Professional Documents
Culture Documents
2 0 1 8;7(1):89–95
www.jmrt.com.br
Original Article
a r t i c l e i n f o a b s t r a c t
Article history: Testing and evaluation of mechanical properties for FRP (Fiber Reinforced Polymer) com-
Received 7 March 2016 posite parts play a significant role to qualify it for the end use. Among the mechanical
Accepted 21 June 2017 properties, the flexural strength is significant and vital as it may vary with specimen depth,
Available online 3 November 2017 temperature and the test span length. The flexural strength varies for different materials
with varying the test span length hence the current work aims to find an optimum span
Keywords: length to test flexural strength for the specimens made of Glass (7781, EC9756) and Carbon
Carbon (HTA7, G801) prepreg materials. Experiments are conducted as per the ASTM Standard D
Glass 790 for flexural test by varying the span lengths to understand the behavior of the flexural
Flexural strength and flexural modulus. The experimental data were compared with those obtained
Prepreg from the finite element program software Altair Hyper works 14.0. The results indicate that
Span length flexural modulus increases with the span length to a point and then it decreases. Thereby,
FEA an optimum span length can be obtained for testing flexural strength, which will be useful
to the designers and the composite manufacturers to accomplish better standard testing
procedures.
© 2018 Brazilian Metallurgical, Materials and Mining Association. Published by Elsevier
Editora Ltda. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).
fraction of fibers on the three-point bend testing of glass fiber- span length for a particular type of composite material. This
reinforced composite laminates. They found that the flexural paper solicits to find the optimum testing span length for flex-
strength obeys a simple law of mixture relationship with fiber ural strength of four commercially used BD Carbon fiber G801,
loading but the shear strengths were independent of fiber BD Glass fiber-7781, UD carbon fiber-HTA7 and UD Glass fiber-
loading. Variation in the amount of overhang had no effect EC9756 materials. Bending moment in a three-point bending
on the shear strength of the composites, but they have not test increases from the support points of the beam to a max-
evaluated the effect of variation in span length on flexural imum value at mid-point, i.e., maximum stress is reached
strength. Nunes et al. [3] have carried studies on polymeric along a line at the center of the beam, where the bending
matrix composite discs supported on three points subjected moment and the flexural stress is given by the following equa-
to a bending test to study their behavior in complex flexural tions.
loading situations. These authors [3] noticed that the flexural
P L PL
behavior of the composites varies on fiber orientation, lam- Bending moment, M = × = (1)
2 2 4
inate stacking and surface waviness. Grande et al. [4] have
carried studies to evaluate whether the span/diameter ratio 3PL
Flexural stress, f = (2)
(L/D) would affect the mechanical properties of fiber reinforced 2bd2
composite posts. They noticed that the span diameter ratio
is an important parameter for the interpretation of flexural where P is the load, L is the length of support span, b is the
strength and flexural modulus. Valarinho et al. [5] conducted width of test specimen and t is the thickness/depth of test
experiments to study the flexural behavior of multi span com- specimen.
posite beams made of annealed glass panes reinforced with If support span-to-depth ratio greater than 16/1 are used
GFRP. They mentioned that the ultimate load and the post- such that deflections in excess of 10% of the support span
cracking performance of the multi span composite beams are occur, the stress in the outer surface of the specimen for a sim-
affected by the type of the adhesive used to bond the GRFP ple beam can be reasonably approximated with the following
to glass panes. Studies on the flexural fatigue behavior and equation [13].
enhancement of residual strength in 2D cross-ply carbon fiber D 2 d D
reinforced carbon composites were done to show that the 3PS
f = 1+6 −4 (3)
three-point bending fracture in both unfatigued and fatigued 2bd2 L L L
specimens is of delamination mode [6]. Few research has been
done on short fiber reinforced composites to study the effect where D is the deflection of the center line of the specimen at
of flexural strength with different span lengths. It was found the middle of the support span.
that as the span length reduces the flexural properties showed When large support span-to-depth ratios are used, signif-
linear reduction [7]. Few studies have been reported earlier to icant end forces are developed at the support noses which
analyze the effects of the specimen thickness and width on will affect the moment in a simply supported beam. Eq. (3)
the flexural modulus in general for a composite laminate using includes additional terms that are an approximate correction
Ansys [8]. However, the effect of the testing span length was factor for the influence of these end forces in large support
not considered and the testing span length set for one class span-to-depth ratio beams where relatively large deflections
of material will not be the same for other types of laminates. exist. Flexural modulus is calculated by drawing a tangent to
Kumar et al. [9] conducted experiments to study the impact the steepest initial straight-line portion of the load-deflection
of the UTM testing speed on the inter-laminar shear stress curve and is given by Eq. (4).
