6 Calculation of Entropy change during
5f. Calculate entropy changes 5.6.1 Phase change
5g. Explain the concept of entropy and 5.6.2 Ideal gas processes
irreversibility 5.6.3 Adiabatic mixing
5h. Solve simple problems on Second 5.6.4 Isothermal mixing
law 5.6.5 Chemical reaction
5.7 Clausius Inequality
5.8 Mathematical statement of Second
law
5.9 Entropy and Irreversibility
5.10 Simple numerical

Reference Books

Sr.
Title of Books Author Publication
No.
Chemical Engineering
1 K. V. Narayanan PHI publishers
Thermodynamics
J. M. Smith
Introduction to Chemical Engineering
2 H.C. Vanness Tata McGraw Hill
Thermodynamics
M. M. Abott
3 Thermodynamics C.P.Arora Tata McGraw Hill
Chemical Engineering
4 Y. V. C. Rao Universities Press
Thermodynamics
A.Hougen
5 Chemical Process Principles Vol.2 K.M.Watson Asia Publications
R.A.Ragatz
Textbook of Engineering
6 R. K. Rajput Laxmi Publication
Thermodynamics
Chemical Engineering
7 R. B .Varia AtulPrakashan
Thermodynamics
8 Applied Thermodynamics P. B. Joshi NiraliPrakashan

Lesson planning
COURSE TITLE: INDUSTRIAL MANAGEMENT
(COURSE CODE 3350501)

Hrs.
Unit No. Name of Topic Planned Date
Alloted
Unit I Concept of System and Management 4
1a. Explain concepts of system
1a.1 State Types of systems
1b. Discuss management and Explain its functions
Unit II Organization Structure and Organizational Dynamics 8
17
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
2a. Describe management structure
2b. Explain various factors for structure
2c. Describe various management processes
2d. Classify the organization
2e. Apply SWOT analysis of organizational structure
2f. Explain factors affecting Organizational culture
2g. Discuss moral and relate it with productivity
2h. Identify factors affecting job satisfaction
Unit III Material Management 13
3a. Discuss importance of material management
3b. Explain purchase procedure and system
3c. Classify stores
3c.1 List out various functions of storekeeping
3d. Compare methods of storekeeping
3e. Describe functions of storekeeper
3f. List Types of records types of storage equipment
3g. Discuss Objectives of inventory control and derive
expression for EOQ
3h. Distinguish inventory analysis and inventory models
Unit IV Management Techniques 13
4a. Explain objectives and applications of PPC and CPM ,
PERT
4b List out functions of PPC
4c Calculate critical ratio using Gantt charts
4d. Draw network diagram and determine its critical path
4e. Determine floats and explain crashing of network
4f. Describe concept of value analysis with its importance
and various method
Unit V Factory Act and Laws 4
5a. Describe various provisions of Factory
act and its important provisions

COURSE TITLE: MASS TRANSFER-II


(COURSE CODE: 3350502)

Hrs.
Unit No. Name of Topic Planned Date
Alloted
Unit – I Equipment for Gas Liquid Operations 6
1a. Describe importance of Gas- Liquid operations
1b. Classify equipments for Gas- Liquid operations
1c. Describe construction of equipments with diagram of
1.3 & 1.4
1d. Explain working principle and operation of equipments
with sketches of 1.3 & 1.4
1d. Distinguish different types of packing with diagram

