Introducere
TEBNICI EXPERIMENTALE DE SEPARARE SI PURIFICARE A
COMPUSILOR ORGANICI
Scpararea si purificarea sunt operat indispentabile Pentru chimia organic, aplicindu-se atit
Teactantilor, cit si produsilor de reactie.
Separate resco sat opfonl a iets de sus in car ace rovin,
secon hence profiplr de rate sat Int ligarse See
utilizarea acestora, deoarece majoritatea procesclor chimice conduc la produsi impuri. Impurificerce
Produsului de interes se poate datora urmatoarelor eauzer
Sean Podtpr secu de rate real fe din proce line prac ipal, fie din
te Satta eo fio misma mare st ta mish ata ee
5 simititi neconsumate de reactant, ca rezaltat al situation
L Metode fizice de separare
pagiliet sstemelor chimico-Szice omogene sau ctsrogene,
incipi oa farperiamPonentslor sistemulni se realizzaci 6 taza proprstitilor fizice
difetite ale acestora - temperatura de topire (t), temperaturtt de fierbere (
ti
, densitate (p), indice de
refractie (a), rotatia planuluilumindi polarize (0, Spectre de absorbtie san de mast etc,
cin Pte ck vacabitpebaza cca oo rslineard ecpaanee sett ce annie se
pot subclasifica in:
. soem, cuaamecanice de separare - Scam so reaizast pe buen diene da
ensitate: cantare; separae lchid-lichid nemisoibil, filtrare; centrifugare,
coryene’ Ode bazate pe solubiliate - Separaroa se realizeand pe besa di i de solubiltxate
inten solvent sau amestec de solvent: eristalizare din solventi (caz particular: recristalizare);
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