and the flexural strength on fiber composites. Singh et al. [10]
have carried experiments and found that with increasing in L3 m
Ef = (4)
weight fraction of reinforcement, the tensile strength and flex- 4bd3
ural strength increased by 14.5% and 123.65% for 20% glass
where m is the slope of the tangent to the initial straight-line
reinforced composites over pure epoxy. Haldar et al. [11] inves-
portion of the load-deflection curve.
tigated the behavior of curved sandwich composite structures
by performing flexural test for two different radii of curvature.
Stiffness, strength and failure initiation were predicted using 2. Materials and method
Finite Element Analysis (FEA) and the numerical simulations
were verified with the experimental measurements. Alander Prepreg materials of Carbon UD (Hexply 913/35%/132/HTA7),
et al. [12] have carried experiments to find flexural strength Carbon BD (Hexply 913/40%/G 801), Glass UD (Hexply
and flexural modulus of fiber-reinforced composite (FRC) spec- 913/28%/192/EC 9756) and Glass BD (Hexply 913/37%/7781)
imens of rectangular and circular cross-sections with varying were used to manufacture the laminates. Hand-lay-up
span length (L) to diameter (D) ratio. On the basis of their method was used to manufacture the laminates of size
results, it was concluded that by increasing L/D ratio, the (150 mm × 150 mm) with [0/90]s layer stacking sequence and
flexural strength and flexural modulus increased for shorter were cured in autoclave. The cured laminates are tested for
span length up to 20 mm. Hence the testing method, speci- NDT tests like Ultrasonic C scan test to check the internal
men dimensions and the process parameters play a significant defects like voids and the compaction of the cured laminates
role in the evaluation of flexural strength of any composite and the C scan images of the four laminates were tested as
laminate. So, it is necessary to determine the effect of the test- shown in Figs. 1–4. The C scan profile indicates the absence of
ing span length on the flexural properties to find an optimum the voids and internal defects in the cured laminates. All four
j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95 91
CFRP-HTA7 CFRP-G801
1000
Without correction factor
With correction factor
950
(80,931.064)
Flexural strength (MPa)
900
(80,877.238)
850 (64,845.8)
800
(48,786.329)
750 (32,750.241)
700
30 40 50 60 70 80
Span length (mm)
Fig. 6 – Flexural strength curves with the testing span length in Carbon BD-G801 laminate.
900
Without correction factor
With correction factor
800
(80,762.408)
Flexural strength (MPa)
700
(64,669.453)
(80,632.87)
(48,606.077) (64,615.51)
600
(48,576.91)
500
(32,449.267)
400
30 40 50 60 70 80
Span length (mm)
Fig. 7 – Flexural strength curves with the testing span length in Glass BD-7781 laminate.
modulus (Ef ) and support span length (L) for all four materials lengths 24 mm and 96 mm. It is concluded that the polynomial
as shown in Figs. 10–13. of degree 3 provides best fit for the data points with minimum
To find the optimum span length, best fit curve approach percentage error between numerical results and experimen-
is used. Apart from the span lengths 32 mm, 48 mm, 64 mm tal results, due to which the data is extrapolated for other two
and 80 mm, the numerical analysis is done for two extra span materials using the equation of curve. The values of flexural
j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95 93
(32,1258.233)
1250
(64,1166.694) (80,1164.58)
1150
(64,1111.275)
1100 (80,1102.282)
1050
1000
30 40 50 60 70 80
Fig. 8 – Flexural strength curves with the testing span length in Carbon UD-HTA7 laminate.
1600
Without correction factor
With correction factor
1500
1400 (32,1402.93)
Flexural strength (MPa)
(48,1373.921)
(64,1327.5) (80,1322.618)
1300
(48,1222.746)
1200
1100
(64,1026.208)
1000
900
(80,862.502)
800
30 40 50 60 70 80
Fig. 9 – Flexural strength curves with the testing span length in Glass UD-EC9756 laminate.