18
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
Unit – II Distillation 15
2a Describe applications
2b Describe the steps to Plot VLE, Constant pressure,
Constant temperature equilibria
2c Explain Relative volatility and laws - Raoult’s, Henry’s
2c.1 State their uses
2d Differenetiateazeotropes
2e Explain
-Flash vaporisation, Differential distillation, Continuous
rectification
2f Calculate amount and composition for Flash
vaporization
2g Calculate product composition for Differential
distillation
2f. Apply McCabe-Theile method for multistage tray tower
for enriching and stripping section
2f.1 Calculate product rates, minimum reflux ratio and
number of trays for the given data
2g. Compare distillation techniques viz
(a) Steam distillation
(b)Vacuum and molecular distillation
(c)Azeotropic and extractive distillation
2h. Distinguish Reboilers
Unit – III Humidification 8
3a. Analyse the VLE for a pure substance
3b. Explain the concepts of Absolute humidity, Relative
saturation, Percentage saturation, Dew point, Dry bulb
temperature, Wet bulb temperature, Adiabatic saturation
temperature, Humid volume, Humid heat, Enthalpy
3c.Evaluate the property of air using DBT and WBT
3e.1 Calculate –absolute humidity, relative saturation,
percentage saturation for the given process data
3d. Draw psychometric chart
3d.1 List Purposes of contact of gas with pure Liquid
3e. Explain construction and working with diagram
Unit – IV Drying 10
4a. Discuss drying equilibrium and related concepts
4a.1 Define and calculation of Moisture content,
Equilibrium and free moisture, Bound and unbound
moisture
4a.2 Calculate - Moisture content, Equilibrium and free
moisture, Bound and unbound moisture from the given
data
4b. Classify drying & drying equipments
4c. Describe construction and working of Drier equipments
4d. Describe drying rate characteristics for batch drying
with sketches
4d.1 Derive equation for drying time for constant rate
period and falling rate period

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PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
4e. Calculate drying time
Unit – V Adsorption & Ion-Exchange 10
5a. Define and state uses of Adsorption
5b. Classify Adsorption and adsorbents
5b.1State Commonly used adsorbents
5d. Analyse Adsorption Equilibria
5d.1 Describe Effect of temperature on adsorption and
Heat of adsorption
5e. Apply Freudlich’s equation for single stage and multi
stage cross-current operation
5e.1Describe adsorption from dilute and concentrated
solution
5f. Describe construction and working of Higgins
contactor, Pressure swing adsorber
5g. Appreciate concepts of Ion Exchange
5g.1 List Applicationv of Ion Exchange
Unit –VI Crystallisation 7
6a. State Industrial applications of crystallization
6b. Explain equilibria mechanism for crystallisation
6b.1 State the methods to get Super saturation
6c. Explain working principle and operation of
Crystallization Equipment with sketch
6c.1Describe construction of Crystallization Equipment
6d. State and explain Meir’s theory
6e. Calculate the crystal yield
6f. List steps to Prevent caking of crystals

Unit NAME OF EXPERIMENT Planned Date


Hrs
No. CH-1 CH-2 CH-3
Demonstrate principle, construction and working
1 of equipments for gas–liquid operations with 4
models
Prepare vapour liquid equilibria curve at
2 4
atmospheric pressure for Benzene-Xylene
3 Carry out simple distillation in glass assembly 4
Find out the effect of vacuum on distillation of
4 4
liquid
Carry out continuous rectification in packed
5 4
column
Find out amount of steam required in steam
6 4
distillation
Find out the property of atmospheric air with the
7 4
help of wet bulb and dry bulb temperature
Set desired conditions of humid air in humidity
8 4
control cabin
Prepare drying curve of moist sand and moist
9 4
limestone
Find out equilibrium moisture content and drying
10 4
time of wet solid
20
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
Characterize industrial adsorbents and observe
11 4
their samples
Remove colour impurities from water using
12 4
charcoal
Find out the yield of crystals from saturated
13 4
solution without seeding
Find out the yield of crystals of from saturated
14 4
solution with seeding

COURSE TITLE: PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY


(COURSE CODE: 3350503)

