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j m a t e r r e s t e c h n o l .

2 0 1 8;7(1):89–95

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Original Article

Experimental investigation of span length for


flexural test of fiber reinforced polymer composite
laminates

Akhil Mehndiratta a,∗ , Spandan Bandyopadhyaya b , Vijaya Kumar c , Dhiraj Kumar a


a Indian Institute of Technology (Indian School of Mines), Dhanbad, Jharkhand, India
b Indian Institute of Engineering Science and Technology, West Bengal, India
c Hindustan Aeronautics Limited, Bangalore, India

a r t i c l e i n f o a b s t r a c t

Article history: Testing and evaluation of mechanical properties for FRP (Fiber Reinforced Polymer) com-
Received 7 March 2016 posite parts play a significant role to qualify it for the end use. Among the mechanical
Accepted 21 June 2017 properties, the flexural strength is significant and vital as it may vary with specimen depth,
Available online 3 November 2017 temperature and the test span length. The flexural strength varies for different materials
with varying the test span length hence the current work aims to find an optimum span
Keywords: length to test flexural strength for the specimens made of Glass (7781, EC9756) and Carbon
Carbon (HTA7, G801) prepreg materials. Experiments are conducted as per the ASTM Standard D
Glass 790 for flexural test by varying the span lengths to understand the behavior of the flexural
Flexural strength and flexural modulus. The experimental data were compared with those obtained
Prepreg from the finite element program software Altair Hyper works 14.0. The results indicate that
Span length flexural modulus increases with the span length to a point and then it decreases. Thereby,
FEA an optimum span length can be obtained for testing flexural strength, which will be useful
to the designers and the composite manufacturers to accomplish better standard testing
procedures.
© 2018 Brazilian Metallurgical, Materials and Mining Association. Published by Elsevier
Editora Ltda. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).

semi rigid materials. However, flexural strength cannot be


1. Introduction determined for those materials that do not break or that do not
fail in the outer surface of the test specimen within the 5.0%
Flexural or bending test can be used to get a semi qualitative
strain limit. These test methods utilize either a three-point
idea of the fiber/matrix interfacial strength of a composite.
or four-point loading system to a simply supported beam.
The flexural tests are conducted to determine the mechanical
Park et al. [1] have carried few studies on the changes in flex-
properties of resin and laminated fiber composite materials.
ural strength with the change in stacking sequence of aramid
These test methods are generally applicable to both rigid and
fiber composite laminates. They found that the flexural fail-
ure mechanism, which had an effect on the flexural strength,
∗ depends on the stacking sequence. Christiansen et al. [2] have
Corresponding author.
E-mail: akhilm.ratta@gmail.com (A. Mehndiratta). investigated the effect of testing variables and the volume
https://doi.org/10.1016/j.jmrt.2017.06.010
2238-7854/© 2018 Brazilian Metallurgical, Materials and Mining Association. Published by Elsevier Editora Ltda. This is an open access
article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
90 j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95