Table 1 – Comparison (reaction force) of the numerical Table 2 – Comparison (displacement) of the numerical
analysis results with the experimental analysis results analysis results with the experimental analysis results
for Carbon UD-HTA7 laminate. for Carbon UD-HTA7 laminate.
Span length (mm) Reaction force (N) Span length (mm) Displacement (mm)
24 600 – 24 0.5 –
32 1691.02 1577.8 32 1.95 2.02
48 943.57 940.8 48 3.3 3.66
64 660.47 627.2 64 6.45 6.53
80 563.58 529.2 80 9.75 9.7
96 247 – 96 10 –
modulus are then calculated for various span lengths below length is at the point where the maxima of flexural modu-
32 mm and above 80 mm. Analysis depicts that the flexural lus vs span length curve occurs. The values of optimum span
modulus initially increases and then decreases gradually with length obtained from the graphs on the modulus basis are the
the increase in the span length for all four materials. The following. For CFRP-G801 was 80 mm, GFRP-7781 was 67 mm,
behavior of the flexural modulus shows the optimum span CFRP-HTA7 was 48 mm and GFRP-EC 9756 was 42 mm.
94 j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95
Glass BD-7781
Table 3 – Comparison (reaction force) of the numerical 25000
analysis results with the experimental analysis results
5000
24 1669 –
32 1079 941 0
0 10 20 30 40 50 60 70 80 90
48 820 617
Span length (mm)
64 595 480
80 449 405 Experimental
96 285 –
Fig. 12 – Flexural modulus behavior with the span length
for Glass BD 7781 laminate.
Table 4 – Comparison (Displacement) of the Numerical
analysis results with the Experimental analysis results
Glass UD-EC9756
for Carbon BD-G801 laminate. 40000
50000
40000
4. Conclusion
30000
50000 HTA7.
40000
their support and encouragement to carry out this research [7] Garoushi S, Lassila LV, Vallittu PK. The effect of span length
work. of flexural testing on properties of short fiber reinforced
composite. J Mater Sci 2012;23(2):325–8.
[8] Kumar MP, Murthy VB. Effect of specimen dimensions on
references flexural modulus in a 3-point bending test. Int J Eng Res
Technol (IJERT) 2012;1(8):1–6.
[9] Kumar KV, Safiulla M, Ahmed ANK. Influence of UTM testing
[1] Park R, Jang J. Stacking sequence effect of aramid-UHMPE speed on ILSS and flexural strength of fiber epoxy
hybrid composites by flexural test method. J Polym Test composites. IJAIR 2012:327–32.
1997;16:549–62. [10] Singh S, Kumar P, Jain SK. An experimental and numerical
[2] Christiansen W, Lilley J, Shortall JB. A three point bend test investigation of mechanical properties of glass fiber
for fiber reinforced composites. J Fiber Sci Technol reinforced epoxy composites. Adv Mater Lett
1974;7:1–13. 2013;4(7):567–72.
[3] Nunes JP, Pouzada AS, Bernardo CA. The use of a three-point [11] Haldar S, Caputo D, Buesking K, Bruck HA. Flexural behavior
support flexural test to predict the stiffness of anisotropic of singly curved X-Cor sandwich composite structures:
composite plates in bending. J Polym Test 2002;21:27–33. experiment and finite element modeling. Compos Struct
[4] Grande NM, Plotino G, Ioppolo P, Bedini R, Pameijer CH, 2015;129:70–9.
Somma F. The effect of custom adaptation and [12] Alander P, Lassila LVJ, Vallittu PK. The span length and
span-diameter ratio on the flexural properties of cross-sectional design affect values of strength. Dent Mater
fiber-reinforced composite posts. J Dent 2009;37:383–9. 2005;21:347–53.
[5] Valarinho L, Correia JR, Branco FA. Experimental study on [13] ASTM D 790-70. Plastics (I). Standard test methods for
the flexural behaviour of multi-span transparent glass–GFRP flexural properties of unreinforced and reinforced plastics
composite beams. J Construct Build Mater 2013;49:1041–53. and electrical insulating materials. Annual book of ASTM
[6] Xue LZ, Li K, Jia Y, Zhang S, Cheng J, Guo J. Flexural fatigue standards. American Society for Testing and Materials;
behavior of 2D cross-ply carbon/carbon composites at room 2002.
temperature. J Mater Sci Eng A 2015;634:209–14.