Hrs.
Unit No. Name of Topic Planned Date
Alloted
Unit – I Basics of Petroleum and Refinery 6
1.1 Occurrence and history of Petroleum
1.2 Crude Petroleum oil reserves in India
1.3 Composition of Petroleum
1.4 Classification of Petroleum
1.5 Refineries development in Gujarat and India
1.6 Types of Refineries
1.7 Refinery processes
1.8 Refinery products
Unit – II Fractionation of Petroleum 8
2.1 Dehydration and Desalting of crude oil
2.2 Pipe still heater
2.3 Atmospheric distillation of crude
2.4 Vacuum distillation of crude residue
2.5 Physical properties of petroleum products and its
measurements :
Unit – III Refinery Processes 10
3.1.1 Purpose of cracking
3.1.2 Effect of temperature and pressure on Cracking
3.1.3 Thermal cracking
3.1.4 catalytic cracking
3.1.5Fluidised bed catalytic cracking
3.2.1 Purpose of Reforming
3.2.2 Differentiate thermal and catalytic reforming
3.2.3 Platforming(Pt catalyst-Reforming)
3.3.1 Hydrotreating
3.3.2 Hydrocracking
3.3.3 Delayed coking
3.3.4 Visbreaking
Unit – IV Treatment Techniques 14
4.1 Purposes and methods of sulphur removal
4.2 Doctor's sweetening
4.3 Catalytic desulfurization
4.4 MEROX treatment
4.5 Treatment of Kerosene by liquid SO2 extraction
21
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
4.6.1 Furtural extraction method
4.6.2 Phenol extraction method
4.6.3 Duo sol extraction process
4.7 Purpose of dewaxingDewaxing Techniques
4.8 Dewaxing without solvent
4.9 Dewaxing with solvent
4.9.1 Ketonedewaxing and propane dewaxing
Unit – V Petrochemicals 18
5.1 Development of petrochemical industry in Gujarat
and in India
5.2.1 Methanol
5.2.2 Formaldehyde
5.3.1 Ethylene dichloride
5.3.2 Vinyl chloride
5.3.3 Ethylene Oxide
5.4.1 Polypropylene.
5.4.2 Propylene oxide
5.5 Chemicals from aromatics
5.6 Manufacture of Linear Alkyl Benzene
5.7 Manufacture of Phenol by benzene sulfonate process

Unit NAME OF EXPERIMENT Hrs Planned Date


No. CH-1 CH-2 CH-3
1 Prepare a detail chart of modern refinery
4
2 Prepare a detail chart of petrochemical products
4
3 Determine flash point by Penskey Martin method
4
4 Determine fire point by Penskey Martin method
4
5 Measure softening point and drop point of Grease
4
6 Measure Aniline point of lubricating oil 4
7 Determine Carbon residue by Ram's bottom method
4
8 Determine Carbon residue by conradson method 4
9 Measure smoke point of kerosene 4
10 Measure cloud point lubricating oil 4
11 Measure pour point lubricating oil 4
Measure Viscosity of lube oil by Redwood
12 /Saybolt/Engler viscometer
4

COURSE TITLE: UTILITIES AND INSTRUMENTATION IN CHEMICAL PLANT


(COURSE CODE: 3350504)
Hrs.
Unit No. Name of Topic Planned Date
Alloted
Unit – I Water as Basic Utility 7
1a. Explain role of Utilities in Chemical Plant
1a.1 List various utilities in chemical plant & uses

22
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
1b. List sources of Water
1c. Differentiate types of Water
1d. Compare Softening processes of water
1e. Explain the process of Purification of water from
raw water with sketches.
Unit – II Steam, Air & Inert Gases 14
2a. Explain uses of utilities - Steam, Air & Inert Gases
2b. Define properties of steam
2c. Label the different part of steam generator
2d. Classify steam generator
2e. Select steam generator
2f. compare steam generators
2g. List the Factors affecting selection of Boiler
2f. Describe construction and
Working of Locomotive Fire tube boiler ,Lancashire
boiler
2g. Discuss utility air
Describe the working principle, application ofAir
compressors – (a) Reciprocating Air
Describe the working principle, application ofAir
compressors – Multistage compressors
Describe the working principle, application ofAir
compressors – (c) Rotary compressors
2i. Describe properties of Inert gases
Unit – III Refrigeration 7
3a. Explain the working principle of refrigeration
3b. Distinguish methods of Refrigeration
3c. Describe COP and TOR of refrigeration
3d. Use primary and secondary Refrigerants
Unit – IV Basics of Instrumentation 4
4a. Classify instruments in chemical plant
4b. Describe Basic elements of instruments
4 4c. Compare Static and Dynamic Characteristics of
instruments
4d. Differentiate First and second order system
Unit- V Measuring Devices 18
5a. Explain Temperature scale
5b. Compare thermometers
5b.1Explain Principle, Construction & Working of :
Mercury in glass, Bi-metallic , pressure spring ,
resistance thermometers
5c. Describe Principles of thermoelectricity and See-
5 back effect, Peltier effect and Thomson effect
5d. Describe principle, construction, working range,
lead wires of thermocouple and Thermowells
5e. Explain principle, construction, and working of
Radiation and optical Pyrometers
5f. Differentiate pressure gauges
5g. Describe principle,
23
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
construction, and working of Target meter, Vortex
Shredding meter, Turbine meter
5h. Classify and explain level measuring devices
5i. Compare viscosity measurement methods
5j. Explain principle, construction, and working
Unit – VI Control Valves, Control Loops & Control System 6
6a. Explain Function of relays and interlocks
6b. Explain schematic control loops for
-Temperature control
-Pressure control
6
- Flow control
- Level control
6c. Describe process control modes with sketches
6d. Explain uses of PLC and DCS System