fraction of fibers on the three-point bend testing of glass fiber- span length for a particular type of composite material. This
reinforced composite laminates. They found that the flexural paper solicits to find the optimum testing span length for flex-
strength obeys a simple law of mixture relationship with fiber ural strength of four commercially used BD Carbon fiber G801,
loading but the shear strengths were independent of fiber BD Glass fiber-7781, UD carbon fiber-HTA7 and UD Glass fiber-
loading. Variation in the amount of overhang had no effect EC9756 materials. Bending moment in a three-point bending
on the shear strength of the composites, but they have not test increases from the support points of the beam to a max-
evaluated the effect of variation in span length on flexural imum value at mid-point, i.e., maximum stress is reached
strength. Nunes et al. [3] have carried studies on polymeric along a line at the center of the beam, where the bending
matrix composite discs supported on three points subjected moment and the flexural stress is given by the following equa-
to a bending test to study their behavior in complex flexural tions.
loading situations. These authors [3] noticed that the flexural
P L PL
behavior of the composites varies on fiber orientation, lam- Bending moment, M = × = (1)
2 2 4
inate stacking and surface waviness. Grande et al. [4] have
carried studies to evaluate whether the span/diameter ratio 3PL
Flexural stress, f = (2)
(L/D) would affect the mechanical properties of fiber reinforced 2bd2
composite posts. They noticed that the span diameter ratio
is an important parameter for the interpretation of flexural where P is the load, L is the length of support span, b is the
strength and flexural modulus. Valarinho et al. [5] conducted width of test specimen and t is the thickness/depth of test
experiments to study the flexural behavior of multi span com- specimen.
posite beams made of annealed glass panes reinforced with If support span-to-depth ratio greater than 16/1 are used
GFRP. They mentioned that the ultimate load and the post- such that deflections in excess of 10% of the support span
cracking performance of the multi span composite beams are occur, the stress in the outer surface of the specimen for a sim-
affected by the type of the adhesive used to bond the GRFP ple beam can be reasonably approximated with the following
to glass panes. Studies on the flexural fatigue behavior and equation [13].
enhancement of residual strength in 2D cross-ply carbon fiber   D 2  d   D 
reinforced carbon composites were done to show that the 3PS
f = 1+6 −4 (3)
three-point bending fracture in both unfatigued and fatigued 2bd2 L L L
specimens is of delamination mode [6]. Few research has been
done on short fiber reinforced composites to study the effect where D is the deflection of the center line of the specimen at
of flexural strength with different span lengths. It was found the middle of the support span.
that as the span length reduces the flexural properties showed When large support span-to-depth ratios are used, signif-
linear reduction [7]. Few studies have been reported earlier to icant end forces are developed at the support noses which
analyze the effects of the specimen thickness and width on will affect the moment in a simply supported beam. Eq. (3)
the flexural modulus in general for a composite laminate using includes additional terms that are an approximate correction
Ansys [8]. However, the effect of the testing span length was factor for the influence of these end forces in large support
not considered and the testing span length set for one class span-to-depth ratio beams where relatively large deflections
of material will not be the same for other types of laminates. exist. Flexural modulus is calculated by drawing a tangent to
Kumar et al. [9] conducted experiments to study the impact the steepest initial straight-line portion of the load-deflection
of the UTM testing speed on the inter-laminar shear stress curve and is given by Eq. (4).
and the flexural strength on fiber composites. Singh et al. [10]
have carried experiments and found that with increasing in L3 m
Ef = (4)
weight fraction of reinforcement, the tensile strength and flex- 4bd3
ural strength increased by 14.5% and 123.65% for 20% glass
where m is the slope of the tangent to the initial straight-line
reinforced composites over pure epoxy. Haldar et al. [11] inves-
portion of the load-deflection curve.
tigated the behavior of curved sandwich composite structures
by performing flexural test for two different radii of curvature.
Stiffness, strength and failure initiation were predicted using 2. Materials and method
Finite Element Analysis (FEA) and the numerical simulations
were verified with the experimental measurements. Alander Prepreg materials of Carbon UD (Hexply 913/35%/132/HTA7),
et al. [12] have carried experiments to find flexural strength Carbon BD (Hexply 913/40%/G 801), Glass UD (Hexply
and flexural modulus of fiber-reinforced composite (FRC) spec- 913/28%/192/EC 9756) and Glass BD (Hexply 913/37%/7781)
imens of rectangular and circular cross-sections with varying were used to manufacture the laminates. Hand-lay-up
span length (L) to diameter (D) ratio. On the basis of their method was used to manufacture the laminates of size
results, it was concluded that by increasing L/D ratio, the (150 mm × 150 mm) with [0/90]s layer stacking sequence and
flexural strength and flexural modulus increased for shorter were cured in autoclave. The cured laminates are tested for
span length up to 20 mm. Hence the testing method, speci- NDT tests like Ultrasonic C scan test to check the internal
men dimensions and the process parameters play a significant defects like voids and the compaction of the cured laminates
role in the evaluation of flexural strength of any composite and the C scan images of the four laminates were tested as
laminate. So, it is necessary to determine the effect of the test- shown in Figs. 1–4. The C scan profile indicates the absence of
ing span length on the flexural properties to find an optimum the voids and internal defects in the cured laminates. All four
j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95 91

Fig. 4 – C scan profile of EC 9756 laminate.


