BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani Campus AUGS/ AGSR Division SECOND SEMESTER 2019-20 COURSE HANDOUT Date: 17.08.2020 In addition to part I (General Handout for all courses appended to the Time table) this portion gives further specific details regarding the course. Course No : CHE F211 Course Title : CHEMICAL PROCESS CALCULATIONS Instructor-in-Charge : BANASRI ROY Instructor(s) : BANASRI ROY ‘Tuto W/Practical Instructors: Bheema Rajesh Kumar (RS) 1. Course Description: Historical overview of Chemical Engineering, Principles of balancing with examples to illustrate differential and integral balances lumped and distributed balances, Material balances in simple systems involving physical changes and chemical reactions, Systems involving recycle, purge and bypass, Properties of substances: single component & multicomponent, single and multiphase systems. Ideal liquid and gaseous mixtures, Energy balance calculations in simple systems, Introduction to Computer aided calculations-steady state material and energy balances for chemical plants 2. Scope and Objective of the Course Scope This course provides an introduction to the basic fundamentals of chemical engineering. It deals with calculations, which form the basis of the design of a chemical industrial plant or process. It aims to inculcate conceptual knowledge as well as systematic and sound problem solving skills in the student. The concept of material and energy balances are introduced, explained, and worked with the help of examples from the real world chemical process plants Fundamentals of this course would be required for other courses like Chemical Process Technology, Chemical Reaction Engineering, Separation Processes and Process Modelling and. Simulation. Objective: At the end of this course, the students must be able to Apply important definitions and conventions in chemical processes. + Solve material and energy balances for single and multiple units with or without chemical reaction and feedback/bypass. 3. Text Books (TB): Himmelblau, D.M. & Riggs, J.B. “Basic Principles and Calculations in ‘Chemical Engineering”, PHI, 8th Edition 2012. 4. Reference Books (RB) : Felder R.M., Rousseau, RW. “Elementary Principles of Chemical Processes” John Wiley & Sons, 3rd Edition 2000.5. Course Pla BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani Campus AUGS/ AGSR Division Review preliminaries: Units & Dimensions, Conversion of units, Dimensional consistency Module Topics Covered in Lecture (L) Reference | Learning Outcomes Number & ChJSec. _ | (students be able Title to-) MI: Li: Introduction to chemical TB: 2.1-23 | Realize utility and Introductory | engineering, Importance of process need for CPC in Concepts —_| calculations in chemical industry. process industry. Review of units. 2: Review preliminaries: Mole, Density, Specific Gravity, Flow Rate, Mole & Mass Fraction, Temperature, Pressure, Energy Balances. Significant figures, Choosing a Basis, Multi-Component Solution & Mixtures, Concentration, TR 2.12 M2: Material L3-L4: Open vs Closed systems, Understand these definitions. Apply in calculations, Prepare to perform material and energy balances. gas vs real gas systems gas mixtures and partial pressure, real gas compressibility L16: Real gas equations of state (only main concept), TB:7. Balance Steady vs Unsteady state systems, preliminaries | Multi component systems, Systems with chemical reactions, Problem solving strategy, solution validation. M3: 5-L6: Application of the M2 TBa Calculate various Material concepts: Material Balance Problems quantities from Balance without Chemical Reaction Material balances, without for different types of Reaction systems M4: L7: Stoichiometry & other Material ‘Terminology for Reaction Systems Balances [L8-L9: Material Balance Problems Involving | with Chemical Reaction: species, Reactions _| elemental and combustion M L10: Primary Concepts , Sequential Material Multi-Unit Systems Balances For [L11-L12: Material balances with Multi-Unit | recycle, bypass and purge Systems L13-L14: The Industrial Application of Material Balances M6: Ideal | L15: Ideal gas law calculations, ideal Leam relevant physics of single phase & multiphase systems.BIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani Campus AUGS/ AGSR Division M7:Multiph_] LA7-L18: Phase diagram, vapor TB: 8.1-8.3 p Apply these ase pressure estimation , vaporization, concepts (and hence Equilibrium | Phase Rule equations) in 19-120; saturation, condensation, | TB: 84, | material & energy Partial saturation and humidity 83 balances T2i: Humidity chart TBIl | Calculate various Terminology, properties from quantities from humidity chart energy balances of MS: Energy | L22: Terminology, Types of Energy. | TB:9 different types of balance 123-125; Energy (Enthalpy) systems Preliminaries | jalances in the absence of chemical reactions: Closed system (steady and unsteady), Open system (steady and unsteady) M9: Energy | 126-127: The Standard Heat TB: 10.1, Balances: | (Enthalpy) of Formation, The Heat | 10.2 HowTo | (Enthalpy) of Reaction Account For [L28: Integration of Heat of TB: 103, Chemical | Formation and Sensible Heat 104 Reaction __ | The Heat (Enthalpy) of Combustion MIO: 129-132; Analysis of the degrees of ‘Analyze integrated Solving freedom, solving material and energy ‘material and energy imultaneous | balances simultaneously problems and material and perform the energy calculations balances, 20. 133-138: Solving examples of real Computer | world industrial problems using aided computing tools material and energy balances 6. Evaluation Scheme: Component] Duration (min) | Weightage | Date & | Nature of (%eyMarks component (Total 300) (Close Book/ Open Book) Test 1 30 TSS OB Test 2 30 1345 0B Test 3 30 1545 0B Group Assignment | Online 1030 OB (Two) Discussion ForumBIRLA INSTITUTE OF TECHNOLOGY AND SCIENCE, Pilani Campus AUGS/ AGSR Division Class Participation [In regularclass | 10/30 ‘OB Component Tutorial tests In tutorial cl 1030 ‘OB ‘Comprehensive 120 25/15 CB and/or OB Examination CB: Close Book OB: Open Book 7. Chamber Consultation Hour: Will be announced in Class 8. IMPORTANT NOT © Tests 1, 2, and 3 will be conducted in regular class hour © Group Assignment (GA; Two): © Out of class learning will be encouraged via Discussion Forum (DF) © Group of 3-4 student © GAL: Oct 21-25, DF & report submission. © GA2: Nov 21-25. DF & report submission. © Class Participation Component (CPC): © 1 to 3 expected in each class; © Both evaluatory & nonevaluatory; © Best 50% of total CPC classes will be considered. © This component aims to benefit students who remain proactive, productive, and regular throughout the course. © Tutorial tests (surprise): © Best 6 out of X conducted will be considered. © Both evaluatory & nonevaluatory. 9. Make-up Policy: Make-up for the tests will be granted only in case of illness requiring hospitalization and accompanying medical certificate. Make-up for comprehensive examination must be obtained from ID. No make-up request for tutorial tests/CPCs/assignments will be considered for any reason. 10, Notices: All announcements will be made in class/Google Classroom/Nalanda Instructor-in-chargel CHE F211