Unit NAME OF EXPERIMENT Hrs Planned Date


No. CH-1 CH-2 CH-3
1 Operate water treatment in water
treatment plant 4
2 Treat water using lime soda process
4
Generate steam in laboratory using
3
baby boiler 4
Operate and test the working of air
4
compressor 4
Demonstrate different refrigeration
5
cycles 4
6 Measure Temperature by 4
thermometer and thermocouple
Measure Temperature by Bi-metallic
7
thermometer 4
Measure Pressure by mechanical
8
pressure gauge 4
Measure gas flow rate
9

10 Measure level using direct method


4
11 Measure viscosity by capillary tube
4
method
12 Measure specific gravity by
4
Hydrometer
13 Measure pH by pH meter
4

COURSE TITLE: CHEMICAL ENGINEERING THERMODYNAMICS


(COURSE CODE: 3350505)

Hrs.
Unit No. Name of Topic Planned Date
Alloted
Unit – I Introduction and Basic Concept
24
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
1a. Describe scope of thermodynamics

1.1 Define System, functions, properties Process and


surrounding
1b. Explain the System, functions, properties , Process and
surrounding with examples of chemical engineering field
1c. Differentiate systems, functions, properties and processes
1d. Describe Extensive and intensive properties
1e. Explain importance of Force, Pressure, Work and Energy
physical quantities, phase rule and zeroth law of
thermodynamics
1f. Solve simple problems on -Force, Pressure, Work and
Energy physical quantities, phase rule and laws of
thermodynamics
First Law of Thermodynamics
2a. Explain first law and energy - Internal Energy, Enthalpy and
Heat capacity concepts with examples of chemical engineering
Unit – II
2b. Apply first law for non-flow & flow process of chemical
engineering
2c. Solve simple problems on first law and energy - Internal
Energy, Enthalpy and Heat capacity
PVT Behavior
3a. Explain PVT behaviour of pure fluids
Unit – III 3b. Distinguish Ideal gas Processes
3c. Compare equations of state for real gases
3d. Solve simple problems on Ideal gas Processes, Equation of
state for real gases,
Heat Effects
4a. Explain the heat effects of chemical reactions
4b. Apply Hess’s law of constant heat summation
Unit – IV
4c. Calculate heat of reaction and temperature of reaction
4 d. Solve simple problems on heat Effects in chemical
reactions
Second Law of Thermodynamics
5a. Discuss limitation of first law
5b. Compare different statements of Second law
5c. Describe the concepts of Heat reservoir, Heat engine and
Unit – V Heat pump
5d. Explain entropy
5e.Explaincarnot cycle and thermodynamic temperature scale
5f. Calculate entropy changes
5g. Explain the concept of entropy and irreversibility
5h. Solve simple problems on Second law

25
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
Mid Session al Exam Schedule

TIME Chemical
DATE

INDUSTRIAL MANAGEMENT (3350501)

MASS TRANSFER-II (3350502)

PETROLEUM REFINING & PETROCHEMICAL


TECHNOLOGY (3350503)

UTILITIES AND INSTRUMENTATION IN CHEMICAL


PLANT (3350504)

CHEMICAL ENGINEERING THERMODYNAMICS


(3350505)

CDC

WEEKLY TEST
DATE TIME SUBJECT SIGN

INDUSTRIAL MANAGEMENT (3350501)

MASS TRANSFER-II (3350502)

PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY


(3350503)

UTILITIES AND INSTRUMENTATION IN CHEMICAL PLANT


(3350504)

CHEMICAL ENGINEERING THERMODYNAMICS (3350505)

INDUSTRIAL MANAGEMENT (3350501)

MASS TRANSFER-II (3350502)

PETROLEUM REFINING & PETROCHEMICAL TECHNOLOGY


(3350503)