Fig. 1 – C scan profile of HTA7 laminate.

laminates show the satisfactory attenuation levels and there


is no indication of poor compaction.
The specimens were prepared from the cured laminates
as per the ASTM D 790 standards in rectangular cross-section
specimens (127 mm × 12.7 mm × 2 mm) as shown in Fig. 5.
Three-point bending test was performed on a Universal
Testing Machine (UTM) manufactured by Star Testing System,
Bombay with a maximum load cell of 50,000 N. The tests were
carried at a crosshead speed of 2 mm/min and at four differ-
ent span-to-depth ratio, i.e., 16 mm, 24 mm, 32 mm and 40 mm
and depth of the specimen is taken as 2 mm for all the spec-
imens. Five specimens of each material were tested and the
load-deflection curves are plotted for different materials with
varying span length to determine the flexural strength and
flexural modulus.

3. Results and discussion


Fig. 2 – C scan profile of G801 laminate.
The flexural strength was calculated for specimens tested
at different span lengths using the formulae given by Eqs.
(2) (with correction factor) and (3) (without correction fac-
tor). From the characteristic graphs, it shows that the flexural
strength increases with increase in span length for both car-
bon and glass BD (G801 & 7781) as shown in Figs. 6 and 7, while
it decreases with increase in span length for carbon and glass
UD laminates (HTA7 & EC 9756) as shown in Figs. 8 and 9, which
signifies that the BD laminates are more stiffer and stronger
than the UD laminates, as the maximum bending displace-
ment is obtained in the BD laminates.
Flexural modulus was calculated using Eq. (4) to determine
the optimum span length for the selected material laminates.
Numerical analysis was carried out using Altair Hyper
Works.14.0 to evaluate the flexural behavior of Carbon UD-
HTA7 and Carbon BD-G801 with span lengths of 24 mm,
32 mm, 48 mm, 64 mm, 80 mm and 96 mm. The comparison
of values of reaction force and displacement obtained from
numerical analysis results with the experimental analysis
Fig. 3 – C scan profile of 7781 laminate. results is presented in Tables 1–4.
Flexural modulus values were obtained from numerical
and experimental results of Carbon UD-HTA7 and Carbon BD-
G801. Characteristic graphs are plotted between the flexural
92 j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95

CFRP-HTA7 CFRP-G801

GFRP-7781 GFRP-EC 9756

Fig. 5 – Flexural test specimens.

1000
Without correction factor
With correction factor
950
(80,931.064)
Flexural strength (MPa)

900
(80,877.238)

850 (64,845.8)

800
(48,786.329)

750 (32,750.241)

700

30 40 50 60 70 80
Span length (mm)

Fig. 6 – Flexural strength curves with the testing span length in Carbon BD-G801 laminate.

900
Without correction factor
With correction factor

800
(80,762.408)
Flexural strength (MPa)

700
(64,669.453)

(80,632.87)
(48,606.077) (64,615.51)
600
(48,576.91)

500

(32,449.267)

400

30 40 50 60 70 80
Span length (mm)

Fig. 7 – Flexural strength curves with the testing span length in Glass BD-7781 laminate.

modulus (Ef ) and support span length (L) for all four materials lengths 24 mm and 96 mm. It is concluded that the polynomial
as shown in Figs. 10–13. of degree 3 provides best fit for the data points with minimum
To find the optimum span length, best fit curve approach percentage error between numerical results and experimen-
is used. Apart from the span lengths 32 mm, 48 mm, 64 mm tal results, due to which the data is extrapolated for other two
and 80 mm, the numerical analysis is done for two extra span materials using the equation of curve. The values of flexural
j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95 93

Without correction factor


1300 With correction factor

(32,1258.233)
1250

Flexural strength (MPa) 1200 (48,1200.92)

(64,1166.694) (80,1164.58)
1150

(64,1111.275)
1100 (80,1102.282)

1050

1000
30 40 50 60 70 80

Span length (mm)

Fig. 8 – Flexural strength curves with the testing span length in Carbon UD-HTA7 laminate.

1600
Without correction factor
With correction factor
1500

1400 (32,1402.93)
Flexural strength (MPa)

(48,1373.921)
(64,1327.5) (80,1322.618)
1300

(48,1222.746)
1200

1100

(64,1026.208)
1000

900
(80,862.502)

800

30 40 50 60 70 80

Span length (mm)

Fig. 9 – Flexural strength curves with the testing span length in Glass UD-EC9756 laminate.

