Expariment No. 4
Course + Chem — 44
Namo of the experiment: STANDARDIZATION OF Soptum
TUIMSULPHATE = SoLUTION WITH A STANDARD POTASSIUM
SICHROMATE = SOLUTION -
Dote of performance: 01-11-2020
bote of Submission: 13-11 ~ 2620
Name: Anas Bin Faceoque
Student Ib: 190414)
Doparctment-: Gj) enginerccing
Seckion: OLIntreoduction :
This oridization eaperdment 16 boged on oxidation
and reeduction copation as well 0s badometrie recaction -
The main gurpese of this reaction ie to stondarcdize
NoqS20, Solution wht, stordand = Falrgbg Seluhon -
Veoge of = Nag&0g !
* Widely vaed +o dochlerernate wictere 5 asta miming » Ag—
based photographie plates and omalpt col chemistry.
x Veed to trooh sm eyomie peleorimg and skin
Aigoases
x WHO lieted — eggontiol —modicine -
Theorey *
Titration of = lodine ore clecting with ledine
libarcated — frcom —ghomies! reaction 16 called Fodimotric,
and jedometrac — reeactrons revepective bj This reachon
16
\ Todemerue according to the definition. Theof this experiment are
Reactions
SEI + IAHOL + Kleen, = Deeelg-+ Bly + Fo+ eka
417+ He 4 Crp 6 + Co = Ded* 4 OIy_+ TH20
2no9S16, tr Ty = NepS20 + QNal
S03" +0o- = Sqoe™” + ce
Here KaGrn is an ondizing agent and I~
ie roduc, agent: Tn the second ranchon
Ty, is an ondiaing agent and Sy bP 15 -am
& — reeducing ogent=
Jn tne second stop a .sporific indiceton hos
used which 16 Starch.
Slacch + Ty = Starch — Iodine (Bue)
Storch - todine + £5902" = Stomh +6I-+ 344927
The blue eslore of the = lution will Alcappeare.
Ol te Velie fe gd
been
OS Bon os
46 fedide ton.Here, L mol Gredf” = B mel Ig = Emel SOR
ue lasizes
Equivalent ross of keel
6
= 24 = 4%
Noremal vhonpaint :
AN Cr0g" = AN 92037"
Encoss ledine enhances solubility and minimizes
doled vol ality
helt = In”
Ix)
fo = Foo
[=] f+)
dota table: Standaredigetion of sodium Hivsulpae Solution
with etandard — potascryum = Aichrewmate Solu on
Bb5. Nol. of Burette roading ren ANG Vo)
No 04 a
[6 fae | ee =
[oe lie 2 5
—a a
18.2. apd 2
at2 | Bor 7Aleulotion
LN Gy Crab = 0-44
Moss of Cradk*” = 0.5%9
Se ak + eT
0.49
Hoes ob Geng = 1 rF I el
Motos ef Ty = FER OTN KS = STAKITT mo]
Moles of So =
[5283] = hoorxie of sx 73
EBV KOT KL = OCH 1S 3 orol
= G118M
Errore on ages ;
0.109 M
[520377] aduol
= lone-ero3l ooo
Se,
7 of orcreore 0105
> B67,Discussion’.
Some precoutions which must be toben to donde the
@rpertyment:
x Suffident amount of kx should be added +o form
lg ion.
% Starch should be added only ofter. the solvtion turns
light yellew.
+ Measurements should bo taken cautiously ,
# End print mug be eteremiined earcofully,
There Were Some ermarns. Rasens Reosons may jndudbe-
The given dichromate solution was nol 1007. pure.
The I, thet was roleased during he todo-
metric proeess got —ovapertetad. “The readivgs
which wera taKon from burette = Were not
100% prease ote.