26
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
UTILITIES AND INSTRUMENTATION IN CHEMICAL PLANT
(3350504)

UTILITIES AND INSTRUMENTATION IN CHEMICAL PLANT


(3350504)

CHEMICAL ENGINEERING THERMODYNAMICS (3350505)

Submission Data Report


Parent
Assignment Lab Manual
Sr. Signature
Subject
NO. Half Full Half Full
Submission Submission Submission Submission

1 Mass Transfer- II

Petroleum Refining
2 & Petrochemical
Technology
Utilities &
3 Instrumentation in
Chemical Plant
Chemical
4 Engineering
Thermodynamics
Industrial
5
Management

INDUSTRIAL VISIT

EXPERT LECTURE

The smooth functioning of the institute depends upon observance of discipline by the students. The
institute can help the students better when Rules of Discipline are observed properly. Violation of these
rules deprives the students of the advantages of different facilities provided by the institute. Following
are some of the important rules of discipline.
Parents/Guardians are requested to direct their wards to observe the following Rules of Discipline:

RULES
1. Students must attend lectures, practicals, tutorials, etc. as per the Time Table. They must not
abstain themselves from classes, practicals, tutorials, examinations etc. without written
permission of the Principal. Students whose attendance and/or progress in various tests and
examinations is not satisfactory and who do not perform the required number of tutorials
and/or practical are likely to lose their terms. Students who do not submit compulsory project

27
PARUL INSTITUTE OF ENGINEERING & TECHNOLOGY (DS) – FIRST SHIFT
FIFTHTH SEMESTER CHEMICAL ENGINEERING
STUDENTS HAND-BOOK-2020-21
work in subject are likely to lose their term. Prolonged absence even on grounds of ill health
may also lead to loss of terms. Defaulters will not be sent up for University Examinations.
2. The Identity Card is meant for identifying bonafide students and is used for permitting the
student to participate in various activities and programs of the institute. Every student must
wear the Identity Card as long as he/ she is in the institute campus. It must be produced by the
student whenever demanded by a member of the teaching or non-teaching staff of the
institute. Every student must bring his /her Identity Card to the institute every day. He/She
must take proper care of it to avoid its misuse by other students and outsiders. In case the
Identity Card is lost, the matter should be immediately reported to the Principal and an
application should be made for a duplicate Identity Card which will be issued on payment of
charges.
3. The conduct of the students in the classes and in the premises of the institute shall be such as
will cause no disturbance to teachers, fellow students or other classes.
4. Every student shall wear a clean and decent dress while coming to the institute. To wear Shoes
for the boys and sandal for the girls are compulsory in the institute campus.
5. No Society or Association shall be formed in the institute and no person should be invited on
the institute campus without the specific permission of the Principal. The Principal has a right
to refuse such permission.
6. No student is allowed to display any Notice/Circular/Poster/Banner in the institute premises
without the prior permission of the Principal. Strict action will be taken against the defaulters.
7. All meetings, cultural programs, debates, elocutions, etc. organized on the institute premises
must be held in presence of teaching staff members and with the prior permission of the
Principal. The subjects of debates/elocutions must have the prior approval of the Principal.
8. Students involved in malpractices at the institute / Board / University Examinations will not be
admitted to the institute.
9. Smoking & use of tobacco is strictly prohibited in the institute premises.
10. Mobile phones is strictly prohibited in the classroom.
11. Students must not loiter on the institute premises while the classes are at work.
12. Students shall do nothing inside or outside the institute that will interfere with the discipline of
the institute or tarnish the image of the institute.
Students must be enter the classroom before starting the lecture.
Half & full submission of all subjects are compulsory otherwise examination form will not be
accepted.
Students should not do any kind of misbehavior with the other students and faculty members.
Acts of misbehavior, misconduct, indiscipline or violation of the Rules of Discipline mentioned above
are liable for one or more punishments as stated below:
1. Warning to the student.
2. Warning to the student as well as a letter to the parents.
3. Imposition of a fine.
4. Denial of library, laboratory, student aid or any other facility for a specified period or for the
whole Term/year.
5. Cancellation of Terms.
6. Refusal of admission in the next term or academic year.
7. Cancellation of admission.
8. Expulsion from the institute for a specified period.
9. Rustication.

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