Table 1 – Comparison (reaction force) of the numerical Table 2 – Comparison (displacement) of the numerical
analysis results with the experimental analysis results analysis results with the experimental analysis results
for Carbon UD-HTA7 laminate. for Carbon UD-HTA7 laminate.
Span length (mm) Reaction force (N) Span length (mm) Displacement (mm)

Numerical analysis Experimental analysis Numerical analysis Experimental analysis

24 600 – 24 0.5 –
32 1691.02 1577.8 32 1.95 2.02
48 943.57 940.8 48 3.3 3.66
64 660.47 627.2 64 6.45 6.53
80 563.58 529.2 80 9.75 9.7
96 247 – 96 10 –

modulus are then calculated for various span lengths below length is at the point where the maxima of flexural modu-
32 mm and above 80 mm. Analysis depicts that the flexural lus vs span length curve occurs. The values of optimum span
modulus initially increases and then decreases gradually with length obtained from the graphs on the modulus basis are the
the increase in the span length for all four materials. The following. For CFRP-G801 was 80 mm, GFRP-7781 was 67 mm,
behavior of the flexural modulus shows the optimum span CFRP-HTA7 was 48 mm and GFRP-EC 9756 was 42 mm.
94 j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95

Glass BD-7781
Table 3 – Comparison (reaction force) of the numerical 25000
analysis results with the experimental analysis results

Flexural modulus (MPa)


for Carbon BD-G801 laminate. 20000

Span length (mm) Reaction force (N) 15000

Numerical analysis Experimental analysis 10000

5000
24 1669 –
32 1079 941 0
0 10 20 30 40 50 60 70 80 90
48 820 617
Span length (mm)
64 595 480
80 449 405 Experimental
96 285 –
Fig. 12 – Flexural modulus behavior with the span length
for Glass BD 7781 laminate.
Table 4 – Comparison (Displacement) of the Numerical
analysis results with the Experimental analysis results
Glass UD-EC9756
for Carbon BD-G801 laminate. 40000

Flexural modulus (MPa)


Span length (mm) Displacement (mm) 35000
30000
25000
Numerical analysis Experimental analysis
20000
24 1.5 – 15000
10000
32 1.65 1.6
5000
48 4.2 3.5 0
0 10 20 30 40 50 60 70 80 90
64 6.5 5.6
Span length (mm)
80 9 8.8
96 12 – Experimental

Fig. 13 – Flexural modulus behavior with the span length


Carbon BD-G801 for Glass UD-EC9756 laminate.
60000
Flexural modulus (MPa)

50000

40000
4. Conclusion
30000

20000 The behavior of flexural strength and flexural modulus with


10000 the test span length was evaluated for four materials at four
0
different test span lengths as per the ASTM standards. The
0 20 40 60 80 100 120 results depict that the flexural strength increases with the test
Span length (mm) span length for the specimens made out of BD (Bi-Directional)
Numerical Experimental prepreg layers. Similarly, the flexural strength decreases grad-
ually with the increase in test span length for the specimens
Fig. 10 – Flexural modulus behavior with the span length made out of UD (Uni-Directional) prepreg layers. However,
for Carbon BD G-801-laminate. the flexural modulus increases with the increase in the span
length up to a point and then it gradually decreases for both
UD and BD materials.
Carbon UD-HTA7
The experimental results and the numerical analysis
70000 proved a good agreement for all four materials as evident from
60000 the results obtained for the Carbon BD-G-801 and Carbon UD-
Flexural modulus (MPa)

50000 HTA7.
40000

30000 Conflicts of interest


20000

10000 The authors declare no conflicts of interest.


0
0 20 40 60 80 100 120
Span length (mm) Acknowledgements
Numerical Experimental
This work was carried out in Composite Manufacturing Divi-
Fig. 11 – Flexural modulus behavior with the span length sion, Hindustan Aeronautics Limited, Bangalore. The authors
for Carbon UD-HTA7 laminate. thank Shri. S.V. Suresh, General Manager (CMD), Shri Krishna
Murari, DGM (QA), Shri Mukhyopadhyay, DGM(Shop), Shri.
Pranab Biswal M (QA), Shri. Parthim Er (QA) and all others for
j m a t e r r e s t e c h n o l . 2 0 1 8;7(1):89–95 95

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